CN105190951A - 电池复合材料及其前驱物的制备方法 - Google Patents
电池复合材料及其前驱物的制备方法 Download PDFInfo
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- CN105190951A CN105190951A CN201480022119.7A CN201480022119A CN105190951A CN 105190951 A CN105190951 A CN 105190951A CN 201480022119 A CN201480022119 A CN 201480022119A CN 105190951 A CN105190951 A CN 105190951A
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/45—Phosphates containing plural metal, or metal and ammonium
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B1/00—Single-crystal growth directly from the solid state
- C30B1/10—Single-crystal growth directly from the solid state by solid state reactions or multi-phase diffusion
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/14—Phosphates
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
- C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Battery Electrode And Active Subsutance (AREA)
Abstract
一种电池复合材料的制备方法,包括步骤:提供磷酸、第一金属源、第二金属源以及水(S100);以第一金属源、第二金属源、磷酸与水进行反应,以生成第一生成物(S200);煅烧第一生成物以生成第一前驱物或第二前驱物(S300),其中第一前驱物及第二前驱物为包含第一金属及第二金属的固溶体;以及以第一前驱物或第二前驱物与第一反应物进行反应,再煅烧反应的混合物,以生成电池复合材料(S400)。因此,可使电池产品具有两种稳定的氧化还原充放电平台,可有效提高产品的稳定性以及电性表现。
Description
PCT国内申请,说明书已公开。
Claims (1)
- PCT国内申请,权利要求书已公开。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201361820935P | 2013-05-08 | 2013-05-08 | |
US61/820,935 | 2013-05-08 | ||
PCT/CN2014/077082 WO2014180334A1 (zh) | 2013-05-08 | 2014-05-08 | 电池复合材料及其前驱物的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN105190951A true CN105190951A (zh) | 2015-12-23 |
CN105190951B CN105190951B (zh) | 2018-06-29 |
Family
ID=51866734
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201480022119.7A Active CN105190951B (zh) | 2013-05-08 | 2014-05-08 | 电池复合材料及其前驱物的制备方法 |
Country Status (8)
Country | Link |
---|---|
US (1) | US10096832B2 (zh) |
EP (1) | EP2996178A4 (zh) |
JP (1) | JP6232493B2 (zh) |
KR (1) | KR101764052B1 (zh) |
CN (1) | CN105190951B (zh) |
CA (1) | CA2911518C (zh) |
TW (1) | TWI612716B (zh) |
WO (1) | WO2014180334A1 (zh) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US10266410B2 (en) | 2015-01-08 | 2019-04-23 | Advanced Lithium Electrochemistry Co., Ltd. | Preparation method of battery composite material and precursor thereof |
CN114057177B (zh) * | 2021-11-23 | 2023-05-23 | 湖北融通高科先进材料集团股份有限公司 | 磷酸亚铁锰及其制备方法和应用 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102791625A (zh) * | 2010-03-09 | 2012-11-21 | 旭硝子株式会社 | 磷酸化合物、二次电池用正极、以及二次电池的制造方法 |
TW201305046A (zh) * | 2011-07-20 | 2013-02-01 | Advanced Lithium Electrochemistry Co Ltd | 電池複合材料及其前驅物之製備方法 |
Family Cites Families (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP3824196B2 (ja) | 1998-06-24 | 2006-09-20 | テイカ株式会社 | ビス(リン酸−水素)チタンの双晶粒子およびその製造方法 |
JP2001082083A (ja) | 1999-09-14 | 2001-03-27 | Tobishima Corp | 継手構造 |
CA2502596C (en) | 2002-10-18 | 2015-03-10 | Japan As Represented By President Of The University Of Kyusyu | Method for producing cathode material for lithium battery and lithium battery |
DE102005015613A1 (de) * | 2005-04-05 | 2006-10-12 | Süd-Chemie AG | Kristallines Ionenleitendes Nanomaterial und Verfahren zu seiner Herstellung |
