CN105213287B - The solidifying of a kind of low irritant protects massage mud film and preparation method thereof - Google Patents
The solidifying of a kind of low irritant protects massage mud film and preparation method thereof Download PDFInfo
- Publication number
- CN105213287B CN105213287B CN201510758339.2A CN201510758339A CN105213287B CN 105213287 B CN105213287 B CN 105213287B CN 201510758339 A CN201510758339 A CN 201510758339A CN 105213287 B CN105213287 B CN 105213287B
- Authority
- CN
- China
- Prior art keywords
- weight portion
- extract
- testa tritici
- mud film
- glycerol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Zoology (AREA)
- Dermatology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to cosmetic technical field, it is specifically related to a kind of massage mud film and preparation method thereof, massage mud film of the present invention includes abrasive and skin conditioning agent, wherein abrasive is Testa Tritici, and skin conditioning agent includes: olive leaf extract, Herba portulacae extract, hydrolysis Lac regis apis albumen, Citrus junos fruit extract.Testa Tritici of the present invention is to be processed by alkali to prepare with addition hydrogen peroxide after acid neutralization again, this Testa Tritici not only has massage effect, and it is relatively low to the zest of skin, " Testa Tritici, olive leaf extract, Herba portulacae extract, hydrolysis Lac regis apis albumen and Citrus junos fruit extract " of the present invention is added in substrate, the mud film of preparation, has skin and the relatively low advantage of eye irritation.
Description
Technical field
The invention belongs to cosmetic technical field, be specifically related to the solidifying of a kind of low irritant and protect massage mud film and preparation side thereof
Method.
Background technology
Along with progress, the improving constantly of living standards of the people of society, cosmetics gradually become people's life from luxury goods
Necessary, the mud film product shown one's talent in many cosmetics of comforming in recent years is increasingly favored by consumer.Wherein press
The mud film that rubs is the product occupying larger proportion in mud film,
Generally adding massage particle in common mud film in massage mud film, existing particle mainly has two classes, a class to be PE
Particle, a class is walnut shell particle.PE has not environmentally and the shortcoming of too hard defects skin, the shortcoming that walnut shell particle has too hard defects skin.
For avoiding drawbacks described above, new massage mud film is had to list in recent years, it is simply that to add Testa Tritici, in order to prevent in massage mud film
Injured skin in massage, but this massage mud film is poor and the most good for skin because adding Testa Tritici rear stability
Protective effect, therefore, researchs and develops the new massage mud film containing Testa Tritici, significant.
Summary of the invention
For these reasons, applicant, through years of researches, obtains a kind of new massage mud film, and this mud film contains little
Testa Tritici, olive leaf extract, Herba portulacae extract, hydrolysis Lac regis apis albumen and Citrus junos fruit extract, Testa Tritici of the present invention is
Being processed addition hydrogen peroxide after neutralizing again with acid to prepare by alkali, this Testa Tritici not only has massage effect, and to skin
Zest relatively low, by " Testa Tritici, olive leaf extract, Herba portulacae extract, hydrolysis Lac regis apis albumen of the present invention
With Citrus junos fruit extract " add in substrate, the mud film of preparation, there is skin and the relatively low advantage of eye irritation.
The present invention is achieved through the following technical solutions.
A kind of massage mud film, mud film includes abrasive and skin conditioning agent, described in it is characterized in that abrasive is Testa Tritici,
Skin conditioning agent includes: olive leaf extract, Herba portulacae extract, hydrolysis Lac regis apis albumen, Citrus junos fruit extract.
The preparation method of described Testa Tritici is: Testa Tritici is ground into 40 mesh, add 10-15 times of weight of Testa Tritici,
Temperature is the purified water of 30 DEG C-40 DEG C, under stirring condition, adds the sodium acetate of wheat bran weight 0.4 times-0.6 times, continues stirring 3-
5 hours, add acetic acid and adjust pH value to be 7.0, filter, retain the clean wheat bran of Semen Tritici aestivi, add the purified water of 3-5 times of weight, add little
The hydrogen peroxide of wheat clean wheat bran weight 0.2-0.3 times, is heated to 35 DEG C-40 DEG C, stirs 25-35 minute, filters, obtains Testa Tritici
Skin, is dried, and Testa Tritici continues through 20 mesh, 40 mesh, the sieve of 60 mesh, and screening obtains Testa Tritici.
Described massage mud film, wherein Testa Tritici 4-6 weight portion, olive leaf extract 0.04-0.06 weight portion, Herba Portulacae
Extract 0.005-0.015 weight portion, hydrolysis Lac regis apis albumen 0.05-0.15 weight portion, Citrus junos fruit extract 0.005-0.015
Weight portion.
Described massage mud film, the least Testa Tritici 5 weight portion, olive leaf extract 0.05 weight portion, Herba Portulacae are extracted
Thing 0.01 weight portion, hydrolysis Lac regis apis albumen 0.1 weight portion, Citrus junos fruit extract 0.01 weight portion.
Described massage mud film raw material includes: Kaolin, glycerol, 1,3 propylene glycol, glycerol three (thylhexoic acid) ester, spermaceti are hard
Lipidol, glyceryl stearate, PEG-100 stearate, behenyl alcohol, Magnesiumaluminumsilicate, Fructus oleae europaeae fruit oil, cetearyl alcohol olive oil
Acid esters, Pyrusussuriensis smooth olive oil acid esters, squalane, bentonite, 1,2-hexanediol, 1,2-pentanediol, beta glucan, glycyrrhizic acid two
Potassium, xanthan gum, tocopherol, 1,3 butylene glycol, phenoxyethanol, benzyl alcohol, caprylyl glycol, essence, allantoin, EDTA-disodium, ethyl
Hexyl glycerol, citric acid, denatonium benzoate, Testa Tritici, olive leaf extract, Herba portulacae extract, hydrolysis Lac regis apis albumen
Part, Citrus junos fruit extract.
