CN105211657A - A kind of quail grows up the feed producing method of laying period - Google Patents

A kind of quail grows up the feed producing method of laying period Download PDF

Info

Publication number
CN105211657A
CN105211657A CN201410225311.8A CN201410225311A CN105211657A CN 105211657 A CN105211657 A CN 105211657A CN 201410225311 A CN201410225311 A CN 201410225311A CN 105211657 A CN105211657 A CN 105211657A
Authority
CN
China
Prior art keywords
quail
mixture
eggshell
parts
feed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201410225311.8A
Other languages
Chinese (zh)
Inventor
张明富
李润开
张丽鈜
张雅澜
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
GUIZHOU MENGRUN QUAIL CO Ltd
Original Assignee
GUIZHOU MENGRUN QUAIL CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by GUIZHOU MENGRUN QUAIL CO Ltd filed Critical GUIZHOU MENGRUN QUAIL CO Ltd
Priority to CN201410225311.8A priority Critical patent/CN105211657A/en
Publication of CN105211657A publication Critical patent/CN105211657A/en
Pending legal-status Critical Current

Links

Landscapes

  • Feed For Specific Animals (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)
  • Fodder In General (AREA)

Abstract

The invention discloses a kind of quail to grow up the feed producing method of laying period, easy by adding pectin hydrolase, cellulase, protein decomposition enzyme, phosphoric acid, acetic acid and saccharomycete to raw material, nutritional labeling in feed is decomposed, quail can absorb the nutritional labeling in feed better, there is egg production high, the features such as egg size amount is large, simultaneously by the specially treated to eggshell, quail is enable to absorb nutritional labeling in eggshell, for the shell of making of quail provides good nutritional labeling, the thickness of eggshell can be increased; And add the coptis, cordate houttuynia, dandelion and the Radix Astragali in feed, quail can be prevented in process apocleisis and the generation of eating the diseases such as stagnant disease, pullorum disease, ulcerative enteritis of laying eggs.

