CN105239354A - Novel anti-ultraviolet baby fabric applicable to ordinary days and preparation method thereof - Google Patents
Novel anti-ultraviolet baby fabric applicable to ordinary days and preparation method thereof Download PDFInfo
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Abstract
The invention provides novel anti-ultraviolet baby fabric applicable to ordinary days and a preparation method thereof. The preparation method comprises the following specific steps: 1, mincing and adding buckwheat, red dates and eggplants to a hydrochloric acid anhydrous ethanol solution, conducting ultrasonic treatment for 20-30 minutes at the power of 200 W, conducting reflux extraction for 50-60 minutes at the temperature of 60-70 DEG C, and obtaining rutin extract; 2, nanometer attapulgite and citric acid to the rutin extract, stirring the mixture uniformly, conducting filtration for removing impurities, then adding honey and deionized water, conducting homogeneous stirring and defoaming, and obtaining an anti-ultraviolet treatment agent; 3, adopting exterior and interior knotting double layer weave as a fabric weave structure, treating spandex elastic covering yarn fibers and superfine polyester fibers as exterior warp and exterior weft respectively, treating cotton fibers and silk fibers as interior warp and interior weft respectively, and forming double layer fabric through weaving; 4, conducting plasma treatment on the double layer fabric, spraying the anti-ultraviolet treatment agent, conducting drying, repeating spraying and drying, conducting washing and drying, and finally obtaining the anti-ultraviolet baby fabric applicable to ordinary days.
Description
Technical field:
The invention belongs to textile material technical field, be specifically related to a kind of daily applicable antiultraviolet baby fabric and preparation method thereof.
Background technology:
Ultraviolet radiation in daylight fully can make the 7-DHC in skin form vitamin D, and the absorption of vitamin D to calcium, phosphorus has positive facilitation, but the ultraviolet in daylight also can injure skin simultaneously.Skin is a kind of special organ of human body; there is many specific functions; skin is as the barrier of human body; the loss of electrolyte, body fluid and protein can be prevented; also protect human body from the invasion and attack of bacterium and other harmful substances; protection human body, from ultraviolet damage, can also experience the spontaneous adjustment temperature of external environment.
Skin is the growth progressively fully-developed along with human body, there is very big-difference in the skin texture of baby and the skin texture of adult of general less than 3 years old, as large in body surface area, low melanin, inelastic fiber, corium is thinner, sebum secretion is stronger, high lipid etc., cause the skin of baby to be especially easily subject to ultraviolet injury, effectively can not resist the invasion and attack etc. of extraneous infectious agent.Ultraviolet is not only radiated at the skin surface of baby, also can infiltrate into skin inside, the elastin laminin of destruction skin cell and collagen, cause melanic increase, the phenomenons such as appearance is lax, wrinkle, and now along with the destruction of ozone layer, the amount of ultraviolet arriving ground increases greatly, and ultraviolet risk is still higher, therefore, skin for baby will carry out special nursing, prevents infant skin to be subject to the damage of sunshine middle-ultraviolet lamp.
Antiultraviolet product at present on the market for baby is few, and most head of a family by painting people's suncream or sun protection clothing to baby, or blocks by normal laundry the effect reaching protectiving ultraviolet, well imagines, this way is imappropriate.The suncream of adult or sun protection clothing to the particularity considering baby tender and lovely skin, in use, easily the skin of infringement baby, loses more than gain on the contrary.Therefore be necessary to research and develop the ultraviolet-resistant fabric that a baby is suitable for.
The disclosed a kind of attapulgite suntan lotion for children of Chinese patent CN101579301B (publication date 2009.11.18), containing paste attapulgite clay, milk, grape, banana, sealing, olive oil, zinc oxide, rutile type titanium white, citric acid, sodium hydroxy methyl glycinate and deionized water composition in this attapulgite suntan lotion for children, through batching, pulverizing, stirring, grave mountain, solvent, homogeneous, emulsification, froth breaking, grinding, canned formation finished product.The viscosity of these goods is high, and quality is soft, good hand touch, strong adhesion, can uv reflectance for a long time, and nutritious, can moisten protection skin, enhance metabolism, not blocked pore, non-stimulated.But suntan lotion use needs be coated with once for each 2-3 hour, and removal trouble, need first to wipe by baby oil, then clean with bath foam, and the excessive ultraviolet existed in daily life is protected in good time.
