CN105296312A - Crocodile bone wine and preparation method thereof - Google Patents
Crocodile bone wine and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a crocodile bone wine which is prepared from crocodile bone, crocodile skin, liquor and traditional Chinese medicine components, wherein the content of the crocodile skin is 10-100 parts by weight; the content of the crocodile bone is 50-250 parts by weight; and the traditional Chinese medicine components are as follows in parts by weight: 100-300 parts of kudzu root, 50-200 parts of licorice, 1.5-2.5 parts of ginseng, 50-200 parts of wolfberry fruits and 20-150 parts of jujubes. The invention also provides a preparation method of the crocodile bone wine. The crocodile bone wine has the effects of relieving fatigue, treating rheumatism and ostealgia and improving immunity; and the preparation process is easy in operation and convenient for industrial production.
Description
Technical field
The present invention relates to a kind of animal wine, be specifically related to a kind of Crocodile bone wine and preparation method thereof.
Background technology
Crocodile as a kind of biological, rich in proteins and amino acid, lipid acid and multivitamin and trace element.At present, except edible, crocodile is also for the preparation of health promoting wine.Crocodile health promoting wine on the market mostly adopts immersion way, and in wine base, soak some months even 1-2 and obtaining, it prepares length consuming time, efficiency is low.And soak enzymolysis by wine base, even if soak time is long again, the effective constituent of its crocodile cannot fully be gone out by enzymolysis and enter in wine, bioactive molecules content in this crocodile health promoting wine, lack nutritive ingredient and health-care effect, do not possess the mouthfeel of Tallow, beef perfume (or spice), even have animal fishy smell, destroy the effective constituent of Chinese medicinal materials simultaneously yet yet.
Summary of the invention
The object of the present invention is to provide the Crocodile bone wine of a kind of nutritious, antifatigue, the immunizing power that can improve, treatment treating rheumatic ostealgia, the present invention also provides the preparation method of this Crocodile bone wine.
For solving the problem, the technical solution adopted in the present invention is as follows:
A kind of Crocodile bone wine, its raw materials comprises alligator bone, crocodile skin, white wine and traditional Chinese medicinal components, described crocodile skin is 10-100 part according to parts by weight, described alligator bone is 50-250 part according to parts by weight, and described traditional Chinese medicinal components is made up of the following component according to parts by weight: root of kudzu vine 100-300 part, Radix Glycyrrhizae 50-200 part, ginseng 1.5-2.5 part, wolfberry fruit 50-200 part and date 20-150 part.
In the present invention, preferred scheme is the alcohol number of degrees in described white wine is 35-65 degree.
In the present invention, the preferred scheme bulk that to be described alligator bone be after rubbing or pulverous alligator bone.
In the present invention, preferred scheme is described crocodile skin is 80 parts according to parts by weight, described alligator bone is 150 parts according to parts by weight, and described traditional Chinese medicinal components is made up of the following component according to parts by weight: the root of kudzu vine 200 parts, 120 parts, Radix Glycyrrhizae, ginseng 2 parts, wolfberry fruit 150 parts and 130 parts, date.
The present invention also provides the preparation method of this Crocodile bone wine, comprises the steps:
A. crocodile skin enzymolysis solution preparation: the crocodile skin getting 10-100 weight part, then the 3-10 distilled water doubly of crocodile skin weight is added, enzymolysis, hydrolysis temperature is 50-70 DEG C, enzymolysis time is 12-36h, and the enzyme adopted is at least three kinds in papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain crocodile skin enzymolysis solution; The mass ratio of described enzyme and crocodile skin is 0.5-10:1000;
B. alligator bone enzymolysis solution preparation: the alligator bone getting 50-250 weight part, then the 3-10 distilled water doubly of alligator bone weight is added, enzymolysis, hydrolysis temperature is 50-70 DEG C, enzymolysis time is 12-36h, and the enzyme adopted is at least three kinds in papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain alligator bone enzymolysis solution; Wherein the mass ratio of enzyme and alligator bone is 0.5-10:1000;
C. herb liquid preparation: get the following traditional Chinese medicinal components according to parts by weight: root of kudzu vine 100-300 part, Radix Glycyrrhizae 50-200 part, ginseng 1.5-2.5 part, wolfberry fruit 50-200 part, date 20-150 part, then the 3-10 distilled water doubly of Chinese medicine component gross weight is added, then be heated to 80-120 DEG C, be then pressurized to 0.5-2kg/cm
2and constant temperature boiling 5-10h, filter and obtain first-time filtrate, then get the 2-5 distilled water doubly of Chinese medicine component gross weight, be heated to 80-120 DEG C together with filter residue, be then pressurized to 0.5-2kg/cm
2and constant temperature boiling 5-10h, filter and obtain secondary filtrate; First-time filtrate and secondary filtrate are merged, obtains herb liquid;
D. product preparation: the alligator bone enzymolysis solution that crocodile skin enzymolysis solution a step obtained, b step obtain and the herb liquid that step c obtains mix, and obtain mixed solution, then add white wine, described mixed solution accounts for the 10-30% of white wine and mixed solution gross weight; Mixing leaves standstill, and removes precipitation and grease, obtains Crocodile bone wine.
