CN105288215A - High-activity dendrobium officinale kimura et migo freeze-drying powder buccal tablets and preparation process thereof - Google Patents
High-activity dendrobium officinale kimura et migo freeze-drying powder buccal tablets and preparation process thereof Download PDFInfo
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Abstract
The present invention discloses high-activity dendrobium officinale kimura et migo freeze-drying powder buccal tablets and a preparation process thereof, and relates to the technical field of traditional Chinese medicines or health products, wherein the buccal tablets are prepared from the following raw materials: dendrobium officinale kimura et migo freeze-drying powder, xylitol, a Chinese wolfberry extract, mannitol, isomaltitol, sodium carboxymethyl starch, and magnesium stearate. According to the present invention, the advanced nanometer crushing technology is used to replace the traditional organic extraction technology so as to avoid the risk of the organic extractant residue in the buccal tablets; the dendrobium officinale kimura et migo freeze-drying powder is prepared into the ultra-micro powder, such that the release of most of the active ingredients in the dendrobium officinale kimura et migo is easily achieved; and the product has characteristics of easy taking, no requirement of water during taking, and no coating component, and can be directly absorbed through oral mucosa, such that the nutrient loss produced during the absorption through the human body gastrointestinal, liver and other organs is avoided, and the absorption utilization rate of the nutrients in the dendrobium officinale kimura et migo is improved.
Description
Technical field
The present invention relates to Chinese medicine or health product technology field, be specifically related to a kind of high activity Herba Dendrobii lyophilized powder buccal tablet and preparation technology thereof.
Background technology
In recent years, along with development and the growth in the living standard of science and technology, the average life of compatriots constantly extends, aging is stepped into gradually in many cities, in order to improve the quality of living, strengthen life effect, the health product of reasonable employment illness prevention and fitness oneself become the conscious requirement of one of people gradually, the research and development in this field also more and more comes into one's own.
Herba Dendrobii, one of orchid, as valuable medical material, is mainly distributed in Tropical Asian and subtropical zone, Australia and Pacific Islands.In China, major part is distributed in the ground such as southwest, south China, Taiwan.As medical material or food materials, its source mostly is the fresh or dry stem of the orchid family herbaceos perennial Dendrobium nobile and Herba Dendrobii; Herba Dendrobii, as the valuable ingredients of traditional Chinese medicine, has reinforcing stomach reg fluid, drives solution deficiency-heat, the curative effects such as beneficial smart reinforcing YIN-essence.Containing a large amount of dendrobines and polysaccharide slime formers matter in Herba Dendrobii; Wherein, dendrobine has certain pain relieving antipyretic effect, similar to phenacetin but more weak; Dendrobium polysaccharide energy enhancing human body immunity function, and there is anti-tumor activity.But adopt conventional decocting method, the effective ingredient not easily stripping of Herba Dendrobii, causes bioavailability low.Application number is the patent of invention of 200910095107.8, provides a kind of dendrobium tea, is made up of the component of following masses part: Herba Dendrobii 3 ~ 7 parts, Herb Gynostemmae Pentaphylli 2 ~ 3 parts, kidney tea 3 ~ 7 parts, Folium Camelliae sinensis 3 ~ 7 parts, 3 ~ 5 parts, sugar.When dendrobium tea uses, with water as solvent, make bioavailability low.Because the dendrobine in Herba Dendrobii, water insoluble as alkaloid, only can be dissolved in the organic solvents such as ethanol, chloroform, ether.For solving the low problem of dissolution, traditional Herba Dendrobii needs to decoct 4-5 hour, and guarantee effective ingredient is used appropriately.Application number is the patent of invention of 201210473859.5, disclose a kind of dendrobium officinale granula, it is primarily of Herba Dendrobii, Poria, Radix Ginseng, Fructus Lycii, Rhizoma Dioscoreae and Semen Coicis composition, wherein, the weight proportion of described Herba Dendrobii, Poria, Radix Ginseng, Fructus Lycii, Rhizoma Dioscoreae, Semen Coicis is: 15 ~ 28:30 ~ 42:7 ~ 18:3 ~ 13:15 ~ 28:15 ~ 28.But this dosage form can not directly act on oral mucosa, and be difficult to the effect realizing Herba Dendrobii cleaning throat and moistening larynx.
Buccal tablet refers to be contained in the compressed tablet slowly dissolved in oral cavity, except the basic demand meeting tablet (as dissolution), also must possess tempting color, the mouthfeel had to make user.Tradition is prepared in the technique of buccal tablet, often adopts organic extraction techniques, can remain organic extractant, not only affect the mouthfeel of buccal tablet, nor be beneficial to healthy in buccal tablet obtained like this.
