CN105174811A - Water permeable brick and preparation method thereof - Google Patents
Water permeable brick and preparation method thereof Download PDFInfo
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- CN105174811A CN105174811A CN201510540237.3A CN201510540237A CN105174811A CN 105174811 A CN105174811 A CN 105174811A CN 201510540237 A CN201510540237 A CN 201510540237A CN 105174811 A CN105174811 A CN 105174811A
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/91—Use of waste materials as fillers for mortars or concrete
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Abstract
The invention provides a water permeable brick and a preparation method thereof. The water permeable brick is prepared from the following raw materials in parts by weight: 60-80 parts of blast furnace slag, 5-15 parts of polished slag, 10-20 parts of coal gangue, 15-25 parts of redware ore soil, 8-15 parts of a flux, 0.8-1.2 parts of an adhesive. The preparation method comprises the following steps of (1) material preparing; (2) crushing; (3) ball milling and wet mixing; (4) drying; (5) molding; and (6) burning. According to the preparation method, the water permeable brick which is prepared by adopting the blast furnace slag and the polished slag as main raw materials and adding the coal gangue and the redware ore soil has a relatively good water permeability, and the tensile structure and bending strength of the water permeable brick can be further improved.
Description
Technical field
The present invention relates to architectural pottery technical field, particularly relate to a kind of water-permeable brick and preparation method thereof.
Background technology
At present, the non-permeable material such as cement, pitch, marble is mostly adopted to lay ground in urban construction, these hard surfaces make the heat of earth's surface and air, exchange of moisture very difficult, the poor ability of Natural regulation urban ground temperature and humidity, earth's surface absorbs heat difficulty, and cause retaining a large amount of waste heat in city space, ground also can be reflected in a large number, radiation solar thermal energy, thus cause the phenomenon that occurs that city nocturnal temperature is higher than countryside nocturnal temperature.And, when the rainy day, hard surface can stop rainwater directly to permeate the ground, cause ponding everywhere, affect comfortableness and the security of road, blocked the approach of the direct recharge of groundwater of rainwater simultaneously, Urban Underground water level is made to be difficult to go up, the direct healthy growth affecting urban surface vegetation, greening difficulty, has increased the weight of the drought and water shortage problem in city; And ponding injects rivers after pouring in water drain, increased the weight of the excretion burden of sewerage system and rivers, during fine day, ground is very dry again, and stir up a cloud of dust, environmental degree of comfort reduces greatly.
At present, people appreciate the seriousness of the problems referred to above gradually, also a large amount of water-permeable bricks has been researched and developed, existing water-permeable brick can overcome above problem to a certain extent, and by the one of iron tailings to be the water-permeable brick mainly made be water-permeable brick, this water-permeable brick due to iron tailings blank deformation in the process preparing water-permeable brick, resistance to compression and bending strength low.
Summary of the invention
The object of the invention is to overcome above deficiency and defect proposes a kind of water-permeable brick and preparation method thereof.
For reaching this object, the present invention by the following technical solutions:
A kind of water-permeable brick, it is prepared by following feed composition by weight:
Blast furnace slag 60-80 part; ;
Polishing slag 5-15 part;
Coal gangue 10-20 part;
Boccaro ore deposit soil 15-25 part;
Flux 8-15 part;
Binding agent 0.8-1.2 part.
Preferably, it also comprises pore former 0.1-0.5 part by weight.
Preferably, described flux is one or more of calcination of talc, Wingdale or middle temperature sandstone.
Preferably, described binding agent is one or more in epoxy resin, urethane and acrylic resin.
Preferably, described pore former is one or more of Strontium carbonate powder, silicon carbide or sodium bicarbonate.