Description

A kind of quail grows up the feed producing method of laying period
Technical field
The invention belongs to quail cultural technique field, particularly relate to a kind of quail and to grow up the feed producing method of laying period.
Background technology
Quail egg has another name called quail bird egg, quail ovum.Quail egg is considered to " ginseng in animal ".Should normal food be nourishing dietotherapy product.Quail egg nutritionally has unique distinction, therefore has the title of " in ovum good merchantable brand ".Subcircular, individuality is very little, generally only has about 5g, and there is sepia spot on surface.The nutritive value of quail egg, not second to egg, has better skin care, skin makeup effect.It is a kind of cuisines that quail egg is generally acknowledged, this little egg usually boil to well done or half-mature after shell, in salad, also can pickled, poach or cook jelly food.Quail egg is to the women having anaemia, irregular menstruation, it adjusts benefit, beauty treatment, skin makeup function significantly, this is because quail egg is containing nutriments such as protein, cephalin, lecithin, lysine, cystine, vitamin a, vitamin b2, vitamin b1, vitamin d, iron, phosphorus, calcium.
In prior art, application number is the patent of invention " feed of the rich selenium quail egg of a kind of output " of CN201310723723.X, its disclosed feed ingredient of growing up laying period is yellow maize 20%, barley 20%, rice bran 10%, wheat bran 5%, cottonseed cake 5%, soya-bean cake 10%, fish meal 5%, vitamin 0.8%, salt 0.2%, shellfish powder 0.2%, calcium dihydrogen phosphate 0.2% and selenium yeast 0.6%, and it can improve selenium constituent content; Application number is the invention " a kind of mixed feed producing red heart quail egg " of CN201310578051.8, it comprises and being mixed by yellow maize, dregs of beans, chili meal, corn protein powder, premix, the percentage by weight of its each component is yellow maize 55-60%, dregs of beans 25-28%, chili meal 2-4%, corn protein powder 3-5%, oyster shell whiting 7-8%, premix 1-1.5%, it improves yolk color, natural in color, pure flavor, not fugitive color.Application number is the patent of invention " a kind of being used for feeds quail to produce the mixed feed of high-iodine quail eggs " of CN94102099.1, it mixes by through pretreated cereals feed, bran feed, dregs of beans, cotton dregs, fish meal, active dry yeasr, high iodine mineral substance premix, vitamin-amino acid-pharmaceutical premixed material and mineral feed of replenishing the calcium, impel iodine rich long-pending in quail egg by controlling the addition of sulfonated bodies and the consumption of other raw material, and its amount of iodine is stable in certain scope, thus produce the quail egg of different amount of iodine.Above three sections of patents all mention the feed of the nutritional labelings such as different proteins, vitamin, amino acid, even be rich in the composition of the element such as selenium, iodine, to a certain extent can the egg production of quail, the element such as Selenium Supplement, iodine, but the processing technology due to its feed is all beat the processes such as powder, heating, granulation and packaging, because raw material major part is plant, there is cell membrane in plant, after heating is boiled, part cell membrane is also had not to be destroyed, after quail eats this kind of feed, the speed digested and assimilated is comparatively slow, can affect the frequency of laying eggs of quail.
Improving quail egg thickness and preventing in eggshell fragmentation, application number is that the patent of invention of CN201210266491.5 discloses a kind of feed addictive improving quail eggshell quality in summer, it comprises CAS Hy.d5-8 part, vitamin C 100-200 part, sodium acid carbonate 3000-5000 part, microlith powder 20000-30000 part, middling flour 60000-70000 part, this technology can strengthen shell thickness and intensity by feed addictive, reduces the breakage rate of quail egg; But microlith powder and middling flour are all insoluble compounds, the digestion and absorption of quail to microlith powder and middling flour is very little, plays effect is very little to eggshell, and be suitable for too much, the stomach burden of quail can be caused large, cannot better absorb other nutritional labelings, affect the quality of quail egg.
Summary of the invention
For solving the problems of the technologies described above, the invention provides a kind of quail to grow up the feed producing method of laying period, this quail grows up the feed of laying period by special raw material and preparation method, nutritional labeling needed for quail egg is provided to greatest extent, the protein content of quail egg and the thickness of eggshell can be increased.
The present invention is achieved by the following technical programs:
A kind of quail provided by the invention grows up the preparation method of feed of laying period, comprises the following steps:
1) 20 parts of corns, 18 portions of barleys, 13 portions of soybean, 12 parts of eggshells, 8 parts of peanut shells, 7 parts of wheat brans, 5 portions of coptiss, 4.6 portions of cordate houttuynias, 3.3 parts of dandelions, 3.4 parts of Radixs Astragali and 0.7 part of vitamin.
2) by corn, barley, soybean, peanut shell, wheat bran, it is for subsequent use that the coptis, cordate houttuynia, dandelion and the Radix Astragali are polished into powder respectively, crushed by eggshell for subsequent use;
3) by step 2) corn, barley and soy meal mix after, spray concentration is the pectin hydrolase of 10 ~ 15% and the cellulase of 5 ~ 10%, leaves standstill 12 ~ 15h and obtains mixture a; By step 2) peanut shell, wheatfeed, the coptis, cordate houttuynia, dandelion and the Radix Astragali mix after, spray the pectin hydrolase of 5 ~ 12% and the cellulase of 15 ~ 25%, leave standstill 12 ~ 15h and obtain mixture b; By step 2) first spray concentration is the protein decomposition enzyme of 10 ~ 20% in the eggshell that crushes, leave standstill 3 ~ 5h, and then spray concentration is the phosphoric acid of 12 ~ 18%, leaves standstill 1 ~ 2h and obtain mixture;
4) by step 3) the mixture a obtained, mixture b and mixture c Homogeneous phase mixing after, put into cooker boiling 30min, then pull cooling out and obtain mixture d;
5) to step 4) to obtain mixture d spray concentration be the acetum of 12 ~ 18%, regulate pH=4.5 ~ 5.0, then spray concentration is the saccharomycete solution of 45% and mixes, then sealed fermenting 3 ~ 5d, keep fermentation temperature at 25 ~ 30 DEG C, obtain semi-finished product;
6) by step 5) semi-finished product that obtain carry out granulating and drying after adding vitamin, packaging of then finding time.
Further, a kind of quail grows up the preparation method of feed of laying period, comprises the following steps:
1) 20 parts of corns, 18 portions of barleys, 13 portions of soybean, 12 parts of eggshells, 8 parts of peanut shells, 7 parts of wheat brans, 5 portions of coptiss, 4.6 portions of cordate houttuynias, 3.3 parts of dandelions, 3.4 parts of Radixs Astragali and 0.7 part of vitamin.
2) by corn, barley, soybean, peanut shell, wheat bran, it is for subsequent use that the coptis, cordate houttuynia, dandelion and the Radix Astragali are polished into powder respectively, crushed by eggshell for subsequent use;
3) by step 2) corn, barley and soy meal mix after, spray concentration is the pectin hydrolase of 13% and the cellulase of 7.5%, leaves standstill 12 ~ 15h and obtains mixture a; By step 2) peanut shell, wheatfeed, the coptis, cordate houttuynia, dandelion and the Radix Astragali mix after, spray the pectin hydrolase of 8% and the cellulase of 20%, leave standstill 12 ~ 15h and obtain mixture b; By step 2) first spray concentration is the protein decomposition enzyme of 15% in the eggshell that crushes, leave standstill 3 ~ 5h, and then spray concentration is the phosphoric acid of 15%, leaves standstill 1 ~ 2h and obtain mixture;
4) by step 3) the mixture a obtained, mixture b and mixture c Homogeneous phase mixing after, put into cooker boiling 30min, then pull cooling out and obtain mixture d;
5) to step 4) to obtain mixture d spray concentration be the acetum of 15%, regulate pH=4.5 ~ 5.0, then spray concentration is the saccharomycete solution of 45% and mixes, then sealed fermenting 3 ~ 5d, keep fermentation temperature at 25 ~ 30 DEG C, obtain semi-finished product;