Described massage mud film preferred feedstock includes: Kaolin 5-15 weight portion, glycerol 1-5 weight portion, 1,3-PD 1-5
Weight portion, glycerol three (thylhexoic acid) ester 1-5 weight portion, cetearyl alcohol 1-5 weight portion, glyceryl stearate 1-3 weight portion,
PEG-100 stearate 1-3 weight portion, behenyl alcohol 0.5-1.5 weight portion, Magnesiumaluminumsilicate 0.5-1.5 weight portion, Fructus oleae europaeae fruit oil
0.4-0.6 weight portion, cetearyl alcohol olive oil acid esters 0.1-0.3 weight portion, Pyrusussuriensis smooth olive oil acid esters 0.1-0.3 weight
Part, squalane 0.05-0.15 weight portion, bentonite 0.3-0.8 weight portion, 1,2-hexanediol 0.1-0.3 weight portion, 1,2-penta 2
Alcohol 0.1-0.3 weight portion, beta glucan 0.1-0.3 weight portion, glycyrrhizic acid dipotassium 0.04-0.06 weight portion, xanthan gum 0.1-0.3
Weight portion, tocopherol 0.05-0.15 weight portion, 1,3 butylene glycol 0.004-0.006 weight portion, phenoxyethanol 0.05-0.15 weight
Amount part, benzyl alcohol 0.1-0.5 weight portion, caprylyl glycol 0.1-0.3 weight portion, essence 0.1-0.2 weight portion, allantoin 0.05-
0.15 weight portion, EDTA-disodium 0.04-0.06 weight portion, Sensiva SC50 0.05-0.15 weight portion, citric acid 0.04-
0.06 weight portion, denatonium benzoate 0.0002 weight portion, Testa Tritici 4-6 weight portion, olive leaf extract 0.04-0.06 weight
Part, Herba portulacae extract 0.005-0.015 weight portion, hydrolysis Lac regis apis albumen 0.05-0.15 weight portion, Citrus junos fruit extract
0.005-0.015 weight portion.
Described preparation method is:
(1) water intaking, Kaolin, glycerol, 1,3-propylene glycol, Magnesiumaluminumsilicate, bentonite, xanthan gum, allantoin, EDTA-bis-
Sodium, adds aqueous phase pot, after being heated to 70-75 DEG C, stirs, in suction vacuum emulsifying machine；
(2) glycerol three (thylhexoic acid) ester, cetearyl alcohol, glyceryl stearate, PEG-100 stearate, behenyl are taken
Alcohol, Fructus oleae europaeae fruit oil, cetearyl alcohol olive oil acid esters, Pyrusussuriensis smooth olive oil acid esters, squalane, tocopherol, add oil phase pot,
It is heated to 70-75 DEG C, stirs, in suction vacuum emulsifying machine；
(3) start is uniformly mixed, and stirring 1000rpm/ divides, and mixing time 20-40 minute stops stirring, is cooled to
40℃；Addition Testa Tritici, water, glycerol, 1,2-hexanediol, 1,2-pentanediol, beta glucan, glycyrrhizic acid dipotassium, leaf of Fructus oleae europaeae carry
Take thing, 1,3 butylene glycol, Herba portulacae extract, hydrolysis Lac regis apis albumen, phenoxyethanol, Citrus junos fruit extract, benzyl alcohol, Xin Gan
Alcohol, essence, Sensiva SC50, citric acid, denatonium benzoate, continue to stir, be cooled to room temperature；Fill, to obtain final product.
Testa Tritici of the present invention is: Semen Tritici aestivi (TRITICUM VULGARE) bran/TRITICUM VULGARE (WHEAT)
BRAN；
Fructus oleae europaeae of the present invention (OLEA EUROPAEA) leaf extract/OLEA EUROPAEA (OLIVE) LEAF
EXTRACT is purchased from Frantoio Galantino, and lot number is: D63；
Herba Portulacae of the present invention (PORTULACA OLERACEA) extract PORTULACA OLERACEA EXTRACT
Purchased from Bioland, lot number is: NMP-L-101335；
Hydrolysis Lac regis apis albumen of the present invention/HYDROLYZED ROYAL JELLY PROTEIN is purchased from Katakura
Chikkarin, lot number is: RBG14H29；
Fragrant citrus of the present invention (CITRUS JUNOS) berry extract/CITRUS JUNOS FRUIT EXTRACT is purchased from
ICHIMARU, lot number is: 150255；
Detailed description of the invention
Below in conjunction with example, the present invention is elaborated.Following example do not limit protection scope of the present invention.
One, Testa Tritici technical study
Testing 1 group (present invention process): Testa Tritici is ground into 40 mesh, addition 12 times of weight of Testa Tritici, temperature are
The purified water of 35 DEG C, under stirring condition, adds the sodium acetate of wheat bran weight 0.5 times, continues stirring 4 hours, adds acetic acid and adjusts pH
Value is 7.0, filters, and retains the clean wheat bran of Semen Tritici aestivi, adds the purified water of 4 times of weight, adds Semen Tritici aestivi clean wheat bran weight 0.25 times
Hydrogen peroxide, is heated to 35 DEG C-40 DEG C, stirs 30 minutes, filters, obtains Testa Tritici, is dried, and Testa Tritici continues through 20
Mesh, 40 mesh, the sieve of 60 mesh, screening obtains Testa Tritici.
Testing 2 groups: Testa Tritici is ground into 40 mesh, addition 12 times of weight of Testa Tritici, temperature are the purified water of 35 DEG C,
Under stirring condition, add the sodium hydroxide of wheat bran weight 0.5 times, continue stirring 4 hours, add hydrochloric acid and adjust pH value to be 7.0, mistake
Filter, retains the clean wheat bran of Semen Tritici aestivi, adds the ethanol of 4 times of weight, is heated to 35 DEG C-40 DEG C, stirs 30 minutes, filters, obtains Semen Tritici aestivi
Wheat bran, is dried, and Testa Tritici continues through 20 mesh, 40 mesh, the sieve of 60 mesh, and screening obtains Testa Tritici.
Test 3 groups: Testa Tritici is ground into the Testa Tritici of 40 mesh, and the Testa Tritici after pulverizing joins 25 matter
In the deionized water of amount times 45 DEG C, and the pH value of aqueous solution is regulated to 9.0, mixture uses 90KHz ultrasonic agitation 2 little
Time, after being sufficiently stirred for, with 80 mesh filter-cloth filterings, obtain the clean wheat bran of Semen Tritici aestivi；The clean wheat bran of Semen Tritici aestivi prepared adds the 85% of 15 times
In ethanol solution, it is heated to micro-boiling (about 80 DEG C), afterwards, keeps micro-boiling, reflux 2.5 hours, use 80 mesh filter-cloth filterings, obtain
Semen Tritici aestivi defat wheat bran；The Semen Tritici aestivi defat wheat bran obtained, under the conditions of 70 DEG C, by fluid bed, is fully dried, and repeatedly transports
After row 3 times, obtain the Semen Tritici aestivi defat wheat bran being dried, the Semen Tritici aestivi defat wheat bran obtained is continued through 20 mesh, 40 mesh, the sieve of 60 mesh
Son, screening obtains Testa Tritici.