In the present invention, the preferred scheme sheet crocodile skin that to be the crocodile skin in described a step be through shredding.
In the present invention, preferred scheme be go out in described b step that the temperature of ferment treatment is 90-120 DEG C, the enzyme time of going out is 10-60min; The temperature of ferment treatment of going out in described a step is 90-120 DEG C, the enzyme time of going out is 10-60min.
In the present invention, preferred scheme is that traditional Chinese medicinal components in described step c is through chopping or pulverization process.
In the present invention, preferred scheme is: the enzyme that the enzymolysis in described a step adopts is papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; The enzyme that enzymolysis in described b step adopts is papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033.
In the present invention, preferred scheme is the preparation method of described Crocodile bone wine, comprises the steps:
A. crocodile skin enzymolysis solution preparation: the crocodile skin getting 80 weight parts, then adds the distilled water of 5 times of crocodile skin weight, enzymolysis, and hydrolysis temperature is 55 DEG C, and enzymolysis time is 24h; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain crocodile skin enzymolysis solution; The temperature of ferment treatment of going out is 100 DEG C, the enzyme time of going out is 40min; The mass ratio of described enzyme and crocodile skin is 1:1000;
B. alligator bone enzymolysis solution preparation: the alligator bone getting 150 weight parts, then adds the distilled water of 6 times of alligator bone weight, enzymolysis, and hydrolysis temperature is 55 DEG C, and enzymolysis time is 24h; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain alligator bone enzymolysis solution; The temperature of ferment treatment of going out is 100 DEG C, the enzyme time of going out is 40min; Wherein the mass ratio of enzyme and crocodile skin is 1:1000;
C. herb liquid preparation: get the following traditional Chinese medicinal components according to parts by weight: the root of kudzu vine 200 parts, 120 parts, Radix Glycyrrhizae, ginseng 2 parts, wolfberry fruit 150 parts and 130 parts, date, then the distilled water of 6 times of Chinese medicine component gross weight is added, then be heated to 105 DEG C, be then pressurized to 1.5kg/cm
2and constant temperature boiling 6h, filter and obtain first-time filtrate, then get the distilled water of 3 times of Chinese medicine component gross weight, be heated to 105 DEG C together with filter residue, be then pressurized to 1.5kg/cm
2and constant temperature boiling 6h, filter and obtain secondary filtrate; First-time filtrate and secondary filtrate are merged, obtains herb liquid;
D. product preparation: the alligator bone enzymolysis solution that crocodile skin enzymolysis solution a step obtained, b step obtain and the herb liquid that step c obtains mix, and obtain mixed solution, then add white wine, described mixed solution accounts for 15% of white wine and mixed solution gross weight; Mixing leaves standstill, and removes precipitation and grease, obtains Crocodile bone wine.
Compared with prior art, tool of the present invention has the following advantages: Crocodile bone wine of the present invention, composite by selecting alligator bone, crocodile skin and traditional Chinese medicinal components to carry out, and utilize papoid to carry out enzymolysis to alligator bone and crocodile skin, then enzymolysis solution and herb liquid and white wine are carried out composite, it is fragrant that the Crocodile bone wine obtained has crocodile ester, and nutritious, can alleviating fatigue, treatment treating rheumatic ostealgia, promote immunizing power; In addition, the preparation technology of this Crocodile bone wine is easy to operate, is convenient to industrial production application.
Below in conjunction with embodiment, the present invention is described in detail.
Embodiment
A kind of Crocodile bone wine, its raw materials comprises alligator bone, crocodile skin, white wine and traditional Chinese medicinal components, described crocodile skin is 10-100 part according to parts by weight, described alligator bone is 50-250 part according to parts by weight, and described traditional Chinese medicinal components is made up of the following component according to parts by weight: root of kudzu vine 100-300 part, Radix Glycyrrhizae 50-200 part, ginseng 1.5-2.5 part, wolfberry fruit 50-200 part and date 20-150 part.