6) by step 5) semi-finished product that obtain carry out granulating and drying after adding vitamin, packaging of then finding time.
Further, described saccharomycete solution is S. cervisiae.
Wherein corn, barley, soybean provide the nutritional labeling such as rich in protein, amino acid for quail, can meet quail and to lay eggs required nutrition, add vitamin simultaneously, meet the daily vitamin needs of quail.
Eggshell is the eggshell that birds, beasts and eggs strip down, and eggshell is mainly divided into film on shell, shell and egg shell membrane, and the main component of shell is CaCO 3, egg shell membrane is divided into periostracum and protein film, and its main component is albumen, and on shell, the main component of film and egg shell membrane is all film fat and memebrane protein, the middle film fat on shell in film and egg shell membrane and Membrane protein's amount different.This choice of technology quail eggshell, the eggshell nutritional labeling that its composition and quail lay eggs required is the same, use eggshell as a kind of raw material of feed, simultaneously peanut shell and wheat bran with the use of, the nutritional labeling of film, shell and egg shell membrane on the shell generating eggshell is provided to quail to greatest extent, the thickness of quail eggshell can be improved, and the generation of the situations such as quail egg is cracked can be prevented.
Coptis this product is the dry bark of rutaceae wampee PhellodendronchinenseSchneid. or cork tree PhellodendronamurenseRupr..Function with cure mainly: heat-clearing and damp-drying drug, purging intense heat and detonicating.Full for damp and hot ruffian, vomiting acid regurgitation, rush down dysentery, jaundice, unconsciousness due to high fever, heart-fire hyperactivity, dysphoria and insomnia, blood-head tells nosebleed, hot eyes, and toothache, quenches one's thirst, and carbuncle swells furunculosis; Control eczema outward, wet sore, duct is suppurated.It is burning hot that prepared RHIZOMA COPTIDIS with vino is apt to the clear part of the body cavity above the diaphragm housing the heart and lungs.For hot eyes, aphtha.Prepared RHIZOMA COPTIDIS with rhizoma zingiberis recens juice clearing stomach and stomach preventing or arresting vomiting.Tie mutually for fever and chills, damp and hot middle resistance, ruffian is completely vomitted.The cornel coptis is relaxed liver and stomach preventing or arresting vomiting.For liver-stomach disharmony, vomiting acid regurgitation.
Cordate houttuynia this product is the dry aerial parts of saururaceae plant houttuynia cordata HouttuyniacordataThunb..Tap when the luxuriant colored fringe of cauline leaf in summer is many, removing impurity, dries.Function with cure mainly: clearing heat and detoxicating, the carbuncle that disappears apocenosis, inducing diuresis for treating strangurtia.For lung carbuncle pyemesis, phlegm heat panting is coughed, hot dysentery, and heat is drenched, carbuncle sore tumefacting virus.
Dandelion this product is feverfew dandelion TaraxacummongolicumHand.-Mazz., alkali ground dandelion Taraxa-cumsinicumKitag. or belong to the dry herb of several plants together.Spend spring to autumn when just opening and excavate, removing impurity, cleans, dries.Function with cure mainly: clearing heat and detoxicating, dispersing swelling and dissipating binds, inducing diuresis for treating strangurtia.For furuncle swelling toxin, acute mastitis, scrofula, hot eyes, pharyngalgia, lung carbuncle, acute appendicitis, jaundice with damp-heat pathogen, heat drenches puckery pain.
Radix Astragali this product is the dry root of legume astragalus mongolicus Astragalusmembranaceus (Fisch.) Bge.Var.mongho-licus (Bge.) Hsiao or Astragalus membranacus Astragalusmembranaceus (Fisch.) Bge..Spring, Qiu Erji excavate, and removing fibrous root and root head, dry.Function with cure mainly: invigorating qi for strengthening superficies, diuresis holder poison, apocenosis, expelling pus and promoting granulation.Weak for the deficiency of vital energy, anorexia and loose stool, the sinking of qi of middle-jiao, rushes down prolapse of the anus for a long time, uterine bleeding of having blood in stool, exterior deficiency spontaneous perspiration, deficiency of vital energy oedema, and ulcer difficulty is burst, and burst for a long time and do not hold back, flaccidity of limbs due to deficiency of blood is yellow, and interior heat is quenched one's thirst; Chronic rephrilis protinuria, diabetes.
The coptis, cordate houttuynia, dandelion and the Radix Astragali with the use of, heat-clearing and damp-drying drug can be realized, purging intense heat and detonicating, the carbuncle that disappears apocenosis, the pharmacology such as inducing diuresis for treating strangurtia, invigorating qi for strengthening superficies, diuresis holder poison, apocenosis and expelling pus and promoting granulation are worth, and quail can be prevented in the disease such as process apocleisis and the stagnant disease of food, pullorum disease, ulcerative enteritis, mycoplasmosis, Marek's disease, quail acne, bronchitis, constipation, product soft-shelled egg disease of laying eggs.
The grow up special feature of preparation method of feed of laying period of the quail of this technology is: first use pectin hydrolase and cellulase can by corn, barley, soybean, peanut shell, wheat bran, the coptis, cordate houttuynia, the cell wall damage of dandelion and the Radix Astragali, protein decomposition enzyme can decompose film and egg shell membrane on eggshell upper casing, phosphoric acid can decompose the shell of eggshell, all raw materials simultaneously add saccharomycete after boiling and ferment, the nutritional labeling in raw material can be decomposed further, be convenient to quail absorb, saccharomycetes to make fermentation can produce the material of aromatic smell simultaneously, the appetite of quail can be increased.
Beneficial effect of the present invention is:
1, make the Middle nutrition composition of feed be easy to quail by various enzyme treatment technique and culture propagation technology to absorb, add the absorptivity of the feed nutrient of quail, add the content of quail egg protein, fat, riboflavin, vitamins and other nutritious components simultaneously;
2, by specially treated to eggshell, enable quail absorb nutritional labeling in eggshell, for the shell of making of quail provides good nutritional labeling, the thickness of eggshell can be increased;
3, by adding the coptis, cordate houttuynia, dandelion and the Radix Astragali in feed, quail can be prevented in the disease such as process apocleisis and the stagnant disease of food, pullorum disease, ulcerative enteritis, mycoplasmosis, Marek's disease, quail acne, bronchitis, constipation, product soft-shelled egg disease of laying eggs; The coptis, cordate houttuynia, dandelion and the Radix Astragali are also by culture propagation technology simultaneously, make medicinal ingredient in the coptis, cordate houttuynia, dandelion and the Radix Astragali be more conducive to the absorption of quail, prophylactic better effects if.
In order to better prove that the present invention can reach beyond thought effect, present specification provides following experimental example:
Experimental example one:
Choose ripe and be in laying period and the quail 50 of health, feed with normal diet, add up the quantity of laying eggs of the 20th day ~ 29 days after laying eggs, egg size amount, the quantity of cracked egg, the morbidity quantity of various disease, and randomly draw 10 quail eggs, detect the thickness of quail eggshell, the content of quail egg albumen, and calculate the average thickness of quail egg eggshell, the average content of the various nutritional labeling of quail egg.
Experimental example two
Choose ripe and be in laying period and the quail 50 of health, by 20kg corn, 18kg barley, 13kg soybean, 12kg eggshell, 8kg peanut shell, 7kg wheat bran, the 5kg coptis, 4.6kg cordate houttuynia, 3.3kg dandelion, the 3.4kg Radix Astragali and 0.7kg vitamin are made quail by above preparation method and to be grown up the feed of laying period, then this 50 quails are fed, add up the quantity of laying eggs of 20th ~ 29 days after laying eggs, egg size amount, the quantity of cracked egg, the morbidity quantity of various disease, and randomly draw 10 quail eggs, detect the thickness of quail eggshell, the content of the various nutritional labeling of quail egg, and calculate the average thickness of quail egg eggshell, the average content of the various nutritional labeling of quail egg.
