CN105198607A - Method for preparing multi-nutrition insecticidal sterilization mixed fertilizer materials - Google Patents
Method for preparing multi-nutrition insecticidal sterilization mixed fertilizer materials Download PDFInfo
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- CN105198607A CN105198607A CN201510634558.XA CN201510634558A CN105198607A CN 105198607 A CN105198607 A CN 105198607A CN 201510634558 A CN201510634558 A CN 201510634558A CN 105198607 A CN105198607 A CN 105198607A
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- disinsection
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/40—Bio-organic fraction processing; Production of fertilisers from the organic fraction of waste or refuse
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Abstract
The invention discloses a method for preparing multi-nutrition insecticidal sterilization mixed fertilizer materials, which comprises steps: quassia, garlic straws, neem tree roots, radix curcumas and phillyrin are dried, smashed and screened for the first time to obtain materials A, the materials A are put into a prefabricated extract liquid, are ultrasonically processed after being uniformly mixed, then are filtered and concentrated to obtain materials B, the materials B, gelatin, chitosan, attapulgite, dicyclohexyl phthalate, low molecular weight polyethylene glycols and ethyl alcohol are uniformly fixed, and are dried to obtain Chinese herbal medicine active bactericidal pesticides, and multi-nutrition insecticidal sterilization mixed fertilizer materials are prep rerated by granulating after the Chinese herbal medicine active bactericidal pesticides and decomposed manure are uniformly fixed. The multi-nutrition insecticidal sterilization mixed fertilizer materials contain rich nutrient substances such as organic matters and microelements and the like, and has insecticidal sterilization effects simultaneously.
Description
Technical field
The present invention relates to Bulk Blending Fertilizer auxiliary material preparing technical field, particularly relate to a kind of preparation method of many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material.
Background technology
Bulk blended fertilizer is fertile also known as BB, be dry mixed fertilizer, it is the chemical fertilizer of in nitrogenous, phosphorus, potassium three kinds of nutritive elements any two or three, for raw material with straight fertilizer or compound manure, made by simple mechanically mixing, without remarkable chemical reaction in mixing process, be a kind of cheap, fertilizer variety easy to use, likes by vast farmers deeply.But along with cultivating for a long time of ploughing, soil fertility is more poor, how while using Bulk Blending Fertilizer, nurses one's health soil fertility, alleviate the soil organism, medium trace element loss, be called the focus direction of research at present; Meanwhile, along with the attention of people's environmental pollution, for the control to widespread pollution from the overuse of fertilizers and pesticides in rural area, environment protection type insecticidal, sterilant are also used more and more widely.
Summary of the invention
Based on the technical problem that background technology exists, the present invention proposes a kind of preparation method of many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material, many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material of gained contains the nutritive substances such as abundant organic matter, trace element, possesses sterilization and disinsection effect simultaneously.
The preparation method of a kind of many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material that the present invention proposes, comprises the following steps:
S1, by quassia, garlic stalk, chinaberry root, turmeric, the capsule of weeping forsythia first time dry, pulverize, sieve and obtain material A;
S2, material A is dropped in prefabricated extracting solution, carry out supersound process after stirring, then filter, concentratedly obtain feed liquid B;
S3, feed liquid B, gelatin, chitosan, attapulgite, dicyclohexyl phthalate, low molecular poly, ethanol are mixed, drying obtains the active sterilizing insecticide of herbal medicine;
S4, active for herbal medicine sterilizing insecticide and decomposed manure are mixed after, granulation obtains many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material.
Preferably, comprise the following steps:
S1, quassia, garlic stalk, chinaberry root, turmeric, capsule of weeping forsythia first time to be dried, pulverize, cross 40-50 mesh sieve and obtain material A;
S2, drop in prefabricated extracting solution by material A, carry out supersound process after stirring, the frequency of supersound process is 62-65kHz, the power 500-600W of supersound process, and the time of supersound process is 7-10min, then filters, and concentratedly obtains feed liquid B;
S3, be that the ethanol of 10-15wt% mixes by feed liquid B, gelatin, chitosan, attapulgite, dicyclohexyl phthalate, low molecular poly, massfraction, drying obtains the active sterilizing insecticide of herbal medicine;
S4, active for herbal medicine sterilizing insecticide and decomposed manure are mixed after, granulation obtains many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material.