Summary of the invention
(1) technical problem solved
For the deficiencies in the prior art, the invention provides a kind of high activity Herba Dendrobii lyophilized powder buccal tablet and preparation technology thereof.High activity Herba Dendrobii lyophilized powder buccal tablet of the present invention uses advanced nano-pulverization technology to instead of traditional organic extraction techniques, avoid the risk that in buccal tablet, organic extractant is residual, Herba Dendrobii lyophilized powder is made the release that superfine powder is very beneficial for most active component in Herba Dendrobii; This product is easily oral simultaneously, without the need to water when taking, and without coating constituents, directly can be absorbed by oral mucosa, avoid nutritional labeling by the loss produced during the absorbed organ such as human intestines and stomach and liver, improve the absorption rate of Herba Dendrobii Middle nutrition composition.
(2) technical scheme
For realizing above object, the present invention is achieved by the following technical programs:
A kind of high activity Herba Dendrobii lyophilized powder buccal tablet, is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 80-120 part, Xylitol 60-80 part, wolfberry fruit extract 35-60 part, mannitol 20-35 part, hydroxyl isomaltulose 15-25 part, carboxymethyl starch sodium 5-16 part, magnesium stearate 20-30 part.
Preferably, described high activity Herba Dendrobii lyophilized powder buccal tablet is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 90-110 part, Xylitol 65-70 part, wolfberry fruit extract 45-56 part, mannitol 26-30 part, hydroxyl isomaltulose 18-22 part, carboxymethyl starch sodium 8-12 part, magnesium stearate 24-28 part.
Preferably, described high activity Herba Dendrobii lyophilized powder buccal tablet is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 100 parts, Xylitol 68 parts, wolfberry fruit extract 50 parts, 28 parts, mannitol, hydroxyl isomaltulose 20 parts, carboxymethyl starch sodium 10 parts, magnesium stearate 26 parts.
Preferably, described high activity Herba Dendrobii lyophilized powder buccal tablet is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 100 parts, Xylitol 68 parts, wolfberry fruit extract 50 parts, 28 parts, mannitol, hydroxyl isomaltulose 20 parts, carboxymethyl starch sodium 10 parts, magnesium stearate 26 parts.
A preparation technology for high activity Herba Dendrobii lyophilized powder buccal tablet, comprises the following steps:
(1) get the raw materials ready: select the measured raw material of matter, take raw material according to weight portion, for subsequent use;
(2) batch mixing: Herba Dendrobii lyophilized powder nano grinder is milled to below 100nm, obtains dendrobe ultrafine powder, subsequently dendrobe ultrafine powder, Xylitol, wolfberry fruit extract and carboxymethyl starch sodium are fully mixed 20min, crosses 80 mesh sieves, obtains compound;
(3) granulate: step (2) gained compound is dropped in Multidimensionblender, then adds distilled water as wetting agent, stir, afterwards sufficient for mixing soft material is dropped into oscillating granulator 14 order nylon screens and granulate;
(4) dry: step (3) gained wet granular is placed in hot air circulation drying oven, and dry 1-2 hour at 55-65 DEG C, makes it water content and be down to 2%-4%, obtains dry granule;
(5) perfuming: described mannitol is fully mixed with dry granule;
(6) tabletting: after step (5), add described hydroxyl isomaltulose and magnesium stearate, carry out tabletting after mix homogeneously, packs and obtains Herba Dendrobii lyophilized powder buccal tablet under purification condition.
Preferably, step (4) described baking temperature is 60 DEG C.
(3) beneficial effect
The invention provides a kind of high activity Herba Dendrobii lyophilized powder buccal tablet and preparation technology thereof, described high activity Herba Dendrobii lyophilized powder buccal tablet uses advanced nano-pulverization technology to instead of traditional organic extraction techniques, avoid the risk that in buccal tablet, organic extractant is residual, Herba Dendrobii lyophilized powder is made the release that superfine powder is very beneficial for most active component in Herba Dendrobii; This product is easily oral simultaneously, without the need to water when taking, and without coating constituents, directly can be absorbed by oral mucosa, avoid nutritional labeling by the loss produced during the absorbed organ such as human intestines and stomach and liver, improve the absorption rate of Herba Dendrobii Middle nutrition composition; In addition, the mannitol correctives added, makes the buccal tablet mouthfeel that obtains better.
