CN105294300A - Efficient slow-release fertilizer for milk vetch on beach saline land and preparation method thereof - Google Patents

Efficient slow-release fertilizer for milk vetch on beach saline land and preparation method thereof Download PDF

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Publication number
CN105294300A
CN105294300A CN201510820054.7A CN201510820054A CN105294300A CN 105294300 A CN105294300 A CN 105294300A CN 201510820054 A CN201510820054 A CN 201510820054A CN 105294300 A CN105294300 A CN 105294300A
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fertilizer
agar
slow
herba astragali
release
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于竞
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Hefei Yongsheng Culture Co Ltd
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Hefei Yongsheng Culture Co Ltd
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Abstract

The invention belongs to the field of slow-release fertilizer, and specifically discloses an efficient slow-release fertilizer for milk vetch on beach saline land. The fertilizer is characterized by including the following components by weight: calcined oyster shell micron powder, agar, lignite wax resin, a resin solvent, stearic acid, mesoporous silica nanoparticles, halophilic composite bacteria, amino acid, common seepweed herb powder, chelated iron, nitrogen phosphorus and potassium microelement fertilizer, methyl salicylate, sodium dodecyl benzene sulfonate, alga dregs, active pond mud doped with silkworm excrement, luffa vine waste and a proper amount of water. The invention uses lignite wax resin as a basic coating material; and materials in different sizes including micron composite hydrogel and mesoporous silica nanoparticles are added in the coating material, so as to enrich the pore size of the coating material, improve dynamic slow release performance and nutrient utilization efficiency, and improve the regulation of fertilizer efficiency. The efficient slow-release fertilizer promotes absorption and utilization of different nutrition materials in environment by milk vetch on beach saline land, and promotes the efficient cultivation.