Test method: taking above-mentioned different Testa Tritici 5g, add purified water 50ml, mix homogeneously is standby；
Take Kunming mouse, carry out repeatedly Skin Irritation Test: repeatedly Skin Irritation Test: randomly select 2 kinds of sexes
Animal, often group 6, before test, back part of animal spinal column diamond wool is cut by 24h, the left and right each about 3cm × 3cm of unhairing scope.By standby
Spreading upon on the skin of side with the Testa Tritici liquid 1ml of mix homogeneously, opposite side is coated with purified water and smears 1-2 time as comparison, every day,
Smear 14d continuously.Every day observes dermoreaction, after the 14th day smears 12 hours, marks according to standards of grading.
Table 1 dermoreaction judgment criteria
Result of the test: be shown in Table 2.
Table 2 different process Testa Tritici is to skin irritation result
Conclusion (of pressure testing): by mouse skin is carried out long-time stimulus experimental study, it can be seen that present invention process method
Obtain Testa Tritici, mouse skin is stimulated and only has 0.17 almost without, average mark, and test 2 groups, test 3 groups of processes and obtain
Obtaining Testa Tritici, have certain zest to mouse skin, therefore, applicant gives up both approaches.
Two, screening test
Test 1 group: Testa Tritici 5g, olive leaf extract 0.05g, glycerol 8g, cetearyl alcohol 5g, emulsifying agent CC 4g,
Silicone oil 6g, iso-octyl palmitate 3g, emulsifying agent MSA 2g, titanium dioxide 5g, butanediol 5g, emollient GTCC 3g, ferrum oxide
0.0003g, emulsifying agent S305 3g, phenoxyethanol 0.2g, N950 preservative 0.002g, essence 0.05g.
Preparation method: take purified water 50g, glycerol, butanediol, titanium dioxide, cetearyl alcohol, silicone oil, emollient GTCC,
Iso-octyl palmitate, Testa Tritici, olive leaf extract put into dispersed with stirring in emulsifying pot until being completely dissolved, then constant temperature 80
℃；After process, in emulsifying pot, add emulsifying agent S305, emulsifying agent CC, emulsifying agent MSA, at a temperature of 80 DEG C, homogenizing in proportion
Stirring starts cooling after fully dissolving to material body；When pot kettle temperature to be emulsified is down to 40 DEG C, add phenoxyethanol, N950 anticorrosion
Agent, essence, ferrum oxide, stirring to dissolving completely, is filtered, is stood, fill, prepare mud film.
Test 2 groups: Testa Tritici 5g, olive leaf extract 0.05g, Citrus junos fruit extract 0.01g, glycerol 8g, spermaceti are hard
Lipidol 5g, emulsifying agent CC 4g, silicone oil 6g, iso-octyl palmitate 3g, emulsifying agent MSA2g, titanium dioxide 5g, butanediol 5g, skin moistening
Agent GTCC 3g, ferrum oxide 0.0003g, emulsifying agent S305 3g, phenoxyethanol 0.2g, N950 preservative 0.002g, essence
0.05g。
Preparation method: take purified water 50g, glycerol, butanediol, titanium dioxide, cetearyl alcohol, silicone oil, emollient GTCC,
Iso-octyl palmitate, Testa Tritici, olive leaf extract, Citrus junos fruit extract put into dispersed with stirring in emulsifying pot until the most molten
Solve, then constant temperature 80 DEG C；After process, in emulsifying pot, add emulsifying agent S305, emulsifying agent CC, emulsifying agent MSA in proportion, 80
At a temperature of DEG C, homogenizing stirring starts cooling after fully dissolving to material body；When pot kettle temperature to be emulsified is down to 40 DEG C, add benzene oxygen
Ethanol, N950 preservative, essence, ferrum oxide, stirring to dissolving completely, is filtered, is stood, fill, prepare mud film.
Test 3 groups: Testa Tritici 5g, olive leaf extract 0.05g, hydrolysis Lac regis apis albumen 0.1g, glycerol 8g, spermaceti are hard
Lipidol 5g, emulsifying agent CC 4g, silicone oil 6g, iso-octyl palmitate 3g, emulsifying agent MSA 2g, titanium dioxide 5g, butanediol 5g, profit
Skin agent GTCC 3g, ferrum oxide 0.0003g, emulsifying agent S305 3g, phenoxyethanol 0.2g, N950 preservative 0.002g, essence
0.05g。
Preparation method: take purified water 50g, glycerol, butanediol, titanium dioxide, cetearyl alcohol, silicone oil, emollient GTCC,
Iso-octyl palmitate, Testa Tritici, olive leaf extract, hydrolysis Lac regis apis albumen put into dispersed with stirring in emulsifying pot until completely
Dissolve, then constant temperature 80 DEG C；After process, in emulsifying pot, add emulsifying agent S305, emulsifying agent CC, emulsifying agent MSA in proportion,
At a temperature of 80 DEG C, homogenizing stirring starts cooling after fully dissolving to material body；When pot kettle temperature to be emulsified is down to 40 DEG C, add benzene
Oxyethanol, N950 preservative, essence, ferrum oxide, stirring to dissolving completely, is filtered, is stood, fill, prepare mud film.
Test 4 groups: Testa Tritici 5g, olive leaf extract 0.05g, hydrolysis Lac regis apis albumen 0.1g, Herba portulacae extract
0.01g, glycerol 8g, cetearyl alcohol 5g, emulsifying agent CC 4g, silicone oil 6g, iso-octyl palmitate 3g, emulsifying agent MSA 2g, dioxy
Change titanium 5g, butanediol 5g, emollient GTCC 3g, ferrum oxide 0.0003g, emulsifying agent S305 3g, phenoxyethanol 0.2g, N950 prevent
Rotten agent 0.002g, essence 0.05g.