JP2007284271A (ja) | 2006-04-13 | 2007-11-01 | Kyoto Univ | リン酸イオン含有排水を用いたリン酸金属塩粒子の製造方法 |
US8491861B2 (en) * | 2006-05-26 | 2013-07-23 | Eltron Research, Inc. | Synthetic process for preparation of high surface area electroactive compounds for battery applications |
KR100805910B1 (ko) | 2006-12-29 | 2008-02-21 | 한양대학교 산학협력단 | 리튬 전지용 올리빈형 양극 활물질, 이의 제조 방법, 및이를 포함하는 리튬 전지 |
US20090220858A1 (en) * | 2008-02-29 | 2009-09-03 | Byd Company Limited | Composite Compound With Mixed Crystalline Structure |
JP2009295465A (ja) | 2008-06-06 | 2009-12-17 | Iwate Univ | リチウム二次電池用正極活物質及びその製造方法 |
US8022009B2 (en) * | 2009-01-16 | 2011-09-20 | Intematix Corporation | Process for synthesizing LixFeMZO4/ carbon and LixMZO4/ carbon composite materials |
US20120237425A1 (en) | 2009-09-09 | 2012-09-20 | Takahisa Nishio | Ferric phosphate hydrate particles and process for producing the same, olivine type lithium iron phosphate particles and process for producing the same, and non-aqueous electrolyte secondary battery |
KR101810259B1 (ko) * | 2010-03-19 | 2017-12-18 | 도다 고교 가부시끼가이샤 | 인산망간철리튬 입자 분말의 제조 방법, 인산망간철리튬 입자 분말, 및 상기 입자 분말을 이용한 비수전해질 이차 전지 |
CN103125037B (zh) | 2010-07-15 | 2016-08-17 | 庄信万丰股份有限公司 | 电池级阴极涂料配制物 |
JP5736865B2 (ja) | 2011-03-16 | 2015-06-17 | 東洋インキScホールディングス株式会社 | リチウム二次電池用正極活物質材料の製造方法、及びそれを用いたリチウム二次電池 |
CN102249208A (zh) * | 2011-05-06 | 2011-11-23 | 朱鸥鹭 | 一种锂离子电池正极材料磷酸锰铁锂的水热合成方法 |
CN102651474A (zh) * | 2012-05-24 | 2012-08-29 | 四川科能锂电有限公司 | 一种锂电池正极活性材料磷酸铁锂的制备方法 |
-
2014
- 2014-05-08 EP EP14794314.6A patent/EP2996178A4/en not_active Withdrawn
- 2014-05-08 TW TW103116451A patent/TWI612716B/zh active
- 2014-05-08 JP JP2016512216A patent/JP6232493B2/ja active Active
- 2014-05-08 WO PCT/CN2014/077082 patent/WO2014180334A1/zh active Application Filing
- 2014-05-08 US US14/889,420 patent/US10096832B2/en active Active
- 2014-05-08 KR KR1020157034870A patent/KR101764052B1/ko active IP Right Grant
- 2014-05-08 CN CN201480022119.7A patent/CN105190951B/zh active Active
- 2014-05-08 CA CA2911518A patent/CA2911518C/en active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102791625A (zh) * | 2010-03-09 | 2012-11-21 | 旭硝子株式会社 | 磷酸化合物、二次电池用正极、以及二次电池的制造方法 |
TW201305046A (zh) * | 2011-07-20 | 2013-02-01 | Advanced Lithium Electrochemistry Co Ltd | 電池複合材料及其前驅物之製備方法 |
Non-Patent Citations (1)
Title |
---|
MAJA PIVKO等: "Synthesis of Nanometric LiMnPO4 via a Two-Step Technique", 《CHEMISTRY OF MATERIALS》 * |
Also Published As
Publication number | Publication date |
---|---|
CA2911518A1 (en) | 2014-11-13 |
CA2911518C (en) | 2019-01-08 |
JP2016519407A (ja) | 2016-06-30 |
CN105190951B (zh) | 2018-06-29 |
US10096832B2 (en) | 2018-10-09 |
EP2996178A4 (en) | 2017-01-18 |
US20160087277A1 (en) | 2016-03-24 |
TWI612716B (zh) | 2018-01-21 |
EP2996178A1 (en) | 2016-03-16 |
JP6232493B2 (ja) | 2017-11-15 |
WO2014180334A1 (zh) | 2014-11-13 |
KR20160005770A (ko) | 2016-01-15 |
TW201513446A (zh) | 2015-04-01 |
KR101764052B1 (ko) | 2017-08-01 |
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