CN105166883A - Fructus phyllanthi lozenge and preparation method thereof - Google Patents
Fructus phyllanthi lozenge and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a Fructus phyllanthi lozenge. 100 Parts by weight of the Fructus phyllanthi lozenge comprise, by weight, 60-80 parts of Fructus phyllanthi powder, 5-10 parts of xylitol, 5-20 parts of beta-cyclodextrin and 0.1-0.5 parts of mannitol. The Fructus phyllanthi lozenge completely reserves nutritional components in Fructus phyllanthi, and has mellow mouthfeel, and sweet aftertaste and beautiful color.
Description
Technical field
The present invention relates to a kind of Phyllanthus embical fruit tablet and preparation method thereof.
Background technology
Yunnan olive (Fusctusphyllanthi) has another name called Phyllanthus embical fruit, is the fruit of Euphorbiaceae phyllanthus plant emblic (PhyllanthusemblicaLinn), is distributed widely in the multiple provinces and regions of Southwestern China and the southeast.Yunnan olive is as a kind of important medicine food dual purpose plant resource, record in version " Yunnan Province's drug standards " in 1974, version " Tibetan medicine standard ", 1977 to 2005 years version Pharmacopoeias of the People's Republic of China in 1978, in the traditional Chinese medicine systems such as China's Chinese herbal medicine and ethnic drug, there is very long history.
The Yunnan olive resource of China is the widest with Yunnan Province's distribution area, output is maximum, be wherein maximum with Chuxiong, Lincang, Simao and the Baoshan and other places especially, and is wild nature.Add up according to investigations, there is Yunnan olive Linda in blocks 60 ~ 700,000 mu in Yunnan Province, and suitable raw area reaches more than 3,000,000 mu, and annual the whole province about produces fresh fruit more than 100,000 ton, is that a few can continue, the natural resources of scale development.
Yunnan olive unique flavor, nutritious and there is important medical value.Yunnan olive contains the nutritional labelings such as 12 kinds of vitamins, 18 seed amino acids, protein and 16 kinds of trace elements; Containing bioactive ingredients such as Polyphenols (comprising tannin class etc.), organic acid, flavonoids, polysaccharide, terpene, sterol and superoxide dismutase SOD.Wherein higher with vitamin C, tannin class, flavonoids and polyoses content.Yunnan olive has antibacterial, antiviral, anti-inflammatory, lipopenicillinase, antiatherosclerosis, hypoglycemic, anti-oxidant, scavenging free radicals, antitumor, health care wait for a long time health-care effect.
The Vitamin C content of Yunnan olive fresh fruit is generally at more than 300mg/100g, higher than oranges and tangerines 10 ~ 23 times, higher than apple 60 ~ 134 times.By the dietary standard that the U.S. is recommended, as long as every day, edible Yunnan olive 10g (about 1 fruit) can meet the demand of body vitamin C.Vitamin C is thermal sensitivity nutritional labeling, and the operation such as boiling, baking, Exposure to Sunlight of food processing process very easily causes oxidational losses.
Yunnan olive is rich in SOD, and the SOD of fresh fruit activity presses fresh fruit conversion up to 800NU/100g.SOD is the cell defendance enzyme that body weight for humans is wanted, and can prevent the lipid peroxidation of skin histology, effectively reduce MDA content, improve body activities of antioxidant enzymes, scavenging free radicals, thus promote tissue cell growth and metabolism, delay senility.SOD does not possess characteristic that is heat-resisting, acid and alkali-resistance.
Yunnan olive is also rich in phenols component, comprises water-soluble tannins, condensed tannin, liposoluble ingredient, flavanol compound composition etc.; Wherein water-soluble tannins composition has the physiologically actives such as antiatherosclerosis.Matter of mixing constituents gives Yunnan olive puckery unique oral sensations.Tannin constituents is in conventional heating refluxing extraction process, and temperature is too high, can cause the change of its chemistry and structure.
Yunnan olive products many employings fresh fruit is in the market squeezed the juice, fresh fruit heats concentrate drying after squeezing the juice, or adopts water or the ethanolic solution extract of Yunnan olive, and then make Yunnan olive products, these methods exist many deficiencies.