Summary of the invention:
The technology book that the present invention will separate this is to provide a kind of daily applicable antiultraviolet baby fabric and preparation method thereof, adopt polyurethane elastic core-spun yarn fiber, ultra-fine polyester fiber, cotton fiber and silk fiber to prepare double-layer fabric as raw material, then obtain daily applicable antiultraviolet baby fabric through plasma and the anti-ultraviolet radiation treatment agent sprayed containing rutin.Daily applicable antiultraviolet baby fabric prepared by the present invention has pro-skin, moisture absorption is breathed freely, perspire quick-drying, also has excellent ultraviolet resistance, meets the psychological need that baby is daily, and can protect daily excessive ultraviolet in good time.
For separating this above-mentioned technology book, technical scheme of the present invention is:
A kind of daily applicable antiultraviolet baby fabric, it is characterized in that, described antiultraviolet baby fabric is double-layer fabric, described double-layer fabric comprises nexine and skin, described nexine is hydrophilic fibers layer, described skin is hydrophobic fiber layer, and described antiultraviolet baby fabric also comprises ultraviolet resistant layer, and described ultraviolet resistant layer comprises Extraction of rutin thing, nano-attapulgite, citric acid, honey and deionized water.
Preferably, described hydrophobic fiber layer is made up of polyurethane elastic core-spun yarn fiber and ultra-fine polyester fiber, and described hydrophilic fibers is made up of cotton fiber and silk fiber.
The present invention also provides a kind of preparation method of daily applicable antiultraviolet baby fabric, it is characterized in that: comprise the following steps:
(1) rub from buckwheat, red date and eggplant, add in hydrochloric acid ethanol solution, ultrasonic wave process 20-30min under 200W power, at 60-70 DEG C, reflux extraction 50-60min obtains Extraction of rutin thing;
(2) add nano-attapulgite and citric acid in Extraction of rutin thing step (1) prepared, stir, filter and remove impurity, then add honey and deionized water, homogeneous stirs, and froth breaking obtains antiultraviolet finishing agent;
(3) adopt Biao Lijiejie double-layered structure as fabric structure, using polyurethane elastic core-spun yarn fiber and ultra-fine polyester fiber as table through table latitude, cotton fiber and silk fiber respectively as back warp back weft, through weaving formation double-layer fabric;
(4) double-layer fabric step (3) prepared is after Cement Composite Treated by Plasma, antiultraviolet finishing agent prepared by spraying process (2), drying, then spray drying, obtain daily applicable antiultraviolet baby fabric finally by washing and drying.
Preferred as technique scheme, in described step (1), in hydrochloric acid ethanol solution, the volume ratio of hydrochloric acid and absolute ethyl alcohol is 1:3-5.
Preferred as technique scheme, in described step (1), the solid content of Extraction of rutin thing is 55-60mg/g.
Preferred as technique scheme, in described step (2), component in antiultraviolet finishing agent, by weight, comprising: Extraction of rutin thing 35-60 part, nano-attapulgite 15-25 part, citric acid 15-20 part, honey 20-30 part and deionized water 0-30 part.
Preferred as technique scheme, in described step (2), the pH value of antiultraviolet finishing agent is 6.5-7.
Preferred as technique scheme, in described step (3), the Gram Mass of double-layer fabric is 179-214g/ ㎡.
Preferred as technique scheme, in described step (4), the power of Cement Composite Treated by Plasma is 150-200W, and the time is 40-50s.
Preferred as technique scheme, in described step (4), in daily applicable antiultraviolet baby fabric, the thickness of ultraviolet resistant layer is 0.15-0.27mm.