Preferably, in S1, the weight ratio of quassia, garlic stalk, chinaberry root, turmeric, the capsule of weeping forsythia is 20-23:14-17:7-10:3-6:2-5.
Preferably, in S2, prefabricated extracting solution is be the ethanol of 90-95wt% and volumetric molar concentration by massfraction is that the aqueous sodium hydroxide solution of 0.7-1mol% is by volume for 4-8:1-3 is mixed.
Preferably, in S2, the degree Beaume of feed liquid B is 30-35 ° of B é.
Preferably, in S3, the molecular weight of low molecular poly is 200-300.
Preferably, in S3, the weight ratio of feed liquid B, gelatin, chitosan, attapulgite is 10-15:24-27:16-19:5-8.
Preferably, in S3, the order number of attapulgite is 230-325 order.
Preferably, in S4, the preparation method of decomposed manure is: after 60-70 part feces of livestock and poultry, 30-40 part stalk slag, 20-22 part Herba Astragali Melilotoidis (Herba Astragali Sinici), 15-18 part rapeseed meal, 7-10 part clover, 10-13 part urea, 3-5 part composite fungus agent being mixed by weight, compost 12-15d, in composting process, every 1-2d stirs once, dry, pulverize and obtain compound organic fertilizer.
Preferably, comprise the steps:
S1, by weight 21-22 part quassia, 15-16 part garlic stalk, 8-9 part chinaberry root, 4-5 part turmeric, 3-4 part capsule of weeping forsythia first time to be dried, pulverize, cross 40-50 mesh sieve and obtain material A;
S2,20-25 part material A dropped in 80-100 part prefabricated extracting solution by weight, carry out supersound process after stirring, the frequency of supersound process is 62-65kHz, the power 500-600W of supersound process, the time of supersound process is 7-10min, then filters, and concentrates and obtains feed liquid B;
S3, be then that the ethanol of 10-15wt% mixes by 12-13 part feed liquid B, 25-26 part gelatin, 17-18 part chitosan, 6-7 part attapulgite, 2.5-3.5 part dicyclohexyl phthalate, 0.3-0.7 part low molecular poly, 110-130 part massfraction by weight, drying obtains the active sterilizing insecticide of herbal medicine;
S4, by weight active for 18-22 part herbal medicine sterilizing insecticide and 57-60 part decomposed manure are mixed after, granulation obtains many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material.
The present invention is to take into account nutrition and sterilization and disinsection performance for starting point, in preparation process, with quassia, garlic stalk, chinaberry root, turmeric, the capsule of weeping forsythia for main raw material, the material A obtained through the broken raw material cell wall of supersound process has extremely strong sterilization and disinsection effect, wherein, in quassia, alkaloid can produce to worm's ovum the toxicity having destructive force; And the extract sterilization and disinsection effect of garlic stalk is obvious; Fructus Forsythiae extract then effectively can suppress the breeding of common spoilage organisms in environment, germ; Rhizoma Curcumae Longae extract can produce volatile flavor, thus insect pest of tagging; And the micro-alkali that the present invention remains in preparation process can be bred by anti-bacteria, reduce soil acidification degree; Then the gelatin added, chitosan, attapulgite can adsorb, the solids component wrapped up in feed liquid B, thus greatly improve sterilization and disinsection effect of the present invention; Be simultaneously softening agent with dicyclohexyl phthalate, take low molecular poly as dispersion agent, can significantly improve degree of scatter and yield polymer films, greatly improve yield rate of the present invention; And in the preparation process of decomposed manure, with feces of livestock and poultry, stalk slag, Herba Astragali Melilotoidis (Herba Astragali Sinici), rapeseed meal, clover for raw material, greatly enrich trophic component of the present invention, the auxiliary material that the present invention is obtained meets required organic, the medium trace element of plant growth after application, effectively can also improve Soil structure, improve soil permeability, be conducive to crop root growth metabolism, promote nutrient in root absorption soil, meet plant growth demand; The urea simultaneously added and composite fungus agent can promote the maturity of decomposed manure greatly, thus significantly improve yield rate of the present invention.
Embodiment
Below, by specific embodiment, technical scheme of the present invention is described in detail.