Application number be 200810058600.8 Chinese patent application disclose a kind of Phyllanthus embical fruit tablet, filling a prescription is: phyllanthus emblica powder 15-50%, D-sorbite 30-80%, xylitol 5-20%, acesulfame potassium 0.01-0.3%, cycloheptaamylose 5-30%, citric acid 0.1-3%, menthol 0.01-0.3%.Add a large amount of auxiliary material in the formula of this Phyllanthus embical fruit tablet, also add menthol, thus in this lozenge, the nutritional labeling of Yunnan olive is relatively less, and mouthfeel also changes more due to the existence of menthol.In addition, phyllanthus emblica powder fresh fruit is squeezed the juice, prepared by spray-dired mode, only make use of the fruit juice constituents of Yunnan olive, and nutritional labeling useful in a large number in pulp goes out of use.
Application number be 201310593499.7 Chinese patent application disclose a kind of Yunnan olive compound chewable tablets, comprise phyllanthus emblica powder, acerola concentrate extract, xylitol, D-sorbite, menthol, dolomol and superfine silica gel powder.Supplementary product kind and large usage quantity in this chewable tablets, and simultaneously containing acerola concentrate extract, menthol, complete nutrition composition and the unique oral sensations of Yunnan olive can not be kept.And this phyllanthus emblica powder is also that employing fresh fruit is squeezed the juice, the preparation of spray-dired method, the beneficiating ingredient in the olive pulp of Yunnan cannot be retained, such as, and fruit juice is when heating concentration, can destroy the heat-sensitive ingredients in the olive of Yunnan, vitamin C, SOD, phenols component etc.
Summary of the invention
The object of the present invention is to provide a kind of Phyllanthus embical fruit tablet, described Phyllanthus embical fruit tablet more intactly remains the nutritional labeling in the olive fruit of Yunnan, and color and luster is attractive in appearance, and mellow in taste is returned sweet.
Another object of the present invention is to the preparation method that above-mentioned Phyllanthus embical fruit tablet is provided.
The invention provides a kind of Phyllanthus embical fruit tablet, comprise: phyllanthus emblica powder end 70 ~ 90 weight portion, filler 5 ~ 30 weight portion and flavouring 5 ~ 15 weight portion.
According to Phyllanthus embical fruit tablet of the present invention, preferably, following component is comprised:
Phyllanthus emblica powder end 70 ~ 90 weight portion,
Filler 5 ~ 20 weight portion, and
Flavouring 5 ~ 10 weight portion.
According to Phyllanthus embical fruit tablet of the present invention, described filler and flavouring all can adopt this area routine use those.Preferably, described filler is selected from least one in starch, Icing Sugar, dextrin, lactose, amylum pregelatinisatum and glycitols filler.Preferably, described glycitols filler comprises sweet mellow wine, sorbierite.More preferably, described filler adopts sweet mellow wine or sorbierite.
According to Phyllanthus embical fruit tablet of the present invention, preferably, described flavouring is selected from least one in sucrose, xylitol, lactitol, isomaltoketose, stevioside, Aspartame.More preferably, described flavouring is selected from sucrose or xylitol.
According to one of the present invention preferred embodiment, described filler is sweet mellow wine, and described flavouring is sucrose or xylitol.
According to one of the present invention preferred embodiment, described Phyllanthus embical fruit tablet comprises phyllanthus emblica powder end 80 ~ 90 weight portion, sweet mellow wine 5-10 weight portion, and xylitol 5 ~ 10 weight portion.
According to one of the present invention preferred embodiment, described Phyllanthus embical fruit tablet comprises phyllanthus emblica powder end 80 ~ 90 weight portion, sweet mellow wine 5-10 weight portion, and sucrose 5 ~ 10 weight portion.
The tablet ingredients of other routines can also be contained, such as disintegrant, lubricant etc. in Phyllanthus embical fruit tablet of the present invention.
According to one of the present invention preferred embodiment, Phyllanthus embical fruit tablet of the present invention is only made up of said components.In above-mentioned preferred Phyllanthus embical fruit tablet, the content at phyllanthus emblica powder end is higher, and three coordinates rear level of sweetness agreeable to the taste, and mouthfeel is better.In addition, phyllanthus emblica powder end, filler and flavouring have good mobility, compressibility and lubricity with the material that ratio of the present invention mixes, and are easily pressed into tablet.
Phyllanthus embical fruit tablet of the present invention can adopt multiple figure of tablet, is preferably circle, ellipse, rectangle, rhombus etc.
According to Phyllanthus embical fruit tablet of the present invention, preferably, described phyllanthus emblica powder end prepares by the following method:
(1) by the sterilization of Yunnan olive fruit, stoning;
(2) the Yunnan olive fruit after step (1) being processed is placed in-10 DEG C to-40 DEG C, vacuum is carry out frozen dried under 30-150pa, obtains the Yunnan olive fruit dry product that water content is 5-15wt%;
(3) described Yunnan olive fruit dry product is pulverized at-10 DEG C to-40 DEG C, obtain phyllanthus emblica powder end.
