CN107523157A - Water-borne wood coating - Google Patents
Water-borne wood coating Download PDFInfo
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- CN107523157A CN107523157A CN201710657300.0A CN201710657300A CN107523157A CN 107523157 A CN107523157 A CN 107523157A CN 201710657300 A CN201710657300 A CN 201710657300A CN 107523157 A CN107523157 A CN 107523157A
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- wood coating
- silver
- borne wood
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
- C09D163/10—Epoxy resins modified by unsaturated compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/02—Emulsion paints including aerosols
- C09D5/024—Emulsion paints including aerosols characterised by the additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/02—Emulsion paints including aerosols
- C09D5/024—Emulsion paints including aerosols characterised by the additives
- C09D5/025—Preservatives, e.g. antimicrobial agents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/02—Emulsion paints including aerosols
- C09D5/024—Emulsion paints including aerosols characterised by the additives
- C09D5/028—Pigments; Filters
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1656—Antifouling paints; Underwater paints characterised by the film-forming substance
- C09D5/1662—Synthetic film-forming substance
- C09D5/1675—Polyorganosiloxane-containing compositions
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1687—Use of special additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0806—Silver
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/08—Metals
- C08K2003/0881—Titanium
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
Abstract
The present invention proposes a kind of water-borne wood coating, according to the number of parts by weight, including following components:40~60 parts of emulsion acrylic resin, 20~30 parts of aqueous alkide resin emulsion, titanium load silver-colored 40~60 parts of 3~6 parts of bactericide, 1~2 part of dispersant, 3~6 parts of levelling agent, 5~10 parts of thickener and deionized water, wherein, titanium loads silver-colored bactericide and is mainly prepared by silver nitrate, inidum chloride and butter of tin.The coating antibiosis excellent performance, environment-protecting and non-poisonous, adhesive force is strong.
Description
Technical field
The invention belongs to technical field of coatings, is related to a kind of water-borne wood coating.
Background technology
In May, 2015, country put into effect most tight environmental law in history ---《Wood furniture manufacturing industry Air Pollutant Emission mark
It is accurate》, wherein for the control requirement of wood furniture manufacturing industry Air Pollutant Emission, and entered July 1 the as defined in standard
One stage.New standard provides that contained benzene particulate matter highest allows the prescribed limits of concentration of emission to be greatly reduced in wood furniture.
If furniture enterprise is not transformed production line, still using oil paint, and without using the lower water of pollutant emission level
Property paint, then hardly consistent with the requirement of new standard, ultimately result in commercially to sell its product.
The data that China Association of Coatings Industry announces show that Chinese application industry is every year to the volatile organic of air discharge
Compound (VOC) total amount counts roughly 4,300,000 tons, and wherein oil paint accounting is about 98%, and water paint accounting is about 2%, it can be seen that, water
The environment-friendly advantage of property paint is obvious.Further, country proposes that water paint will substitute comprehensively with requiring that oil changes water in the 2-3 years
Solvent based coating.Shenzhen has put into effect to prohibit selling comprehensively in succession seriously endangers the solvent based coating of citizen's health.Believe, water-based ring
Friendly coating has welcome its spring.Compared with oil paint, water paint is disperseed with water, the coating of dilution, and feature is environmental protection
It is nontoxic, it is nonflammable, without the carcinogens such as benzaldehyde and heavy metal.However, existing water paint using aqueous polyurethane as
Raw material is prepared, and such water paint still has the presence of the carcinogens such as formaldehyde.
Chinese patent (200710026888.6) discloses a kind of nano antibacterial water woodenware paint, different water-based with three kinds
Ester-polyurethane resin emulsion, aqueous acrylic modified ester-polyurethane resin emulsion and nano modified acrylic resin emulsion are in varing proportions
Mixture is prefabricated molten with organic expander soil as film forming matter, and nano composite inorganic antiseptic, the nano composite inorganic antiseptic
Glue is carrier, includes Nano Silver, nano zine oxide, nano aluminium oxide, nano titanium oxide and nano silicon.The invention
The coating VOC values being prepared are low, and resist blocking and that, damage resistant, anti-pollution, color inhibition and closure are good, but it adds inorganic receive
Rice grain is more, and production cost is low, and poor with matrix resin emulsion compatibility, and stability is bad.
