CN105191953A - Apple tree wound protective agent and preparation method thereof - Google Patents

Apple tree wound protective agent and preparation method thereof Download PDF

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Publication number
CN105191953A
CN105191953A CN201510310474.0A CN201510310474A CN105191953A CN 105191953 A CN105191953 A CN 105191953A CN 201510310474 A CN201510310474 A CN 201510310474A CN 105191953 A CN105191953 A CN 105191953A
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China
Prior art keywords
protective agent
kilogram
kilograms
apple tree
preparation
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CN201510310474.0A
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Chinese (zh)
Inventor
李敏
程存刚
厉恩茂
徐锴
李壮
安秀红
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Fruit Tree Institute of CAAS
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Fruit Tree Institute of CAAS
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Priority to CN201510310474.0A priority Critical patent/CN105191953A/en
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  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)

Abstract

The invention provides an apple tree wound protective agent and a preparation method thereof. The apple tree wound protective agent comprises the following components by weight: 10 kg of vaseline, 10 kg of liquid paraffin, 2 kg of potassium humate, 3 kg of polyvinyl alcohol, 5 kg of glycerine, 0.0003 kg of IBA, 0.0002 kg of NAA, 0.0001 kg of 6-BA, 0.0001 kg of TDZ, 0.01 kg of Ca(NO3)2, 0.001 kg of FeSO4.7H2O and 70 kg of distilled water; the preparation method comprises the steps of dissolving potassium humate in water, dissolving liquid paraffin and compounding. The apple tree wound protective agent provided by the invention has the advantages of being highly efficient, safe, low-cost, low in toxicity, pollution-free and good in healing effect, and can rapidly form a film at or around wounds after being applied, so that the moisture is maintained, the cell division is stimulated, the cell viability is enhanced, the formation of callus tissues is promoted, germs infection is prevented, and the apple tree wound protective agent is suitable for being applied.