The root of kudzu vine is the dry root of legume pueraria lobata, practises and claims elegant jessamine; There is expelling pathogenic factors from muscles for reducing heat, promoting eruption, promote the production of body fluid to quench thirst, rise the merit of positive antidiarrheal.Be usually used in illness that has not attacked the vital organs of the human body heating, stiff nape and back, measles without adequate eruption, pyreticosis is thirsty, and the deficiency of Yin is quenched one's thirst, and heat is purged heat dysentery, diarrhea due to hypofunction of the spleen.
Radix Glycyrrhizae, have another name called old, the sweet grass of state, Glycyrrhiza uralensis Fisch. or sweet root, gas is micro-, and taste is sweet and special.Function cures mainly clearing heat and detoxicating, expelling phlegm for arresting cough, gastral cavity abdomen etc.
Wolfberry fruit, containing abundant carotene, multivitamin and calcium, iron, trimethyl-glycine, coromegine and l-tropine tropate, the effect such as there is Promote immunity, anti-ageing, antitumor, scavenging free radicals, antifatigue, radioprotective, protect the liver.
Date, has another name called red date, and vitamin contents is high, has the good reputation of " natural complex ball ", has nourishing YIN and invigorating YANG, the effect of enriching blood.
In the present invention, preferred scheme is the alcohol number of degrees in described white wine is 35-65 degree.
In the present invention, the preferred scheme bulk that to be described alligator bone be after rubbing or pulverous alligator bone.
In the present invention, preferred scheme is described crocodile skin is 80 parts according to parts by weight, described alligator bone is 150 parts according to parts by weight, and described traditional Chinese medicinal components is made up of the following component according to parts by weight: the root of kudzu vine 200 parts, 120 parts, Radix Glycyrrhizae, ginseng 2 parts, wolfberry fruit 150 parts and 130 parts, date.
The present invention also provides the preparation method of this Crocodile bone wine, comprises the steps:
A. crocodile skin enzymolysis solution preparation: the crocodile skin getting 10-100 weight part, then the 3-10 distilled water doubly of crocodile skin weight is added, enzymolysis, hydrolysis temperature is 50-70 DEG C, enzymolysis time is 12-36h, and the enzyme adopted is at least three kinds in papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain crocodile skin enzymolysis solution; The mass ratio of described enzyme and crocodile skin is 0.5-10:1000;
B. alligator bone enzymolysis solution preparation: the alligator bone getting 50-250 weight part, then the 3-10 distilled water doubly of alligator bone weight is added, enzymolysis, hydrolysis temperature is 50-70 DEG C, enzymolysis time is 12-36h, and the enzyme adopted is at least three kinds in papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain alligator bone enzymolysis solution; Wherein the mass ratio of enzyme and alligator bone is 0.5-10:1000;
C. herb liquid preparation: get the following traditional Chinese medicinal components according to parts by weight: root of kudzu vine 100-300 part, Radix Glycyrrhizae 50-200 part, ginseng 1.5-2.5 part, wolfberry fruit 50-200 part, date 20-150 part, then the 3-10 distilled water doubly of Chinese medicine component gross weight is added, then be heated to 80-120 DEG C, be then pressurized to 0.5-2kg/cm
2and constant temperature boiling 5-10h, filter and obtain first-time filtrate, then get the 2-5 distilled water doubly of Chinese medicine component gross weight, be heated to 80-120 DEG C together with filter residue, be then pressurized to 0.5-2kg/cm
2and constant temperature boiling 5-10h, filter and obtain secondary filtrate; First-time filtrate and secondary filtrate are merged, obtains herb liquid;
D. product preparation: the alligator bone enzymolysis solution that crocodile skin enzymolysis solution a step obtained, b step obtain and the herb liquid that step c obtains mix, and obtain mixed solution, then add white wine, described mixed solution accounts for the 10-30% of white wine and mixed solution gross weight; Mixing leaves standstill, and removes precipitation and grease, obtains Crocodile bone wine.
In the present invention, the preferred scheme sheet crocodile skin that to be the crocodile skin in described a step be through shredding.
In the present invention, preferred scheme be go out in described b step that the temperature of ferment treatment is 90-120 DEG C, the enzyme time of going out is 10-60min; The temperature of ferment treatment of going out in described a step is 90-120 DEG C, the enzyme time of going out is 10-60min.
In the present invention, preferred scheme is that traditional Chinese medicinal components in described step c is through chopping or pulverization process.
In the present invention, preferred scheme is: the enzyme that the enzymolysis in described a step adopts is papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; The enzyme that enzymolysis in described b step adopts is papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033.
