CN105177537B - 一种铜包覆单晶蓝宝石纤维的制备方法 - Google Patents
一种铜包覆单晶蓝宝石纤维的制备方法 Download PDFInfo
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- CN105177537B CN105177537B CN201510588762.2A CN201510588762A CN105177537B CN 105177537 B CN105177537 B CN 105177537B CN 201510588762 A CN201510588762 A CN 201510588762A CN 105177537 B CN105177537 B CN 105177537B
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- CN
- China
- Prior art keywords
- monocrystalline sapphire
- copper clad
- monocrystalline
- sapphire fiber
- copper
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 229910052594 sapphire Inorganic materials 0.000 title claims abstract description 100
- 239000010980 sapphire Substances 0.000 title claims abstract description 100
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 title claims abstract description 66
- 229910052802 copper Inorganic materials 0.000 title claims abstract description 66
- 239000010949 copper Substances 0.000 title claims abstract description 66
- 239000000835 fiber Substances 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 83
- 235000011121 sodium hydroxide Nutrition 0.000 claims abstract description 31
- 229910000033 sodium borohydride Inorganic materials 0.000 claims abstract description 19
- 239000012279 sodium borohydride Substances 0.000 claims abstract description 19
- 238000005406 washing Methods 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 11
- 230000009467 reduction Effects 0.000 claims abstract description 8
- 239000012029 Fehling's reagent Substances 0.000 claims abstract description 3
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 23
- 239000000243 solution Substances 0.000 claims description 19
- 239000008367 deionised water Substances 0.000 claims description 14
- 229910021641 deionized water Inorganic materials 0.000 claims description 14
- 239000007788 liquid Substances 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 14
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- 239000011259 mixed solution Substances 0.000 claims description 12
- 238000001035 drying Methods 0.000 claims description 10
- 238000013019 agitation Methods 0.000 claims description 8
- 239000002131 composite material Substances 0.000 claims description 8
- VZOPRCCTKLAGPN-ZFJVMAEJSA-L potassium;sodium;(2r,3r)-2,3-dihydroxybutanedioate;tetrahydrate Chemical compound O.O.O.O.[Na+].[K+].[O-]C(=O)[C@H](O)[C@@H](O)C([O-])=O VZOPRCCTKLAGPN-ZFJVMAEJSA-L 0.000 claims description 7
- 229940074446 sodium potassium tartrate tetrahydrate Drugs 0.000 claims description 7
- 239000010437 gem Substances 0.000 claims description 6
- 229910001751 gemstone Inorganic materials 0.000 claims description 6
- 238000012545 processing Methods 0.000 claims description 4
- ORTQZVOHEJQUHG-UHFFFAOYSA-L copper(II) chloride Chemical compound Cl[Cu]Cl ORTQZVOHEJQUHG-UHFFFAOYSA-L 0.000 claims description 3
- XTVVROIMIGLXTD-UHFFFAOYSA-N copper(II) nitrate Chemical compound [Cu+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O XTVVROIMIGLXTD-UHFFFAOYSA-N 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 claims description 2
- 238000005253 cladding Methods 0.000 claims description 2
- 150000001879 copper Chemical class 0.000 claims description 2
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 claims description 2
- 239000012266 salt solution Substances 0.000 claims description 2
- 238000004140 cleaning Methods 0.000 claims 1
- OPQARKPSCNTWTJ-UHFFFAOYSA-L copper(ii) acetate Chemical compound [Cu+2].CC([O-])=O.CC([O-])=O OPQARKPSCNTWTJ-UHFFFAOYSA-L 0.000 claims 1
- 238000002474 experimental method Methods 0.000 abstract description 2
- 238000011112 process operation Methods 0.000 abstract description 2
- 239000013078 crystal Substances 0.000 description 10