Embodiment 1
The preparation method of a kind of many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material that the present invention proposes, comprises the steps:
S1, by weight 22 parts of quassias, 15 parts of garlic stalks, 9 parts of chinaberry roots, 4 parts of turmerics, 4 parts of capsules of weeping forsythia first times to be dried, pulverize, cross 40 mesh sieves and obtain material A;
S2, by weight 25 parts of material A are dropped in 80 parts of prefabricated extracting solutions, prefabricated extracting solution is be the ethanol of 90wt% and volumetric molar concentration by massfraction is that the aqueous sodium hydroxide solution of 1mol% is by volume for 4:3 is mixed, supersound process is carried out after stirring, the frequency of supersound process is 65kHz, the power 500W of supersound process, the time of supersound process is 10min, then filters, and concentrates and obtains the feed liquid B that degree Beaume is 30 ° of B é;
S3, by weight be then the polyoxyethylene glycol of 300 by 13 parts of feed liquid B, 25 parts of gelatin, 18 parts of chitosans, 6 part of 230 object attapulgite, 3.5 parts of dicyclohexyl phthalates, 0.3 part of molecular weight, 130 parts of massfractions are that the ethanol of 10wt% mixes, drying obtains the active sterilizing insecticide of herbal medicine;
S4, by weight the active sterilizing insecticides of 22 parts of herbal medicine and 57 parts of decomposed manures are mixed after, granulation obtains many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material; Wherein, the preparation method of decomposed manure is: after 70 parts of feces of livestock and poultry, 30 parts of stalk slags, 22 parts of Herba Astragali Melilotoidis (Herba Astragali Sinici)s, 15 parts of rapeseed meal, 10 parts of clovers, 10 parts of urea, 5 parts of composite fungus agents being mixed by weight, compost 12d, in composting process, every 2d stirs once, dry, pulverize and obtain compound organic fertilizer.
Embodiment 2
The preparation method of a kind of many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material that the present invention proposes, comprises the steps:
S1, by weight 21 parts of quassias, 16 parts of garlic stalks, 8 parts of chinaberry roots, 5 parts of turmerics, 3 parts of capsules of weeping forsythia first times to be dried, pulverize, cross 50 mesh sieves and obtain material A;
S2, by weight 20 parts of material A are dropped in 100 parts of prefabricated extracting solutions, prefabricated extracting solution is be the ethanol of 95wt% and volumetric molar concentration by massfraction is that the aqueous sodium hydroxide solution of 0.7mol% is by volume for 8:1 is mixed, supersound process is carried out after stirring, the frequency of supersound process is 62kHz, the power 600W of supersound process, the time of supersound process is 7min, then filters, and concentrates and obtains the feed liquid B that degree Beaume is 35 ° of B é;
S3, by weight be then the polyoxyethylene glycol of 200 by 12 parts of feed liquid B, 26 parts of gelatin, 17 parts of chitosans, 7 part of 325 object attapulgite, 2.5 parts of dicyclohexyl phthalates, 0.7 part of molecular weight, 110 parts of massfractions are that the ethanol of 15wt% mixes, drying obtains the active sterilizing insecticide of herbal medicine;
S4, by weight the active sterilizing insecticides of 18 parts of herbal medicine and 60 parts of decomposed manures are mixed after, granulation obtains many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material; Wherein, the preparation method of decomposed manure is: after 60 parts of feces of livestock and poultry, 40 parts of stalk slags, 20 parts of Herba Astragali Melilotoidis (Herba Astragali Sinici)s, 18 parts of rapeseed meal, 7 parts of clovers, 13 parts of urea, 3 parts of composite fungus agents being mixed by weight, compost 15d, in composting process, every 1d stirs once, dry, pulverize and obtain compound organic fertilizer.