In the present invention, preferred scheme is the preparation method of described Crocodile bone wine, comprises the steps:
A. crocodile skin enzymolysis solution preparation: the crocodile skin getting 80 weight parts, then adds the distilled water of 5 times of crocodile skin weight, enzymolysis, and hydrolysis temperature is 55 DEG C, and enzymolysis time is 24h; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain crocodile skin enzymolysis solution; The temperature of ferment treatment of going out is 100 DEG C, the enzyme time of going out is 40min; The mass ratio of described enzyme and crocodile skin is 1:1000;
B. alligator bone enzymolysis solution preparation: the alligator bone getting 150 weight parts, then adds the distilled water of 6 times of alligator bone weight, enzymolysis, and hydrolysis temperature is 55 DEG C, and enzymolysis time is 24h; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain alligator bone enzymolysis solution; The temperature of ferment treatment of going out is 100 DEG C, the enzyme time of going out is 40min; Wherein the mass ratio of enzyme and crocodile skin is 1:1000;
C. herb liquid preparation: get the following traditional Chinese medicinal components according to parts by weight: the root of kudzu vine 200 parts, 120 parts, Radix Glycyrrhizae, ginseng 2 parts, wolfberry fruit 150 parts and 130 parts, date, then the distilled water of 6 times of Chinese medicine component gross weight is added, then be heated to 105 DEG C, be then pressurized to 1.5kg/cm
2and constant temperature boiling 6h, filter and obtain first-time filtrate, then get the distilled water of 3 times of Chinese medicine component gross weight, be heated to 105 DEG C together with filter residue, be then pressurized to 1.5kg/cm
2and constant temperature boiling 6h, filter and obtain secondary filtrate; First-time filtrate and secondary filtrate are merged, obtains herb liquid;
D. product preparation: the alligator bone enzymolysis solution that crocodile skin enzymolysis solution a step obtained, b step obtain and the herb liquid that step c obtains mix, and obtain mixed solution, then add white wine, described mixed solution accounts for 15% of white wine and mixed solution gross weight; Mixing leaves standstill, and removes precipitation and grease, obtains Crocodile bone wine.
In embodiments of the invention 1-5, the various papoids that the papoid adopted is adopted by each embodiment form according to identical weight is composite, if papoid used in embodiment 1 is papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033, weight part as papoid is 1 part, then the weight part of these 8 kinds concrete proteolytic enzyme is 0.125 part.
Embodiment 1
A kind of Crocodile bone wine, its raw materials comprises alligator bone, crocodile skin, white wine and traditional Chinese medicinal components, described crocodile skin is 80 parts according to parts by weight, described alligator bone is 150 parts according to parts by weight, and described traditional Chinese medicinal components is made up of the following component according to parts by weight: the root of kudzu vine 200 parts, 120 parts, Radix Glycyrrhizae, ginseng 2 parts, wolfberry fruit 150 parts and 130 parts, date; The alcohol number of degrees in described white wine are 50 degree; Described alligator bone is the block alligator bone after rubbing; Crocodile skin in described a step is the sheet crocodile skin through shredding.
The preparation method of this Crocodile bone wine, comprises the steps:
A. crocodile skin enzymolysis solution preparation: the crocodile skin getting 80 weight parts, then adds the distilled water of 5 times of crocodile skin weight, enzymolysis, and hydrolysis temperature is 55 DEG C, and enzymolysis time is 24h; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain crocodile skin enzymolysis solution; The temperature of ferment treatment of going out is 100 DEG C, the enzyme time of going out is 40min; The enzyme that enzymolysis adopts is papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; The mass ratio of described enzyme and crocodile skin is 1:1000;
B. alligator bone enzymolysis solution preparation: the alligator bone getting 150 weight parts, then adds the distilled water of 6 times of alligator bone weight, enzymolysis, and hydrolysis temperature is 55 DEG C, and enzymolysis time is 24h; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain alligator bone enzymolysis solution; The temperature of ferment treatment of going out is 100 DEG C, the enzyme time of going out is 40min; The enzyme that enzymolysis adopts is papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; Wherein the mass ratio of enzyme and crocodile skin is 1:1000;
C. herb liquid preparation: get the following traditional Chinese medicinal components according to parts by weight: the root of kudzu vine 200 parts, 120 parts, Radix Glycyrrhizae, ginseng 2 parts, wolfberry fruit 150 parts and 130 parts, date, then the distilled water of 6 times of Chinese medicine component gross weight is added, then be heated to 105 DEG C, be then pressurized to 1.5kg/cm
2and constant temperature boiling 6h, filter and obtain first-time filtrate, then get the distilled water of 3 times of Chinese medicine component gross weight, be heated to 105 DEG C together with filter residue, be then pressurized to 1.5kg/cm
2and constant temperature boiling 6h, filter and obtain secondary filtrate; First-time filtrate and secondary filtrate are merged, obtains herb liquid;
D. product preparation: the alligator bone enzymolysis solution that crocodile skin enzymolysis solution a step obtained, b step obtain and the herb liquid that step c obtains mix, and obtain mixed solution, then add white wine, described mixed solution accounts for 15% of white wine and mixed solution gross weight; Mixing leaves standstill, and removes precipitation and grease, obtains Crocodile bone wine;
Traditional Chinese medicinal components in described step c is through chopping process.