Preparation method: take purified water 50g, glycerol, butanediol, titanium dioxide, cetearyl alcohol, silicone oil, emollient GTCC,
Iso-octyl palmitate, Testa Tritici, olive leaf extract, Herba portulacae extract, hydrolysis Lac regis apis albumen are put in emulsifying pot and are stirred
Mix and disperse until being completely dissolved, then constant temperature 80 DEG C；After process, in emulsifying pot, add emulsifying agent S305, emulsifying agent in proportion
CC, emulsifying agent MSA, at a temperature of 80 DEG C, homogenizing stirring starts cooling after fully dissolving to material body；Pot kettle temperature to be emulsified drops
During to 40 DEG C, adding phenoxyethanol, N950 preservative, essence, ferrum oxide, stirring, to dissolving completely, is filtered, and stands, fill, system
For obtaining mud film.
Test 5 groups: Testa Tritici 5g, olive leaf extract 0.05g, hydrolysis Lac regis apis albumen 0.1g, Herba portulacae extract
0.01g, Citrus junos fruit extract 0.01g, glycerol 8g, cetearyl alcohol 5g, emulsifying agent CC 4g, silicone oil 6g, iso-octyl palmitate
3g, emulsifying agent MSA 2g, titanium dioxide 5g, butanediol 5g, emollient GTCC 3g, ferrum oxide 0.0003g, emulsifying agent S305
3g, phenoxyethanol 0.2g, N950 preservative 0.002g, essence 0.05g.
Preparation method: take purified water 50g, glycerol, butanediol, titanium dioxide, cetearyl alcohol, silicone oil, emollient GTCC,
Iso-octyl palmitate, Testa Tritici, olive leaf extract, Herba portulacae extract, hydrolysis Lac regis apis albumen, Citrus junos fruit extract are put
Enter dispersed with stirring in emulsifying pot until being completely dissolved, then constant temperature 80 DEG C；After process, in emulsifying pot, add emulsifying agent in proportion
S305, emulsifying agent CC, emulsifying agent MSA, at a temperature of 80 DEG C, homogenizing stirring starts cooling after fully dissolving to material body；To be emulsified
When pot kettle temperature is down to 40 DEG C, adding phenoxyethanol, N950 preservative, essence, ferrum oxide, stirring, to dissolving completely, is filtered,
Stand, fill, prepare mud film.
Test 6 groups: volcanic mud 4g, glycerol 8g, cetearyl alcohol 5g, emulsifying agent CC 4g, silicone oil 6g, iso-octyl palmitate
3g, emulsifying agent MSA 2g, titanium dioxide 5g, butanediol 5g, emollient GTCC 3g, ferrum oxide 0.0003g, emulsifying agent S305
3g, phenoxyethanol 0.2g, N950 preservative 0.002g, essence 0.05g.
Preparation method: take purified water 50g, volcanic mud, glycerol, butanediol, titanium dioxide, cetearyl alcohol, silicone oil, skin moistening
Agent GTCC, iso-octyl palmitate put into dispersed with stirring in emulsifying pot until being completely dissolved, then constant temperature 80 DEG C；After process, by than
Example adds emulsifying agent S305, emulsifying agent CC, emulsifying agent MSA in emulsifying pot, and at a temperature of 80 DEG C, homogenizing stirring is abundant to material body
Cooling is started after dissolving；When pot kettle temperature to be emulsified is down to 40 DEG C, add phenoxyethanol, N950 preservative, essence, oxidation
Ferrum, stirring to dissolving completely, is filtered, is stood, fill, to obtain final product.
Above-mentioned test Testa Tritici is to test 1 group of Testa Tritici obtained in test one.
Eye irritant test
Test method: female volunteers 60, ophthalmologic examination, without disease of eye, random packet, takes above-mentioned different mud film
1.0g, uniform application is at volunteer's upper eyelid, and volunteer closes one's eyes and has a rest 5 minutes, washes mud film, repeats after 3 hours
Testing 1 time, carry out altogether 5 times, after the 5th test, ophthalmologist checks, marks.
Table 3 eye irritation test scores standard
| Mark | Conjunctiva blood vessel | Edema | Secretions |
| 0 | Normally | Nothing | Nothing |
| 1 | Suspicious hyperemia | Suspicious edema | Have individually |
| 2 | Slight congested | Slight edema | A little |
| 3 | Congested | Edema | Have |
| 4 | Serious congested | Severe edema | Many secretions |
Result of the test: the results are shown in Table 4.
Table 4 different tests group is to eye irritation result
| Group | Conjunctiva blood vessel average score | Edema average score | Secretions average score |
| Test 1 group | 1.55 | 1.76 | 1.02 |
| Test 2 groups | 1.67 | 1.94 | 1.21 |
| Test 3 groups | 1.81 | 1.73 | 1.04 |
| Test 4 groups | 0.42 | 0.37 | 0.53 |
| Test 5 groups | 0.00 | 0.10 | 0.20 |
| Test 6 groups | 0.86 | 0.81 | 1.24 |
Conclusion (of pressure testing): by Testa Tritici of the present invention and olive leaf extract, Herba portulacae extract, hydrolysis Lac regis apis albumen,
Citrus junos fruit extract is put into and is prepared as mud film in substrate, to eye irritation almost without, and other group mud films, stings eyes
Swash the biggest, therefore give up.
Three, checking test
Test 1 group: Kaolin 5g, glycerol 1g, 1,3 propylene glycol 1g, glycerol three (thylhexoic acid) ester 1g, cetearyl alcohol
1g, glyceryl stearate 1g, PEG-100 stearate 1g, behenyl alcohol 0.5g, Magnesiumaluminumsilicate 0.5g, Fructus oleae europaeae fruit oil 0.4g, whale
Wax stearyl alcohol olive oil acid esters 0.1g, Pyrusussuriensis smooth olive oil acid esters 0.1g, squalane 0.05g, bentonite 0.3g, 1,2-hexanediol
0.1g, 1,2-pentanediol 0.1g, beta glucan 0.1g, glycyrrhizic acid dipotassium 0.04g, xanthan gum 0.1g, tocopherol 0.05g, 1,3-
Butanediol 0.004g, phenoxyethanol 0.05g, benzyl alcohol 0.1-g, caprylyl glycol 0.1g, essence 0.1g, allantoin 0.05g, EDTA-
Disodium 0.04g, Sensiva SC50 0.05g, citric acid 0.04g, denatonium benzoate 0.0002g, Testa Tritici 4g, leaf of Fructus oleae europaeae carry
Take thing 0.04g, Herba portulacae extract 0.005g, hydrolysis Lac regis apis albumen 0.05g, Citrus junos fruit extract 0.005g.