The present invention also provides the preparation method of described Phyllanthus embical fruit tablet, comprising:
A. mix: described phyllanthus emblica powder end, filler and flavouring are mixed, obtains mixture;
B. compressing tablet: by described mixture compressing tablet, obtain described Phyllanthus embical fruit tablet.
According to the preparation method of Phyllanthus embical fruit tablet of the present invention, preferably, also comprise the step preparing phyllanthus emblica powder end, comprising:
(1) by the sterilization of Yunnan olive fruit, stoning;
(2) the Yunnan olive fruit after step (1) being processed is placed in-10 DEG C to-40 DEG C, vacuum is carry out frozen dried under 30-150pa, obtains the Yunnan olive fruit dry product that water content is 5-15wt%;
(3) described Yunnan olive fruit dry product is pulverized at-10 DEG C to-40 DEG C, obtain phyllanthus emblica powder end.
According to the preparation method at phyllanthus emblica powder end of the present invention, preferably, step (1) described Yunnan olive fruit is Yunnan olive fresh fruit.Yunnan of the present invention olive fresh fruit is preferably ripe, complete, without the fresh fruit rotted, nothing is gone mouldy.
Preparation in accordance with the present invention, preferably, step (1) described Yunnan olive fruit is Yunnan olive fresh fruit.Yunnan of the present invention olive fresh fruit is preferably ripe, complete, without the fresh fruit rotted, nothing is gone mouldy.
Preparation in accordance with the present invention, step (1) can adopt aqueous hydrogen peroxide solution, aqueous sodium hypochlorite solution, the postassium hypochlorite aqueous solution or potassium permanganate solution Yunnan olive fruit to be sterilized; Preferably, aqueous hydrogen peroxide solution is adopted Yunnan olive fruit to be sterilized.According to a kind of detailed description of the invention of the present invention, adopt 0.05-0.6wt%, Yunnan olive fruit is soaked or drip washing sterilization by the aqueous hydrogen peroxide solution being preferably 0.1-0.5wt%, then rinses the residual hydrogen peroxide of removing with clear water.Above-mentioned immersion or drip washing time are 2-15min, are preferably 3-10min, are more preferably 4-5min.In step (1), first described Yunnan olive fruit sterilizes, then stoning, thus avoids disinfectant to the destruction of Yunnan olive pulp.
In step (1), described stoning can adopt artificial or stoner realization, preferably adopts stoner to realize.
Preparation in accordance with the present invention, preferably, described preparation method also comprises the step that the Yunnan olive fruit after by sterilization, stoning carries out cutting into slices.Yunnan olive fruit is carried out slicing treatment, is more conducive to follow-up drying and pulverization process.
In step (2), said temperature and vacuum is adopted to carry out drying to Yunnan olive, and when reaching above-mentioned water content, nutritional labeling in the olive of Yunnan is less to be damaged, can comparatively complete, stable, retain muchly, such as, the activity of SOD is well kept, and avoids inactivation.In addition, such processing method can keep the original color and luster of Yunnan olive fresh fruit preferably.
Preparation in accordance with the present invention, preferably, in step (2), the Yunnan olive fruit after step (1) being processed is placed in-20 DEG C to-40 DEG C, vacuum is carry out frozen dried under 50-100pa.
Preparation in accordance with the present invention, preferably, frozen dried described in step (2) also comprises the step that first the Yunnan olive fruit after step (1) being processed carries out precooling.Preferably, described precooling temperature is-80 DEG C to-40 DEG C, is preferably-70 DEG C to-40 DEG C; The precooling time is 8-20min, is more preferably 10-15min.
In step (2), described frozen dried can adopt the freeze dryer of this area routine to realize.
Preparation in accordance with the present invention, preferably, in step (2), is dried to the dry product of water content 8-10wt% by Yunnan olive fruit.Such Yunnan olive dry product, compared with other drying modes, avoids the change of Yunnan olive fruit chemistry, physics, keeps the original nutritional labeling of Yunnan olive, color and luster and mouthfeel to greatest extent.
In common crushing process, material and mechanical high-speed are collided, are rubbed, and easily cause material to heat up.In step (3), Yunnan olive dry product is pulverized under low temperature of the present invention, can effectively avoid high temperature to the destruction of Yunnan olive Middle nutrition composition, thus relatively intactly retain nutritional labeling and the medicinal active ingredient of Yunnan olive.