The preparation method of described water-permeable brick described above, is characterized in that: it comprises the following steps:
1) prepare burden: the composition preparing material by required and proportioning are prepared burden, with parts by weight: by blast furnace slag 60-80 part; , polishing slag 5-15 part, coal gangue 10-20 part, boccaro ore deposit soil 15-25 part, flux 8-15 part, binding agent 0.8-1.2 part and pore former 0.1-0.5 part batching;
2), broken: fragmentation to be carried out to coal gangue and obtains colliery powder;
3), ball milling, wet mixing: carry out ball milling by adding water after blast furnace slag, polishing slag, flux, colliery powder, boccaro ore deposit soil and pore former mixing; Finally add binding agent;
4), dry: to dry under the slurry after wet mixing is put into baking oven;
5), shaping: the powder after oven dry directly to be put into mould dry-pressing formed;
6), fire: by the goods tunnel furnace that suppresses or roller kiln.
Preferred in step 3) in by the compound prepared with material: ball milling: water is that the ratio of 0.7:1.2:0.5 carries out the wet ball-milling time for 8-11 hour.
Preferably, in step 4) in, drying temperature is 80-95 DEG C, and time of drying is 1-2.5 hour.
Preferably, in step 5) in, forming pressure is 25MPa-35MPa.
Preferably, in step 6) in, firing temperature is 950-1050 DEG C; Firing time is 6.5-8 hour.
The present invention, by adopting blast furnace slag and polishing slag to be main raw material, while interpolation coal gangue and the seepage brick obtained by the soil of boccaro ore deposit have good water-permeable simultaneously, further increases ultimate compression strength and bending strength.
Embodiment
Technical scheme of the present invention is further illustrated below by embodiment.
Embodiment 1
A preparation method for water-permeable brick, it comprises the following steps:
1), prepare burden: the composition preparing material by required and proportioning are prepared burden, with parts by weight: by blast furnace slag 75 parts; , polishing slag 7 parts, coal gangue 12 parts, 20 parts, boccaro ore deposit soil, calcination of talc 9 parts, urethane 0.8 part and 0.2 part, silicon carbide batching;
2), broken: fragmentation to be carried out to coal gangue and obtains colliery powder;
3), ball milling, wet mixing: carry out ball milling by adding water after blast furnace slag, polishing slag, flux, colliery powder, boccaro ore deposit soil and pore former mixing; Finally add binding agent;
4), dry: to dry under the slurry after wet mixing is put into baking oven; Drying temperature is 80 DEG C, and time of drying is 2.5 hours;
5), shaping: the powder after oven dry directly to be put into mould dry-pressing formed; Forming pressure is 30MPa;
6), fire: by the goods tunnel furnace that suppresses or roller kiln, firing temperature is 980 DEG C; Firing time is 7.5 hours.
In step 3) in by the compound prepared with material: ball milling: water is that to carry out the wet ball-milling time be 8.5 hours to the ratio of 0.7:1.2:0.5.
The permeability rate of the water-permeable brick that the present embodiment obtains is 0.042cm/s, and ultimate compression strength is 70MPa, and bending strength is 12.95MPa.
Boccaro ore deposit soil is primarily of quartz, clay, hydromica and rhombohedral iron ore composition, it makes boccaro product mud tool plasticity-, green strength is high, dry, the processing performance that the little grade of percent of firing shrinkage is good and the name throughout the world that becomes make pottery purple placer soil by purple mud, this mountain green mud and the basic mud of three kinds, red soil are formed, be referred to as pearl jade peace foot between purple clay laudatory title five color soil rich and honour natives to get, admire small stream first ball soil as sun and it serves to show that the precious boccaro ore deposit local products of boccaro ore deposit soil are in Ding Shu town, Yixing Huanglong Mountain, appoint near western Fragrance Hill, villa and Fu Dongyi band, in crystalloid, and it is few by glassy phase, there is the intensity that religion is high, heat-shock resistance and ventilation property.
Because blast furnace slag can produce crystal in sintering procedure, and boccaro ore deposit soil and the combination of coal gangue make the water-permeable brick obtained have the little and good water-permeable of stronger water-absorbent, shrinking percentage; Simultaneously comparatively hard, there is higher intensity.