Test 2 groups: Kaolin 15g, glycerol 5g, 1,3 propylene glycol 5g, glycerol three (thylhexoic acid) ester 5g, cetearyl alcohol
5g, glyceryl stearate 3g, PEG-100 stearate 3g, behenyl alcohol 1.5g, Magnesiumaluminumsilicate 1.5g, Fructus oleae europaeae fruit oil 0.6g, whale
Wax stearyl alcohol olive oil acid esters 0.3g, Pyrusussuriensis smooth olive oil acid esters 0.3g, squalane 0.15g, bentonite 0.8g, 1,2-hexanediol
0.3g, 1,2-pentanediol 0.3g, beta glucan 0.3g, glycyrrhizic acid dipotassium 0.06g, xanthan gum 0.3g, tocopherol 0.15g, 1,3-
Butanediol 0.006g, phenoxyethanol 0.15g, benzyl alcohol 0.5g, caprylyl glycol 0.3g, essence 0.2g, allantoin 0.15g, EDTA-bis-
Sodium 0.06g, Sensiva SC50 0.15g, citric acid 0.06g, denatonium benzoate 0.0002g, Testa Tritici 6g, leaf of Fructus oleae europaeae extract
Thing 0.06g, Herba portulacae extract 0.015g, hydrolysis Lac regis apis albumen 0.15g, Citrus junos fruit extract 0.015g.
Test 3 groups: Kaolin 10g, glycerol 3g, 1,3 propylene glycol 2.5g, glycerol three (thylhexoic acid) ester 2.5g, spermaceti are hard
Lipidol 3g, glyceryl stearate 2g, PEG-100 stearate 2g, behenyl alcohol 1g, Magnesiumaluminumsilicate 1g, Fructus oleae europaeae fruit oil 0.5g, whale
Wax stearyl alcohol olive oil acid esters 0.2g, Pyrusussuriensis smooth olive oil acid esters 0.2g, squalane 0.1g, bentonite 0.6g, 1,2-hexanediol
0.2g, 1,2-pentanediol 0.2g, beta glucan 0.2g, glycyrrhizic acid dipotassium 0.05g, xanthan gum 0.2g, tocopherol 0.1g, 1,3-fourth
Glycol 0.005g, phenoxyethanol 0.1g, benzyl alcohol 0.3g, caprylyl glycol 0.2g, essence 0.15g, allantoin 0.1g, EDTA-disodium
0.05g, Sensiva SC50 0.1g, citric acid 0.05g, denatonium benzoate 0.0002g, Testa Tritici 5g, olive leaf extract
0.05g, Herba portulacae extract 0.01g, hydrolysis Lac regis apis albumen 0.1g, Citrus junos fruit extract 0.01g.
Preparation method: (1) water intaking 60g, Kaolin, glycerol 0.7g, 1,3-propylene glycol, Magnesiumaluminumsilicate, bentonite, xanthan
Glue, allantoin, EDTA-disodium, add aqueous phase pot, after being heated to 70-75 DEG C, stir, in suction vacuum emulsifying machine；
(2) glycerol three (thylhexoic acid) ester, cetearyl alcohol, glyceryl stearate, PEG-100 stearate, behenyl are taken
Alcohol, Fructus oleae europaeae fruit oil, cetearyl alcohol olive oil acid esters, Pyrusussuriensis smooth olive oil acid esters, squalane, tocopherol, add oil phase pot,
It is heated to 70-75 DEG C, stirs, in suction vacuum emulsifying machine；
(3) start is uniformly mixed, and stirring 1000rpm/ divides, and mixing time 30 minutes stops stirring, is cooled to 40
℃；Add Testa Tritici, water 4.5g, glycerol 0.3g, 1,2-hexanediol, 1,2-pentanediol, beta glucan, glycyrrhizic acid dipotassium, oil olive
Olive leaf extract, 1,3 butylene glycol, Herba portulacae extract, hydrolysis Lac regis apis albumen, phenoxyethanol, Citrus junos fruit extract, benzene first
Alcohol, caprylyl glycol, essence, Sensiva SC50, citric acid, denatonium benzoate, continue to stir, be cooled to room temperature；Fill, i.e.
?.
Two testing according to above-mentioned test one, test, result of the test is shown in Table 5, table 6.
Table 5 is to skin irritation result
Table 6 different tests group is to eye irritation result
| Group | Conjunctiva blood vessel average score | Edema average score | Secretions average score |
| Test 1 group | 0.10 | 0.20 | 0.25 |
| Test 2 groups | 0.00 | 0.30 | 0.30 |
| Test 3 groups | 0.10 | 0.00 | 0.10 |
Conclusion (of pressure testing): above-mentioned test shows, new mud film is the lowest to the zest of skin and eyes.
Preparation embodiment
Embodiment 1
Kaolin 5g, glycerol 1g, 1,3 propylene glycol 1g, glycerol three (thylhexoic acid) ester 1g, cetearyl alcohol 1g, glycerol are hard
Fat acid ester 1g, PEG-100 stearate 1g, behenyl alcohol 0.5g, Magnesiumaluminumsilicate 0.5g, Fructus oleae europaeae fruit oil 0.4g, cetearyl alcohol
Olive oil acid esters 0.1g, Pyrusussuriensis smooth olive oil acid esters 0.1g, squalane 0.05g, bentonite 0.3g, 1,2-hexanediol 0.1g, 1,
2-pentanediol 0.1g, beta glucan 0.1g, glycyrrhizic acid dipotassium 0.04g, xanthan gum 0.1g, tocopherol 0.05g, 1,3 butylene glycol
0.004g, phenoxyethanol 0.05g, benzyl alcohol 0.1-g, caprylyl glycol 0.1g, essence 0.1g, allantoin 0.05g, EDTA-disodium
0.04g, Sensiva SC50 0.05g, citric acid 0.04g, denatonium benzoate 0.0002g, Testa Tritici 4g, olive leaf extract
0.04g, Herba portulacae extract 0.005g, hydrolysis Lac regis apis albumen 0.05g, Citrus junos fruit extract 0.005g.