The content of the invention
The present invention proposes a kind of water-borne wood coating, and the coating antibiosis excellent performance, environment-protecting and non-poisonous, adhesive force is strong.
The technical proposal of the invention is realized in this way:
A kind of water-borne wood coating, according to the number of parts by weight, including following components:
40~60 parts of emulsion acrylic resin, 20~30 parts of aqueous alkide resin emulsion, titanium load silver-colored 3~6 parts of bactericide,
40~60 parts of 1~2 part of dispersant, 3~6 parts of levelling agent, 5~10 parts of thickener and deionized water, wherein, titanium loads silver-colored bactericide
Mainly it is prepared by silver nitrate, inidum chloride and butter of tin.
Preferably, the preparation method of the silver-colored bactericide of the titanium load is:
In the water that silver nitrate is dissolved in, titanium sulfate solution is then added dropwise, after stirring, adds urea, is progressively warming up to
60 DEG C~80 DEG C are precipitated, and precipitation terminates laggard water-filling and washed, in 500 DEG C~600 DEG C calcinings after drying, you can obtain titanium load
Silver-colored bactericide.
Further, the concentration of titanium sulfate solution is 50~80g/L.
Preferably, the emulsion acrylic resin is organosilicon modified crylic acid resin emulsion, epoxy-modified acrylic acid tree
At least one of fat liquor, aromatic urethane emulsion acrylic resin.
Preferably, the dispersant is in for sldium lauryl sulfate, dioctyl succinate disulfonate acid and sodium glycocholate
It is one or more kinds of.
Preferably, the levelling agent is dimethyl silicone polymer, organic silicon modified by polyether oxygen alkane and polyester resin change properties of organic silicon
One or more in oxygen alkane.
Preferably, the thickener is bentonite and diatomite.
The preparation method of the water-borne wood coating of the present invention, comprises the following steps:
1) emulsion acrylic resin, aqueous alkide resin emulsion and the silver-colored bactericide of titanium load are weighed to be mixed evenly, is stirred
It is 30~40min to mix the time, and discharging obtains mixture A;
2) dispersant is added in mixture A and is uniformly mixing to obtain mixture B;
3) levelling agent, thickener and deionized water are added in mixture B and stirred, cross screen filtration, i.e.,
Obtain water-borne wood coating.
Beneficial effects of the present invention:
1st, water-borne wood coating of the invention loads silver-colored bactericide from titanium and not only acts as bactericidal effect, even more important its
There can also be decomposing formaldehyde function.4 are both greater than to the antibacterial value of staphylococcus aureus and Escherichia coli, antibiotic rate reaches
97.2%.Hardness is high, resistance to scratching, and content of formaldehyde is low (being less than 1.5ppm).
2nd, from emulsion acrylic resin and aqueous alkide resin emulsion as film forming matter, resistance tocrocking and resistance to is improved
Acid-base property, additionally aid the silver-colored bactericide of titanium load and play its heat-proof quality.
Embodiment
Embodiment 1
The preparation method that titanium loads silver-colored bactericide is:
In the 200g water that 10g silver nitrates are dissolved in, 50g/L titanium sulfate solutions are then added dropwise, after stirring, add urine
Element, progressively it is warming up to 60 DEG C and is precipitated, precipitation terminates laggard water-filling and washed, in 500 DEG C~600 DEG C calcinings after drying, you can obtain
Obtain titanium and load silver-colored bactericide.
Embodiment 2
The preparation method that titanium loads silver-colored bactericide is:
In the 150g water that 10g silver nitrates are dissolved in, 100g/L titanium sulfate solutions are then added dropwise, after stirring, add urine
Element, progressively it is warming up to 80 DEG C and is precipitated, precipitation terminates laggard water-filling and washed, in 500 DEG C~600 DEG C calcinings after drying, you can obtain
Obtain titanium and load silver-colored bactericide.
