CN105273552A - Wood lacquer and preparing method thereof - Google Patents
Wood lacquer and preparing method thereof Download PDFInfo
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- CN105273552A CN105273552A CN201510796272.1A CN201510796272A CN105273552A CN 105273552 A CN105273552 A CN 105273552A CN 201510796272 A CN201510796272 A CN 201510796272A CN 105273552 A CN105273552 A CN 105273552A
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Abstract
The invention discloses wood lacquer and a preparing method thereof. The water-based wood lacquer is prepared from a component A and a component B. The component A is prepared from, by weight, 20-40 parts of acrylate emulsion, 20-60 parts of alkyd resin, 5-30 parts of nitrocellulose and/or cellulose acetate butyrate, 0.5-3 parts of extinction powder, 1-4 parts of anti-settling agents, 0.5-1 part of wetting agent, 0.1-0.5 part of defoaming agent, 0.2-1 part of flatting agent and 5-20 parts of solvent. The component B is prepared from, by weight, 1-10 parts of accelerant and 1-10 parts of initiator. The solvent release property and construction fluidity of the wood lacquer can be remarkably improved, the drying time is shortened, adhesive force and frost crack resistance of the wood lacquer are enhanced, particularly, due to improvement of the construction fluidity of the wood lacquer, the hole access performance of the wood lacquer can be improved, and the wood grain is highlighted better; in addition, hydroxyl groups contained in acrylate emulsion, alkyd resin, nitrocellulose and cellulose acetate can react with cobalt naphthenate and butyl ester, and then the hardness and tenacity of a lacquer film can be improved.
Description
Technical field
The present invention relates to a kind of water-miscible paint, be specifically related to particularly relate to one dry at normal temperatures, for wood product surface, there is a kind of wood lacquer of high rigidity, high-wearing feature.
Background technology
Environmental protection and the energy are our two challenging greatly of facing of 21 century.In order to tackle this challenge, coatings industry turns to the such environmental friendliness of water-borne coatings, radiation curable coating, powder coating and high solid coating, the type that economizes on resources product gradually by high pollution, high energy consumption, the traditional category that extremely depends on petroleum industry product.The more and more stricter laws and regulations in various countries accelerate the paces that water-borne coatings replaces solvent based coating.China is global coating material production big country, is also that furniture maximum in the world and toy are produced, export State simultaneously.Given this, the new variety of exploitation aqueous woodware paint, the performance improving aqueous woodware paint and the coatings industry of technology content to China constantly promoting aqueous woodware paint have major and immediate significance.The Macroeconomic Control Policy of the Chinese government plays sizable effect: the Chinese government has promulgated the pressure standard of VOC contained by a series of restriction solvent-home and water-iome paint; Within 2006, Government Green Purchase inventory clear stipulaties can only select environmentally friendly water-borne coatings.Coating industry Eleventh Five-Year Plan scientific and technical innovation development outline requires will reach more than 20% in the Water-borne modification degree of the Eleventh Five-Year Plan period woodwork coating.And the Water-borne modification of scholarly forecast woodwork coating between 8 years of future will reach more than 50%.Now commercially there is the aqueous wooden ware production marketing that some producers develop, and had relevant patent to disclose.
As Chinese invention patent application CN104327635A discloses a kind of furniture use wood lacquer, be made up of the raw material of following parts by weight: Paris white 8-14 part, Mierocrystalline cellulose 3-7 part, titanium dioxide 4-6 part, organic polymer 3-5 part, glass powder 1_3 part, acrylic resin 15-22 part, coupling agent 1-3 part, composite assistant 4-7 part, Sodium hexametaphosphate 99 7_11 part, kaolin 3_8 part, polyvinyl alcohol 3-9 part, aminoresin 4-8 part, dimethylol propionic acid 3-6 part, deionized water 20 parts, and there is good anti-solarization antiknock split ability, adhesivity is good simultaneously, the advantages such as long service life.