Detailed description of the invention
For making the object of the embodiment of the present invention, technical scheme and advantage clearly, below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described, obviously, described embodiment is the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Embodiment 1:
The present embodiment high activity Herba Dendrobii lyophilized powder buccal tablet, is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 90 parts, Xylitol 65 parts, wolfberry fruit extract 45 parts, 26 parts, mannitol, hydroxyl isomaltulose 18 parts, carboxymethyl starch sodium 8 parts, magnesium stearate 24 parts.
Preparation method, comprises the following steps:
(1) get the raw materials ready: select the measured raw material of matter, take raw material according to weight portion, for subsequent use;
(2) batch mixing: Herba Dendrobii lyophilized powder nano grinder is milled to below 100nm, obtains dendrobe ultrafine powder, subsequently dendrobe ultrafine powder, Xylitol, wolfberry fruit extract and carboxymethyl starch sodium are fully mixed 20min, crosses 80 mesh sieves, obtains compound;
(3) granulate: step (2) gained compound is dropped in Multidimensionblender, then adds distilled water as wetting agent, stir, afterwards sufficient for mixing soft material is dropped into oscillating granulator 14 order nylon screens and granulate;
(4) dry: step (3) gained wet granular is placed in hot air circulation drying oven, and dry 1-2 hour at 60 DEG C, makes it water content and be down to 2%-4%, obtains dry granule;
(5) perfuming: described mannitol is fully mixed with dry granule;
(6) tabletting: after step (5), add described hydroxyl isomaltulose and magnesium stearate, carry out tabletting after mix homogeneously, packs and obtains Herba Dendrobii lyophilized powder buccal tablet under purification condition.
Embodiment 2:
The present embodiment high activity Herba Dendrobii lyophilized powder buccal tablet, is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 100 parts, Xylitol 68 parts, wolfberry fruit extract 50 parts, 28 parts, mannitol, hydroxyl isomaltulose 20 parts, carboxymethyl starch sodium 10 parts, magnesium stearate 26 parts.
According to the present embodiment parts by weight of raw materials, preparation method is with embodiment 1.
Embodiment 3:
The present embodiment high activity Herba Dendrobii lyophilized powder buccal tablet, is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 110 parts, Xylitol 70 parts, wolfberry fruit extract 56 parts, 30 parts, mannitol, hydroxyl isomaltulose 22 parts, carboxymethyl starch sodium 12 parts, magnesium stearate 28 parts.
According to the present embodiment parts by weight of raw materials, preparation method is with embodiment 1.
Embodiment 4:
The present embodiment high activity Herba Dendrobii lyophilized powder buccal tablet, is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 80 parts, Xylitol 60 parts, wolfberry fruit extract 35 parts, 20 parts, mannitol, hydroxyl isomaltulose 15 parts, carboxymethyl starch sodium 5 parts, magnesium stearate 20 parts.
According to the present embodiment parts by weight of raw materials, preparation method is with embodiment 1.
Embodiment 5:
The present embodiment high activity Herba Dendrobii lyophilized powder buccal tablet, is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 120 parts, Xylitol 80 parts, wolfberry fruit extract 60 parts, 35 parts, mannitol, hydroxyl isomaltulose 25 parts, carboxymethyl starch sodium 16 parts, magnesium stearate 30 parts.
According to the present embodiment parts by weight of raw materials, preparation method is with embodiment 1.
Embodiment 6:
The present embodiment high activity Herba Dendrobii lyophilized powder buccal tablet, is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 100 parts, Xylitol 68 parts, wolfberry fruit extract 50 parts, 28 parts, mannitol, hydroxyl isomaltulose 20 parts, carboxymethyl starch sodium 10 parts, magnesium stearate 26 parts.
According to the present embodiment parts by weight of raw materials, preparation method is with embodiment 1.
Clinical experiment
Embodiment 1 buccal tablet obtained respectively by above-described embodiment 1,2,3,4,5,6, embodiment 2 buccal tablet, embodiment 3 buccal tablet, embodiment 4 buccal tablet, embodiment 5 buccal tablet and embodiment 6 buccal tablet, taking convenience mouthfeel is good, after testing not to the composition that human body has side effects.Take through hundred people, take for each person every day 3 (1g/ sheets), prove diabetes-alleviating, improve the intestines and stomach, raising mental status has remarkable result.
Result of use is as shown in the table:
As can be seen from upper table data, take buccal tablet 1 of the present invention, buccal tablet 2 and buccal tablet 3 pairs of type Ⅱdiabetes mellitus, the incongruous tired lassitude person of the intestines and stomach has obvious curative effects, and the effect of buccal tablet 2 is best.