Test example three
Choose ripe and be in laying period and the quail 50 of health, by 20kg corn, 18kg barley, 13kg soybean, 12kg eggshell, 8kg peanut shell, 7kg wheat bran, the 5kg coptis, 4.6kg cordate houttuynia, 3.3kg dandelion, the 3.4kg Radix Astragali and 0.7kg vitamin commonsense method make feed, then this 50 quails are fed, add up the quantity of laying eggs of 20th ~ 29 days after laying eggs, egg size amount, the quantity of cracked egg, the morbidity quantity of various disease, and randomly draw 10 quail eggs, detect the thickness of quail eggshell, the content of the various nutritional labeling of quail egg, and calculate the average thickness of quail egg eggshell, the average content of the various nutritional labeling of quail egg.
Test data statistical conditions:
Table 1
Sequence number Quantity of laying eggs (individual) Egg size amount (kg) The quantity (individual) of cracked egg
Test example one 435 21.55 28
Test example two 490 30.48 15
Test example three 468 24.12 21
As can be seen from Table 1, quantity three coefficients of the quantity of laying eggs in experimental example one, egg size amount and cracked egg are all not so good as test example two, three, illustrate that this quail grows up being of high nutritive value of feed ratio general feeds of laying period, good absorbing effect; Example two is compared with experimental example three by experiment, test example two is in egg production, all good than test three in egg size amount, few in the number ratio test example five of cracked egg, illustrate this feed through this preparation method make make with common process technique compared with, nutrient absorption is effective, has obvious superiority.
Table 2
As can be seen from Table 2, food in experimental example one and food stagnant disease, pullorum disease, ulcerative enteritis, mycoplasmosis, bronchitis, constipation, product soft-shelled egg disease the incidence of disease on all than test example two, three, illustrate that this quail grows up the feed ratio general feeds of laying period, can realize preventing to eat the effect with the stagnant disease of food, pullorum disease, ulcerative enteritis, mycoplasmosis, bronchitis, constipation, product soft-shelled egg disease better; Example two is compared with experimental example three by experiment, test example two is in egg production, the food of test two is significantly less than test three with the stagnant disease of food, pullorum disease, ulcerative enteritis, mycoplasmosis, bronchitis, constipation, the sick incidence of disease of product soft-shelled egg, illustrate this feed through this preparation method make make with common process technique compared with, medicinal ingredient absorbs better, better can prevent to eat and the generation of eating the diseases such as stagnant disease, pullorum disease, ulcerative enteritis, mycoplasmosis, bronchitis, constipation, product soft-shelled egg disease, there is obvious superiority.
The thickness (10 quail eggs of extraction, unit mm) of table 3 eggshell
As can be seen from Table 3, the shell thickness in experimental example one average on be all not so good as test example two, three, illustrate that this quail grows up being of high nutritive value of feed ratio general feeds of laying period, good absorbing effect, the nutrition supply that quail makes shell is more abundant; Example two is compared with experimental example three by experiment, test example two is better than test three on shell thickness, few in the number ratio test example three of cracked egg, illustrate this feed through this preparation method make make with common process technique compared with, nutrient absorption is effective, has obvious superiority.
Table 4 Analysis of Nutritive Composition (10 quail eggs of extraction)
As can be seen from Table 4, the protein in experimental example one, riboflavin, vitamin and energy are all not so good as test example two, three, illustrate that this quail grows up being of high nutritive value of feed ratio general feeds of laying period, good absorbing effect; Example two is compared with experimental example three by experiment, test example four is better than test three on protein, riboflavin, vitamin and energy, few in the number ratio test example three of cracked egg, illustrate this feed through this preparation method make make with common process technique compared with, nutrient absorption is effective, has obvious superiority.
Detailed description of the invention
Further describe technical scheme of the present invention below, but described in claimed scope is not limited to.
Embodiment one
Meanwhile, in order to realize the Expected Results that application claims reaches, the preparation method of the feed that the present invention also provides a kind of quail to grow up laying period, comprises the following steps:
2) by the raw material corn in embodiment one or two or three, barley, soybean, peanut shell, wheat bran, it is for subsequent use that the coptis, cordate houttuynia, dandelion and the Radix Astragali are polished into powder respectively, crushed by eggshell for subsequent use;
2) by step 2) corn, barley and soy meal mix after, spray concentration is the pectin hydrolase of 10% and the cellulase of 10%, leaves standstill 12 ~ 15h and obtains mixture a; By step 2) peanut shell, wheatfeed, the coptis, cordate houttuynia, dandelion and the Radix Astragali mix after, spray the pectin hydrolase of 5% and the cellulase of 25%, leave standstill 12 ~ 15h and obtain mixture b; By step 2) first spray concentration is the protein decomposition enzyme of 10% in the eggshell that crushes, leave standstill 3 ~ 5h, and then spray concentration is the phosphoric acid of 18%, leaves standstill 1 ~ 2h and obtain mixture;
3) by step 2) the mixture a obtained, mixture b and mixture c Homogeneous phase mixing after, put into cooker boiling 30min, then pull cooling out and obtain mixture d;
4) to step 3) to obtain mixture d spray concentration be the acetum of 12%, regulate pH=4.5 ~ 5.0, then spray concentration is the saccharomycete solution of 45% and mixes, then sealed fermenting 3 ~ 5d, keep fermentation temperature at 25 ~ 30 DEG C, obtain semi-finished product;
5) by step 4) semi-finished product that obtain carry out granulating and drying after adding vitamin, packaging of then finding time.
Wherein said saccharomycete solution is saccharomyces cerevisiae solution.
Wherein corn, barley, soybean provide the nutritional labeling such as rich in protein, amino acid for quail, can meet quail and to lay eggs required nutrition, add vitamin simultaneously, meet the daily vitamin needs of quail.
Eggshell is the eggshell that birds, beasts and eggs strip down, and eggshell is mainly divided into film on shell, shell and egg shell membrane, and the main component of shell is CaCO 3, egg shell membrane is divided into periostracum and protein film, and its main component is albumen, and on shell, the main component of film and egg shell membrane is all film fat and memebrane protein, the middle film fat on shell in film and egg shell membrane and Membrane protein's amount different.This choice of technology quail eggshell, the eggshell nutritional labeling that its composition and quail lay eggs required is the same, use eggshell as a kind of raw material of feed, simultaneously peanut shell and wheat bran with the use of, the nutritional labeling of film, shell and egg shell membrane on the shell generating eggshell is provided to quail to greatest extent, the thickness of quail eggshell can be improved, and the generation of the situations such as quail egg is cracked can be prevented.