Description

The high-efficiency sustained-release fertilizer of a kind of coastal saline soil ground Herba Astragali Melilotoidis (Herba Astragali Sinici) and preparation method
Technical field
The invention belongs to slow release fertilizer field, be specifically related to high-efficiency sustained-release fertilizer and the preparation method of a kind of coastal saline soil ground Herba Astragali Melilotoidis (Herba Astragali Sinici).
Background technology
Film-coated and slow release fertilizer has the effect significantly improving utilization rate of fertilizer.But, the most slow-release fertilizers sold in the market are faced with problems, such as: 1, coated fertilizer adopts the non-degradable high molecular polymer of chemosynthesis, and these refractory organics polymer coated fertilizers very easily remain in agricultural soil and cause Soil degradation and serious pollution; 2, coated fertilizer adopts natural polymer degradation material, but slow-release fertilizer selling at exorbitant prices on the one hand prepared by these natural high molecular degradable materials, controlled-release effect is bad on the other hand, along with the degraded of natural macromolecular material can rapid releasing nutrients composition, cause the slow-release fertilizer cycle short, range of application is narrow; 3, existing film-coated and slow release fertilizer can not realize the two-ways regulation of controlled release and slowly-releasing, can not realize the supply of chemical fertilizer Middle nutrition element and crop to the demand basic synchronization of nutrient by dog, can not realize running balance; 4, present slow-release fertilizer is too single to the consideration of external natural condition, for different edatopes, such as paddy field and dry land, acid soil and salt affected soil, high temperature soil and freezing soil etc. do not take into full account, do not consider the water tolerance of coating material, crushing resistance, photosensitivity, pH irritability etc.; 5, the function of existing coating material is more single, usually just sustained-release and controlled release, gives the functions such as coating material water-absorbing-retaining function, antibacterial, deinsectization, weeding, is significant to the development of coating material; 6, production efficiency, service efficiency, the low cost of dressing control release controlled fertilizer will be considered.For release-controlled coated fertilizer Problems existing, efficient, cheap, multi-functional and environmentally friendly coated fertilizer research and development become the prior development direction of domestic and international coated slow release fertilizer research and production application.
Coastal beach soil belongs to marine solonchak type, due to the impact for a long time by oceanic tide, salinification effect causes that soil salt content is higher, the soil body grow not obvious, physicochemical character is poor, fertility level is low, and beach area is also with certain speed increment, simultaneously arable area successively decrease year by year and the something lost day by day of Freshwater resources weary, the exploitation of coastal saline soil more and more receive the concern of people.
The fertilizer efficiency of slow release fertilizer depends on slow-release material, capsule form, market common are and adopt identical or different coated fertilizer realize layering coating and then realize slowly-releasing regulation and control, but can increase material cost and cost of manufacture like this.
Two channels coated fertilizer is built in nanochannel and microchannel, the structure of microchannel and nanochannel can be absorbed and used the space composition caused by means of the structure of material itself and micron/nano material, simply be easy to realize, give slow release fertilizer new function, for the development of slow release fertilizer opens new way simultaneously.
How the High-efficient Production of herbage and green manure plant is the problem always received much concern, and it is good problem to study that the High-efficient Production realizing coastal saline soil herbage and green manure plant on the ground by slow release fertilizer realizes that beach Efficient Development saline land utilizes.
Summary of the invention
The present invention is directed to the growth requirement of the High-efficient Production of saltings tame forage grass crop, propose high-efficiency sustained-release fertilizer and the preparation method of a kind of coastal saline soil ground Herba Astragali Melilotoidis (Herba Astragali Sinici).
The technical solution used in the present invention is as follows:
The high-efficiency sustained-release fertilizer of a kind of coastal saline soil ground Herba Astragali Melilotoidis (Herba Astragali Sinici), it is characterized in that, comprise following parts by weight of component: calcining oyster shells micropowder 3-4, agar 3-4, montanin wax resin 30-32, resin solvent 4-5, stearic acid 2-3, the sub-6-7 of mesoporous silicon dioxide nano particle, bite salt composite bacteria 1.5-1.7, amino acid 2-2.2, the fluffy powder 3-3.4 of alkali, chelated iron 1.2-1.3, the micro-fertile 2.4-2.6 of N P and K, wintergreen oil 1-1.2, Sodium dodecylbenzene sulfonate 1.3-1.4, marine alga slag 40-42, the active lotus pool mud 45-47 of doping silkworm excrement, Towel Gourd Stem waste 46-48, appropriate water.
A high-efficiency sustained-release method for preparing fertilizer for coastal saline soil ground Herba Astragali Melilotoidis (Herba Astragali Sinici), is characterized in that, comprise the following steps:
(1) by agar and gross weight 3-4 water mixing doubly, and stirring reaction 8-10min obtains agar-agar soln at 110-120 DEG C, by calcining oyster shells micropowder and bite salt composite bacteria and add agar-agar soln, stir 15-20min to evenly, cooling, the composite aquogel being prepared into micron-scale is for subsequent use; By montanin wax resin, resin solvent mixing, at 180-190 DEG C of heated and stirred 1-1.2h, add gross weight 2-3 water mixing and stirring doubly, stop heating, and add simultaneously micron-scale composite aquogel, mesoporous silicon dioxide nano particle and stearic acid, rapid stirring 4-5min, to evenly, must have twin-channel coated fertilizer for subsequent use;