Embodiment 3
A kind of water-borne wood coating, according to the number of parts by weight, including following components:
52 parts of organosilicon modified crylic acid resin emulsion, 24 parts of aqueous alkide resin emulsion, the titanium load silver of embodiment 1 kill
50 parts of 4 parts of microbial inoculum, 1 part of sldium lauryl sulfate, 6 parts of dimethyl silicone polymer, 4 parts of bentonite, 3 parts of diatomite and deionized water.
Embodiment 4
A kind of water-borne wood coating, according to the number of parts by weight, including following components:
The titanium load silver sterilization of 40 parts of epoxy modified acrylic resin emulsion, 30 parts of aqueous alkide resin emulsion, embodiment 2
3 parts of agent, 2 parts of dioctyl succinate disulfonate acid, 3 parts of organic silicon modified by polyether oxygen alkane, 2 parts of bentonite, 3 parts of diatomite and deionization
60 parts of water.
Embodiment 5
A kind of water-borne wood coating, according to the number of parts by weight, including following components:
60 parts of aromatic urethane emulsion acrylic resin, 20 parts of aqueous alkide resin emulsion, the titanium load silver of embodiment 1
4 parts of bactericide, 2 parts of dioctyl succinate disulfonate acid, 6 parts of dimethyl silicone polymer, 5 parts of bentonite, 5 parts of diatomite and deionization
40 parts of water.
Test example
The coating of embodiment 3~5 is subjected to performance detection, it is as a result as follows:
The water-borne wood coating the performance test results of the embodiment 3~5 of table 1
Detection project | Embodiment 3 | Embodiment 4 | Embodiment 5 | Standard |
Adhesive force is tested | 1 grade | 1 grade | 1 grade | QB/T2763 |
Content of formaldehyde | 1.2ppm | 1.4ppm | 1.1ppm | GB/T15516 |
Impact resistance is tested | Corrosion-free point | Corrosion-free point | Corrosion-free point | QB/T2763 |
Antibacterium aptitude tests | Antibacterial value is 4.4 | Antibacterial value is 4.5 | Antibacterial value is 4.2 | ISO22196 |
Durability of antimicrobial effect is tested | Antibacterial value is 2.5 | Antibacterial value is 2.2 | Antibacterial value is 2.3 | ISO22196 |
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
God any modification, equivalent substitution and improvements made etc., should be included in the scope of the protection with principle.
Claims (7)
- A kind of 1. water-borne wood coating, it is characterised in that according to the number of parts by weight, including following components:40~60 parts of emulsion acrylic resin, 20~30 parts of aqueous alkide resin emulsion, titanium load silver-colored 3~6 parts of bactericide, disperseed 40~60 parts of 1~2 part of agent, 3~6 parts of levelling agent, 5~10 parts of thickener and deionized water, wherein, it is main that titanium loads silver-colored bactericide It is prepared by silver nitrate, inidum chloride and butter of tin.
- 2. water-borne wood coating according to claim 1, it is characterised in that the titanium loads the preparation method of silver-colored bactericide For:In the water that silver nitrate is dissolved in, titanium sulfate solution is then added dropwise, after stirring, adds urea, is progressively warming up to 60 DEG C ~80 DEG C are precipitated, and precipitation terminates laggard water-filling and washed, in 500 DEG C~600 DEG C calcinings after drying, you can are obtained titanium load silver and killed Microbial inoculum.
- 3. water-borne wood coating according to claim 2, it is characterised in that the concentration of titanium sulfate solution is 50~80g/L.
- 4. water-borne wood coating according to claim 1 or 2, it is characterised in that the emulsion acrylic resin is organic In fluorine-silicon modified acrylic resin emulsion, epoxy modified acrylic resin emulsion, aromatic urethane emulsion acrylic resin extremely Few one kind.
- 5. water-borne wood coating according to claim 1 or 2, it is characterised in that it is laruyl alcohol sulphur that the dispersant, which is selected from, One or more in sour sodium, dioctyl succinate disulfonate acid and sodium glycocholate.
