CN105176217A - Waterborne composite heat-insulating decoration coating and preparation method thereof - Google Patents
Waterborne composite heat-insulating decoration coating and preparation method thereof Download PDFInfo
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- CN105176217A CN105176217A CN201510678644.0A CN201510678644A CN105176217A CN 105176217 A CN105176217 A CN 105176217A CN 201510678644 A CN201510678644 A CN 201510678644A CN 105176217 A CN105176217 A CN 105176217A
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Abstract
The invention discloses a waterborne composite heat-insulating decoration coating. The decoration coating comprises the following components: epoxy resin modified styrene-acrylic latex, a pigment filler, a film forming assistant, an anti-freezing agent, a defoaming agent, a dispersing agent, a thickening agent and deionized water, wherein the film forming assistant is mixture of lauryl alcohol ester and dipropylene glycol butyl ether which are mixed according to a ratio of 1:1; the anti-freezing agent is glycol; the defoaming agent is one of dimethicone, organosilicone and polyvinyl acetate; the dispersing agent is one or more of hydrophobic modified sodium carboxylate, sodium polyacrylate and ammonium salt; the thickening agent is one or more of kieselguhr, sodium bentonite, polyurethane, polyvinyl alcohol and polyacrylamide. The invention further discloses a preparation method of the waterborne composite heat-insulating decoration coating, the decoration coating has good heat insulating performance, the heat energy is saved, the cost is low, the preparation method is simple and feasible and the preparation cost is low.
Description
Technical field
The present invention relates to a kind of decorative paint and preparation method thereof, be specifically related to a kind of water-based composite thermal-insulating decorative paint and preparation method thereof.
Background technology
At present, China is in the peak time of building construction, and traditional exterior wall or construction coating for internal wall mainly emphasize anticorrosion, antifouling, ageing-resistant, self-cleaning is good, but pay close attention to not in heat-insulating property, building energy conservation is more and more being subject to national attention in recent years, building roof and heat preservation and decoration of outer wall coating are a kind of building heat preservation solutions very popular in recent years;
Thermal insulation coatings is generally divided three classes, 1-isolation-type isolation-type thermal insulating coating is a kind of coating realizing heat-insulation and heat-preservation by adding high thermal resistance filler, the extremely low air of thermal conductivity is introduced to obtain good effect of heat insulation in the combination that general employing thermal conductivity is lower or film, such coating is usually low with apparent density, internal structure is loosened, the material that void content is high, water content is little, as light skeletal, has glass bead, expanded vermiculite, polystyrene foamed etc. usually for the insulation light skeletal used in thermal insulating coating; 2-reflection type thermal insulation coating mainly distributes according to solar spectrum energy, portion of energy sunlight being produced heat reflects away, the sunlight overwhelming majority is in visible ray and near-infrared region, therefore by selecting suitable resin, metal, metal oxide color stuffing and production technique, the coating of obtained high heat insulation rate is to reach heat insulation object; 3-Anti-radiation type thermal insulating coating is by be fallen by the heat radiation of absorption with the form of heat emission thus impel the indoor speed same with outdoor cooling, but choosing and complete processing more complicated of Radiation Heat-insulated Paint base-material, wanting to reach stable emittance also needs further further investigation; The insulation mechanism of this three classes coating is different, application scenario is also different with the effect obtained, the good thermal insulation coatings of a kind of effect of heat insulation is the result that simultaneously works of two or more heat-insulation mechanisms often, its advantage is respectively had based on above-mentioned three kinds of thermal insulation coatings, if three kinds of insulating mechanism organically can be combined, give full play to respective feature, realize having complementary advantages, the compound heat insulating coatings of development water-based is of far-reaching significance to development high-performance heat insulating coatings.
Summary of the invention
Technical problem to be solved by this invention is, for the shortcoming that above prior art exists, a kind of water-based composite thermal-insulating decorative paint and preparation method thereof is proposed, this decorative paint has good thermal and insulating performance, saving heat energy, reduce costs, preparation method is simple, and preparation cost is cheap.