Comparative example 1
Iron tailings is utilized to prepare a method for environment protection type water permeable brick,
Be basic aggregate with iron tailings, with waste broken glass bits and feldspar for sintering aid, being caking agent with clay, take silicon carbide as auxiliary blowing agent;
Concrete technology step is as follows;
(1) broken: fragmentation to be carried out to granular iron mine tailing and waste broken glass bits and obtains blast furnace slag and glass powder;
(2) ball milling: carry out fine grinding to through the waste glass powder of fragmentation and blast furnace slag, require that its granularity reaches below 200 orders, carborundum granularity requires to reach below 320 orders;
(3) prepare burden: the composition preparing material by required and proportioning are prepared burden; By weight percentage, by iron tailings 30%-60%, glass powder 5%-15%, clay 15%-30%, quartzy 15%-24%, potassium felspar sand 5%-15%, silicon carbide 0.25%-1.5% prepare burden;
(4) wet mixing: by the compound prepared with material: abrading-ball: water is that the ratio of 1:2:0.8 carries out ball milling mixing, and the wet mixing time is 12-16 hour;
(5) dry: the slurry after wet mixing to be put into baking oven and dry at 60 DEG C-70 DEG C;
(6) shaping: the powder after drying directly is put into the square frame that refractory materials baffle plate surrounds and forms by a firing, or it is dry-pressing formed to put into mould, forming pressure is 10MPa-40MPa;
(7) burn till: the goods suppressed are put into high temperature box type resistance furnace, its calcining system is: with the ramp to 500 of 3 DEG C/min-5 DEG C/min DEG C-600 DEG C, with the ramp to 900 of 6 DEG C/min-7 DEG C/min DEG C ~ 1000 DEG C, to be incubated 40min after the ramp to 1100 of 1 DEG C/min-2 DEG C/min DEG C-1200 DEG C, finally in stove, naturally cool to normal temperature.
The ultimate compression strength of the water-permeable brick that this comparative example 1 is obtained is 30-60MPa, and permeability rate is 0.010cm/s-0.030cm/s.
Embodiment 2
A preparation method for water-permeable brick, it comprises the following steps:
1), prepare burden: the composition preparing material by required and proportioning are prepared burden, with parts by weight: by blast furnace slag 68 parts; , polishing slag 8 parts, coal gangue 10 parts, 18 parts, boccaro ore deposit soil, 3 parts, Wingdale, middle temperature sandstone 5 parts, epoxy resin 0.6 part, urethane 0.5 part and sodium bicarbonate 0.4 part batching;
2), broken: fragmentation to be carried out to coal gangue and obtains colliery powder;
3), ball milling, wet mixing: carry out ball milling by adding water after blast furnace slag, polishing slag, flux, colliery powder, boccaro ore deposit soil and pore former mixing; Finally add binding agent;
4), dry: to dry under the slurry after wet mixing is put into baking oven; Drying temperature is 95 DEG C, and time of drying is 1 hour;
5), shaping: the powder after oven dry directly to be put into mould dry-pressing formed; Forming pressure is 32MPa;
6), fire: by the goods tunnel furnace that suppresses or roller kiln, firing temperature is 950 DEG C; Firing time is 8 hours.
In the present embodiment, by the compound prepared with material: ball milling: water is that to carry out the wet ball-milling time be 11 hours to the ratio of 0.7:1.2:0.5.
The permeability rate of the water-permeable brick that the present embodiment obtains is 0.032cm/s, and ultimate compression strength is 78MPa, and bending strength is 13.16MPa.
Embodiment 3
A preparation method for water-permeable brick, it comprises the following steps:
1), prepare burden: the composition preparing material by required and proportioning are prepared burden, with parts by weight: by blast furnace slag 60 parts; , polishing slag 10 parts, coal gangue 15 parts, 15 parts, boccaro ore deposit soil, 10 parts, Wingdale, acrylic resin 1.2 parts and Strontium carbonate powder 0.3 part batching;
2), broken: fragmentation to be carried out to coal gangue and obtains colliery powder;
3), ball milling, wet mixing: carry out ball milling by adding water after blast furnace slag, polishing slag, flux, colliery powder, boccaro ore deposit soil and pore former mixing; Finally add binding agent;
4), dry: to dry under the slurry after wet mixing is put into baking oven; Drying temperature is 88 DEG C, and time of drying is 1.5 hours;
5), shaping: the powder after oven dry directly to be put into mould dry-pressing formed; Forming pressure is 25MPa;
6), fire: by the goods tunnel furnace that suppresses or roller kiln, firing temperature is 1050 DEG C; Firing time is 6.5 hours.