Description

A kind of apple tree Wound protective agent and preparation method thereof
Technical field
What the present invention proposed is the chemicals that field of plant cultivation uses, specifically a kind of apple tree Wound protective agent and preparation method thereof.
Background technology
Apple is the of paramount importance fruit tree of China's economic status; pruning is the requisite technical measures that apple tree builds skeleton, regulating illumination, short bow structure fruit, raising quality; in the pruning in annual winter; due to the utilization of the technology such as sparse branching, retraction; can produce and a large amount of cut saw kerf; if these wounds are protected not in time; then easily there is frostbite, dry and cracked, withered; nutrient and dredging of moisture is caused to be obstructed; seriously undermine tree vigo(u)r; the healthy growth of impact tree body, even causes infecting of rotten pathogenic bacteria, causes the generation in Si Shuhui garden.According to Wang Caixia 2011, newborn rot scar 80.04% derived from and cut saw kerf spring, and the survey showed that for Wu Yu star, and cut the principal pathogenetic position that saw kerf is ulcer type rot, average attack rate is 47.4%, is up to 79.0%.Therefore, cut quickly-healing and the healthy growth of saw kerf, particularly important for APPLE QUALITY, high yield and fruit safety.
It is reported; China once adopted tung oil lead oil mixture, rosin edible vegetable oil mixture, soya-bean oil blue vitriol lime mixture, solid wax, lanolin, cow dung, yellow mud etc. as Wound protective agent in the 80-90 age in 20th century; not only weak effect; and environmental pollution, residual serious, safety, nontoxic production requirement can not be met.At present, commercially available product mainly with bactericidal, to treat disease scar be main, seldom consider healthy protection of cutting saw kerf, healing effect is unsatisfactory.In recent years, promote that the research of wound healing obtains certain progress for growth regulator, the research of Zhang Xicai showed, 6-BA and NAA has certain effect to wound healing, and the research of the people such as Gao Yujun, Xu Guixuan also proves that NAA is conducive to wound healing.In addition, along with the development of science and technology, Novel high-end chemical products are applied to agricultural production, and the development for Wound-healing agent provides new opportunity.
Existing apple tree wound makes to paint usually, machine oil dressing, there is the shortcomings such as healing effect difference, residence time length, contaminated environment, use be inconvenient.
Summary of the invention
In order to overcome the deficiency that prior art and material exist, the present invention proposes a kind of apple tree Wound protective agent and preparation method thereof.This protectant is by vaseline, atoleine, humic acid potassium, polyvinyl alcohol, glycerine, IBA, NAA, 6-BA, TDZ, Ca(NO 3), FeSO 47H 2o and distilled water composition, by protectant preparation process.Solve the technical problem of apple tree Wound protection.
The scheme that technical solution problem of the present invention adopts is:
Apple tree Wound protective agent is by 10 kilograms, vaseline, atoleine 10 kilograms, humic acid potassium 2 kilograms, polyvinyl alcohol 3 kilograms, glycerine 5 kilograms, IBA0.0003 kilogram, NAA0.0002 kilogram, 6-BA0.0001 kilogram, TDZ0.0001 kilogram, Ca(NO 3) 20.01 kilogram, FeSO 47H 2o0.001 kilogram and distilled water 70 kilograms composition.
Protectant preparation method:
1. humic acid potassium being dissolved in distilled water, heating water bath to 85 DEG C, adding polyvinyl alcohol, glycerine after dissolving completely respectively to dissolving completely; Above-mentioned solution is proceeded to after first being dissolved with the NaOH of a small amount of 1mol/L by IBA; NAA dissolves in above-mentioned solution after dissolving with a small amount of 95% ethanol again; 6-BA and TDZ slowly joins in above-mentioned solution after first dissolving completely with the NaOH of 0.1mol/L respectively again; Then Ca(NO is added 3) 2and FeSO 47H 2o, to dissolving, is prepared into solution A.
2. the vaseline, the atoleine heating water bath to 80 DEG C that will weigh up, stir, make mixed liquid B, for subsequent use.
3. solution A is slowly added in B solution, and stirred by agitator, mixing time 20 minutes, naturally cool.
Good effect; apple tree Wound protective agent of the present invention has efficiently, safety, abridged edition, low toxicity, the advantage that pollution-free and healing effect is good; after smearing can wound and around rapid film formation; keep moisture; irritation cell divides; strengthen cytoactive, promote Callus formation, control infection process.Be suitable for applying as apple tree Wound protective agent.
Embodiment
Apple tree Wound protective agent is by 10 kilograms, vaseline, atoleine 10 kilograms, humic acid potassium 2 kilograms, polyvinyl alcohol 3 kilograms, glycerine 5 kilograms, IBA0.0003 kilogram, NAA0.0002 kilogram, 6-BA0.0001 kilogram, TDZ0.0001 kilogram, Ca(NO 3) 20.01 kilogram, FeSO 47H 2o0.001 kilogram and distilled water 70 kilograms composition.
Protectant preparation method:
1. humic acid potassium being dissolved in distilled water, heating water bath to 85 DEG C, adding polyvinyl alcohol, glycerine after dissolving completely respectively to dissolving completely; Above-mentioned solution is proceeded to after first being dissolved with the NaOH of a small amount of 1mol/L by IBA; NAA dissolves in above-mentioned solution after dissolving with a small amount of 95% ethanol again; 6-BA and TDZ slowly joins in above-mentioned solution after first dissolving completely with the NaOH of 0.1mol/L respectively again; Then Ca(NO is added 3) 2and FeSO 47H 2o, to dissolving, is prepared into solution A.
2. the vaseline, the atoleine heating water bath to 80 DEG C that will weigh up, stir, make mixed liquid B, for subsequent use.
3. solution A is slowly added in B solution, and stirred by agitator, mixing time 20 minutes, naturally cool.
Technical characterstic of the present invention:
1. first Application IBA, NAA, 6-BA and TDZ is as healing factor, stimulates the generation of callus, and obtains optimum formula ratio.6-BA and TDZ is the growth regulator belonging to cytokinin, and activity is very high, the cell cutting saw kerf or wound circumference can be stimulated to divide, form callus fast.IBA and NAA is the material of growth promoting effects, and the basic element of cell division coordinates promotion wound healing.
2. first polyvinyl alcohol is prepared Wound protective agent as film forming agent; it is a kind of organic compound; there is the feature of film forming, hygroscopic effect and low toxicity, low-residual; the film of thin layer can be formed fast in wound after smearing; moisturizing, air permeable effect are good, can promote that phloem is to the absorption of active ingredient.
3. humic acid potassium is a kind of efficient organic potassic fertilizer, adds Ca 2+, Fe 2+after, not only can provide nutrient for wound healing, promote that callus grows fast, the resistance of fruit tree can also be improved, strengthen the frost resistance of wound.
4. the glycerine contained in the present invention, vaseline have good lock water, moisture-keeping functions, spread upon on wound, energy long time retaining water content, stop moisture evaporation, are beneficial to the absorption of active ingredient, prevent xylem dry and cracked.
5., first using the carrier as main ingredient after vaseline, atoleine mixing, form solid fraction oil emu after stirring completely with main ingredient, be convenient to packaging and carry, can directly wear gloves during use or be applied in wound with small brushes, facilitating saving of labor.
6. the present invention's composition used has safe, nontoxic, green, non-harmful feature, and the extensive use in medical science, foods and cosmetics of the composition such as vaseline, polyvinyl alcohol, the growth regulators such as NAA, 6-BA, potassium humate are also widely applied in agricultural production.
Field information test procedure and result:
1. test examination material: this test is that Demonstration Garden carries out tested by the Chinese Academy of Agricultural Sciences's fruit tree research, with main breed Fuji for examination material, carried out field demonstration test in continuous 2 years in 2012 and 2013, the life in 8 years of tree body, tree-like is slender spindle like, and rich water quality management is medium level, and other management are normal.
2. test method:
(1) start process at annual late March, the middle and lower part of doing at Shu Ti center select diameter be 3-6cm cut saw kerf coating, coating immediately after cutting, wear rubber gloves when smearing, wound is coated with last layer ointment, thickness is 1-2mm, during coating evenly, put in place, make wound completely closed.
2 process are set in this test: process I for this product, process II for fruit tree health consolidant, not smear any protectant wound for CK, often process 15 wounds, totally 45 wounds.
(2) investigation method: with reference to the method for Zhang Xicai, and slightly improve.The investigation of wound healing is carried out after falling leaves completely annual December.First be overlying on wound with blank sheet of paper during investigation, depict the contour of wound periphery and the contour of the part that do not heal, take back laboratory afterwards, be imprinted on slightly thick hardboard with carbon paper again, first cut by wound periphery, obtain the wound gross area with the scanning of leaf area instrument, then cut along the partial circuit that do not heal, record the area that do not heal.
3. test results and analysis
By the field trial of continuous 2 years, achieve good result of use.This product can improve the healing rate (P≤0.01) cutting saw kerf extremely significantly, and 2012 and 2013 respectively than contrast raising 40.93% and 32.38%.Compared with commercially available product, within 2012, this product healing rate is higher than fruit tree Kandy by 13.54%, reaches the difference of 5% level, within 2013, improves 15.42%, reaches the difference of 1% level.Illustrate that the product that the present invention develops significantly can promote wound healing, can apple production be applied to.