The technical scheme that the present invention solves above technical problem is:
A kind of water-based composite thermal-insulating decorative paint, this decorative paint comprises following component according to the mass fraction:
Epoxy resin modification styrene-acrylic latex 20-40 part
Color stuffing 10-20 part
Film coalescence aid 5-8 part
Frostproofer 1-2 part
Defoamer 1-3 part
Dispersion agent 2-5 part
Thickening material 1-3 part
Deionized water 30-40 part
Wherein: color stuffing comprises the far-infrared powder of the titanium dioxide of 1-2 part, the wollastonite of 1-3 part, the hollow ceramic microspheres of 2-5 part, the aluminum silicate fiber of 5-7 part and 1-3 part according to the mass fraction; Film coalescence aid be equal proportion mixing lauryl alcohol ester and dipropylene compound make; Frostproofer is ethylene glycol; Defoamer is the one in dimethyl silicone oil, organosilicon, polyvinyl acetate (PVA); Dispersion agent is comprise one or more in hydrophobic modified carboxylic acid sodium salt, polyacrylic acid sodium salt or ammonium salt; Thickening material is one or several in diatomite, sodium bentonite, urethane, polyvinyl alcohol or polyacrylamide;
The preparation technology of epoxy resin modification styrene-acrylic latex specifically comprises the following steps:
A. the preparation of pre-emulsion, emulsifying agent SDS, PH conditioning agent, the mix monomer vinylbenzene of dissolved epoxy and deionized water is added in the there-necked flask that electric mixer, constant pressure funnel are housed, high-speed stirring pre-emulsification 20-30mim under 500-600r/min, obtained pre-emulsion;
B. emulsion synthesize, add water stirring in the four-hole boiling flask that electric mixer, reflux condensing tube, constant pressure funnel are housed, be warming up to 85-87 DEG C, add pre-emulsion and the initiator ammonium persulfate of 1/3rd content, there is obvious blue light in the system of being stirred to, start to drip remaining pre-emulsion and initiator ammonium persulfate solution, evenly drip in 2-3h, isothermal reaction 1-2h, be warming up to 88-90 DEG C, insulation 0.5-1h, is then cooled to 40-50 DEG C, discharging, obtains epoxy resin modification styrene-acrylic latex.
The technical scheme that the present invention limits further is:
Aforementioned water-based composite thermal-insulating decorative paint, this decorative paint comprises following component according to the mass fraction:
Epoxy resin modification styrene-acrylic latex: 20 parts, color stuffing: 20 parts, film coalescence aid: 6 parts, frostproofer: 1 part, defoamer: 2 parts, dispersion agent: 5 parts, thickening material: 1 part, deionized water: 30 parts;
Color stuffing comprises the far-infrared powder of the titanium dioxide of 2 parts, the wollastonite of 3 parts, the hollow ceramic microspheres of 5 parts, the aluminum silicate fiber of 7 parts and 3 parts according to the mass fraction.
Aforementioned water-based composite thermal-insulating decorative paint, this decorative paint comprises following component according to the mass fraction:
Epoxy resin modification styrene-acrylic latex: 40 parts, color stuffing: 10 parts, film coalescence aid: 8 parts, frostproofer: 2 parts, defoamer: 3 parts, dispersion agent: 2 parts, thickening material: 2 parts, deionized water: 35 parts;
Color stuffing comprises the far-infrared powder of the titanium dioxide of 1 part, the wollastonite of 1 part, the hollow ceramic microspheres of 2 parts, the aluminum silicate fiber of 5 parts and 1 part according to the mass fraction.
Aforementioned water-based composite thermal-insulating decorative paint, this decorative paint comprises following component according to the mass fraction:
Epoxy resin modification styrene-acrylic latex: 30 parts, color stuffing: 15 parts, film coalescence aid: 5 parts, frostproofer: 2 parts, defoamer: 1 part, dispersion agent: 4 parts, thickening material: 3 parts, deionized water: 40 parts;
Color stuffing comprises the far-infrared powder of the titanium dioxide of 2 parts, the wollastonite of 2 parts, the hollow ceramic microspheres of 3 parts, the aluminum silicate fiber of 6 parts and 2 parts according to the mass fraction.