Preparation in accordance with the present invention, preferably, in step (3), described dry product is pulverized at-10 DEG C to-20 DEG C, such temperature can either ensure that temperature when pulverizing is unlikely to destroy the composition in the olive dry product of Yunnan, and economize energy, reduces costs simultaneously.
In step (3), Yunnan olive dry product is crushed to particle diameter D50 (median particle diameter, particle diameter corresponding when the cumulative particle sizes percentile of a sample reaches 50%) lower than 45 microns.According to the preferred embodiment of the invention, Yunnan olive dry product is crushed to particle diameter D50 lower than 25 microns, more preferably less than 10 microns by step (3).
Preparation in accordance with the present invention, in step (3), can adopt any conventional method to be pulverized by described Yunnan olive fruit dry product.According to the preferred embodiment of the present invention, ultramicro grinding method is adopted to be pulverized by described Yunnan olive fruit dry product.According to a kind of preferred embodiment of the present invention, adopt the broken method of low-temperature submicron powder that described Yunnan olive fruit is crushed to D50 lower than 25 microns.Ultramicro grinding method can break cell membrane, the nutritional labeling in the olive of Yunnan is fully come out, thus greatly improves dissolution rate and the bioavilability of Yunnan olive Middle nutrition composition, makes it to be absorbed more fully by human body.
In step (3), by low-temperature submicron powder broken machine, Yunnan olive dry product is pulverized.
Compared with existing Phyllanthus embical fruit tablet, in Phyllanthus embical fruit tablet of the present invention, primary raw material phyllanthus emblica powder end is prepared at low temperatures, do not relate to high-temperature heating process, organic solvent extracting process is not related to yet, especially can not destroy the composition such as vitamin C, SOD of thermal sensitivity, avoid the medicinal ingredient Yin Wendu such as tannin too high and chemistry and the change of structure occur simultaneously, remain the nutritional labeling in the olive of Yunnan near-completely.Phyllanthus embical fruit tablet of the present invention is due to the above-mentioned phyllanthus emblica powder end containing high-load, and auxiliary material content is lower, thus remains the peculiar flavour of Yunnan olive fresh fruit almost genuinely.
In the preferred embodiment of the present invention, due to the specific filler containing proper ratio and flavouring component, make the level of sweetness of Phyllanthus embical fruit tablet agreeable to the taste, mellow time sweet, and watered down astringent sense, and mouthfeel is better.In addition, Phyllanthus embical fruit tablet of the present invention presents the natural light green of Yunnan olive fresh fruit in appearance, and color and luster is very attractive in appearance, is easily esthetically acceptable to the consumers.
Detailed description of the invention
Below by specific embodiment, preparation method of the present invention is described in further details, but therefore protection scope of the present invention is not subject to any restriction.
The vacuum freeze drying freeze dryer adopted in following examples is that Dong Fulong Science and Technology Ltd. produces, model Ly0-1.0 (CIP.SIP); The broken machine of low-temperature submicron powder adopted is that Jinan Dong Yao test apparatus Co., Ltd produces, model XDW6-BI (low temperature).The mixer adopted is Zhejiang Canaan pharmaceutical equipment Co., Ltd, model HZ0 series automatic lifting hopper mixer; The tablet press machine adopted is Zibo Machinery Manufacturing Co., Ltd. of Yi Ma Xinhua, KILIAIV high speed tablet press.
preparation example 1
Adopt and prepare phyllanthus emblica powder end with the following method: the aqueous hydrogen peroxide solution of ripe, complete, that nothing is rotted, nothing is gone mouldy Yunnan olive fruit 0.1wt% is soaked 10min by (1), and clear water rinses, and uses stoner stoning, cuts into slices; Yunnan olive fruit after section adopt vacuum freeze drying freeze dryer in-20 DEG C, carry out frozen dried under 30Pa, obtain the Yunnan olive fruit dry product of water content 15wt%; Gained dry product is crushed at-10 DEG C D50 about 45 microns, obtains phyllanthus emblica powder end.
preparation example 2
Adopt and prepare phyllanthus emblica powder end with the following method: the aqueous hydrogen peroxide solution of ripe, complete, that nothing is rotted, nothing is gone mouldy Yunnan olive fruit 0.6wt% is soaked 5min by (1), and clear water rinses, and uses stoner stoning, cuts into slices; (2) the Yunnan olive fruit after section adopts vacuum freeze drying freeze dryer precooling 8min at-80 DEG C, then in-10 DEG C, freeze-drying under 100Pa, obtains the dry product of water content 10wt%.(3) gained dry product is placed in the broken machine of low-temperature submicron powder, at-20 DEG C, ultramicro grinding is to D50 about 5 microns, obtains phyllanthus emblica powder end.