As Chinese invention patent application CN104341932A discloses a kind of highlight water-based wood lacquer, comprise following component and proportioning: ACRYLIC EMULSION 80 ~ 85 parts, N-Methyl pyrrolidone 2 ~ 5 parts, polar organic compounds defoamer 0.2 ~ I part, BYK-3460.3 ~ 0.5 part, propylene glycol I ~ 2 part, BYK3010.2 ~ 0.8 part, 0K6072 ~ 4 part, water miscible polyacrylate 0.5 ~ L5 part, nano-silver liquid 0.1 ~ 0.5 part, described ACRYLIC EMULSION is by following Material synthesis: butyl acrylate 33 parts of methyl methacrylates 17 parts of methacrylic acid I part deionized waters, 63 parts of alkylbenzene polyethers sodium sulfonates 1.5 parts of ammonium persulphates 0.2 part, with low cost, reasonable ratio, there is excellent water tolerance.
But the performance that aqueous woodware paint also exists the aspect such as hardness, wear resistance is in actual use worse than the problem of solvent-borne type wood lacquer, so can not get the generally accreditation of user.
Summary of the invention
For the deficiencies in the prior art, the invention provides a kind of wood lacquer, there is hardness of paint film and wear resistance greatly improves, wear resistance is also close to oil-base paint level, and solve the problem of ubiquitous water-miscible paint froth breaking difficulty, this product also has good leveling property, paint film is plentiful attractive in appearance, easily constructs.
The present invention can be achieved through the following technical solutions:
The invention discloses a kind of wood lacquer, comprise component A and B component, described component A comprises the raw material composition of following weight part: acrylic ester emulsion 20-40; Synolac 20 ~ 60; Soluble cotton and/or cellulose acetate butyrate 5 ~ 30; Flatting silica 0.5 ~ 3; Anti-settling agent 1 ~ 4; Wetting agent 0.5 ~ 1; Defoamer 0.1 ~ 0.5; Flow agent 0.2 ~ 1; Solvent 5 ~ 20; Described B component comprises the raw material composition of following weight part: promotor 1-10; Initiator 1-10.The present invention can significantly improve wood lacquer solvent release, product construction mobility, shorten time of drying, strengthen wood lacquer sticking power and cold-check resistance energy, what especially the increase of product construction mobility can improve wood lacquer enters pore performance, thus allows woody texture more highlight; In addition, hydroxyl contained in acrylic ester emulsion, Synolac, soluble cotton and cellulose acetate all can react with cobalt naphthenate and butyl ester, and then can increase hardness and the tenacity of paint film.
Described component A comprises the raw material composition of following weight part: acrylic ester emulsion 30-40; Synolac 40 ~ 60; Soluble cotton and/or cellulose acetate butyrate 15 ~ 30; Flatting silica 1 ~ 3; Anti-settling agent 2 ~ 4; Wetting agent 0.5 ~ 1; Defoamer 0.1 ~ 0.5; Flow agent 0.2 ~ 1; Solvent 5 ~ 20; Described B component comprises the raw material composition of following weight part: promotor 1-5; Initiator 1-5.
Described component A comprises the raw material composition of following weight part: acrylic ester emulsion 35; Synolac 50; Soluble cotton and/or cellulose acetate butyrate 20; Flatting silica 2; Anti-settling agent 3; Wetting agent 0.5; Defoamer 0.3; Flow agent 0.5; Solvent 10; Described B component comprises the raw material composition of following weight part: promotor 2; Initiator 3.
Described flow agent is at least one in organic silicon modified by polyether flow agent, fluorine richness polyacrylate flow agent, and described defoamer is that solvent-borne type does not contain silicon defoaming agent, and flow agent adjusts as required.
Described flow agent is that organic silicon modified by polyether flow agent and fluorine richness polyacrylate flow agent combine by proportioning 1:1, two kinds of flow agents are combined use, fluorine richness polyacrylate flow agent can play ground and soak and nonshrink hole effect, organic silicon modified by polyether can play quick levelling, reduce the effect of dynamic surface tension, can obtain better film effect.