Embodiment 2
A kind of Crocodile bone wine, its raw materials comprises alligator bone, crocodile skin, white wine and traditional Chinese medicinal components, described crocodile skin is 10 parts according to parts by weight, described alligator bone is 250 parts according to parts by weight, and described traditional Chinese medicinal components is made up of the following component according to parts by weight: the root of kudzu vine 100 parts, 200 parts, Radix Glycyrrhizae, ginseng 1.5 parts, wolfberry fruit 50 parts and 150 parts, date; The alcohol number of degrees in described white wine are 65 degree; Described alligator bone is the block alligator bone after rubbing; Crocodile skin in described a step is the sheet crocodile skin through shredding.
The preparation method of this Crocodile bone wine, comprises the steps:
A. crocodile skin enzymolysis solution preparation: the crocodile skin getting 10 weight parts, then the distilled water of 10 times of crocodile skin weight is added, enzymolysis, hydrolysis temperature is 70 DEG C, enzymolysis time is 12h, and the enzyme adopted is papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain crocodile skin enzymolysis solution; The mass ratio of described enzyme and crocodile skin is 0.5:1000;
B. alligator bone enzymolysis solution preparation: the alligator bone getting 250 weight parts, then the distilled water of 10 times of alligator bone weight is added, enzymolysis, hydrolysis temperature is 70 DEG C, enzymolysis time is 12h, and the enzyme adopted is papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain alligator bone enzymolysis solution; Wherein the mass ratio of enzyme and crocodile skin is 0.5:1000;
C. herb liquid preparation: get the following traditional Chinese medicinal components according to parts by weight: the root of kudzu vine 100 parts, 200 parts, Radix Glycyrrhizae, ginseng 1.5 parts, wolfberry fruit 50 parts and 150 parts, date, then the distilled water of 10 times of Chinese medicine component gross weight is added, then be heated to 80 DEG C, be then pressurized to 0.5kg/cm
2and constant temperature boiling 10h, filter and obtain first-time filtrate, then get the distilled water of 5 times of Chinese medicine component gross weight, be heated to 80 DEG C together with filter residue, be then pressurized to 0.5kg/cm
2and constant temperature boiling 10h, filter and obtain secondary filtrate; First-time filtrate and secondary filtrate are merged, obtains herb liquid;
D. product preparation: the alligator bone enzymolysis solution that crocodile skin enzymolysis solution a step obtained, b step obtain and the herb liquid that step c obtains mix, and obtain mixed solution, then add white wine, described mixed solution accounts for 10% of white wine and mixed solution gross weight; Mixing leaves standstill, and removes precipitation and grease, obtains Crocodile bone wine;
The temperature of ferment treatment of going out in described b step is 90 DEG C, the enzyme time of going out is 60min; The temperature of ferment treatment of going out in described a step is 90 DEG C, the enzyme time of going out is 60min;
Traditional Chinese medicinal components in described step c is through chopping or pulverization process.
Embodiment 3
A kind of Crocodile bone wine, its raw materials comprises alligator bone, crocodile skin, white wine and traditional Chinese medicinal components, described crocodile skin is 100 parts according to parts by weight, described alligator bone is 50 parts according to parts by weight, and described traditional Chinese medicinal components is made up of the following component according to parts by weight: the root of kudzu vine 300 parts, 50 parts, Radix Glycyrrhizae, ginseng 2.5 parts, wolfberry fruit 50-200 part and 150 parts, date; The alcohol number of degrees in described white wine are 35 degree; Described alligator bone is the block alligator bone after rubbing; Crocodile skin in described a step is the sheet crocodile skin through shredding.