With prior art with than, the present invention has following beneficial effect:
(1) in the daily applicable antiultraviolet baby fabric prepared of the present invention, UV resistance material is rutin; rutin belongs to flavone compound; mainly be present in plant; there is anti-inflammation, anti-oxidant, effect ultraviolet to stronger absorption; it is a kind of natural safe anti ultraviolet agent; non-stimulated to the skin of baby, protection skin can also be moistened, be applicable to Long contact time.
(2) in the ultraviolet resistant layer of daily applicable antiultraviolet baby fabric prepared of the present invention also containing nano-attapulgite, rutin, honey and other substances can absorb in the hole of rod soil by nano-attapulgite, along with time and environmental stimulus slow releasing, improve anti-ultraviolet persistence, and the activity through the surface of the outer layer fiber layer of Cement Composite Treated by Plasma increases, and surface is containing fluted, be conducive to nano-attapulgite to adhere to securely and the surface of outer layer fiber layer and fibrous inside, improve the water-fastness ability of fabric.
(3) the daily applicable antiultraviolet baby fabric that prepared by the present invention is double-layer fabric, nexine is hydrophilic fibers layer, skin is hydrophobic fiber layer, the main raw material of hydrophilic fibers layer is cotton fiber and silk fiber, good pro-skin effect can be played, moisture permeability is excellent, the body fluid that infant skin can be discharged and sweat absorb as soon as possible, prevent from damaging the tender and lovely skin of baby, hydrophobic outer layer, the sweat that nexine can be absorbed and body fluid drain into the volatilization of fabric top layer in time, reach the object of quick-drying, and make nurse personnel discover stain as soon as possible, timely nursing.
(4) the daily applicable antiultraviolet baby fabric that prepared by the present invention has that pro-skin is breathed freely, the performance of hydroscopic fast-drying, and fabric softness is abundant, flexible, and there is excellent anti-ultraviolet function and wash durability, be suitable as the clothing fabric of baby's everyday general purpose.
Detailed description of the invention:
Describe the present invention in detail below in conjunction with specific embodiment, be used for explaining the present invention in this illustrative examples of the present invention and explanation, but not as a limitation of the invention.Embodiment 1:
(1) rub from buckwheat, red date and eggplant, add in hydrochloric acid ethanol solution, wherein the volume ratio of hydrochloric acid and absolute ethyl alcohol is 1:3, ultrasonic wave process 20min under 200W power, reflux extraction 50min at 60 DEG C, obtains the Extraction of rutin thing that solid content is 55mg/g.
(2) by weight, the nano-attapulgite of 15 parts and the citric acid of 15 parts is added in the Extraction of rutin thing that the steps of 35 parts (1) are prepared, stir, filter and remove impurity, then the honey of 20 parts is added, homogeneous stirs, and froth breaking obtains the antiultraviolet finishing agent that pH value is 6.5.
(3) adopt Biao Lijiejie double-layered structure as fabric structure, using polyurethane elastic core-spun yarn fiber and ultra-fine polyester fiber as table through table latitude, cotton fiber and silk fiber respectively as back warp back weft, through weaving the shell fabric forming 179g/ ㎡.
(4) double-layer fabric step (3) prepared is after the Cement Composite Treated by Plasma 40s of 150W power, antiultraviolet finishing agent prepared by spraying process (2), dry, spray drying again, obtain daily applicable antiultraviolet baby fabric finally by washing and drying, wherein the thickness of ultraviolet resistant layer is 0.15mm.
Embodiment 2:
(1) rub from buckwheat, red date and eggplant, add in hydrochloric acid ethanol solution, wherein the volume ratio of hydrochloric acid and absolute ethyl alcohol is 1:5, ultrasonic wave process 30min under 200W power, reflux extraction 60min at 70 DEG C, obtains the Extraction of rutin thing that solid content is 60mg/g.
(2) by weight, the nano-attapulgite of 25 parts and the citric acid of 20 parts is added in the Extraction of rutin thing that the steps of 60 parts (1) are prepared, stir, filter and remove impurity, then the honey of 30 parts and the deionized water of 30 parts is added, homogeneous stirs, and froth breaking obtains the antiultraviolet finishing agent that pH value is 7.