Coptis this product is the dry bark of rutaceae wampee PhellodendronchinenseSchneid. or cork tree PhellodendronamurenseRupr..Function with cure mainly: heat-clearing and damp-drying drug, purging intense heat and detonicating.Full for damp and hot ruffian, vomiting acid regurgitation, rush down dysentery, jaundice, unconsciousness due to high fever, heart-fire hyperactivity, dysphoria and insomnia, blood-head tells nosebleed, hot eyes, and toothache, quenches one's thirst, and carbuncle swells furunculosis; Control eczema outward, wet sore, duct is suppurated.It is burning hot that prepared RHIZOMA COPTIDIS with vino is apt to the clear part of the body cavity above the diaphragm housing the heart and lungs.For hot eyes, aphtha.Prepared RHIZOMA COPTIDIS with rhizoma zingiberis recens juice clearing stomach and stomach preventing or arresting vomiting.Tie mutually for fever and chills, damp and hot middle resistance, ruffian is completely vomitted.The cornel coptis is relaxed liver and stomach preventing or arresting vomiting.For liver-stomach disharmony, vomiting acid regurgitation.
Cordate houttuynia this product is the dry aerial parts of saururaceae plant houttuynia cordata HouttuyniacordataThunb..Tap when the luxuriant colored fringe of cauline leaf in summer is many, removing impurity, dries.Function with cure mainly: clearing heat and detoxicating, the carbuncle that disappears apocenosis, inducing diuresis for treating strangurtia.For lung carbuncle pyemesis, phlegm heat panting is coughed, hot dysentery, and heat is drenched, carbuncle sore tumefacting virus.
Dandelion this product is feverfew dandelion TaraxacummongolicumHand.-Mazz., alkali ground dandelion Taraxa-cumsinicumKitag. or belong to the dry herb of several plants together.Spend spring to autumn when just opening and excavate, removing impurity, cleans, dries.Function with cure mainly: clearing heat and detoxicating, dispersing swelling and dissipating binds, inducing diuresis for treating strangurtia.For furuncle swelling toxin, acute mastitis, scrofula, hot eyes, pharyngalgia, lung carbuncle, acute appendicitis, jaundice with damp-heat pathogen, heat drenches puckery pain.
Radix Astragali this product is the dry root of legume astragalus mongolicus Astragalusmembranaceus (Fisch.) Bge.Var.mongho-licus (Bge.) Hsiao or Astragalus membranacus Astragalusmembranaceus (Fisch.) Bge..Spring, Qiu Erji excavate, and removing fibrous root and root head, dry.Function with cure mainly: invigorating qi for strengthening superficies, diuresis holder poison, apocenosis, expelling pus and promoting granulation.Weak for the deficiency of vital energy, anorexia and loose stool, the sinking of qi of middle-jiao, rushes down prolapse of the anus for a long time, uterine bleeding of having blood in stool, exterior deficiency spontaneous perspiration, deficiency of vital energy oedema, and ulcer difficulty is burst, and burst for a long time and do not hold back, flaccidity of limbs due to deficiency of blood is yellow, and interior heat is quenched one's thirst; Chronic rephrilis protinuria, diabetes.
The coptis, cordate houttuynia, dandelion and the Radix Astragali with the use of, heat-clearing and damp-drying drug can be realized, purging intense heat and detonicating, the carbuncle that disappears apocenosis, the pharmacology such as inducing diuresis for treating strangurtia, invigorating qi for strengthening superficies, diuresis holder poison, apocenosis and expelling pus and promoting granulation are worth, and quail can be prevented in the disease such as process apocleisis and the stagnant disease of food, pullorum disease, ulcerative enteritis, mycoplasmosis, Marek's disease, quail acne, bronchitis, constipation, product soft-shelled egg disease of laying eggs.
Embodiment two
Meanwhile, in order to realize the Expected Results that application claims reaches, the preparation method of the feed that the present invention also provides a kind of quail to grow up laying period, comprises the following steps:
2) by the raw material corn in embodiment one or two or three, barley, soybean, peanut shell, wheat bran, it is for subsequent use that the coptis, cordate houttuynia, dandelion and the Radix Astragali are polished into powder respectively, crushed by eggshell for subsequent use;
2) by step 2) corn, barley and soy meal mix after, spray concentration is the pectin hydrolase of 15% and the cellulase of 5%, leaves standstill 12 ~ 15h and obtains mixture a; By step 2) peanut shell, wheatfeed, the coptis, cordate houttuynia, dandelion and the Radix Astragali mix after, spray the pectin hydrolase of 12% and the cellulase of 15%, leave standstill 12 ~ 15h and obtain mixture b; By step 2) first spray concentration is the protein decomposition enzyme of 20% in the eggshell that crushes, leave standstill 3 ~ 5h, and then spray concentration is the phosphoric acid of 12%, leaves standstill 1 ~ 2h and obtain mixture;
3) by step 2) the mixture a obtained, mixture b and mixture c Homogeneous phase mixing after, put into cooker boiling 30min, then pull cooling out and obtain mixture d;
4) to step 3) to obtain mixture d spray concentration be the acetum of 18%, regulate pH=4.5 ~ 5.0, then spray concentration is the saccharomycete solution of 45% and mixes, then sealed fermenting 3 ~ 5d, keep fermentation temperature at 25 ~ 30 DEG C, obtain semi-finished product;
5) by step 4) semi-finished product that obtain carry out granulating and drying after adding vitamin, packaging of then finding time.
Wherein corn, barley, soybean provide the nutritional labeling such as rich in protein, amino acid for quail, can meet quail and to lay eggs required nutrition, add vitamin simultaneously, meet the daily vitamin needs of quail.
Eggshell is the eggshell that birds, beasts and eggs strip down, and eggshell is mainly divided into film on shell, shell and egg shell membrane, and the main component of shell is CaCO 3, egg shell membrane is divided into periostracum and protein film, and its main component is albumen, and on shell, the main component of film and egg shell membrane is all film fat and memebrane protein, the middle film fat on shell in film and egg shell membrane and Membrane protein's amount different.This choice of technology quail eggshell, the eggshell nutritional labeling that its composition and quail lay eggs required is the same, use eggshell as a kind of raw material of feed, simultaneously peanut shell and wheat bran with the use of, the nutritional labeling of film, shell and egg shell membrane on the shell generating eggshell is provided to quail to greatest extent, the thickness of quail eggshell can be improved, and the generation of the situations such as quail egg is cracked can be prevented.
Coptis this product is the dry bark of rutaceae wampee PhellodendronchinenseSchneid. or cork tree PhellodendronamurenseRupr..Function with cure mainly: heat-clearing and damp-drying drug, purging intense heat and detonicating.Full for damp and hot ruffian, vomiting acid regurgitation, rush down dysentery, jaundice, unconsciousness due to high fever, heart-fire hyperactivity, dysphoria and insomnia, blood-head tells nosebleed, hot eyes, and toothache, quenches one's thirst, and carbuncle swells furunculosis; Control eczema outward, wet sore, duct is suppurated.It is burning hot that prepared RHIZOMA COPTIDIS with vino is apt to the clear part of the body cavity above the diaphragm housing the heart and lungs.For hot eyes, aphtha.Prepared RHIZOMA COPTIDIS with rhizoma zingiberis recens juice clearing stomach and stomach preventing or arresting vomiting.Tie mutually for fever and chills, damp and hot middle resistance, ruffian is completely vomitted.The cornel coptis is relaxed liver and stomach preventing or arresting vomiting.For liver-stomach disharmony, vomiting acid regurgitation.
Cordate houttuynia this product is the dry aerial parts of saururaceae plant houttuynia cordata HouttuyniacordataThunb..Tap when the luxuriant colored fringe of cauline leaf in summer is many, removing impurity, dries.Function with cure mainly: clearing heat and detoxicating, the carbuncle that disappears apocenosis, inducing diuresis for treating strangurtia.For lung carbuncle pyemesis, phlegm heat panting is coughed, hot dysentery, and heat is drenched, carbuncle sore tumefacting virus.
Dandelion this product is feverfew dandelion TaraxacummongolicumHand.-Mazz., alkali ground dandelion Taraxa-cumsinicumKitag. or belong to the dry herb of several plants together.Spend spring to autumn when just opening and excavate, removing impurity, cleans, dries.Function with cure mainly: clearing heat and detoxicating, dispersing swelling and dissipating binds, inducing diuresis for treating strangurtia.For furuncle swelling toxin, acute mastitis, scrofula, hot eyes, pharyngalgia, lung carbuncle, acute appendicitis, jaundice with damp-heat pathogen, heat drenches puckery pain.