Preparation method: (1) water intaking 60g, Kaolin, glycerol 0.7g, 1,3-propylene glycol, Magnesiumaluminumsilicate, bentonite, xanthan
Glue, allantoin, EDTA-disodium, add aqueous phase pot, after being heated to 70-75 DEG C, stir, in suction vacuum emulsifying machine；
(2) glycerol three (thylhexoic acid) ester, cetearyl alcohol, glyceryl stearate, PEG-100 stearate, behenyl are taken
Alcohol, Fructus oleae europaeae fruit oil, cetearyl alcohol olive oil acid esters, Pyrusussuriensis smooth olive oil acid esters, squalane, tocopherol, add oil phase pot,
It is heated to 70-75 DEG C, stirs, in suction vacuum emulsifying machine；
(3) start is uniformly mixed, and stirring 1000rpm/ divides, and mixing time 20-40 minute stops stirring, is cooled to
40℃；Add Testa Tritici, water 4.5g, glycerol 0.3g, 1,2-hexanediol, 1,2-pentanediol, beta glucan, glycyrrhizic acid dipotassium, oil
Olive leaf P.E, 1,3 butylene glycol, Herba portulacae extract, hydrolysis Lac regis apis albumen, phenoxyethanol, Citrus junos fruit extract, benzene
Methanol, caprylyl glycol, essence, Sensiva SC50, citric acid, denatonium benzoate, continue to stir, be cooled to room temperature；Fill,
Obtain.
Embodiment 2
Kaolin 15g, glycerol 5g, 1,3 propylene glycol 5g, glycerol three (thylhexoic acid) ester 5g, cetearyl alcohol 5g, glycerol are hard
Fat acid ester 3g, PEG-100 stearate 3g, behenyl alcohol 1.5g, Magnesiumaluminumsilicate 1.5g, Fructus oleae europaeae fruit oil 0.6g, cetearyl alcohol
Olive oil acid esters 0.3g, Pyrusussuriensis smooth olive oil acid esters 0.3g, squalane 0.15g, bentonite 0.8g, 1,2-hexanediol 0.3g, 1,
2-pentanediol 0.3g, beta glucan 0.3g, glycyrrhizic acid dipotassium 0.06g, xanthan gum 0.3g, tocopherol 0.15g, 1,3 butylene glycol
0.006g, phenoxyethanol 0.15g, benzyl alcohol 0.5g, caprylyl glycol 0.3g, essence 0.2g, allantoin 0.15g, EDTA-disodium
0.06g, Sensiva SC50 0.15g, citric acid 0.06g, denatonium benzoate 0.0002g, Testa Tritici 6g, olive leaf extract
0.06g, Herba portulacae extract 0.015g, hydrolysis Lac regis apis albumen 0.15g, Citrus junos fruit extract 0.015g.
Preparation method: (1) water intaking 60g, Kaolin, glycerol 0.7g, 1,3-propylene glycol, Magnesiumaluminumsilicate, bentonite, xanthan
Glue, allantoin, EDTA-disodium, add aqueous phase pot, after being heated to 70-75 DEG C, stir, in suction vacuum emulsifying machine；
(2) glycerol three (thylhexoic acid) ester, cetearyl alcohol, glyceryl stearate, PEG-100 stearate, behenyl are taken
Alcohol, Fructus oleae europaeae fruit oil, cetearyl alcohol olive oil acid esters, Pyrusussuriensis smooth olive oil acid esters, squalane, tocopherol, add oil phase pot,
It is heated to 70-75 DEG C, stirs, in suction vacuum emulsifying machine；
(3) start is uniformly mixed, and stirring 1000rpm/ divides, and mixing time 20-40 minute stops stirring, is cooled to
40℃；Add Testa Tritici, water 4.5g, glycerol 0.3g, 1,2-hexanediol, 1,2-pentanediol, beta glucan, glycyrrhizic acid dipotassium, oil
Olive leaf P.E, 1,3 butylene glycol, Herba portulacae extract, hydrolysis Lac regis apis albumen, phenoxyethanol, Citrus junos fruit extract, benzene
Methanol, caprylyl glycol, essence, Sensiva SC50, citric acid, denatonium benzoate, continue to stir, be cooled to room temperature；Fill,
Obtain.
Embodiment 3
Kaolin 10g, glycerol 3g, 1,3 propylene glycol 2.5g, glycerol three (thylhexoic acid) ester 2.5g, cetearyl alcohol 3g, sweet
Oleostearin acid esters 2g, PEG-100 stearate 2g, behenyl alcohol 1g, Magnesiumaluminumsilicate 1g, Fructus oleae europaeae fruit oil 0.5g, cetearyl alcohol
Olive oil acid esters 0.2g, Pyrusussuriensis smooth olive oil acid esters 0.2g, squalane 0.1g, bentonite 0.6g, 1,2-hexanediol 0.2g, 1,2-
Pentanediol 0.2g, beta glucan 0.2g, glycyrrhizic acid dipotassium 0.05g, xanthan gum 0.2g, tocopherol 0.1g, 1,3 butylene glycol
0.005g, phenoxyethanol 0.1g, benzyl alcohol 0.3g, caprylyl glycol 0.2g, essence 0.15g, allantoin 0.1g, EDTA-disodium
0.05g, Sensiva SC50 0.1g, citric acid 0.05g, denatonium benzoate 0.0002g, Testa Tritici 5g, olive leaf extract
0.05g, Herba portulacae extract 0.01g, hydrolysis Lac regis apis albumen 0.1g, Citrus junos fruit extract 0.01g.