(3) adopt Biao Lijiejie double-layered structure as fabric structure, using polyurethane elastic core-spun yarn fiber and ultra-fine polyester fiber as table through table latitude, cotton fiber and silk fiber respectively as back warp back weft, through weaving the shell fabric forming 214g/ ㎡.
(4) double-layer fabric step (3) prepared is after the Cement Composite Treated by Plasma 50s of 200W power, antiultraviolet finishing agent prepared by spraying process (2), dry, spray drying again, obtain daily applicable antiultraviolet baby fabric finally by washing and drying, wherein the thickness of ultraviolet resistant layer is 0.27mm.
Embodiment 3:
(1) rub from buckwheat, red date and eggplant, add in hydrochloric acid ethanol solution, wherein the volume ratio of hydrochloric acid and absolute ethyl alcohol is 1:4, ultrasonic wave process 25min under 200W power, reflux extraction 55min at 65 DEG C, obtains the Extraction of rutin thing that solid content is 58mg/g.
(2) by weight, the nano-attapulgite of 20 parts and the citric acid of 17 parts is added in the Extraction of rutin thing that the steps of 50 parts (1) are prepared, stir, filter and remove impurity, then the honey of 25 parts and the deionized water of 15 parts is added, homogeneous stirs, and froth breaking obtains the antiultraviolet finishing agent that pH value is 6.7.
(3) adopt Biao Lijiejie double-layered structure as fabric structure, using polyurethane elastic core-spun yarn fiber and ultra-fine polyester fiber as table through table latitude, cotton fiber and silk fiber respectively as back warp back weft, through weaving the shell fabric forming 194g/ ㎡.
(4) double-layer fabric step (3) prepared is after the Cement Composite Treated by Plasma 45s of 180W power, antiultraviolet finishing agent prepared by spraying process (2), dry, spray drying again, obtain daily applicable antiultraviolet baby fabric finally by washing and drying, wherein the thickness of ultraviolet resistant layer is 0.19mm.
Embodiment 4:
(1) rub from buckwheat, red date and eggplant, add in hydrochloric acid ethanol solution, wherein the volume ratio of hydrochloric acid and absolute ethyl alcohol is 1:3.5, ultrasonic wave process 27min under 200W power, reflux extraction 50min at 70 DEG C, obtains the Extraction of rutin thing that solid content is 56mg/g.
(2) by weight, the nano-attapulgite of 17 parts and the citric acid of 19 parts is added in the Extraction of rutin thing that the steps of 45 parts (1) are prepared, stir, filter and remove impurity, then the honey of 27 parts and the deionized water of 10 parts is added, homogeneous stirs, and froth breaking obtains the antiultraviolet finishing agent that pH value is 6.8.
(3) adopt Biao Lijiejie double-layered structure as fabric structure, using polyurethane elastic core-spun yarn fiber and ultra-fine polyester fiber as table through table latitude, cotton fiber and silk fiber respectively as back warp back weft, through weaving the shell fabric forming 201g/ ㎡.
(4) double-layer fabric step (3) prepared is after the Cement Composite Treated by Plasma 40s of 200W power, antiultraviolet finishing agent prepared by spraying process (2), dry, spray drying again, obtain daily applicable antiultraviolet baby fabric finally by washing and drying, wherein the thickness of ultraviolet resistant layer is 0.25mm.
Embodiment 5:
(1) rub from buckwheat, red date and eggplant, add in hydrochloric acid ethanol solution, wherein the volume ratio of hydrochloric acid and absolute ethyl alcohol is 1:5, ultrasonic wave process 20min under 200W power, reflux extraction 50min at 70 DEG C, obtains the Extraction of rutin thing that solid content is 58mg/g.
(2) by weight, the nano-attapulgite of 15 parts and the citric acid of 20 parts is added in the Extraction of rutin thing that the steps of 55 parts (1) are prepared, stir, filter and remove impurity, then the honey of 30 parts and the deionized water of 20 parts is added, homogeneous stirs, and froth breaking obtains the antiultraviolet finishing agent that pH value is 6.8.