The preparation method of this Crocodile bone wine, comprises the steps:
A. crocodile skin enzymolysis solution preparation: the crocodile skin getting 100 weight parts, then the distilled water of 3 times of crocodile skin weight is added, enzymolysis, hydrolysis temperature is 50 DEG C, enzymolysis time is 36h, and the enzyme adopted is at least three kinds in papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain crocodile skin enzymolysis solution; The mass ratio of described enzyme and crocodile skin is 10:1000;
B. alligator bone enzymolysis solution preparation: the alligator bone getting 50 weight parts, then the distilled water of 3 times of alligator bone weight is added, enzymolysis, hydrolysis temperature is 50 DEG C, enzymolysis time is 36h, and the enzyme adopted is papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain alligator bone enzymolysis solution; Wherein the mass ratio of enzyme and crocodile skin is 10:1000;
C. herb liquid preparation: get the following traditional Chinese medicinal components according to parts by weight: the root of kudzu vine 300 parts, 50 parts, Radix Glycyrrhizae, ginseng 2.5 parts, wolfberry fruit 50-200 part and 150 parts, date, then the distilled water of 3 times of Chinese medicine component gross weight is added, then be heated to 120 DEG C, be then pressurized to 2kg/cm
2and constant temperature boiling 5h, filter and obtain first-time filtrate, then get the distilled water of 2 times of Chinese medicine component gross weight, be heated to 120 DEG C together with filter residue, be then pressurized to 2kg/cm
2and constant temperature boiling 5h, filter and obtain secondary filtrate; First-time filtrate and secondary filtrate are merged, obtains herb liquid;
D. product preparation: the alligator bone enzymolysis solution that crocodile skin enzymolysis solution a step obtained, b step obtain and the herb liquid that step c obtains mix, and obtain mixed solution, then add white wine, described mixed solution accounts for 30% of white wine and mixed solution gross weight; Mixing leaves standstill, and removes precipitation and grease, obtains Crocodile bone wine;
The temperature of ferment treatment of going out in described b step is 120 DEG C, the enzyme time of going out is 10min; The temperature of ferment treatment of going out in described a step is 120 DEG C, the enzyme time of going out is 10min;
Traditional Chinese medicinal components in described step c is through chopping or pulverization process.
Embodiment 4
A kind of Crocodile bone wine, the enzyme that in step a, the b of its preparation method, enzymolysis adopts is papoid PA1, papoid PS1 and papoid JC1033, and all the other components, proportioning, preparation technology are all identical with embodiment 1.
Embodiment 5
A kind of Crocodile bone wine, the enzyme that in step a, the b of its preparation method, enzymolysis adopts is papoid PA1, papoid PA2, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033, and all the other components, proportioning, preparation technology are all identical with embodiment 2.
Experimental example 1
The Crocodile wine (Crocodile wine of certain commercially available brand) of the Crocodile bone wine that Example 1-5 obtains and comparative example 1, detect the protein content in above-mentioned Crocodile bone wine, aminoacids content with the method on standard GB5009.5, test result refers to following table 1:
The Crocodile bone wine protein content of table 1: embodiment 1-5, comparative example 1, aminoacids content data sheet
| Test item | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| Protein (g/100ml) | 2.15 | 0.68 | 2.04 |
| Amino acid (in N, g/100ml) | 0.83 | 0.24 | 0.79 |
| Test item | Embodiment 4 | Embodiment 5 | Comparative example 1 |
| Protein (g/100ml) | 1.92 | 0.54 | 0.36 |
| Amino acid (in N, g/100ml) | 0.71 | 0.21 | 0.13 |
As can be seen from the data of upper table 1, in Crocodile bone wine of the present invention containing Amino acid and protein content all higher than commercially available Crocodile bone wine, visible Crocodile bone wine of the present invention is nutritious, be of high nutritive value.
Get the Crocodile wine of Crocodile bone wine that Example 1-5 obtains and comparative example 1, then choose 120 volunteers, these 120 volunteers all have the fatigue of severe and the symptom of hypoimmunity, are embodied in lassitude, drowsiness; Then above-mentioned 120 volunteers are divided into 6 groups, often organize 20 people, take above-mentioned 6 kinds of Crocodile wines respectively, drink 2 every day, Chinese meal, dinner respectively once, each 20ml, light diet in the meantime, then every 5 days record symptoms are eased and the number of curing and time, refer to following table 2 and table 3:
Table 2: volunteer's lassitude symptom tracking table record
Note: the number of healing is included in the statistical number of person in improvement, as improved 16, cure 5, the number namely representing healing is 5 people; The number improved is 16 people, comprising number 5 people improved.
As can be seen from the above table, Crocodile bone wine of the present invention, can be good at the symptom changing lassitude, and instant effect, curative ratio is high.
Table 3: volunteer is drowsiness symptom tracking table record
Note: the number of healing is included in the statistical number of person in improvement, as improved 16, cure 12, the number namely representing healing is 12 people; The number improved is 16 people, comprising number 12 people improved.
As can be seen from the above table, Crocodile bone wine of the present invention, can be good at changing drowsiness symptom, and instant effect, curative ratio is high.