The present invention have also been devised a kind of preparation method of water-based composite thermal-insulating decorative paint, and the preparation method of this decorative paint specifically comprises the following steps:
(1) deionized water of a point content of three and dispersion agent are uniformly mixed at 1200-1500r/min, stir 10-15min, the more modified stirring velocity of silicate fiber added in color stuffing is that 1800-2000r/min stirring 10-20min is mixed and made into slurry;
(2) deionized water of residual content, slurry, film coalescence aid, frostproofer and defoamer are stirred, then adding the titanium dioxide in epoxy resin modification styrene-acrylic latex and color stuffing, far-infrared powder, hollow ceramic microspheres and wollastonite successively, governing speed is that 500-600r/min stirs 20-30min;
(3) speed adjustment is obtained water-based composite thermal-insulating decorative paint to adding thickening material adjustment viscosity during 600rpm.
The invention has the beneficial effects as follows:
Styrene acrylic elasticity latex has excellent weathering resistance, the advantage such as film forming properties and ultraviolet light, but still have many deficiencies when some occasion uses, as poor in chemical-resistant, mechanical mechanics property, limit further application, and the alkali resistance of epoxy resin excellence, chemical-resistant, solvent resistance, physical strength high, there is good sticking power, the present invention adopts it to carry out modification to styrene-acrylic latex effectively can improve sticking power, the mechanical property of latex film, the over-all properties such as thermomechanical mechanical strength and chemical-resistant of latex to base material.
Embodiment
embodiment 1
The present embodiment provides a kind of water-based composite thermal-insulating decorative paint, and this decorative paint comprises following component according to the mass fraction:
Epoxy resin modification styrene-acrylic latex: 20 parts, color stuffing: 20 parts, film coalescence aid: 6 parts, antifreeze glycol: 1 part, defoamer polyvinyl acetate (PVA): 2 parts, the hydrophobic modified carboxylic acid sodium salt of dispersion agent: 5 parts, thickening material diatomite: 1 part, deionized water: 30 parts;
Color stuffing comprises the far-infrared powder of the titanium dioxide of 2 parts, the wollastonite of 3 parts, the hollow ceramic microspheres of 5 parts, the aluminum silicate fiber of 7 parts and 3 parts according to the mass fraction;
Film coalescence aid be equal proportion mixing lauryl alcohol ester and dipropylene compound make;
The preparation technology of epoxy resin modification styrene-acrylic latex specifically comprises the following steps:
A. the preparation of pre-emulsion, emulsifying agent SDS, PH conditioning agent, the mix monomer vinylbenzene of dissolved epoxy and deionized water is added in the there-necked flask that electric mixer, constant pressure funnel are housed, high-speed stirring pre-emulsification 25mim under 550r/min, obtained pre-emulsion;
B. emulsion synthesize, add water stirring in the four-hole boiling flask that electric mixer, reflux condensing tube, constant pressure funnel are housed, and is warming up to 86 DEG C, add pre-emulsion and the initiator ammonium persulfate of 1/3rd content, there is obvious blue light in the system of being stirred to, starts to drip remaining pre-emulsion and initiator ammonium persulfate solution, evenly drips in 2h, isothermal reaction 2h, be warming up to 89 DEG C, insulation 0.8h, is then cooled to 45 DEG C, discharging, obtains epoxy resin modification styrene-acrylic latex.
The preparation method of above-mentioned water-based composite thermal-insulating decorative paint, the preparation method of this decorative paint specifically comprises the following steps:
(1) deionized water of a point content of three and dispersion agent are uniformly mixed at 1350r/min, stir 12min, the more modified stirring velocity of silicate fiber added in color stuffing is that 1900r/min stirring 15min is mixed and made into slurry;
(2) deionized water of residual content, slurry, film coalescence aid, frostproofer and defoamer are stirred, then adding the titanium dioxide in epoxy resin modification styrene-acrylic latex and color stuffing, far-infrared powder, hollow ceramic microspheres and wollastonite successively, governing speed is that 550r/min stirs 25min;
(3) speed adjustment is obtained water-based composite thermal-insulating decorative paint to adding thickening material adjustment viscosity during 600rpm.