Preparation method: (1) water intaking 60g, Kaolin, glycerol 0.7g, 1,3-propylene glycol, Magnesiumaluminumsilicate, bentonite, xanthan
Glue, allantoin, EDTA-disodium, add aqueous phase pot, after being heated to 70-75 DEG C, stir, in suction vacuum emulsifying machine；
(2) glycerol three (thylhexoic acid) ester, cetearyl alcohol, glyceryl stearate, PEG-100 stearate, behenyl are taken
Alcohol, Fructus oleae europaeae fruit oil, cetearyl alcohol olive oil acid esters, Pyrusussuriensis smooth olive oil acid esters, squalane, tocopherol, add oil phase pot,
It is heated to 70-75 DEG C, stirs, in suction vacuum emulsifying machine；
(3) start is uniformly mixed, and stirring 1000rpm/ divides, and mixing time 20-40 minute stops stirring, is cooled to
40℃；Add Testa Tritici, water 4.5g, glycerol 0.3g, 1,2-hexanediol, 1,2-pentanediol, beta glucan, glycyrrhizic acid dipotassium, oil
Olive leaf P.E, 1,3 butylene glycol, Herba portulacae extract, hydrolysis Lac regis apis albumen, phenoxyethanol, Citrus junos fruit extract, benzene
Methanol, caprylyl glycol, essence, Sensiva SC50, citric acid, denatonium benzoate, continue to stir, be cooled to room temperature；Fill,
Obtain.Preparation embodiment includes but not limited to above-mentioned.
Claims (7)
1. a massage mud film, mud film includes abrasive and skin conditioning agent, it is characterised in that abrasive is Testa Tritici, and skin is adjusted
Reason agent includes: olive leaf extract, Herba portulacae extract, hydrolysis Lac regis apis albumen, Citrus junos fruit extract.
A kind of massage mud film the most according to claim 1, wherein the preparation method of Testa Tritici is: be ground into by Testa Tritici
40 mesh, addition 10-15 times of weight of Testa Tritici, temperature are the water for injection of 30 DEG C-40 DEG C, under stirring condition, add wheat bran weight
Measure the sodium acetate of 0.4 times-0.6 times, continue stirring 3-5 hour, add acetic acid and adjust pH value to be 7.0, filter, retain the clean bran of Semen Tritici aestivi
Skin, add 3-5 times of weight water for injection, add the hydrogen peroxide of Semen Tritici aestivi clean wheat bran weight 0.2-0.3 times, be heated to 35 DEG C-
40 DEG C, stirring 25-35 minute, filter, obtain Testa Tritici, be dried, Testa Tritici continues through 20 mesh, 40 mesh, the sieve of 60 mesh
Son, screening obtains Testa Tritici.
A kind of massage mud film, wherein Testa Tritici 4-6 weight portion, olive leaf extract 0.04-the most according to claim 1
0.06 weight portion, Herba portulacae extract 0.005-0.015 weight portion, hydrolysis Lac regis apis albumen 0.05-0.15 weight portion, Citrus junos fruit
Extract 0.005-0.015 weight portion.
A kind of massage mud film, wherein Testa Tritici 5 weight portion, olive leaf extract 0.05 weight
Part, Herba portulacae extract 0.01 weight portion, hydrolysis Lac regis apis albumen 0.1 weight portion, Citrus junos fruit extract 0.01 weight portion.
5. according to a kind of massage mud film described in any one of claim 1-4, it is characterised in that massage mud film raw material includes: kaolinite
Soil, glycerol, 1,3 propylene glycol, glycerol three (thylhexoic acid) ester, cetearyl alcohol, glyceryl stearate, PEG-100 stearate,
Behenyl alcohol, Magnesiumaluminumsilicate, Fructus oleae europaeae fruit oil, cetearyl alcohol olive oil acid esters, Pyrusussuriensis smooth olive oil acid esters, squalane, swelling
Soil, 1,2-hexanediol, 1,2-pentanediol, beta glucan, glycyrrhizic acid dipotassium, xanthan gum, tocopherol, 1,3 butylene glycol, benzene oxygen second
Alcohol, benzyl alcohol, caprylyl glycol, essence, allantoin, EDTA-disodium, Sensiva SC50, citric acid, denatonium benzoate, Testa Tritici,
Olive leaf extract, Herba portulacae extract, hydrolysis Lac regis apis albumen part, Citrus junos fruit extract.
6., according to a kind of massage mud film described in any one of right 1-3, wherein massage mud film raw material includes: Kaolin 5-15 weight
Part, glycerol 1-5 weight portion, 1,3-PD 1-5 weight portion, glycerol three (thylhexoic acid) ester 1-5 weight portion, cetearyl alcohol 1-
5 weight portions, glyceryl stearate 1-3 weight portion, PEG-100 stearate 1-3 weight portion, behenyl alcohol 0.5-1.5 weight portion, silicon
Acid magnalium 0.5-1.5 weight portion, Fructus oleae europaeae fruit oil 0.4-0.6 weight portion, cetearyl alcohol olive oil acid esters 0.1-0.3 weight
Part, Pyrusussuriensis smooth olive oil acid esters 0.1-0.3 weight portion, squalane 0.05-0.15 weight portion, bentonite 0.3-0.8 weight portion, 1,
2-hexanediol 0.1-0.3 weight portion, 1,2-pentanediol 0.1-0.3 weight portion, beta glucan 0.1-0.3 weight portion, glycyrrhizic acid two
Potassium 0.04-0.06 weight portion, xanthan gum 0.1-0.3 weight portion, tocopherol 0.05-0.15 weight portion, 1,3 butylene glycol 0.004-
0.006 weight portion, phenoxyethanol 0.05-0.15 weight portion, benzyl alcohol 0.1-0.5 weight portion, caprylyl glycol 0.1-0.3 weight portion,
Essence 0.1-0.2 weight portion, allantoin 0.05-0.15 weight portion, EDTA-disodium 0.04-0.06 weight portion, Sensiva SC50
0.05-0.15 weight portion, citric acid 0.04-0.06 weight portion, denatonium benzoate 0.0002 weight portion, Testa Tritici 4-6 weight portion,
Olive leaf extract 0.04-0.06 weight portion, Herba portulacae extract 0.005-0.015 weight portion, hydrolysis Lac regis apis albumen
0.05-0.15 weight portion, Citrus junos fruit extract 0.005-0.015 weight portion.