Radix Astragali this product is the dry root of legume astragalus mongolicus Astragalusmembranaceus (Fisch.) Bge.Var.mongho-licus (Bge.) Hsiao or Astragalus membranacus Astragalusmembranaceus (Fisch.) Bge..Spring, Qiu Erji excavate, and removing fibrous root and root head, dry.Function with cure mainly: invigorating qi for strengthening superficies, diuresis holder poison, apocenosis, expelling pus and promoting granulation.Weak for the deficiency of vital energy, anorexia and loose stool, the sinking of qi of middle-jiao, rushes down prolapse of the anus for a long time, uterine bleeding of having blood in stool, exterior deficiency spontaneous perspiration, deficiency of vital energy oedema, and ulcer difficulty is burst, and burst for a long time and do not hold back, flaccidity of limbs due to deficiency of blood is yellow, and interior heat is quenched one's thirst; Chronic rephrilis protinuria, diabetes.
The coptis, cordate houttuynia, dandelion and the Radix Astragali with the use of, heat-clearing and damp-drying drug can be realized, purging intense heat and detonicating, the carbuncle that disappears apocenosis, the pharmacology such as inducing diuresis for treating strangurtia, invigorating qi for strengthening superficies, diuresis holder poison, apocenosis and expelling pus and promoting granulation are worth, and quail can be prevented in the disease such as process apocleisis and the stagnant disease of food, pullorum disease, ulcerative enteritis, mycoplasmosis, Marek's disease, quail acne, bronchitis, constipation, product soft-shelled egg disease of laying eggs.
Embodiment three
Described quail grows up the preparation method of feed of laying period, comprises the following steps:
2) by corn, barley, soybean, peanut shell, wheat bran, it is for subsequent use that the coptis, cordate houttuynia, dandelion and the Radix Astragali are polished into powder respectively, crushed by eggshell for subsequent use;
2) by step 2) corn, barley and soy meal mix after, spray concentration is the pectin hydrolase of 13% and the cellulase of 7.5%, leaves standstill 12 ~ 15h and obtains mixture a; By step 2) peanut shell, wheatfeed, the coptis, cordate houttuynia, dandelion and the Radix Astragali mix after, spray the pectin hydrolase of 8% and the cellulase of 20%, leave standstill 12 ~ 15h and obtain mixture b; By step 2) first spray concentration is the protein decomposition enzyme of 15% in the eggshell that crushes, leave standstill 3 ~ 5h, and then spray concentration is the phosphoric acid of 15%, leaves standstill 1 ~ 2h and obtain mixture;
3) by step 2) the mixture a obtained, mixture b and mixture c Homogeneous phase mixing after, put into cooker boiling 30min, then pull cooling out and obtain mixture d;
4) to step 3) to obtain mixture d spray concentration be the acetum of 15%, regulate pH=4.5 ~ 5.0, then spray concentration is the saccharomycete solution of 45% and mixes, then sealed fermenting 3 ~ 5d, keep fermentation temperature at 25 ~ 30 DEG C, obtain semi-finished product;
5) by step 4) semi-finished product that obtain carry out granulating and drying after adding vitamin, packaging of then finding time.
Wherein corn, barley, soybean provide the nutritional labeling such as rich in protein, amino acid for quail, can meet quail and to lay eggs required nutrition, add vitamin simultaneously, meet the daily vitamin needs of quail.
Eggshell is the eggshell that birds, beasts and eggs strip down, and eggshell is mainly divided into film on shell, shell and egg shell membrane, and the main component of shell is CaCO 3, egg shell membrane is divided into periostracum and protein film, and its main component is albumen, and on shell, the main component of film and egg shell membrane is all film fat and memebrane protein, the middle film fat on shell in film and egg shell membrane and Membrane protein's amount different.This choice of technology quail eggshell, the eggshell nutritional labeling that its composition and quail lay eggs required is the same, use eggshell as a kind of raw material of feed, simultaneously peanut shell and wheat bran with the use of, the nutritional labeling of film, shell and egg shell membrane on the shell generating eggshell is provided to quail to greatest extent, the thickness of quail eggshell can be improved, and the generation of the situations such as quail egg is cracked can be prevented.
Coptis this product is the dry bark of rutaceae wampee PhellodendronchinenseSchneid. or cork tree PhellodendronamurenseRupr..Function with cure mainly: heat-clearing and damp-drying drug, purging intense heat and detonicating.Full for damp and hot ruffian, vomiting acid regurgitation, rush down dysentery, jaundice, unconsciousness due to high fever, heart-fire hyperactivity, dysphoria and insomnia, blood-head tells nosebleed, hot eyes, and toothache, quenches one's thirst, and carbuncle swells furunculosis; Control eczema outward, wet sore, duct is suppurated.It is burning hot that prepared RHIZOMA COPTIDIS with vino is apt to the clear part of the body cavity above the diaphragm housing the heart and lungs.For hot eyes, aphtha.Prepared RHIZOMA COPTIDIS with rhizoma zingiberis recens juice clearing stomach and stomach preventing or arresting vomiting.Tie mutually for fever and chills, damp and hot middle resistance, ruffian is completely vomitted.The cornel coptis is relaxed liver and stomach preventing or arresting vomiting.For liver-stomach disharmony, vomiting acid regurgitation.
Cordate houttuynia this product is the dry aerial parts of saururaceae plant houttuynia cordata HouttuyniacordataThunb..Tap when the luxuriant colored fringe of cauline leaf in summer is many, removing impurity, dries.Function with cure mainly: clearing heat and detoxicating, the carbuncle that disappears apocenosis, inducing diuresis for treating strangurtia.For lung carbuncle pyemesis, phlegm heat panting is coughed, hot dysentery, and heat is drenched, carbuncle sore tumefacting virus.
Dandelion this product is feverfew dandelion TaraxacummongolicumHand.-Mazz., alkali ground dandelion Taraxa-cumsinicumKitag. or belong to the dry herb of several plants together.Spend spring to autumn when just opening and excavate, removing impurity, cleans, dries.Function with cure mainly: clearing heat and detoxicating, dispersing swelling and dissipating binds, inducing diuresis for treating strangurtia.For furuncle swelling toxin, acute mastitis, scrofula, hot eyes, pharyngalgia, lung carbuncle, acute appendicitis, jaundice with damp-heat pathogen, heat drenches puckery pain.
Radix Astragali this product is the dry root of legume astragalus mongolicus Astragalusmembranaceus (Fisch.) Bge.Var.mongho-licus (Bge.) Hsiao or Astragalus membranacus Astragalusmembranaceus (Fisch.) Bge..Spring, Qiu Erji excavate, and removing fibrous root and root head, dry.Function with cure mainly: invigorating qi for strengthening superficies, diuresis holder poison, apocenosis, expelling pus and promoting granulation.Weak for the deficiency of vital energy, anorexia and loose stool, the sinking of qi of middle-jiao, rushes down prolapse of the anus for a long time, uterine bleeding of having blood in stool, exterior deficiency spontaneous perspiration, deficiency of vital energy oedema, and ulcer difficulty is burst, and burst for a long time and do not hold back, flaccidity of limbs due to deficiency of blood is yellow, and interior heat is quenched one's thirst; Chronic rephrilis protinuria, diabetes.
The coptis, cordate houttuynia, dandelion and the Radix Astragali with the use of, heat-clearing and damp-drying drug can be realized, purging intense heat and detonicating, the carbuncle that disappears apocenosis, the pharmacology such as inducing diuresis for treating strangurtia, invigorating qi for strengthening superficies, diuresis holder poison, apocenosis and expelling pus and promoting granulation are worth, and quail can be prevented in the disease such as process apocleisis and the stagnant disease of food, pullorum disease, ulcerative enteritis, mycoplasmosis, Marek's disease, quail acne, bronchitis, constipation, product soft-shelled egg disease of laying eggs.