embodiment 1
The Phyllanthus embical fruit tablet of the present embodiment, comprises following component: phyllanthus emblica powder end 80 weight portions, sweet mellow wine 15 weight portion, xylitol 5 weight portion, wherein phyllanthus emblica powder end adopts preparation example 1 method to obtain.The Phyllanthus embical fruit tablet preparation method of the present embodiment adds in mixer by phyllanthus emblica powder end, then adds sweet mellow wine, xylitol mixes, and obtains mixture, tabletting machine, obtain Phyllanthus embical fruit tablet.
embodiment 2
The Phyllanthus embical fruit tablet of the present embodiment, comprises following component: phyllanthus emblica powder end 70 weight portions, sweet mellow wine 25 weight portion, xylitol 5 weight portion, wherein phyllanthus emblica powder end adopts preparation example 1 method to obtain.The Phyllanthus embical fruit tablet preparation method of the present embodiment adds in mixer by phyllanthus emblica powder end, then adds sweet mellow wine, xylitol mixes, and obtains mixture, tabletting machine, obtain Phyllanthus embical fruit tablet.
embodiment 3
The Phyllanthus embical fruit tablet of the present embodiment, comprises following component: phyllanthus emblica powder end 90 weight portions, sweet mellow wine 5 weight portion, sucrose 5 weight portion, wherein phyllanthus emblica powder end adopts preparation example 2 method to obtain.The Phyllanthus embical fruit tablet preparation method of the present embodiment adds in mixer by phyllanthus emblica powder end, then adds sweet mellow wine, sucrose mixes, and obtains mixture, tabletting machine, obtain Phyllanthus embical fruit tablet.
embodiment 4
The Phyllanthus embical fruit tablet of the present embodiment, comprises following component: phyllanthus emblica powder end 80 weight portions, sweet mellow wine 0.5 weight portion, beta-schardinger dextrin-14 weight portion and xylitol 5.5 weight portion, wherein phyllanthus emblica powder end adopts preparation example 2 method to obtain.The Phyllanthus embical fruit tablet preparation method of the present embodiment adds in mixer by phyllanthus emblica powder end, then adds sweet mellow wine, beta-schardinger dextrin-and xylitol and mix, obtain mixture, tabletting machine, obtain Phyllanthus embical fruit tablet.
comparative example 1
By the aqueous hydrogen peroxide solution drip washing 10min of ripe, complete, that nothing is rotted, nothing is gone mouldy Yunnan olive fruit 0.1wt%, clear water rinses, and uses stoner stoning, squeezes the juice with juice extractor, filters, and filtrate is heated concentrated, dry, pulverize, obtains phyllanthus emblica powder end.
comparative example 2
By the aqueous hydrogen peroxide solution drip washing 10min of ripe, complete, that nothing is rotted, nothing is gone mouldy Yunnan olive fruit 0.1wt%, clear water rinses removing hydrogen peroxide, uses stoner stoning, Yunnan olive fruit after the stoning ethanolic solution of 50% extracts, concentrated, dry, pulverize, obtain phyllanthus emblica powder end.
comparative example 3
According to application number be the Chinese patent application file of 200810058600.8 detailed description of the invention part record formula and method prepare Phyllanthus embical fruit tablet.
test example 1
Get preparation example 1-2, phyllanthus emblica powder that comparative example 1-2 obtains end, measure the active and tannin constituents content of wherein Vitamin C content, SOD respectively, and be converted to the content in the olive fresh fruit of every 100g Yunnan.
Method of testing is described as follows:
Vitamin C content is according to GB GB/T6195-and 1986 methods recorded measure; The active method recorded according to GB/T5009.171-2003 of SOD measures; The method that tannin constituents content is recorded according to Chinese Pharmacopoeia 2010 editions annex XB measures.Measurement result (be 100g conversion by fresh fruit quality) and the mouthfeel at various phyllanthus emblica powder end, outward appearance are in table 1.