- 239000000463 material Substances 0.000 description 6
- 239000004575 stone Substances 0.000 description 6
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 5
- 238000005259 measurement Methods 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 229910052708 sodium Inorganic materials 0.000 description 5
- 239000011734 sodium Substances 0.000 description 5
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- UMRSVAKGZBVPKD-UHFFFAOYSA-N acetic acid;copper Chemical compound [Cu].CC(O)=O UMRSVAKGZBVPKD-UHFFFAOYSA-N 0.000 description 2
- 229910045601 alloy Inorganic materials 0.000 description 2
- 239000000956 alloy Substances 0.000 description 2
- OJMOMXZKOWKUTA-UHFFFAOYSA-N aluminum;borate Chemical compound [Al+3].[O-]B([O-])[O-] OJMOMXZKOWKUTA-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 239000002905 metal composite material Substances 0.000 description 2
- 239000007769 metal material Substances 0.000 description 2
- 239000011156 metal matrix composite Substances 0.000 description 2
- 230000003068 static effect Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 238000004833 X-ray photoelectron spectroscopy Methods 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000011157 advanced composite material Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000005452 bending Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- -1 copper complex ion Chemical class 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 229910001092 metal group alloy Inorganic materials 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000003014 reinforcing effect Effects 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
Landscapes
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
Description
Claims (8)
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CN201510588762.2A CN105177537B (zh) | 2015-09-16 | 2015-09-16 | 一种铜包覆单晶蓝宝石纤维的制备方法 |
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CN201510588762.2A CN105177537B (zh) | 2015-09-16 | 2015-09-16 | 一种铜包覆单晶蓝宝石纤维的制备方法 |
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CN105177537A CN105177537A (zh) | 2015-12-23 |
CN105177537B true CN105177537B (zh) | 2018-02-23 |
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Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101372740A (zh) * | 2007-08-23 | 2009-02-25 | 北京中科三环高技术股份有限公司 | 用于铜覆的镀铜液及其对永磁材料的表面镀铜方法 |
CN101517123A (zh) * | 2006-09-15 | 2009-08-26 | 宇部日东化成株式会社 | 包覆金属层的基材及其制造方法 |
CN103060779A (zh) * | 2012-12-04 | 2013-04-24 | 复旦大学 | 一种铜/莫代尔纤维复合材料的制备方法 |
CN104204292A (zh) * | 2012-03-23 | 2014-12-10 | 奈克松有限公司 | 经蚀刻的硅结构、形成经蚀刻的硅结构的方法及其用途 |
-
2015
- 2015-09-16 CN CN201510588762.2A patent/CN105177537B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101517123A (zh) * | 2006-09-15 | 2009-08-26 | 宇部日东化成株式会社 | 包覆金属层的基材及其制造方法 |
CN101372740A (zh) * | 2007-08-23 | 2009-02-25 | 北京中科三环高技术股份有限公司 | 用于铜覆的镀铜液及其对永磁材料的表面镀铜方法 |
CN104204292A (zh) * | 2012-03-23 | 2014-12-10 | 奈克松有限公司 | 经蚀刻的硅结构、形成经蚀刻的硅结构的方法及其用途 |
CN103060779A (zh) * | 2012-12-04 | 2013-04-24 | 复旦大学 | 一种铜/莫代尔纤维复合材料的制备方法 |
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Effective date of registration: 20231115 Address after: 523000 Building 1, No.1 Xuefu Road, Songshanhu Park, Dongguan City, Guangdong Province Patentee after: Guangdong Qingda Innovation Research Institute Co.,Ltd. Patentee after: DONGGUAN NIUKA NEW MATERIAL SCIENCE & TECHNOLOGY Co.,Ltd. Address before: 523000 Innovation Science Park, Songshan Lake High-tech Industrial Development Zone, Dongguan City, Guangdong Province, 8 Tsinghua Dongguan Innovation Center Patentee before: TSINGHUA INNOVATION CENTER IN DONGGUAN Patentee before: DONGGUAN NIUKA NEW MATERIAL SCIENCE & TECHNOLOGY Co.,Ltd. |
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