Claims (3)

1. quail grows up the preparation method of feed of laying period, it is characterized in that comprising the following steps:
1) 20 parts of corns, 18 portions of barleys, 13 portions of soybean, 12 parts of eggshells, 8 parts of peanut shells, 7 parts of wheat brans, 5 portions of coptiss, 4.6 portions of cordate houttuynias, 3.3 parts of dandelions, 3.4 parts of Radixs Astragali and 0.7 part of vitamin.
2) by corn, barley, soybean, peanut shell, wheat bran, it is for subsequent use that the coptis, cordate houttuynia, dandelion and the Radix Astragali are polished into powder respectively, crushed by eggshell for subsequent use;
3) by step 2) corn, barley and soy meal mix after, spray concentration is the pectin hydrolase of 10 ~ 15% and the cellulase of 5 ~ 10%, leaves standstill 12 ~ 15h and obtains mixture a; By step 2) peanut shell, wheatfeed, the coptis, cordate houttuynia, dandelion and the Radix Astragali mix after, spray the pectin hydrolase of 5 ~ 12% and the cellulase of 15 ~ 25%, leave standstill 12 ~ 15h and obtain mixture b; By step 2) first spray concentration is the protein decomposition enzyme of 10 ~ 20% in the eggshell that crushes, leave standstill 3 ~ 5h, and then spray concentration is the phosphoric acid of 12 ~ 18%, leaves standstill 1 ~ 2h and obtain mixture;
4) by step 3) the mixture a obtained, mixture b and mixture c Homogeneous phase mixing after, put into cooker boiling 30min, then pull cooling out and obtain mixture d;
5) to step 4) to obtain mixture d spray concentration be the acetum of 12 ~ 18%, regulate pH=4.5 ~ 5.0, then spray concentration is the saccharomycete solution of 45% and mixes, then sealed fermenting 3 ~ 5d, keep fermentation temperature at 25 ~ 30 DEG C, obtain semi-finished product;
6) by step 5) semi-finished product that obtain carry out granulating and drying after adding vitamin, packaging of then finding time.
2. quail as claimed in claim 1 grows up the preparation method of feed of laying period, it is characterized in that comprising the following steps:
1) 20 parts of corns, 18 portions of barleys, 13 portions of soybean, 12 parts of eggshells, 8 parts of peanut shells, 7 parts of wheat brans, 5 portions of coptiss, 4.6 portions of cordate houttuynias, 3.3 parts of dandelions, 3.4 parts of Radixs Astragali and 0.7 part of vitamin.
2) by corn, barley, soybean, peanut shell, wheat bran, it is for subsequent use that the coptis, cordate houttuynia, dandelion and the Radix Astragali are polished into powder respectively, crushed by eggshell for subsequent use;
3) by step 2) corn, barley and soy meal mix after, spray concentration is the pectin hydrolase of 13% and the cellulase of 7.5%, leaves standstill 12 ~ 15h and obtains mixture a; By step 2) peanut shell, wheatfeed, the coptis, cordate houttuynia, dandelion and the Radix Astragali mix after, spray the pectin hydrolase of 8% and the cellulase of 20%, leave standstill 12 ~ 15h and obtain mixture b; By step 2) first spray concentration is the protein decomposition enzyme of 15% in the eggshell that crushes, leave standstill 3 ~ 5h, and then spray concentration is the phosphoric acid of 15%, leaves standstill 1 ~ 2h and obtain mixture;
4) by step 3) the mixture a obtained, mixture b and mixture c Homogeneous phase mixing after, put into cooker boiling 30min, then pull cooling out and obtain mixture d;
5) to step 4) to obtain mixture d spray concentration be the acetum of 15%, regulate pH=4.5 ~ 5.0, then spray concentration is the saccharomycete solution of 45% and mixes, then sealed fermenting 3 ~ 5d, keep fermentation temperature at 25 ~ 30 DEG C, obtain semi-finished product;
6) by step 5) semi-finished product that obtain carry out granulating and drying after adding vitamin, packaging of then finding time.
3. quail as claimed in claim 1 or 2 grows up the preparation method of feed of laying period, it is characterized in that described saccharomycete solution is S. cervisiae.
CN201410225311.8A 2014-05-26 2014-05-26 A kind of quail grows up the feed producing method of laying period Pending CN105211657A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201410225311.8A CN105211657A (en) 2014-05-26 2014-05-26 A kind of quail grows up the feed producing method of laying period