Table 1
Can be found out by table 1, the activity of the vitamin C at the phyllanthus emblica powder end that preparation method of the present invention obtains and tannin constituents retention rate, SOD is all significantly higher than prior art, and remains the distinctive mellow time sweet mouthfeel of Yunnan olive fresh fruit, and color and luster is attractive in appearance.
test example 2
Recruit 198 persons of foretasting and foretaste experiment to the Phyllanthus embical fruit tablet that embodiment 1 and comparative example 3 obtain, wherein the person of foretasting of about 92% thinks that the Phyllanthus embical fruit tablet of embodiment 1 is more attractive in appearance than the Phyllanthus embical fruit tablet color and luster of comparative example 3; The person of foretasting of about 88% thinks compared with the Phyllanthus embical fruit tablet of comparative example 3, and the Phyllanthus embical fruit tablet unique flavor of embodiment 1, mouthfeel is better.
The present invention is not limited to above-mentioned embodiment, and when not deviating from flesh and blood of the present invention, any distortion that it may occur to persons skilled in the art that, improvement, replacement all fall into scope of the present invention.
Claims (10)
1. a Phyllanthus embical fruit tablet, comprises following component:
Phyllanthus emblica powder end 70 ~ 90 weight portion, filler 5 ~ 30 weight portion and flavouring 5 ~ 15 weight portion.
2. Phyllanthus embical fruit tablet according to claim 1, is characterized in that, described filler is selected from least one in starch, Icing Sugar, dextrin, lactose, amylum pregelatinisatum and glycitols auxiliary material; Described flavouring is selected from least one in sucrose, xylitol, lactitol, isomaltoketose, stevioside, Aspartame.
3. Phyllanthus embical fruit tablet according to claim 2, is characterized in that, described filler is sweet mellow wine, and described flavouring is sucrose or xylitol.
4. the Phyllanthus embical fruit tablet according to any one of claim 1-3, is characterized in that, described phyllanthus emblica powder end prepares as follows:
(1) by the sterilization of Yunnan olive fruit, stoning;
(2) the Yunnan olive fruit after step (1) being processed is placed in-10 DEG C to-40 DEG C, vacuum is carry out frozen dried under 30-150pa, obtains the Yunnan olive fruit dry product that water content is 5-15wt%;
(3) described Yunnan olive fruit dry product is pulverized at-10 DEG C to-40 DEG C, obtain phyllanthus emblica powder end.
5. the preparation method of the Phyllanthus embical fruit tablet according to any one of claim 1-3, comprising:
A. mix: described phyllanthus emblica powder end, filler, flavouring are mixed, obtains mixture;
B. compressing tablet: by described mixture compressing tablet, obtain described Phyllanthus embical fruit tablet.
6. the preparation method of Phyllanthus embical fruit tablet according to claim 5, is characterized in that, described method also comprises the step preparing phyllanthus emblica powder end, and the described step preparing phyllanthus emblica powder end comprises:
(1) by the sterilization of Yunnan olive fruit, stoning;
(2) the Yunnan olive fruit after step (1) being processed is placed in-10 DEG C to-40 DEG C, vacuum is carry out frozen dried under 30-150pa, obtains the Yunnan olive fruit dry product that water content is 5-15wt%;
(3) described Yunnan olive fruit dry product is pulverized at-10 DEG C to-40 DEG C, obtain phyllanthus emblica powder end.
7. the preparation method of Phyllanthus embical fruit tablet according to claim 6, it is characterized in that, frozen dried described in step (2) also comprises the step that first the Yunnan olive fruit after step (1) being processed carries out precooling, precooling temperature is-80 DEG C to-40 DEG C, and the precooling time is 8-20min.
8. the preparation method of Phyllanthus embical fruit tablet according to claim 6, is characterized in that, in step (3), Yunnan olive dry product is crushed to particle diameter D50 lower than 25 microns.
9. the preparation method of Phyllanthus embical fruit tablet according to claim 6, is characterized in that, in step (1), adopts aqueous hydrogen peroxide solution, aqueous sodium hypochlorite solution, the postassium hypochlorite aqueous solution or potassium permanganate solution Yunnan olive fruit to be sterilized.
10. the preparation method of Phyllanthus embical fruit tablet according to claim 6, is characterized in that, described prepare in the step at phyllanthus emblica powder end also to comprise Yunnan olive fruit sterilized, carry out the step of cutting into slices after stoning.
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| CN107232593A (en) * | 2017-06-22 | 2017-10-10 | 云南中医学院 | Composition of the olive containing Yunnan and its production and use |
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| CN108991215A (en) * | 2018-07-11 | 2018-12-14 | 广东泓睿科技有限公司 | A kind of Yunnan olive preserved fruit and preparation method thereof |
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