Claims (2)

1. apple tree Wound protective agent and preparation method thereof, is characterized in that: by 10 kilograms, vaseline, atoleine 10 kilograms, humic acid potassium 2 kilograms, polyvinyl alcohol 3 kilograms, glycerine 5 kilograms, IBA0.0003 kilogram, NAA0.0002 kilogram, 6-BA0.0001 kilogram, TDZ0.0001 kilogram, Ca(NO 3) 20.01 kilogram, FeSO 47H 2o0.001 kilogram and distilled water 70 kilograms composition.
2. a kind of apple tree Wound protective agent according to claim 1 and preparation method thereof, is characterized in that: protectant preparation method:
1) humic acid potassium being dissolved in distilled water, heating water bath to 85 DEG C, adding polyvinyl alcohol, glycerine after dissolving completely respectively to dissolving completely; Above-mentioned solution is proceeded to after first being dissolved with the NaOH of a small amount of 1mol/L by IBA; NAA dissolves in above-mentioned solution after dissolving with a small amount of 95% ethanol again; 6-BA and TDZ slowly joins in above-mentioned solution after first dissolving completely with the NaOH of 0.1mol/L respectively again; Then Ca(NO is added 3) 2and FeSO 47H 2o, to dissolving, is prepared into solution A;
2) vaseline, the atoleine heating water bath to 80 DEG C that will weigh up, stir, make mixed liquid B, for subsequent use;
3) solution A is slowly added in B solution, and stirred by agitator, mixing time 20 minutes, naturally cool.
CN201510310474.0A 2015-06-09 2015-06-09 Apple tree wound protective agent and preparation method thereof Pending CN105191953A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105753574A (en) * 2016-03-03 2016-07-13 和县朱韩瓜果种植家庭农场 Red pear fruit tree wound filling paste and preparation method thereof
CN105777341A (en) * 2016-03-03 2016-07-20 和县朱韩瓜果种植家庭农场 Red pear fruit tree wound protecting spray agent and preparation method thereof
CN107011031A (en) * 2017-04-07 2017-08-04 河南科技大学 A kind of cut protecting agent for fruit trees and its preparation method and application
WO2021063007A1 (en) * 2019-09-30 2021-04-08 枣庄学院 Plaster used for repairing tree wound and preparation method and use thereof
CN114451410A (en) * 2022-03-17 2022-05-10 山西和丰生物科技有限公司 Medicinal plaster for treating rot and cut healing of fruit trees and preparation method thereof

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CN101731243A (en) * 2009-12-04 2010-06-16 山东农业大学 Consolidant for wounds on forest fruits
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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105753574A (en) * 2016-03-03 2016-07-13 和县朱韩瓜果种植家庭农场 Red pear fruit tree wound filling paste and preparation method thereof
CN105777341A (en) * 2016-03-03 2016-07-20 和县朱韩瓜果种植家庭农场 Red pear fruit tree wound protecting spray agent and preparation method thereof
CN107011031A (en) * 2017-04-07 2017-08-04 河南科技大学 A kind of cut protecting agent for fruit trees and its preparation method and application
WO2021063007A1 (en) * 2019-09-30 2021-04-08 枣庄学院 Plaster used for repairing tree wound and preparation method and use thereof
CN114451410A (en) * 2022-03-17 2022-05-10 山西和丰生物科技有限公司 Medicinal plaster for treating rot and cut healing of fruit trees and preparation method thereof

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Application publication date: 20151230