Embodiment 3
The preparation method of a kind of many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material that the present invention proposes, comprises the steps:
S1, by weight 23 parts of quassias, 14 parts of garlic stalks, 10 parts of chinaberry roots, 3 parts of turmerics, 5 parts of capsules of weeping forsythia first times to be dried, pulverize, cross 40 mesh sieves and obtain material A;
S2, by weight 23 parts of material A are dropped in 85 parts of prefabricated extracting solutions, prefabricated extracting solution is be the ethanol of 92wt% and volumetric molar concentration by massfraction is that the aqueous sodium hydroxide solution of 0.9mol% is by volume for 5:2 is mixed, supersound process is carried out after stirring, the frequency of supersound process is 64kHz, the power 530W of supersound process, the time of supersound process is 9min, then filters, and concentrates and obtains the feed liquid B that degree Beaume is 33 ° of B é;
S3, by weight be then the polyoxyethylene glycol of 300 by 15 parts of feed liquid B, 24 parts of gelatin, 19 parts of chitosans, 5 part of 230 object attapulgite, 3.2 parts of dicyclohexyl phthalates, 0.4 part of molecular weight, 123 parts of massfractions are that the ethanol of 12wt% mixes, drying obtains the active sterilizing insecticide of herbal medicine;
S4, by weight the active sterilizing insecticides of 21 parts of herbal medicine and 58 parts of decomposed manures are mixed after, granulation obtains many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material; Wherein, the preparation method of decomposed manure is: after 67 parts of feces of livestock and poultry, 33 parts of stalk slags, 21 parts of Herba Astragali Melilotoidis (Herba Astragali Sinici)s, 16 parts of rapeseed meal, 9 parts of clovers, 11 parts of urea, 4 parts of composite fungus agents being mixed by weight, compost 13d, in composting process, every 2d stirs once, dry, pulverize and obtain compound organic fertilizer.
Embodiment 4
The preparation method of a kind of many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material that the present invention proposes, comprises the steps:
S1, by weight 20 parts of quassias, 17 parts of garlic stalks, 7 parts of chinaberry roots, 6 parts of turmerics, 2 parts of capsules of weeping forsythia first times to be dried, pulverize, cross 50 mesh sieves and obtain material A;
S2, by weight 22 parts of material A are dropped in 90 parts of prefabricated extracting solutions, prefabricated extracting solution is be the ethanol of 93wt% and volumetric molar concentration by massfraction is that the aqueous sodium hydroxide solution of 0.8mol% is by volume for 7:1.5 is mixed, supersound process is carried out after stirring, the frequency of supersound process is 63kHz, the power 560W of supersound process, the time of supersound process is 8min, then filters, and concentrates and obtains the feed liquid B that degree Beaume is 34 ° of B é;
S3, by weight be then the polyoxyethylene glycol of 250 by 10 parts of feed liquid B, 27 parts of gelatin, 16 parts of chitosans, 8 part of 325 object attapulgite, 2.8 parts of dicyclohexyl phthalates, 0.5 part of molecular weight, 116 parts of massfractions are that the ethanol of 13wt% mixes, drying obtains the active sterilizing insecticide of herbal medicine;
S4, by weight the active sterilizing insecticides of 19 parts of herbal medicine and 59 parts of decomposed manures are mixed after, granulation obtains many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material; Wherein, the preparation method of decomposed manure is: after 64 parts of feces of livestock and poultry, 36 parts of stalk slags, 20.5 parts of Herba Astragali Melilotoidis (Herba Astragali Sinici)s, 17 parts of rapeseed meal, 8 parts of clovers, 12 parts of urea, 3.5 parts of composite fungus agents being mixed by weight, compost 14d, in composting process, every 1d stirs once, dry, pulverize and obtain compound organic fertilizer.
The above; be only the present invention's preferably embodiment; but protection scope of the present invention is not limited thereto; anyly be familiar with those skilled in the art in the technical scope that the present invention discloses; be equal to according to technical scheme of the present invention and inventive concept thereof and replace or change, all should be encompassed within protection scope of the present invention.
Claims (10)
1. a preparation method for the sterilization and disinsection of nutrition more than Bulk Blending Fertilizer auxiliary material, is characterized in that, comprise the following steps:
S1, by quassia, garlic stalk, chinaberry root, turmeric, the capsule of weeping forsythia first time dry, pulverize, sieve and obtain material A;
S2, material A is dropped in prefabricated extracting solution, carry out supersound process after stirring, then filter, concentratedly obtain feed liquid B;
S3, feed liquid B, gelatin, chitosan, attapulgite, dicyclohexyl phthalate, low molecular poly, ethanol are mixed, drying obtains the active sterilizing insecticide of herbal medicine;
S4, active for herbal medicine sterilizing insecticide and decomposed manure are mixed after, granulation obtains many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material.