From smell, the Crocodile bone wine of embodiment of the present invention 1-5 without fishy smell, and has light crocodile ester fragrance.
Experimental example 2
Liu, lives Chancheng District of Foshan City, suffers from rheumatosis, and Changes in weather feels sore muscle often, the Crocodile bone wine of the edible embodiment of the present invention 1, and each 10ml, every 7 days is a course for the treatment of sooner or later; After 1 course for the treatment of, symptom is alleviated to some extent; After 5 courses for the treatment of, substantially can not nociception; After 10 courses for the treatment of, recovery from illness.
Dong, lives Jing'an District, Shanghai City, suffers from sacroiliitis, and Changes in weather feels that joint pain is unable often, the Crocodile bone wine of the edible embodiment of the present invention 2, and each 10ml, every 7 days is a course for the treatment of sooner or later; After 1 course for the treatment of, symptom is alleviated to some extent; After 6 courses for the treatment of, symptom be improved significantly; After 12 courses for the treatment of, recovery from illness.
Liu, lives Dongcheng District, Beijing during March, suffers from rheumatosis, and Changes in weather feels sore muscle often, the Crocodile bone wine of the edible embodiment of the present invention 3, and each 10ml, every 7 days is a course for the treatment of sooner or later; After 1 course for the treatment of, symptom is alleviated to some extent; After 6 courses for the treatment of, substantially can not nociception; After 12 courses for the treatment of, recovery from illness.
Above-mentioned embodiment is only the preferred embodiment of the present invention; can not limit the scope of protection of the invention with this, change and the replacement of any unsubstantiality that those skilled in the art does on basis of the present invention all belong to the present invention's scope required for protection.
Claims (10)
1. a Crocodile bone wine, its raw materials comprises alligator bone, crocodile skin, white wine and traditional Chinese medicinal components, it is characterized in that: described crocodile skin is 10-100 part according to parts by weight, described alligator bone is 50-250 part according to parts by weight, and described traditional Chinese medicinal components is made up of the following component according to parts by weight: root of kudzu vine 100-300 part, Radix Glycyrrhizae 50-200 part, ginseng 1.5-2.5 part, wolfberry fruit 50-200 part and date 20-150 part.
2. Crocodile bone wine according to claim 1, is characterized in that: the alcohol number of degrees in described white wine are 35-65 degree.
3. Crocodile bone wine according to claim 1, is characterized in that: described alligator bone be through rub after bulk or pulverous alligator bone.
4. Crocodile bone wine according to claim 1, it is characterized in that: described crocodile skin is 80 parts according to parts by weight, described alligator bone is 150 parts according to parts by weight, and described traditional Chinese medicinal components is made up of the following component according to parts by weight: the root of kudzu vine 200 parts, 120 parts, Radix Glycyrrhizae, ginseng 2 parts, wolfberry fruit 150 parts and 130 parts, date.
5. the preparation method of Crocodile bone wine according to claim 1, is characterized in that comprising the steps:
A. crocodile skin enzymolysis solution preparation: the crocodile skin getting 10-100 weight part, then the 3-10 distilled water doubly of crocodile skin weight is added, enzymolysis, hydrolysis temperature is 50-70 DEG C, enzymolysis time is 12-36h, and the enzyme adopted is at least three kinds in papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain crocodile skin enzymolysis solution; The mass ratio of described enzyme and crocodile skin is 0.5-10:1000;
B. alligator bone enzymolysis solution preparation: the alligator bone getting 50-250 weight part, then the 3-10 distilled water doubly of alligator bone weight is added, enzymolysis, hydrolysis temperature is 50-70 DEG C, enzymolysis time is 12-36h, and the enzyme adopted is at least three kinds in papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain alligator bone enzymolysis solution; Wherein the mass ratio of enzyme and alligator bone is 0.5-10:1000;
C. herb liquid preparation: get the following traditional Chinese medicinal components according to parts by weight: root of kudzu vine 100-300 part, Radix Glycyrrhizae 50-200 part, ginseng 1.5-2.5 part, wolfberry fruit 50-200 part, date 20-150 part, then the 3-10 distilled water doubly of Chinese medicine component gross weight is added, then be heated to 80-120 DEG C, be then pressurized to 0.5-2kg/cm
2and constant temperature boiling 5-10h, filter and obtain first-time filtrate, then get the 2-5 distilled water doubly of Chinese medicine component gross weight, be heated to 80-120 DEG C together with filter residue, be then pressurized to 0.5-2kg/cm
2and constant temperature boiling 5-10h, filter and obtain secondary filtrate; First-time filtrate and secondary filtrate are merged, obtains herb liquid;
D. product preparation: the alligator bone enzymolysis solution that crocodile skin enzymolysis solution a step obtained, b step obtain and the herb liquid that step c obtains mix, and obtain mixed solution, then add white wine, described mixed solution accounts for the 10-30% of white wine and mixed solution gross weight; Mixing leaves standstill, and removes precipitation and grease, obtains Crocodile bone wine.