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201410225311.8A CN105211657A (en) 2014-05-26 2014-05-26 A kind of quail grows up the feed producing method of laying period

Publications (1)

Publication Number Publication Date
CN105211657A true CN105211657A (en) 2016-01-06

Family

ID=54981271

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201410225311.8A Pending CN105211657A (en) 2014-05-26 2014-05-26 A kind of quail grows up the feed producing method of laying period

Country Status (1)

Country Link
CN (1) CN105211657A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107439839A (en) * 2017-09-15 2017-12-08 河南科技大学 A kind of feed addictive for improving egg quail egg laying performance and preparation method thereof

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102726594A (en) * 2012-06-04 2012-10-17 郝伟星 High-efficiency multienzyme concentration forage
CN102894215A (en) * 2012-09-13 2013-01-30 吉林省农业科学院 Traditional Chinese medicine multi-enzyme bacterium straw composite feed for livestock and poultry
CN103299951A (en) * 2012-03-09 2013-09-18 张惠蓉 Efficient high-quality quail cultivation technique
CN103461694A (en) * 2013-08-09 2013-12-25 江苏农林职业技术学院 Chinese herbal medicinal additive for improving laying rate of quails, and preparation method and application thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103299951A (en) * 2012-03-09 2013-09-18 张惠蓉 Efficient high-quality quail cultivation technique
CN102726594A (en) * 2012-06-04 2012-10-17 郝伟星 High-efficiency multienzyme concentration forage
CN102894215A (en) * 2012-09-13 2013-01-30 吉林省农业科学院 Traditional Chinese medicine multi-enzyme bacterium straw composite feed for livestock and poultry
CN103461694A (en) * 2013-08-09 2013-12-25 江苏农林职业技术学院 Chinese herbal medicinal additive for improving laying rate of quails, and preparation method and application thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107439839A (en) * 2017-09-15 2017-12-08 河南科技大学 A kind of feed addictive for improving egg quail egg laying performance and preparation method thereof

Similar Documents

Publication Publication Date Title
CN103039745B (en) Daily ration concentrated feed of egg-laying sheldrake and preparation method thereof
CN103141679B (en) Composite sheep feed containing Chinese medicinal herbs
CN105124230A (en) Taihu sheep feed and production method thereof
CN103931913A (en) Snakehead formula feed and its preparation method
CN103355543A (en) Piglet forage
CN105265821A (en) Disease-resistant bean-dreg fermentation chicken feed and preparing method thereof
CN105249305A (en) Goose fat liver-containing fish flesh ball and preparation method thereof
CN105851611A (en) Feed for promoting egg laying of peacocks
CN104719907A (en) Nutritious powder of red cereals
CN105249271A (en) Goose fat liver-containing traditional Chinese medicine health ball and preparation method thereof
CN105249256A (en) Goose fat liver-containing livestock meat ball and preparation method thereof
CN104664315B (en) A kind of preparation method of the seafood soy-sauce being exclusively used in pregnant, the puerpera's diet of the cooking
CN105211658A (en) A kind of quail grows up the feed of laying period
CN105410353A (en) Selenium-rich sheep-breeding feed and preparation method thereof
CN104824387A (en) Composite free-range chicken feed containing residue from silkworm pupae and preparation method of same
CN104068233A (en) Pig feed for clearing heat and preventing diseases and preparation method thereof
CN107373176A (en) Diseases prevention feed of one breeder and preparation method thereof
CN105211657A (en) A kind of quail grows up the feed producing method of laying period
CN104068244A (en) Palatable fermented crucian feed and preparing method of palatable fermented crucian feed
CN106974127A (en) A kind of feed addictive and preparation method thereof
CN106306568A (en) Feed capable of improving selenium content of snakeheads
CN105941959A (en) Laying hen feed capable of alleviating heat stress and preparation method thereof
CN105249257A (en) Wild vegetable-containing goose fat liver ball with effects of reducing blood pressure and blood fat and preparation method thereof
CN104824385A (en) Free-range chicken feed containing residue from silkworm pupae and preparation method of same
CN104304701A (en) Meat duck feed containing corn root fermentation material and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20160106

RJ01 Rejection of invention patent application after publication