Described promotor is 6%Co
2+cobalt naphthenate and the mixing solutions of butyl ester, described initiator is the dibutyl phthalate solution of the methylethyl ketone peroxide of 10% of active oxygen, promotor is the cobalt naphthenate of 6%Co2+ and the mixing solutions of butyl ester, select the cobalt naphthenate product of 6% of the long weathering work in Shanghai, the glued membrane selecting this kind of promotor can make to be cross-linked is more even and improve the glued membrane intensity after being cross-linked.Initiator be containing active oxygen 10% the dibutyl phthalate solution of methylethyl ketone peroxide, select the methylethyl ketone peroxide product of the long weathering work in Shanghai, select this kind of initiator can reach initiated polymerization within the rational time complete, and reacting balance in the course of the polymerization process, make paint film have the features such as high rigidity, high fullness ratio, high glossiness.
Another side of the present invention, a kind of preparation method of wood lacquer, concrete scheme, comprises the following steps:
ACRYLIC EMULSION, Synolac, solvent and soluble cotton are stirred and obtains the first mixture;
Flatting silica, anti-settling agent, wetting agent, flow agent and defoamer to be added in the first mixture and stir and obtain component A;
Promotor and initiator are stirred and obtains B component.
Described flatting silica, anti-settling agent, wetting agent, flow agent and defoamer to be added in the first mixture and stir obtain in the step of component A, with under the rotating speed of per minute 800 ~ 1000, drop into successively in the first mixture flatting silica, anti-settling agent, wetting agent, flow agent and defoamer dispersion 10 ~ 15min and whipping temp control below 50 DEG C.
Described preparation method also comprises, by 200 object strainer filtering component A, and, satisfactory filter screen can be selected flexibly according to actual needs.
A kind of wood lacquer of the present invention, has following beneficial effect:
The first, significantly can improve the solvent release of wood lacquer, product construction mobility, shorten time of drying, strengthen wood lacquer sticking power and cold-check resistance energy, what especially the increase of product construction mobility can improve wood lacquer enters pore performance, thus allows woody texture more highlight;
The second, contained in acrylic ester emulsion, Synolac, soluble cotton and cellulose acetate hydroxyl all can react with the mixing solutions of cobalt naphthenate and butyl ester, and then can increase hardness and the tenacity of paint film.
Embodiment
In order to make those skilled in the art person understand technical scheme of the present invention better, below in conjunction with embodiment, product of the present invention is described in further detail.
Embodiment 1
A kind of wood lacquer, comprises component A and B component, and component A comprises the raw material composition of following weight part: acrylic ester emulsion 20; Synolac 20; Soluble cotton and/or cellulose acetate butyrate 5; Flatting silica 0.5; Anti-settling agent 1; Wetting agent 0.5; Defoamer 0.1; Flow agent 0.2; B component comprises the raw material composition of following weight part: promotor 1; Initiator 1, promotor, initiator and acrylic ester emulsion, Synolac and soluble cotton and/or cellulose acetate butyrate carry out polyreaction, significantly can improve the product construction mobility of wood lacquer, shorten time of drying, strengthen wood lacquer sticking power and cold-check resistance energy, what especially the increase of product construction mobility can improve wood lacquer enters pore performance, thus allows woody texture more highlight; In addition, hydroxyl contained in acrylic ester emulsion, Synolac, soluble cotton and cellulose acetate all can react with cobalt naphthenate and butyl ester, and then can increase hardness and the tenacity of paint film.
Embodiment 2
A kind of wood lacquer, comprises component A and B component, and component A comprises the raw material composition of following weight part: acrylic ester emulsion 40; Synolac 60; Soluble cotton and/or cellulose acetate butyrate 30; Flatting silica 3; Anti-settling agent 4; Wetting agent 1; Defoamer 0.5; Flow agent 1; B component comprises the raw material composition of following weight part: promotor 10; Initiator 10, promotor, initiator and acrylic ester emulsion, Synolac and soluble cotton and/or cellulose acetate butyrate carry out polyreaction, significantly can improve the product construction mobility of wood lacquer, shorten time of drying, strengthen wood lacquer sticking power and cold-check resistance energy, what especially the increase of product construction mobility can improve wood lacquer enters pore performance, thus allows woody texture more highlight; In addition, hydroxyl contained in acrylic ester emulsion, Synolac, soluble cotton and cellulose acetate all can react with cobalt naphthenate and butyl ester, and then can increase hardness and the tenacity of paint film.