6. the preparation method of Crocodile bone wine according to claim 5, is characterized in that: the temperature of the ferment treatment that goes out in described a step is 90-120 DEG C, the enzyme time of going out is 10-60min; The temperature of ferment treatment of going out in described b step is 90-120 DEG C, the enzyme time of going out is 10-60min.
7. the preparation method of Crocodile bone wine according to claim 5, is characterized in that: the crocodile skin in described a step is the sheet crocodile skin through shredding.
8. the preparation method of Crocodile bone wine according to claim 5, is characterized in that: the traditional Chinese medicinal components in described step c is through chopping or pulverization process.
9. the preparation method of Crocodile bone wine according to claim 5, is characterized in that: the enzyme that the enzymolysis in described a step adopts is papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033; The enzyme that enzymolysis in described b step adopts is papoid PA1, papoid PA2, papoid PA3, papoid PA4, papoid PS1, papoid PS3, papoid PS101 and papoid JC1033.
10. the preparation method of Crocodile bone wine according to claim 9, is characterized in that comprising the steps:
A. crocodile skin enzymolysis solution preparation: the crocodile skin getting 80 weight parts, then adds the distilled water of 5 times of crocodile skin weight, enzymolysis, and hydrolysis temperature is 55 DEG C, and enzymolysis time is 24h; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain crocodile skin enzymolysis solution; The temperature of ferment treatment of going out is 100 DEG C, the enzyme time of going out is 40min; The mass ratio of described enzyme and crocodile skin is 1:1000;
B. alligator bone enzymolysis solution preparation: the alligator bone getting 150 weight parts, then adds the distilled water of 6 times of alligator bone weight, enzymolysis, and hydrolysis temperature is 55 DEG C, and enzymolysis time is 24h; Go out enzyme, then filters and remove filter residue, the filtrate obtained is carried out oily water separation, then the filtrate of removing grease adopted Plate Filtration, obtain alligator bone enzymolysis solution; The temperature of ferment treatment of going out is 100 DEG C, the enzyme time of going out is 40min; Wherein the mass ratio of enzyme and crocodile skin is 1:1000;
C. herb liquid preparation: get the following traditional Chinese medicinal components according to parts by weight: the root of kudzu vine 200 parts, 120 parts, Radix Glycyrrhizae, ginseng 2 parts, wolfberry fruit 150 parts and 130 parts, date, then the distilled water of 6 times of Chinese medicine component gross weight is added, then be heated to 105 DEG C, be then pressurized to 1.5kg/cm
2and constant temperature boiling 6h, filter and obtain first-time filtrate, then get the distilled water of 3 times of Chinese medicine component gross weight, be heated to 105 DEG C together with filter residue, be then pressurized to 1.5kg/cm
2and constant temperature boiling 6h, filter and obtain secondary filtrate; First-time filtrate and secondary filtrate are merged, obtains herb liquid;
D. product preparation: the alligator bone enzymolysis solution that crocodile skin enzymolysis solution a step obtained, b step obtain and the herb liquid that step c obtains mix, and obtain mixed solution, then add white wine, described mixed solution accounts for 15% of white wine and mixed solution gross weight; Mixing leaves standstill, and removes precipitation and grease, obtains Crocodile bone wine.
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| CN105362470A (en) * | 2015-12-03 | 2016-03-02 | 蔡建中 | Alligator egg liquor and preparation method thereof |
| CN105362471A (en) * | 2015-12-03 | 2016-03-02 | 蔡建中 | Crocodile's head liquor and preparation method thereof |
| CN105713785A (en) * | 2016-03-25 | 2016-06-29 | 浙江海洋学院 | Squid bone rice wine and preparation method thereof |
| CN106858204A (en) * | 2016-12-30 | 2017-06-20 | 广东宏益鳄鱼产业有限公司 | A kind of drink containing alligator bone |
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| US20140234488A1 (en) * | 2013-02-15 | 2014-08-21 | Alice Chang | Beverage system, including bubble beverage, instant beverage, beverage with dissolved gas, and beverage with ingredient |
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| CN105713785A (en) * | 2016-03-25 | 2016-06-29 | 浙江海洋学院 | Squid bone rice wine and preparation method thereof |
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