In step 3) in by the compound prepared with material: ball milling: water is that to carry out the wet ball-milling time be 9 hours to the ratio of 0.7:1.2:0.5.
The permeability rate of the water-permeable brick that the present embodiment obtains is 0.035cm/s, and ultimate compression strength is 74MPa, and bending strength is 13.07MPa.
Embodiment 4
A preparation method for water-permeable brick, it comprises the following steps:
1), prepare burden: the composition preparing material by required and proportioning are prepared burden, with parts by weight: by blast furnace slag 78 parts; , polishing slag 15 parts, coal gangue 20 parts, 22 parts, boccaro ore deposit soil, calcination of talc 8 parts, middle temperature sandstone 7 parts, epoxy resin 0.4 part, acrylic resin 0.5 part and 0.1 part, silicon carbide batching;
2), broken: fragmentation to be carried out to coal gangue and obtains colliery powder;
3), ball milling, wet mixing: carry out ball milling by adding water after blast furnace slag, polishing slag, flux, colliery powder, boccaro ore deposit soil and pore former mixing; Finally add binding agent;
4), dry: to dry under the slurry after wet mixing is put into baking oven; Drying temperature is 82 DEG C, and time of drying is 2.5 hours;
5), shaping: the powder after oven dry directly to be put into mould dry-pressing formed; Forming pressure is 28MPa;
6), fire: by the goods tunnel furnace that suppresses or roller kiln, firing temperature is 1000 DEG C; Firing time is 7 hours.
In step 3) in by the compound prepared with material: ball milling: water is that to carry out the wet ball-milling time be 10.5 hours to the ratio of 0.7:1.2:0.5.
The permeability rate of the water-permeable brick that the present embodiment obtains is 0.046cm/s, and ultimate compression strength is 68MPa, and bending strength is 12.80MPa.
Embodiment 5
A preparation method for water-permeable brick, it comprises the following steps:
1), prepare burden: the composition preparing material by required and proportioning are prepared burden, with parts by weight: by blast furnace slag 80 parts; , polishing slag 9 parts, coal gangue 18 parts, 25 parts, boccaro ore deposit soil, calcination of talc 5 parts, 7 parts, Wingdale, epoxy resin 1.0 parts, 0.2 part, silicon carbide and sodium bicarbonate 0.2 part batching;
2), broken: fragmentation to be carried out to coal gangue and obtains colliery powder;
3), ball milling, wet mixing: carry out ball milling by adding water after blast furnace slag, polishing slag, flux, colliery powder, boccaro ore deposit soil and pore former mixing; Finally add binding agent;
4), dry: to dry under the slurry after wet mixing is put into baking oven; Drying temperature is 85 DEG C, and time of drying is 2 hours;
5), shaping: the powder after oven dry directly to be put into mould dry-pressing formed; Forming pressure is 35MPa;
6), fire: by the goods tunnel furnace that suppresses or roller kiln, firing temperature is 960 DEG C; Firing time is 8 hours.
In step 3) in by the compound prepared with material: ball milling: water is that to carry out the wet ball-milling time be 9 hours to the ratio of 0.7:1.2:0.5.
The permeability rate of the water-permeable brick that the present embodiment obtains is 0.048cm/s, and ultimate compression strength is 66MPa, and bending strength is 12.75MPa.