embodiment 2
The present embodiment provides a kind of water-based composite thermal-insulating decorative paint, and this decorative paint comprises following component according to the mass fraction:
Epoxy resin modification styrene-acrylic latex: 40 parts, color stuffing: 10 parts, film coalescence aid: 8 parts, antifreeze glycol: 2 parts, defoamer organosilicon: 3 parts, dispersion agent ammonium salt: 2 parts, thickening material urethane: 2 parts, deionized water: 35 parts;
Color stuffing comprises the far-infrared powder of the titanium dioxide of 1 part, the wollastonite of 1 part, the hollow ceramic microspheres of 2 parts, the aluminum silicate fiber of 5 parts and 1 part according to the mass fraction;
Film coalescence aid be equal proportion mixing lauryl alcohol ester and dipropylene compound make;
The preparation technology of epoxy resin modification styrene-acrylic latex specifically comprises the following steps:
A. the preparation of pre-emulsion, emulsifying agent SDS, PH conditioning agent, the mix monomer vinylbenzene of dissolved epoxy and deionized water is added in the there-necked flask that electric mixer, constant pressure funnel are housed, high-speed stirring pre-emulsification 20mim under 600r/min, obtained pre-emulsion;
B. emulsion synthesize, add water stirring in the four-hole boiling flask that electric mixer, reflux condensing tube, constant pressure funnel are housed, and is warming up to 87 DEG C, add pre-emulsion and the initiator ammonium persulfate of 1/3rd content, there is obvious blue light in the system of being stirred to, starts to drip remaining pre-emulsion and initiator ammonium persulfate solution, evenly drips in 2h, isothermal reaction 1h, be warming up to 90 DEG C, insulation 0.5h, is then cooled to 50 DEG C, discharging, obtains epoxy resin modification styrene-acrylic latex.
The preparation method of above-mentioned water-based composite thermal-insulating decorative paint, the preparation method of this decorative paint specifically comprises the following steps:
(1) deionized water of a point content of three and dispersion agent are uniformly mixed at 1500r/min, stir 10min, the more modified stirring velocity of silicate fiber added in color stuffing is that 2000r/min stirring 10min is mixed and made into slurry;
(2) deionized water of residual content, slurry, film coalescence aid, frostproofer and defoamer are stirred, then adding the titanium dioxide in epoxy resin modification styrene-acrylic latex and color stuffing, far-infrared powder, hollow ceramic microspheres and wollastonite successively, governing speed is that 600r/min stirs 30min;
(3) speed adjustment is obtained water-based composite thermal-insulating decorative paint to adding thickening material adjustment viscosity during 600rpm.
embodiment 3
The present embodiment provides a kind of water-based composite thermal-insulating decorative paint, and this decorative paint comprises following component according to the mass fraction:
Epoxy resin modification styrene-acrylic latex: 30 parts, color stuffing: 15 parts, film coalescence aid: 5 parts, antifreeze glycol: 2 parts, defoamer dimethyl silicone oil: 1 part, dispersion agent polyacrylic acid sodium salt: 4 parts, thickening material sodium bentonite: 3 parts, deionized water: 40 parts;
Color stuffing comprises the far-infrared powder of the titanium dioxide of 2 parts, the wollastonite of 2 parts, the hollow ceramic microspheres of 3 parts, the aluminum silicate fiber of 6 parts and 2 parts according to the mass fraction;
Film coalescence aid be equal proportion mixing lauryl alcohol ester and dipropylene compound make;
The preparation technology of epoxy resin modification styrene-acrylic latex specifically comprises the following steps:
A. the preparation of pre-emulsion, emulsifying agent SDS, PH conditioning agent, the mix monomer vinylbenzene of dissolved epoxy and deionized water is added in the there-necked flask that electric mixer, constant pressure funnel are housed, high-speed stirring pre-emulsification 30mim under 500r/min, obtained pre-emulsion;
B. emulsion synthesize, add water stirring in the four-hole boiling flask that electric mixer, reflux condensing tube, constant pressure funnel are housed, and is warming up to 85 DEG C, add pre-emulsion and the initiator ammonium persulfate of 1/3rd content, there is obvious blue light in the system of being stirred to, starts to drip remaining pre-emulsion and initiator ammonium persulfate solution, evenly drips in 3h, isothermal reaction 1h, be warming up to 88 DEG C, insulation 1h, is then cooled to 40 DEG C, discharging, obtains epoxy resin modification styrene-acrylic latex.