2. many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material according to claim 1, is characterized in that, comprise the following steps:
S1, quassia, garlic stalk, chinaberry root, turmeric, capsule of weeping forsythia first time to be dried, pulverize, cross 40-50 mesh sieve and obtain material A;
S2, drop in prefabricated extracting solution by material A, carry out supersound process after stirring, the frequency of supersound process is 62-65kHz, the power 500-600W of supersound process, and the time of supersound process is 7-10min, then filters, and concentratedly obtains feed liquid B;
S3, be that the ethanol of 10-15wt% mixes by feed liquid B, gelatin, chitosan, attapulgite, dicyclohexyl phthalate, low molecular poly, massfraction, drying obtains the active sterilizing insecticide of herbal medicine;
S4, active for herbal medicine sterilizing insecticide and decomposed manure are mixed after, granulation obtains many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material.
3. many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material according to claim 1 or 2, is characterized in that, in S1, the weight ratio of quassia, garlic stalk, chinaberry root, turmeric, the capsule of weeping forsythia is 20-23:14-17:7-10:3-6:2-5.
4. many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material according to any one of claim 1-3, it is characterized in that, in S2, prefabricated extracting solution is be the ethanol of 90-95wt% and volumetric molar concentration by massfraction is that the aqueous sodium hydroxide solution of 0.7-1mol% is by volume for 4-8:1-3 is mixed.
5. many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material according to any one of claim 1-4, is characterized in that, in S2, the degree Beaume of feed liquid B is 30-35 ° of B é.
6. many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material according to any one of claim 1-5, is characterized in that, in S3, the molecular weight of low molecular poly is 200-300.
7. many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material according to any one of claim 1-6, is characterized in that, in S3, the weight ratio of feed liquid B, gelatin, chitosan, attapulgite is 10-15:24-27:16-19:5-8.
8. many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material according to any one of claim 1-7, is characterized in that, in S3, the order number of attapulgite is 230-325 order.
9. many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material according to any one of claim 1-8, it is characterized in that, in S4, the preparation method of decomposed manure is: after 60-70 part feces of livestock and poultry, 30-40 part stalk slag, 20-22 part Herba Astragali Melilotoidis (Herba Astragali Sinici), 15-18 part rapeseed meal, 7-10 part clover, 10-13 part urea, 3-5 part composite fungus agent being mixed by weight, compost 12-15d, in composting process, every 1-2d stirs once, dry, pulverize and obtains compound organic fertilizer.
10. many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material according to any one of claim 1-9, is characterized in that, comprise the steps:
S1, by weight 21-22 part quassia, 15-16 part garlic stalk, 8-9 part chinaberry root, 4-5 part turmeric, 3-4 part capsule of weeping forsythia first time to be dried, pulverize, cross 40-50 mesh sieve and obtain material A;
S2,20-25 part material A dropped in 80-100 part prefabricated extracting solution by weight, carry out supersound process after stirring, the frequency of supersound process is 62-65kHz, the power 500-600W of supersound process, the time of supersound process is 7-10min, then filters, and concentrates and obtains feed liquid B;
S3, be then that the ethanol of 10-15wt% mixes by 12-13 part feed liquid B, 25-26 part gelatin, 17-18 part chitosan, 6-7 part attapulgite, 2.5-3.5 part dicyclohexyl phthalate, 0.3-0.7 part low molecular poly, 110-130 part massfraction by weight, drying obtains the active sterilizing insecticide of herbal medicine;
S4, by weight active for 18-22 part herbal medicine sterilizing insecticide and 57-60 part decomposed manure are mixed after, granulation obtains many nutrition sterilization and disinsection Bulk Blending Fertilizer auxiliary material.
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| CN201510634558.XA CN105198607A (en) | 2015-09-29 | 2015-09-29 | Method for preparing multi-nutrition insecticidal sterilization mixed fertilizer materials |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108440099A (en) * | 2018-04-20 | 2018-08-24 | 曾治中 | A kind of multifunctional bio pharmacological property trace-element fertilizer |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108440099A (en) * | 2018-04-20 | 2018-08-24 | 曾治中 | A kind of multifunctional bio pharmacological property trace-element fertilizer |
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