It should be noted that, in this article, the such as relational terms of first and second grades and so on is only used for an entity or operation to separate with another entity or operating space, and not necessarily requires or imply the relation that there is any this reality between these entities or operation or sequentially.And, term " comprises ", " comprising " or its any other variant are intended to contain comprising of nonexcludability, thus make to comprise the process of a series of key element, method, article or equipment and not only comprise those key elements, but also comprise other key elements clearly do not listed, or also comprise by the intrinsic key element of this process, method, article or equipment.When not more restrictions, the key element limited by statement " comprising ... ", and be not precluded within process, method, article or the equipment comprising described key element and also there is other identical element.
Above embodiment is only in order to illustrate technical scheme of the present invention, be not intended to limit, although with reference to previous embodiment to invention has been detailed description, those of ordinary skill in the art is to be understood that: it still can be modified to the technical scheme described in foregoing embodiments, or carries out equivalent replacement to wherein portion of techniques feature; And these amendments or replacement, do not make the essence of appropriate technical solution depart from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (6)
1. a high activity Herba Dendrobii lyophilized powder buccal tablet, it is characterized in that, described high activity Herba Dendrobii lyophilized powder buccal tablet is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 80-120 part, Xylitol 60-80 part, wolfberry fruit extract 35-60 part, mannitol 20-35 part, hydroxyl isomaltulose 15-25 part, carboxymethyl starch sodium 5-16 part, magnesium stearate 20-30 part.
2. high activity Herba Dendrobii lyophilized powder buccal tablet according to claim 1, it is characterized in that, described high activity Herba Dendrobii lyophilized powder buccal tablet is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 90-110 part, Xylitol 65-70 part, wolfberry fruit extract 45-56 part, mannitol 26-30 part, hydroxyl isomaltulose 18-22 part, carboxymethyl starch sodium 8-12 part, magnesium stearate 24-28 part.
3. high activity Herba Dendrobii lyophilized powder buccal tablet according to claim 1, it is characterized in that, described high activity Herba Dendrobii lyophilized powder buccal tablet is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 100 parts, Xylitol 68 parts, wolfberry fruit extract 50 parts, 28 parts, mannitol, hydroxyl isomaltulose 20 parts, carboxymethyl starch sodium 10 parts, magnesium stearate 26 parts.
4. high activity Herba Dendrobii lyophilized powder buccal tablet according to claim 1, it is characterized in that, described high activity Herba Dendrobii lyophilized powder buccal tablet is made up of the raw material of following weight portion: Herba Dendrobii lyophilized powder 100 parts, Xylitol 75 parts, wolfberry fruit extract 40 parts, 32 parts, mannitol, hydroxyl isomaltulose 23 parts, carboxymethyl starch sodium 10 parts, magnesium stearate 22 parts.
5. a preparation technology for the high activity Herba Dendrobii lyophilized powder buccal tablet as described in as arbitrary in claim 1-4, is characterized in that, comprise the following steps:
(1) get the raw materials ready: select the measured raw material of matter, take raw material according to weight portion, for subsequent use;
(2) batch mixing: Herba Dendrobii lyophilized powder nano grinder is milled to below 100nm, obtain dendrobe ultrafine powder, subsequently dendrobe ultrafine powder, Xylitol, wolfberry fruit extract and carboxymethyl starch sodium are fully mixed 18-25min, cross 80-100 mesh sieve, obtain compound;
(3) granulate: step (2) gained compound is dropped in Multidimensionblender, then adds distilled water as wetting agent, stir, afterwards sufficient for mixing soft material is dropped into oscillating granulator 14 order nylon screens and granulate;
(4) dry: step (3) gained wet granular is placed in hot air circulation drying oven, and dry 1-2 hour at 55-65 DEG C, makes it water content and be down to 2%-4%, obtains dry granule;
(5) perfuming: described mannitol is fully mixed with dry granule;
(6) tabletting: after step (5), add described hydroxyl isomaltulose and magnesium stearate, carry out tabletting after mix homogeneously, packs and obtains Herba Dendrobii lyophilized powder buccal tablet under purification condition.
6. the preparation technology of high activity Herba Dendrobii lyophilized powder buccal tablet according to claim 5, it is characterized in that, step (4) described baking temperature is 60 DEG C.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109528933A (en) * | 2018-12-29 | 2019-03-29 | 中南民族大学 | A kind of application of the compound formulation including tomorrow leaf in prevention or medicaments for treating sexual disorder |
| CN116251154A (en) * | 2023-04-04 | 2023-06-13 | 六安康顺堂石斛有限公司 | Dendrobium nobile freeze-dried powder processing method |
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Application publication date: 20160203 |