(3) adopt Biao Lijiejie double-layered structure as fabric structure, using polyurethane elastic core-spun yarn fiber and ultra-fine polyester fiber as table through table latitude, cotton fiber and silk fiber respectively as back warp back weft, through weaving the shell fabric forming 198g/ ㎡.
(4) double-layer fabric step (3) prepared is after the Cement Composite Treated by Plasma 50s of 150W power, antiultraviolet finishing agent prepared by spraying process (2), dry, spray drying again, obtain daily applicable antiultraviolet baby fabric finally by washing and drying, wherein the thickness of ultraviolet resistant layer is 0.17mm.
Embodiment 6:
(1) rub from buckwheat, red date and eggplant, add in hydrochloric acid ethanol solution, wherein the volume ratio of hydrochloric acid and absolute ethyl alcohol is 1:3, ultrasonic wave process 30min under 200W power, reflux extraction 50min at 70 DEG C, obtains the Extraction of rutin thing that solid content is 59mg/g.
(2) by weight, the nano-attapulgite of 15 parts and the citric acid of 15 parts is added in the Extraction of rutin thing that the steps of 60 parts (1) are prepared, stir, filter and remove impurity, then the honey of 30 parts and the deionized water of 30 parts is added, homogeneous stirs, and froth breaking obtains the antiultraviolet finishing agent that pH value is 6.9.
(3) adopt Biao Lijiejie double-layered structure as fabric structure, using polyurethane elastic core-spun yarn fiber and ultra-fine polyester fiber as table through table latitude, cotton fiber and silk fiber respectively as back warp back weft, through weaving the shell fabric forming 210g/ ㎡.
(4) double-layer fabric step (3) prepared is after the Cement Composite Treated by Plasma 45s of 150W power, antiultraviolet finishing agent prepared by spraying process (2), dry, spray drying again, obtain daily applicable antiultraviolet baby fabric finally by washing and drying, wherein the thickness of ultraviolet resistant layer is 0.20mm.
After testing, the result of the anti-ultraviolet property of the daily applicable antiultraviolet baby fabric prepared of embodiment 1-6, hygroscopicity, gas permeability, quick-drying, security is as follows:
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Embodiment 6 | |
| Unwashed ultraviolet ray transmissivity (%) | 4.1 | 2.4 | 3.6 | 3.7 | 2.7 | 3.9 |
| Wash the ultraviolet ray transmissivity (%) of 100 times | 5.6 | 4.2 | 5.0 | 5.1 | 4.9 | 4.5 |
| Content of formaldehyde (mg/kg) | 5 | 4 | 5 | 4 | 3 | 4 |
| Hydroscopicity (g/g) | 0.67 | 0.91 | 0.75 | 0.84 | 0.86 | 0.75 |
| Gas permeability (mm/s) | 1279 | 1301 | 1297 | 1286 | 1284 | 1296 |
| Seepage of water | Excellent | Excellent | Excellent | Excellent | Excellent | Excellent |
As seen from the above table, daily applicable antiultraviolet baby fabric anti-ultraviolet property prepared by the present invention is excellent, through washing after 100 times, still there is excellent anti-ultraviolet property, and the sucting wet air permeability of fabric, quick-drying and security are all excellent, meet all standard of new-born baby clothes, be applicable to the garment material of baby's everyday general purpose, can shield daily unnecessary ultraviolet, prevent baby to be subject to too much ultraviolet infringement.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, and and for limiting the present invention.The people Ren Ren of ripe this technology is appointed to appoint not appointing of the present invention of the back of the body and under a farmland, to carry out to decorations or to right above-described embodiment.Therefore, lift in art have the person that usually knows tool appointing of not departing from that institute of the present invention tool shows to think with technology tool that lower institute tool becomes one equivalence to adorn or to right, still by still sharp requirement of the present invention still.
Claims (10)
1. a daily applicable novel antiultraviolet baby fabric, it is characterized in that, described antiultraviolet baby fabric is double-layer fabric, described double-layer fabric comprises nexine and skin, described nexine is hydrophilic fibers layer, described skin is hydrophobic fiber layer, and described antiultraviolet baby fabric also comprises ultraviolet resistant layer, and described ultraviolet resistant layer comprises Extraction of rutin thing, nano-attapulgite, citric acid, honey and deionized water.