Embodiment 3
A kind of wood lacquer, comprises component A and B component, and component A comprises the raw material composition of following weight part: acrylic ester emulsion 30; Synolac 40; Soluble cotton and/or cellulose acetate butyrate 15; Flatting silica 1; Anti-settling agent 2; Wetting agent 0.5; Defoamer 0.1; Flow agent 0.2; B component comprises the raw material composition of following weight part: promotor 5; Initiator 5, promotor, initiator and acrylic ester emulsion, Synolac and soluble cotton and/or cellulose acetate butyrate carry out polyreaction, significantly can improve the product construction mobility of wood lacquer, shorten time of drying, strengthen wood lacquer sticking power and cold-check resistance energy, what especially the increase of product construction mobility can improve wood lacquer enters pore performance, thus allows woody texture more highlight; In addition, hydroxyl contained in acrylic ester emulsion, Synolac, soluble cotton and cellulose acetate all can react with cobalt naphthenate and butyl ester, and then can increase hardness and the tenacity of paint film.
Embodiment 4
A kind of wood lacquer, comprises component A and B component, and component A comprises the raw material composition of following weight part: acrylic ester emulsion 35; Synolac 50; Soluble cotton and/or cellulose acetate butyrate 20; Flatting silica 2; Anti-settling agent 3; Wetting agent 0.5; Defoamer 0.3; Flow agent 0.5; B component comprises the raw material composition of following weight part: promotor 2; Initiator 3, promotor, initiator and acrylic ester emulsion, Synolac and soluble cotton and/or cellulose acetate butyrate carry out polyreaction, significantly can improve the product construction mobility of wood lacquer, shorten time of drying, strengthen wood lacquer sticking power and cold-check resistance energy, what especially the increase of product construction mobility can improve wood lacquer enters pore performance, thus allows woody texture more highlight; In addition, hydroxyl contained in acrylic ester emulsion, Synolac, soluble cotton and cellulose acetate all can react with cobalt naphthenate and butyl ester, and then can increase hardness and the tenacity of paint film.
The present invention one is preferred but in unrestriced embodiment, flow agent is at least one in organic silicon modified by polyether flow agent, fluorine richness polyacrylate flow agent, defoamer is that solvent-borne type is not containing silicon defoaming agent; Further flow agent is that organic silicon modified by polyether flow agent and fluorine richness polyacrylate flow agent combine by proportioning 1:1, two kinds of flow agents are combined use, fluorine richness polyacrylate flow agent can play ground and soak and nonshrink hole effect, organic silicon modified by polyether can play quick levelling, reduce the effect of dynamic surface tension, better film effect can be obtained, further, the 10%BYK-333 of organic silicon modified by polyether flow agent employing after butyl ester dilution, fluorine richness polyacrylate flow agent is the EFKA-FL3777 product of German BASF.Wherein preferred, promotor is the cobalt naphthenate of 6%Co2+ and the mixing solutions of butyl ester, selects the cobalt naphthenate product of 6% of the long weathering work in Shanghai, and the glued membrane selecting this kind of promotor can make to be cross-linked is more even and improve the glued membrane intensity after being cross-linked.Initiator be containing active oxygen 10% the dibutyl phthalate solution of methylethyl ketone peroxide, select the methylethyl ketone peroxide product of the long weathering work in Shanghai, select this kind of initiator can reach initiated polymerization within the rational time complete, and reacting balance in the course of the polymerization process, make paint film have the features such as high rigidity, high fullness ratio, high glossiness.The preferred proportion of promotor and initiator is 2:3 in the present invention, and this kind of design makes the hardness of glued membrane reach optimum.That is, in the present invention, by initiator and promotor, the cross-link intensity of ACRYLIC EMULSION, soluble cotton, cellulose acetate butyrate and Synolac can be made to have obvious advantage than the intensity of existing wood lacquer, specifically as shown in table 1.