- 6. water-borne wood coating according to claim 1, it is characterised in that the levelling agent be dimethyl silicone polymer, Organic silicon modified by polyether oxygen alkane and the one or more in polyester modified organic siloxane.
- 7. water-borne wood coating according to claim 1, it is characterised in that the thickener is bentonite and diatomite.
Priority Applications (1)
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CN201710657300.0A CN107523157A (en) | 2017-08-03 | 2017-08-03 | Water-borne wood coating |
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CN201710657300.0A CN107523157A (en) | 2017-08-03 | 2017-08-03 | Water-borne wood coating |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108795270A (en) * | 2018-07-27 | 2018-11-13 | 深圳市得志电子科技有限公司 | A kind of environment-friendlywater-based water-based paint and preparation method thereof |
CN109054558A (en) * | 2018-07-27 | 2018-12-21 | 深圳市得志电子科技有限公司 | Novel aqueous paint of one kind and preparation method thereof |
CN109111810A (en) * | 2018-08-02 | 2019-01-01 | 安徽信达家居有限公司 | A kind of outdoor wooden coatings of door and window paint of sun-proof type |
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EP1331249A1 (en) * | 2002-01-29 | 2003-07-30 | PPG Industries Ohio, Inc. | Mixing scheme and process for the preparation of a refinish coating composition |
CN103073964A (en) * | 2012-11-23 | 2013-05-01 | 高凡 | Preparation method of novel nano modified antibiosis aqueous woodenware paint |
CN104841015A (en) * | 2015-05-21 | 2015-08-19 | 吉林大学 | High-specific-surface-area silver-loaded titanium dioxide composite antibacterial material and preparation method thereof |
CN104910729A (en) * | 2015-06-23 | 2015-09-16 | 陈良伢 | Environment-friendly nano antimicrobial water-based wood paint |
CN105273552A (en) * | 2015-11-18 | 2016-01-27 | 广州聚注专利研发有限公司 | Wood lacquer and preparing method thereof |
CN105647362A (en) * | 2016-04-12 | 2016-06-08 | 湖州新奥克化工有限公司 | High-durability high-efficiency nano antimicrobial water-based wood paint and preparation method thereof |
CN105778749A (en) * | 2016-05-17 | 2016-07-20 | 兰州科天环保节能科技有限公司 | Formaldehyde degrading waterborne wood coating |
-
2017
- 2017-08-03 CN CN201710657300.0A patent/CN107523157A/en active Pending
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EP1331249A1 (en) * | 2002-01-29 | 2003-07-30 | PPG Industries Ohio, Inc. | Mixing scheme and process for the preparation of a refinish coating composition |
CN103073964A (en) * | 2012-11-23 | 2013-05-01 | 高凡 | Preparation method of novel nano modified antibiosis aqueous woodenware paint |
CN104841015A (en) * | 2015-05-21 | 2015-08-19 | 吉林大学 | High-specific-surface-area silver-loaded titanium dioxide composite antibacterial material and preparation method thereof |
CN104910729A (en) * | 2015-06-23 | 2015-09-16 | 陈良伢 | Environment-friendly nano antimicrobial water-based wood paint |
CN105273552A (en) * | 2015-11-18 | 2016-01-27 | 广州聚注专利研发有限公司 | Wood lacquer and preparing method thereof |
CN105647362A (en) * | 2016-04-12 | 2016-06-08 | 湖州新奥克化工有限公司 | High-durability high-efficiency nano antimicrobial water-based wood paint and preparation method thereof |
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Title |
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张世英等: "《一维氧化钛纳米材料》", 30 September 2015, 中南大学出版社 * |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108795270A (en) * | 2018-07-27 | 2018-11-13 | 深圳市得志电子科技有限公司 | A kind of environment-friendlywater-based water-based paint and preparation method thereof |
CN109054558A (en) * | 2018-07-27 | 2018-12-21 | 深圳市得志电子科技有限公司 | Novel aqueous paint of one kind and preparation method thereof |
CN109111810A (en) * | 2018-08-02 | 2019-01-01 | 安徽信达家居有限公司 | A kind of outdoor wooden coatings of door and window paint of sun-proof type |
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Application publication date: 20171229 |