(2) by amino acid, the fluffy powder of alkali, chelated iron, the micro-fertilizer of N P and K, wintergreen oil and gross weight 2-3 water mixing and stirring doubly, nutritive medium is obtained for subsequent use;
(3) by active lotus pool mud, the Towel Gourd Stem waste hybrid composting 40d of marine alga slag, doping silkworm excrement, put into pulverizer afterwards and pulverize 20-30min, cross 300 order steel sieves, obtain major ingredient powder, major ingredient powder is put into the stirrer of top with shower nozzle, first evenly sprayed into 3 times of water diluting solns of nutritive medium and Sodium dodecylbenzene sulfonate by shower nozzle in whipping process, and stir 5-6min to even, first centrifuge dehydration afterwards to moisture content is 30% of gross weight, there is twin-channel coated fertilizer evenly being sprayed into by shower nozzle, form the wet stock with coated fertilizer;
(4) wet stock with coated fertilizer is sent into the roller pelletizer with calorifier; setting speed 380-390r/min; temperature 86-90 DEG C; granulation 46-50min; cross 50 order steel sieves, obtain spherical fertilizer, this spherical fertilizer is first used the freezing 20-22min of low temperature-3 DEG C; 100 DEG C are progressively warming up to, with 1 DEG C/min heating mode baking 40min to doing and get final product employing 60 DEG C.
Beneficial effect of the present invention is embodied in:
The present invention adopts montanin wax resin as basic coated fertilizer, the material of the composite aquogel of micron-scale, the sub-different size of mesoporous silicon dioxide nano particle is added in coated fertilizer, the pore dimension of coated fertilizer, dynamically sustained release performance, nutrient utilization efficiency are enriched, improve the control of fertilizer efficiency, facilitate beach and saline land cultivate Herba Astragali Melilotoidis (Herba Astragali Sinici) absorbing different nutriments in environment, promote its Efficient Cultivation.Composite aquogel, mesoporous silicon dioxide nano particle of the montanin wax resin complex micron-scale adopted prepare slow-release fertilizer coating membrance material jointly, improve the dynamic of coating membrance material in fertilizer dispose procedure, utilized by the decomposition of the composite aquogel of micron-scale, increase pore channel, promote the orderly release of other nutritive substance, extend degradation time, maintain fertility.
Embodiment
Embodiment
The high-efficiency sustained-release fertilizer of the coastal saline soil ground Herba Astragali Melilotoidis (Herba Astragali Sinici) described in the present embodiment, it is characterized in that, comprise following parts by weight of component: calcining oyster shells micropowder 3.5, agar 3.5, montanin wax resin 31, resin solvent 4.5, stearic acid 2.5, mesoporous silicon dioxide nano particle 6.5, bite active lotus pool mud 46, Towel Gourd Stem waste 47, the appropriate water of salt composite bacteria 1.6, amino acid 2.1, the fluffy powder of alkali 3.2, chelated iron 1.25, N P and K micro-fertile 2.5, wintergreen oil 1.1, Sodium dodecylbenzene sulfonate 1.35, marine alga slag 41, doping silkworm excrement.
The high-efficiency sustained-release method for preparing fertilizer of the coastal saline soil ground Herba Astragali Melilotoidis (Herba Astragali Sinici) described in the present embodiment, is characterized in that, comprise the following steps:
(1) water of agar and gross weight 3.5 times is mixed, and stirring reaction 9min obtains agar-agar soln at 115 DEG C, by calcining oyster shells micropowder and bite salt composite bacteria and add agar-agar soln, stir 17.5min to evenly, cooling, the composite aquogel being prepared into micron-scale is for subsequent use; By montanin wax resin, resin solvent mixing, at 185 DEG C of heated and stirred 1.1h, add the water mixing and stirring of gross weight 2.5 times, stop heating, and add simultaneously micron-scale composite aquogel, mesoporous silicon dioxide nano particle and stearic acid, rapid stirring 4.5min, to evenly, must have twin-channel coated fertilizer for subsequent use;
(2) by the water mixing and stirring of amino acid, the fluffy powder of alkali, chelated iron, the micro-fertilizer of N P and K, wintergreen oil and gross weight 2.5 times, nutritive medium is obtained for subsequent use;
(3) by active lotus pool mud, the Towel Gourd Stem waste hybrid composting 40d of marine alga slag, doping silkworm excrement, put into pulverizer afterwards and pulverize 25min, cross 300 order steel sieves, obtain major ingredient powder, major ingredient powder is put into the stirrer of top with shower nozzle, first evenly sprayed into 3 times of water diluting solns of nutritive medium and Sodium dodecylbenzene sulfonate by shower nozzle in whipping process, and stir 5.5min to even, first centrifuge dehydration afterwards to moisture content is 30% of gross weight, there is twin-channel coated fertilizer evenly being sprayed into by shower nozzle, form the wet stock with coated fertilizer;
(4) wet stock with coated fertilizer is sent into the roller pelletizer with calorifier; setting speed 385r/min; temperature 88 DEG C; granulation 48min; cross 50 order steel sieves, obtain spherical fertilizer, this spherical fertilizer is first used the freezing 21min of low temperature-3 DEG C; 100 DEG C are progressively warming up to, with 1 DEG C/min heating mode baking 40min to doing and get final product employing 60 DEG C.
Get two parts of 1 mu of coastal saline soil ground Herba Astragali Melilotoidis (Herba Astragali Sinici)s respectively as experimental group and control group, experimental group every mu Herba Astragali Melilotoidis (Herba Astragali Sinici) executes fertilizer 30Kg of the present invention, control group does not process, other cultivation condition is consistent, find, experimental group Herba Astragali Melilotoidis (Herba Astragali Sinici) is better than control group Herba Astragali Melilotoidis (Herba Astragali Sinici) growing way, finally gathers in and takes Herba Astragali Melilotoidis (Herba Astragali Sinici) weight in wet base, finds that experimental group Herba Astragali Melilotoidis (Herba Astragali Sinici) weight in wet base is 2.024 times of control group Herba Astragali Melilotoidis (Herba Astragali Sinici) weight in wet base.