2. a kind of daily applicable novel antiultraviolet baby fabric according to claim 1, it is characterized in that, described hydrophobic fiber layer is made up of polyurethane elastic core-spun yarn fiber and ultra-fine polyester fiber, and described hydrophilic fibers is made up of cotton fiber and silk fiber.
3. a preparation method for daily applicable novel antiultraviolet baby fabric, is characterized in that: comprise the following steps:
(1) rub from buckwheat, red date and eggplant, add in hydrochloric acid ethanol solution, ultrasonic wave process 20-30min under 200W power, at 60-70 DEG C, reflux extraction 50-60min obtains Extraction of rutin thing;
(2) add nano-attapulgite and citric acid in Extraction of rutin thing step (1) prepared, stir, filter and remove impurity, then add honey and deionized water, homogeneous stirs, and froth breaking obtains antiultraviolet finishing agent;
(3) adopt Biao Lijiejie double-layered structure as fabric structure, using polyurethane elastic core-spun yarn fiber and ultra-fine polyester fiber as table through table latitude, cotton fiber and silk fiber respectively as back warp back weft, through weaving formation double-layer fabric;
(4) double-layer fabric step (3) prepared is after Cement Composite Treated by Plasma, antiultraviolet finishing agent prepared by spraying process (2), drying, then spray drying, obtain daily applicable antiultraviolet baby fabric finally by washing and drying.
4. the preparation method of a kind of daily applicable novel antiultraviolet baby fabric according to claim 3, it is characterized in that: in described step (1), in hydrochloric acid ethanol solution, the volume ratio of hydrochloric acid and absolute ethyl alcohol is 1:3-5.
5. the preparation method of a kind of daily applicable novel antiultraviolet baby fabric according to claim 3, it is characterized in that: in described step (1), the solid content of Extraction of rutin thing is 55-60mg/g.
6. the preparation method of a kind of daily applicable novel antiultraviolet baby fabric according to claim 3, it is characterized in that: in described step (2), component in antiultraviolet finishing agent, by weight, comprising: Extraction of rutin thing 35-60 part, nano-attapulgite 15-25 part, citric acid 15-20 part, honey 20-30 part and deionized water 0-30 part.
7. the preparation method of a kind of daily applicable novel antiultraviolet baby fabric according to claim 3, it is characterized in that: in described step (2), the pH value of antiultraviolet finishing agent is 6.5-7.
8. the preparation method of a kind of daily applicable novel antiultraviolet baby fabric according to claim 3, it is characterized in that: in described step (3), the Gram Mass of double-layer fabric is 179-214g/ ㎡.
9. the preparation method of a kind of daily applicable novel antiultraviolet baby fabric according to claim 3, it is characterized in that: in described step (4), the power of Cement Composite Treated by Plasma is 150-200W, and the time is 40-50s.
10. the preparation method of a kind of daily applicable novel antiultraviolet baby fabric according to claim 3, it is characterized in that: in described step (4), in daily applicable antiultraviolet baby fabric, the thickness of ultraviolet resistant layer is 0.15-0.27mm.
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| CN107385912A (en) * | 2017-07-11 | 2017-11-24 | 盐城工业职业技术学院 | A kind of recessed soil/sodium alginate organic-inorganic hybrid material and preparation method thereof and application |
| CN107385912B (en) * | 2017-07-11 | 2019-09-13 | 盐城工业职业技术学院 | A kind of recessed soil/sodium alginate hybrid inorganic-organic materials and preparation method thereof and application |
| CN108385377A (en) * | 2018-03-21 | 2018-08-10 | 宁波必博母婴科技有限公司 | A kind of antiultraviolet vapor-permeable type baby's antibacterial fabric |
| CN111321601A (en) * | 2020-03-16 | 2020-06-23 | 南通大学 | Anti-ultraviolet bamboo fiber fabric and preparation method thereof |
| CN111321601B (en) * | 2020-03-16 | 2021-10-12 | 南通大学 | Anti-ultraviolet bamboo fiber fabric and preparation method thereof |
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