The preparation method of above-mentioned water-based composite thermal-insulating decorative paint, the preparation method of this decorative paint specifically comprises the following steps:
(1) deionized water of a point content of three and dispersion agent are uniformly mixed at 1200r/min, stir 15min, the more modified stirring velocity of silicate fiber added in color stuffing is that 1800r/min stirring 20min is mixed and made into slurry;
(2) deionized water of residual content, slurry, film coalescence aid, frostproofer and defoamer are stirred, then adding the titanium dioxide in epoxy resin modification styrene-acrylic latex and color stuffing, far-infrared powder, hollow ceramic microspheres and wollastonite successively, governing speed is that 500r/min stirs 20min;
(3) speed adjustment is obtained water-based composite thermal-insulating decorative paint to adding thickening material adjustment viscosity during 600rpm.
In addition to the implementation, the present invention can also have other embodiments.All employings are equal to the technical scheme of replacement or equivalent transformation formation, all drop on the protection domain of application claims.
Claims (5)
1. a water-based composite thermal-insulating decorative paint, is characterized in that, this decorative paint comprises following component according to the mass fraction:
Epoxy resin modification styrene-acrylic latex 20-40 part
Color stuffing 10-20 part
Film coalescence aid 5-8 part
Frostproofer 1-2 part
Defoamer 1-3 part
Dispersion agent 2-5 part
Thickening material 1-3 part
Deionized water 30-40 part
Wherein: described color stuffing comprises the far-infrared powder of the titanium dioxide of 1-2 part, the wollastonite of 1-3 part, the hollow ceramic microspheres of 2-5 part, the aluminum silicate fiber of 5-7 part and 1-3 part according to the mass fraction; Described film coalescence aid be equal proportion mixing lauryl alcohol ester and dipropylene compound make; Described frostproofer is ethylene glycol; Described defoamer is the one in dimethyl silicone oil, organosilicon, polyvinyl acetate (PVA); Described dispersion agent is comprise one or more in hydrophobic modified carboxylic acid sodium salt, polyacrylic acid sodium salt or ammonium salt; Described thickening material is one or several in diatomite, sodium bentonite, urethane, polyvinyl alcohol or polyacrylamide;
The preparation technology of described epoxy resin modification styrene-acrylic latex specifically comprises the following steps:
A. the preparation of pre-emulsion, emulsifying agent SDS, PH conditioning agent, the mix monomer vinylbenzene of dissolved epoxy and deionized water is added in the there-necked flask that electric mixer, constant pressure funnel are housed, high-speed stirring pre-emulsification 20-30mim under 500-600r/min, obtained pre-emulsion;
B. emulsion synthesize, add water stirring in the four-hole boiling flask that electric mixer, reflux condensing tube, constant pressure funnel are housed, be warming up to 85-87 DEG C, add pre-emulsion and the initiator ammonium persulfate of 1/3rd content, there is obvious blue light in the system of being stirred to, start to drip remaining pre-emulsion and initiator ammonium persulfate solution, evenly drip in 2-3h, isothermal reaction 1-2h, be warming up to 88-90 DEG C, insulation 0.5-1h, is then cooled to 40-50 DEG C, discharging, obtains epoxy resin modification styrene-acrylic latex.
2. water-based composite thermal-insulating decorative paint according to claim 1, is characterized in that: this decorative paint comprises following component according to the mass fraction:
Epoxy resin modification styrene-acrylic latex: 20 parts, color stuffing: 20 parts, film coalescence aid: 6 parts, frostproofer: 1 part, defoamer: 2 parts, dispersion agent: 5 parts, thickening material: 1 part, deionized water: 30 parts;
Described color stuffing comprises the far-infrared powder of the titanium dioxide of 2 parts, the wollastonite of 3 parts, the hollow ceramic microspheres of 5 parts, the aluminum silicate fiber of 7 parts and 3 parts according to the mass fraction.