Embodiment 6
A preparation method for water-permeable brick, it comprises the following steps:
1), prepare burden: the composition preparing material by required and proportioning are prepared burden, with parts by weight: by blast furnace slag 63 parts; , polishing slag 14 parts, coal gangue 16 parts, 21 parts, boccaro ore deposit soil, middle temperature sandstone 14 parts, urethane 0.9 part, Strontium carbonate powder 0.3 part and sodium bicarbonate 0.2 part batching;
2), broken: fragmentation to be carried out to coal gangue and obtains colliery powder;
3), ball milling, wet mixing: carry out ball milling by adding water after blast furnace slag, polishing slag, flux, colliery powder, boccaro ore deposit soil and pore former mixing; Finally add binding agent;
4), dry: to dry under the slurry after wet mixing is put into baking oven; Drying temperature is 87 DEG C, and time of drying is 2 hours;
5), shaping: the powder after oven dry directly to be put into mould dry-pressing formed; Forming pressure is 29MPa;
6), fire: by the goods tunnel furnace that suppresses or roller kiln, firing temperature is 1010 DEG C; Firing time is 7 hours.
In step 3) in by the compound prepared with material: ball milling: water is that to carry out the wet ball-milling time be 11 hours to the ratio of 0.7:1.2:0.5.
The permeability rate of the water-permeable brick that the present embodiment obtains is 0.040cm/s, and ultimate compression strength is 72MPa, and bending strength is 13.09MPa.
Embodiment 7
A preparation method for water-permeable brick, it comprises the following steps:
1), prepare burden: the composition preparing material by required and proportioning are prepared burden, with parts by weight: by blast furnace slag 65 parts; , polishing slag 12 parts, coal gangue 14 parts, 17 parts, boccaro ore deposit soil, calcination of talc 11 parts, urethane 0.8 part and sodium bicarbonate 0.3 part batching;
2), broken: fragmentation to be carried out to coal gangue and obtains colliery powder;
3), ball milling, wet mixing: carry out ball milling by adding water after blast furnace slag, polishing slag, flux, colliery powder, boccaro ore deposit soil and pore former mixing; Finally add binding agent;
4), dry: to dry under the slurry after wet mixing is put into baking oven; Drying temperature is 90 DEG C, and time of drying is 1.5 hours;
5), shaping: the powder after oven dry directly to be put into mould dry-pressing formed; Forming pressure is 33MPa;
6), fire: by the goods tunnel furnace that suppresses or roller kiln, firing temperature is 990 DEG C; Firing time is 7 hours.
In step 3) in by the compound prepared with material: ball milling: water is that to carry out the wet ball-milling time be 10 hours to the ratio of 0.7:1.2:0.5.
The permeability rate of the water-permeable brick that the present embodiment obtains is 0.050cm/s, and ultimate compression strength is 65MPa, and bending strength is 12.73MPa.
Embodiment 8
A preparation method for water-permeable brick, it comprises the following steps:
1), prepare burden: the composition preparing material by required and proportioning are prepared burden, with parts by weight: by blast furnace slag 72 parts; , polishing slag 5 parts, coal gangue 17 parts, 24 parts, boccaro ore deposit soil, 10 parts, Wingdale, asphalt mixtures modified by epoxy resin part, 0.3 urethane 0.8 part and 0.2 part, silicon carbide batching;
2), broken: fragmentation to be carried out to coal gangue and obtains colliery powder;
3), ball milling, wet mixing: carry out ball milling by adding water after blast furnace slag, polishing slag, flux, colliery powder, boccaro ore deposit soil and pore former mixing; Finally add binding agent;
4), dry: to dry under the slurry after wet mixing is put into baking oven; Drying temperature is 92 DEG C, and time of drying is 1 hour;
5), shaping: the powder after oven dry directly to be put into mould dry-pressing formed; Forming pressure is 30MPa;
6), fire: by the goods tunnel furnace that suppresses or roller kiln, firing temperature is 1030 DEG C; Firing time is 6.5 hours.
In step 3) in by the compound prepared with material: ball milling: water is that to carry out the wet ball-milling time be 8 hours to the ratio of 0.7:1.2:0.5.
The permeability rate of the water-permeable brick that the present embodiment obtains is 0.033cm/s, and ultimate compression strength is 76MPa, and bending strength is 13.11MPa.