Claims (2)

1. the high-efficiency sustained-release fertilizer of a coastal saline soil ground Herba Astragali Melilotoidis (Herba Astragali Sinici), it is characterized in that, comprise following parts by weight of component: calcining oyster shells micropowder 3-4, agar 3-4, montanin wax resin 30-32, resin solvent 4-5, stearic acid 2-3, the sub-6-7 of mesoporous silicon dioxide nano particle, bite salt composite bacteria 1.5-1.7, amino acid 2-2.2, the fluffy powder 3-3.4 of alkali, chelated iron 1.2-1.3, the micro-fertile 2.4-2.6 of N P and K, wintergreen oil 1-1.2, Sodium dodecylbenzene sulfonate 1.3-1.4, marine alga slag 40-42, the active lotus pool mud 45-47 of doping silkworm excrement, Towel Gourd Stem waste 46-48, appropriate water.
2. the high-efficiency sustained-release method for preparing fertilizer of a kind of coastal saline soil ground as claimed in claim 1 Herba Astragali Melilotoidis (Herba Astragali Sinici), is characterized in that, comprise the following steps:
(1) by agar and gross weight 3-4 water mixing doubly, and stirring reaction 8-10min obtains agar-agar soln at 110-120 DEG C, by calcining oyster shells micropowder and bite salt composite bacteria and add agar-agar soln, stir 15-20min to evenly, cooling, the composite aquogel being prepared into micron-scale is for subsequent use; By montanin wax resin, resin solvent mixing, at 180-190 DEG C of heated and stirred 1-1.2h, add gross weight 2-3 water mixing and stirring doubly, stop heating, and add simultaneously micron-scale composite aquogel, mesoporous silicon dioxide nano particle and stearic acid, rapid stirring 4-5min, to evenly, must have twin-channel coated fertilizer for subsequent use;
(2) by amino acid, the fluffy powder of alkali, chelated iron, the micro-fertilizer of N P and K, wintergreen oil and gross weight 2-3 water mixing and stirring doubly, nutritive medium is obtained for subsequent use;
(3) by active lotus pool mud, the Towel Gourd Stem waste hybrid composting 40d of marine alga slag, doping silkworm excrement, put into pulverizer afterwards and pulverize 20-30min, cross 300 order steel sieves, obtain major ingredient powder, major ingredient powder is put into the stirrer of top with shower nozzle, first evenly sprayed into 3 times of water diluting solns of nutritive medium and Sodium dodecylbenzene sulfonate by shower nozzle in whipping process, and stir 5-6min to even, first centrifuge dehydration afterwards to moisture content is 30% of gross weight, there is twin-channel coated fertilizer evenly being sprayed into by shower nozzle, form the wet stock with coated fertilizer;
(4) wet stock with coated fertilizer is sent into the roller pelletizer with calorifier; setting speed 380-390r/min; temperature 86-90 DEG C; granulation 46-50min; cross 50 order steel sieves, obtain spherical fertilizer, this spherical fertilizer is first used the freezing 20-22min of low temperature-3 DEG C; 100 DEG C are progressively warming up to, with 1 DEG C/min heating mode baking 40min to doing and get final product employing 60 DEG C.
CN201510820054.7A 2015-11-24 2015-11-24 Efficient slow-release fertilizer for milk vetch on beach saline land and preparation method thereof Withdrawn CN105294300A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105985195A (en) * 2016-07-01 2016-10-05 宁德市益荣生物工程有限公司 Organic liquid fertilizer and preparation method thereof
CN106008032A (en) * 2016-07-11 2016-10-12 全椒县志恒庄园 Seedling strengthening nutrition agent special for middle and late rice
CN109180361A (en) * 2018-11-19 2019-01-11 湖南雪峰山酒庄有限责任公司 A kind of wine-growing chemical fertilizer and preparation method thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105985195A (en) * 2016-07-01 2016-10-05 宁德市益荣生物工程有限公司 Organic liquid fertilizer and preparation method thereof
CN105985195B (en) * 2016-07-01 2019-07-19 宁德市益荣生物工程有限公司 Organic fertilizer and preparation method thereof
CN106008032A (en) * 2016-07-11 2016-10-12 全椒县志恒庄园 Seedling strengthening nutrition agent special for middle and late rice
CN109180361A (en) * 2018-11-19 2019-01-11 湖南雪峰山酒庄有限责任公司 A kind of wine-growing chemical fertilizer and preparation method thereof

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Application publication date: 20160203