Massage mud film the most according to claim 6, wherein the preparation method of massage mud film is:
(1) water intaking, Kaolin, glycerol, 1,3-PD, Magnesiumaluminumsilicate, bentonite, xanthan gum, allantoin, EDTA-disodium, add
Enter aqueous phase pot, after being heated to 70-75 DEG C, stir, in suction vacuum emulsifying machine；
(2) glycerol three (thylhexoic acid) ester, cetearyl alcohol, glyceryl stearate, PEG-100 stearate, behenyl alcohol, oil are taken
Fructus Canarii albi fruit oil, cetearyl alcohol olive oil acid esters, Pyrusussuriensis smooth olive oil acid esters, squalane, tocopherol, add oil phase pot, heating
To 70-75 DEG C, stir, in suction vacuum emulsifying machine；
(3) start is uniformly mixed, and stirring 1000rpm/ divides, and mixing time 20-40 minute stops stirring, is cooled to 40 DEG C；
Add Testa Tritici, water, glycerol, 1,2-hexanediol, 1,2-pentanediol, beta glucan, glycyrrhizic acid dipotassium, olive leaf extract,
1,3 butylene glycol, Herba portulacae extract, hydrolysis Lac regis apis albumen, phenoxyethanol, Citrus junos fruit extract, benzyl alcohol, caprylyl glycol, perfume (or spice)
Essence, Sensiva SC50, citric acid, denatonium benzoate, continue to stir, be cooled to room temperature；Fill, to obtain final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510758339.2A CN105213287B (en) | 2015-11-08 | 2015-11-08 | The solidifying of a kind of low irritant protects massage mud film and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510758339.2A CN105213287B (en) | 2015-11-08 | 2015-11-08 | The solidifying of a kind of low irritant protects massage mud film and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN105213287A CN105213287A (en) | 2016-01-06 |
| CN105213287B true CN105213287B (en) | 2016-11-02 |
Family
ID=54982813
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510758339.2A Active CN105213287B (en) | 2015-11-08 | 2015-11-08 | The solidifying of a kind of low irritant protects massage mud film and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105213287B (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106333885B (en) * | 2016-08-25 | 2019-08-27 | 广州睿森生物科技有限公司 | One Plant Extracts and eye essence |
| CN107440958A (en) * | 2017-08-16 | 2017-12-08 | 广州市裕朝化妆品有限公司 | Power mineral nutrition is planted to releive skin makeup mud and preparation method |
| CN107550745A (en) * | 2017-08-31 | 2018-01-09 | 北京明弘科贸有限责任公司 | A kind of anticorrosive composite and its application |
| CN107648123A (en) * | 2017-11-08 | 2018-02-02 | 诺斯贝尔化妆品股份有限公司 | A kind of gentle oil-free cleaning mud film |
| CN109453079A (en) * | 2018-11-30 | 2019-03-12 | 广东科盈科技有限公司 | A kind of medical facial mask and preparation method thereof for facial skin |
| CN113666671A (en) * | 2021-08-10 | 2021-11-19 | 萍乡亨厚新材科技有限公司 | Method for manufacturing safe type color toy molding sand |
| CN114939099A (en) * | 2022-06-30 | 2022-08-26 | 哈尔滨敷尔佳科技股份有限公司 | Oil sludge control film composition and preparation method thereof |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102005054976A1 (en) * | 2005-11-16 | 2007-05-31 | Stockhausen Gmbh | Process for the preparation of a cosmetic abrasive |
| CN101427990A (en) * | 2008-12-12 | 2009-05-13 | 上海蔻漫生物科技有限公司 | Skin cleaning article |
| CN104758234A (en) * | 2015-03-11 | 2015-07-08 | 浏阳河农业产业集团股份有限公司 | Mung bean protein composite facial mask powder and preparation method thereof |
-
2015
- 2015-11-08 CN CN201510758339.2A patent/CN105213287B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN105213287A (en) | 2016-01-06 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105213287B (en) | The solidifying of a kind of low irritant protects massage mud film and preparation method thereof | |
| WO2018196481A1 (en) | Moisturizing cosmetics composition | |
| DE60320380T2 (en) | COENZYM Q10 FORMULATIONS | |
| JP4693963B2 (en) | Estrogen-like agent, collagen production promoter, and fibroblast proliferating agent | |
| CN111973641B (en) | Antidandruff compositions and methods of use thereof | |
| CN115252465B (en) | Oil-control, soothing and skin-care composition, cosmetic and preparation method and application thereof | |
| CN104622740B (en) | Purposes of the Horse chest Nut P.E in cosmeceutical is prepared | |
| CN107260571A (en) | Protein skin care item with skin repair and care action | |
| JP2000229832A (en) | Skin lotion | |
| CN110302223A (en) | A kind of hair nourishing liquid preparation and preparation method thereof for repairing hair follicle | |
| CN113995693B (en) | Essence composition of liposome with anti-inflammatory effect, and preparation method and application thereof | |
| US11331263B2 (en) | Male cleanser and manufacturing method thereof | |
| CN107802582A (en) | A kind of net white skin care compositions, its preparation method and the net white skin care item containing said composition containing birds nest extract | |
| CN105213270A (en) | Whitening spot-eliminating composition | |
| KR20140130830A (en) | Cleansing agent composition including natural compounds and method for manufacturing the same | |
| JPH08119870A (en) | Agent for normalizing turn over from rice | |
| CN112263512B (en) | Low-irritation and foam-rich cleaning composition and application thereof and shower gel | |
| CN102105142A (en) | Compositions for treating rosacea comprising chitosan and a dicarboxylic acid | |
| CN111100179B (en) | Method for obtaining compounds | |
| CN113876671A (en) | Anti-aging composition containing rape bud extract and preparation method thereof | |
| CN113876612A (en) | A facial cream composition containing liposome for increasing skin collagen density and its preparation method | |
| JP4105498B2 (en) | A composition effective for prevention and alleviation of symptoms of atopic disease | |
| CN106265155A (en) | A kind of breast of removing ornaments and formal dress, wet tissue containing this makeup removing breast and preparation method thereof | |
| WO2019233158A1 (en) | Traditional chinese medicine gel composition, preparation method and use thereof | |
| CN109700690A (en) | A kind of Poria cocos moisturizing emulsion and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder | ||
| CP01 | Change in the name or title of a patent holder |
Address after: Panyu District Hualong Town Guangzhou city Guangdong province 511434 Liu Wai Street No. 13 (No. 1 building) Patentee after: Hua An Tang biotech Group Co., Ltd. Address before: Panyu District Hualong Town Guangzhou city Guangdong province 511434 Liu Wai Street No. 13 (No. 1 building) Patentee before: City flower An Tang bio tech ltd, Guangzhou |