Below know-why of the present invention is described in conjunction with specific embodiments.These describe just in order to explain principle of the present invention, and can not be interpreted as limiting the scope of the invention by any way.Based on explanation herein, those skilled in the art does not need to pay performing creative labour can associate other embodiment of the present invention, and these modes all will fall within protection scope of the present invention.
Claims (10)
1. a water-permeable brick, is characterized in that: it is prepared by following feed composition by weight:
Blast furnace slag 60-80 part;
Polishing slag 5-15 part;
Coal gangue 10-20 part;
Boccaro ore deposit soil 15-25 part;
Flux 8-15 part;
Binding agent 0.8-1.2 part.
2. water-permeable brick according to claim 1, is characterized in that: it also comprises pore former 0.1-0.5 part by weight.
3. water-permeable brick according to claim 2, is characterized in that: described flux is one or more of calcination of talc, Wingdale or middle temperature sandstone.
4. water-permeable brick according to claim 2, is characterized in that: described binding agent is one or more in epoxy resin, urethane and acrylic resin.
5. water-permeable brick according to claim 2, is characterized in that: described pore former is one or more of Strontium carbonate powder, silicon carbide or sodium bicarbonate.
6. the preparation method of the water-permeable brick as described in claim 2-5 any one, is characterized in that: it comprises the following steps:
1) prepare burden: the composition preparing material by required and proportioning are prepared burden, with parts by weight: by blast furnace slag 60-80 part; , polishing slag 5-15 part, coal gangue 10-20 part, boccaro ore deposit soil 15-25 part, flux 8-15 part, binding agent 0.8-1.2 part and pore former 0.1-0.5 part batching;
2), broken: fragmentation to be carried out to coal gangue and obtains colliery powder;
3), ball milling, wet mixing: carry out ball milling by adding water after blast furnace slag, polishing slag, flux, colliery powder, boccaro ore deposit soil and pore former mixing; Finally add binding agent;
4), dry: to dry under the slurry after wet mixing is put into baking oven;
5), shaping: the powder after oven dry directly to be put into mould dry-pressing formed;
6), fire: by the goods tunnel furnace that suppresses or roller kiln.
7. the preparation method of water-permeable brick according to claim 6, is characterized in that: in step 3) in by the compound prepared with material: ball milling: water is that the ratio of 0.7:1.2:0.5 carries out the wet ball-milling time for 8-11 hour.
8. the preparation method of water-permeable brick according to claim 6, is characterized in that: in step 4) in, drying temperature is 80-95 DEG C, and time of drying is 1-2.5 hour.
9. the preparation method of water-permeable brick according to claim 6, is characterized in that: in step 5) in, forming pressure is 25MPa-35MPa.
10. the preparation method of water-permeable brick according to claim 6, is characterized in that: in step 6) in, firing temperature is 950-1050 DEG C; Firing time is 6.5-8 hour.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105948704A (en) * | 2016-04-21 | 2016-09-21 | 辽宁利盟高科新材料有限公司 | Full-solid-waste foamed ceramic insulation board based on ceramic-polished residues and preparation method thereof |
| CN106278365A (en) * | 2016-07-27 | 2017-01-04 | 北京大学 | With sintering brick permeable to water that shraff is prepared for major ingredient and preparation method thereof |
| CN106747620A (en) * | 2017-01-04 | 2017-05-31 | 内蒙古科技大学 | A kind of low energy consumption sintering seepage brick and its manufacture method |
| CN107500624A (en) * | 2017-08-22 | 2017-12-22 | 普定县银丰农业科技发展有限公司 | A kind of water-permeable brick and preparation method thereof |
| CN107555951A (en) * | 2017-08-25 | 2018-01-09 | 昆明理工大学 | A kind of water conservation porous brick for sponge city and preparation method thereof |
| CN111635245A (en) * | 2020-06-25 | 2020-09-08 | 张家港宏昌钢板有限公司 | Method for preparing water permeable brick by using waste castable |
| CN114195544A (en) * | 2021-12-10 | 2022-03-18 | 江西英矿新型墙体材料有限公司 | Method for preparing perforated brick by recycling coal gangue |
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Application publication date: 20151223 |