3. water-based composite thermal-insulating decorative paint according to claim 1, is characterized in that: this decorative paint comprises following component according to the mass fraction:
Epoxy resin modification styrene-acrylic latex: 40 parts, color stuffing: 10 parts, film coalescence aid: 8 parts, frostproofer: 2 parts, defoamer: 3 parts, dispersion agent: 2 parts, thickening material: 2 parts, deionized water: 35 parts;
Described color stuffing comprises the far-infrared powder of the titanium dioxide of 1 part, the wollastonite of 1 part, the hollow ceramic microspheres of 2 parts, the aluminum silicate fiber of 5 parts and 1 part according to the mass fraction.
4. water-based composite thermal-insulating decorative paint according to claim 1, is characterized in that: this decorative paint comprises following component according to the mass fraction:
Epoxy resin modification styrene-acrylic latex: 30 parts, color stuffing: 15 parts, film coalescence aid: 5 parts, frostproofer: 2 parts, defoamer: 1 part, dispersion agent: 4 parts, thickening material: 3 parts, deionized water: 40 parts;
Described color stuffing comprises the far-infrared powder of the titanium dioxide of 2 parts, the wollastonite of 2 parts, the hollow ceramic microspheres of 3 parts, the aluminum silicate fiber of 6 parts and 2 parts according to the mass fraction.
5. the preparation method of water-based composite thermal-insulating decorative paint as claimed in claim 1, it is characterized in that, the preparation method of this decorative paint specifically comprises the following steps:
(1) deionized water of a point content of three and dispersion agent are uniformly mixed at 1200-1500r/min, stir 10-15min, the more modified stirring velocity of silicate fiber added in color stuffing is that 1800-2000r/min stirring 10-20min is mixed and made into slurry;
(2) deionized water of residual content, slurry, film coalescence aid, frostproofer and defoamer are stirred, then adding the titanium dioxide in epoxy resin modification styrene-acrylic latex and color stuffing, far-infrared powder, hollow ceramic microspheres and wollastonite successively, governing speed is that 500-600r/min stirs 20-30min;
(3) speed adjustment is obtained water-based composite thermal-insulating decorative paint to adding thickening material adjustment viscosity during 600rpm.
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| CN106751940A (en) * | 2017-01-17 | 2017-05-31 | 江苏卡欧化工股份有限公司 | A kind of efficient rubber cracking preventing agent |
| CN107033685A (en) * | 2017-06-13 | 2017-08-11 | 合肥聪亨新型建材科技有限公司 | A kind of aquosity heat insulating heat preserving ornament materials and preparation method thereof |
| CN107234835A (en) * | 2017-06-30 | 2017-10-10 | 宁波爱美佳环保科技有限公司 | Heat-insulation and heat-preservation sheet material and container prepared therefrom and preparation method thereof |
| CN107286799A (en) * | 2017-08-02 | 2017-10-24 | 合肥帧讯低温科技有限公司 | Water-based heat insulation coating and preparation method thereof |
| CN108854588A (en) * | 2018-07-09 | 2018-11-23 | 河北工业大学 | A kind of preparation method and application of the hollow fiber ceramic membrane with dual persulfate mobilizing function |
| CN111154357A (en) * | 2020-01-17 | 2020-05-15 | 谭建军 | Exterior wall heat-insulating coating and preparation method thereof |
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| CN112409852A (en) * | 2020-11-17 | 2021-02-26 | 苏州皇冠涂料科技发展有限公司 | Production process of interior wall coating for decoration |
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| CN116426200A (en) * | 2023-04-28 | 2023-07-14 | 广东坚派新材料有限公司 | Waterproof finish paint for outer wall and preparation method thereof |
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| CN112409852A (en) * | 2020-11-17 | 2021-02-26 | 苏州皇冠涂料科技发展有限公司 | Production process of interior wall coating for decoration |
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| CN113416464A (en) * | 2021-06-07 | 2021-09-21 | 徐州大光涂料厂 | Water-based environment-friendly coating and preparation method thereof |
| CN116426200A (en) * | 2023-04-28 | 2023-07-14 | 广东坚派新材料有限公司 | Waterproof finish paint for outer wall and preparation method thereof |
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Application publication date: 20151223 |