Meanwhile, in order to the parameter of the concrete technique effect and existing wood lacquer of assessing wood lacquer of the present invention contrasts.Concrete test data is as shown in table 1:
Table 1 is the parameter comparison of wood lacquer of the present invention and existing wood lacquer
As can be seen from Table 1, wood lacquer of the present invention has higher glued membrane hardness, better wear resistance, and has good product construction mobility and shorten time of drying, compared with various and existing wood lacquer, there is significant lifting, thus be with a wide range of applications.
Another side of the present invention, a kind of preparation method of wood lacquer, comprises the following steps:
Step S1: ACRYLIC EMULSION, Synolac, soluble cotton are stirred and obtain the first mixture, is specially and stirs ACRYLIC EMULSION, Synolac and soluble cotton 1 hour with the rotating speed of per minute 500 ~ 700 under normal temperature condition;
Step S2: flatting silica, anti-settling agent, wetting agent, flow agent and defoamer to be added in the first mixture and stir and obtain component A, be specially with under the rotating speed of per minute 800 ~ 1000, drop into successively in the first mixture by flatting silica, anti-settling agent, wetting agent, flow agent and defoamer dispersion 10 ~ 15min and whipping temp control below 50 DEG C.
Step S2: promotor and initiator are stirred and obtain B component, preparation method also comprises, by 200 object strainer filtering component A.In the process used, A and B component are carried out mixing and stirring.
The above, be only preferred embodiment of the present invention, not does any pro forma restriction to the present invention; The those of ordinary skill of all industry all can shown in by specification and the above and implement the present invention swimmingly; But all those skilled in the art are not departing within the scope of technical solution of the present invention, disclosed above technology contents can be utilized and make a little change, modify with differentiation equivalent variations, be Equivalent embodiments of the present invention; Meanwhile, all according to substantial technological of the present invention to the change of any equivalent variations that above embodiment is done, modify and differentiation etc., within the protection domain all still belonging to technical scheme of the present invention.
Claims (10)
1. a wood lacquer, is characterized in that, comprises component A and B component, and described component A comprises the raw material composition of following weight part: acrylic ester emulsion 20-40; Synolac 20 ~ 60; Soluble cotton and/or cellulose acetate butyrate 5 ~ 30; Flatting silica 0.5 ~ 3; Anti-settling agent 1 ~ 4; Wetting agent 0.5 ~ 1; Defoamer 0.1 ~ 0.5; Flow agent 0.2 ~ 1; Described B component comprises the raw material composition of following weight part: promotor 1-10; Initiator 1-10.
2. a kind of wood lacquer as claimed in claim 1, is characterized in that, comprises component A and B component, and described component A comprises the raw material composition of following weight part: acrylic ester emulsion 30-40; Synolac 40 ~ 60; Soluble cotton and/or cellulose acetate butyrate 15 ~ 30; Flatting silica 1 ~ 3; Anti-settling agent 2 ~ 4; Wetting agent 0.5 ~ 1; Defoamer 0.1 ~ 0.5; Flow agent 0.2 ~ 1; Described B component comprises the raw material composition of following weight part: promotor 1-5; Initiator 1-5.
3. a kind of wood lacquer as claimed in claim 1, is characterized in that, comprises component A and B component, and described component A comprises the raw material composition of following weight part: acrylic ester emulsion 35; Synolac 50; Soluble cotton and/or cellulose acetate butyrate 20; Flatting silica 2; Anti-settling agent 3; Wetting agent 0.5; Defoamer 0.3; Flow agent 0.5; Described B component comprises the raw material composition of following weight part: promotor 2; Initiator 3.
4. a kind of wood lacquer as described in as arbitrary in claim 1-3, it is characterized in that, described flow agent is at least one in organic silicon modified by polyether flow agent, fluorine richness polyacrylate flow agent, and described defoamer is that solvent-borne type is not containing silicon defoaming agent.
5. a kind of wood lacquer as claimed in claim 4, is characterized in that, described flow agent is that organic silicon modified by polyether flow agent and fluorine richness polyacrylate flow agent combine by proportioning 1:1.
6. a kind of wood lacquer as claimed in claim 4, is characterized in that, described promotor is 6%Co
2+cobalt naphthenate and the mixing solutions of butyl ester, described initiator is the dibutyl phthalate solution of the methylethyl ketone peroxide of 10% of active oxygen.
7. a preparation method for wood lacquer, is characterized in that, comprises the following steps:
ACRYLIC EMULSION, Synolac, solvent and soluble cotton are stirred and obtains the first mixture;
Flatting silica, anti-settling agent, wetting agent, flow agent and defoamer to be added in the first mixture and stir and obtain component A;
Promotor and initiator are stirred and obtains B component.
8. the preparation method of a kind of wood lacquer as claimed in claim 7, it is characterized in that, described ACRYLIC EMULSION, Synolac, solvent and soluble cotton are stirred obtain the first mixture step in, under normal temperature condition, stir ACRYLIC EMULSION, Synolac and soluble cotton 1 hour with the rotating speed of per minute 500 ~ 700.
9. the preparation method of a kind of wood lacquer as claimed in claim 7, it is characterized in that, described flatting silica, anti-settling agent, wetting agent, flow agent and defoamer to be added in the first mixture and stir obtain in the step of component A, with under the rotating speed of per minute 800 ~ 1000, drop into successively in the first mixture flatting silica, anti-settling agent, wetting agent, flow agent and defoamer dispersion 10 ~ 15min and whipping temp control below 50 DEG C.
10. the preparation method of a kind of wood lacquer as described in as arbitrary in claim 7-9, it is characterized in that, described preparation method also comprises, by 200 object strainer filtering component A.
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| CN201510796272.1A CN105273552A (en) | 2015-11-18 | 2015-11-18 | Wood lacquer and preparing method thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106349845A (en) * | 2016-08-29 | 2017-01-25 | 广东花王涂料有限公司 | Preparation process of double-component seal primer |
| CN106349843A (en) * | 2016-08-29 | 2017-01-25 | 广东花王涂料有限公司 | Preparation process of single-component thermoplastic acrylic acid seal primer |
| CN107384102A (en) * | 2017-08-03 | 2017-11-24 | 合肥隆延科技有限公司 | Environment-friendly type woodwork coating |
| CN107523157A (en) * | 2017-08-03 | 2017-12-29 | 合肥隆延科技有限公司 | Water-borne wood coating |
| CN112680075A (en) * | 2020-12-14 | 2021-04-20 | 成都展辰涂料有限公司 | Non-mask aqueous colorant and preparation method thereof |
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| CN101654586A (en) * | 2008-08-22 | 2010-02-24 | 深圳市展辰达化工有限公司 | Environment-friendly PE gloss black piano lacquer |
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| CN101654586A (en) * | 2008-08-22 | 2010-02-24 | 深圳市展辰达化工有限公司 | Environment-friendly PE gloss black piano lacquer |
| CN101613565A (en) * | 2009-07-24 | 2009-12-30 | 惠州市长润发涂料有限公司 | A kind of polyurethane matt varnish |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106349845A (en) * | 2016-08-29 | 2017-01-25 | 广东花王涂料有限公司 | Preparation process of double-component seal primer |
| CN106349843A (en) * | 2016-08-29 | 2017-01-25 | 广东花王涂料有限公司 | Preparation process of single-component thermoplastic acrylic acid seal primer |
| CN107384102A (en) * | 2017-08-03 | 2017-11-24 | 合肥隆延科技有限公司 | Environment-friendly type woodwork coating |
| CN107523157A (en) * | 2017-08-03 | 2017-12-29 | 合肥隆延科技有限公司 | Water-borne wood coating |
| CN112680075A (en) * | 2020-12-14 | 2021-04-20 | 成都展辰涂料有限公司 | Non-mask aqueous colorant and preparation method thereof |
| CN112680075B (en) * | 2020-12-14 | 2023-03-28 | 成都展辰涂料有限公司 | Non-mask aqueous colorant and preparation method thereof |
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Application publication date: 20160127 |