CN105133287A - Manufacture method for all-cotton super-soft silk-protein silk-like yarn-dyed fabric - Google Patents
Manufacture method for all-cotton super-soft silk-protein silk-like yarn-dyed fabric Download PDFInfo
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- CN105133287A CN105133287A CN201510511331.6A CN201510511331A CN105133287A CN 105133287 A CN105133287 A CN 105133287A CN 201510511331 A CN201510511331 A CN 201510511331A CN 105133287 A CN105133287 A CN 105133287A
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Abstract
The invention discloses a manufacture method for all-cotton super-soft silk-protein silk-like yarn-dyed fabric. The method comprises (1) performing oxidation processing on cotton cloth, employing sodium periodate as an oxidant, controlling the temperature to about 50-55 DEG C, performing warm-keeping processing, and keeping the pH value to 5-6; (2) dipping the oxidized fabric in a silk protein solution, and employing polyurethane as a cross-linking agent, adjusting the pH value to 6-7, performing low-temperature drying, then performing baking, so as to enable protein molecules to be crosslinked on the fabric surface and form a film; and (3) performing air softening arrangement, and breaking up the backbone of the fabric through air beating. The fabric is soft in handfeeling and good in surface luster, the drape coefficient is about 15%, the strength retention rate is larger than 80% and the flatness is larger than 2.5 grade.
Description
Technical field
The application belongs to textile technology field, particularly relates to a kind of cotton and surpasses the manufacture method that flexible silk albumen imitates a color-woven fabric.
Background technology
Cotton fiber, as the abundant renewable cellulose resource of occurring in nature, is the key industry raw material in the fields such as weaving for a long time, and its renewable, biodegradability and cost advantage are subject to people's attention always.But the high-crystallinity of cotton fiber and slightly solubility make it utilize scope to be restricted.Along with the aggravation that growing tension and the ball ecological environment of oil, coal equal energy source pollute, effectively utilize cellulose resource further, the application of developing cellulose in new technology, new material just becomes study hotspot.
Summary of the invention
The object of the present invention is to provide a kind of cotton to surpass manufacture method that flexible silk albumen imitates a color-woven fabric, to overcome deficiency of the prior art.
For achieving the above object, the invention provides following technical scheme:
The embodiment of the present application discloses a kind of cotton and surpasses the manufacture method that flexible silk albumen imitates a color-woven fabric, comprising:
(1), to cotton carry out oxidation processes, employing sodium metaperiodate is oxidant, and temperature controls, at about 50 ~ 55 DEG C, to carry out isothermal holding, and pH value remains between 5 ~ 6;
(2), by well-oxygenated COTTON FABRIC dipping silk protein solution, adopt polyurethane to be crosslinking agent, adjust ph is 6 ~ 7, and low temperature drying, then bakes, and makes protein molecule be cross-linked film forming at fabric face simultaneously;
(3), carry out air soft finish, by the beating of air, the backbone of fabric is broken up.
Preferably, surpass flexible silk albumen imitate in the manufacture method of a color-woven fabric at above-mentioned cotton, the consumption of described sodium metaperiodate is 5g/L, and the time of isothermal holding is 1 hour.
Preferably, surpass flexible silk albumen imitate in the manufacture method of a color-woven fabric at above-mentioned cotton, the consumption of silk protein solution is 20g/L.
Preferably, surpass flexible silk albumen imitate in the manufacture method of a color-woven fabric at above-mentioned cotton, the consumption of polyurethane is 30g/L.
Preferably, surpass flexible silk albumen imitate in the manufacture method of a color-woven fabric at above-mentioned cotton, in described step (2), the temperature of low temperature drying is 95 DEG C, and drying time is 2min.
Preferably, surpass flexible silk albumen at above-mentioned cotton and imitate in the manufacture method of a color-woven fabric, in described step (2), under 165 DEG C of conditions, bake 3min.
Compared with prior art, the invention has the advantages that: fabrics feel soft of the present invention, lustrous surface is good, suspended coefficient about 15%, strength retention > 80%, flatness > 2.5 grade.
Accompanying drawing explanation
In order to be illustrated more clearly in the embodiment of the present application or technical scheme of the prior art, be briefly described to the accompanying drawing used required in embodiment or description of the prior art below, apparently, the accompanying drawing that the following describes is only some embodiments recorded in the application, for those of ordinary skill in the art, under the prerequisite not paying creative work, other accompanying drawing can also be obtained according to these accompanying drawings.
Figure 1 shows that longitudinal SEM photo of common cotton fiber;
Figure 2 shows that longitudinal SEM photo of the rear cotton fiber of oxidation;
Figure 3 shows that the rear longitudinal SEM photo of cotton fiber after silk protein solution process of oxidation.
Detailed description of the invention
The present invention is described further by the following example: according to following embodiment, the present invention may be better understood.But those skilled in the art will readily understand, concrete material ratio, process conditions and result thereof described by embodiment only for illustration of the present invention, and should can not limit the present invention described in detail in claims yet.
Embodiment 1
For the characteristic of cotton, optimize cotton oxidation processing technique, employing sodium metaperiodate is oxidant, and consumption is 5g/L, and temperature controls at about 50 DEG C, and carry out isothermal holding 1 hours, pH value remains between 5, guarantees the optimum state that dialdehyde cellulose is formed.
By well-oxygenated COTTON FABRIC dipping silk protein solution, the consumption of silk protein solution is 20g/L, adopts polyurethane to be crosslinking agent simultaneously, consumption is 30g/L, and adjust ph is 6,95 DEG C of low temperature drying 2min, then under 165 DEG C of conditions, bake 3min, make protein molecule be cross-linked film forming at fabric face.
After sizing, carry out air soft finish, by the beating of air, the backbone of fabric is broken up, obtain feel soft as silk fabrics.
Carry out calendering arrangement, improve the gloss of fabric face.
To obtain the decayed tooth technical indicator of fabric as follows:
1, suspended coefficient is about 15%;
2, strength retention > 80%;
3, flatness > 2.5 grades.
Figure 1 shows that longitudinal SEM photo of common cotton fiber, can find out in figure, common cotton fiber surface is more smooth.
Figure 2 shows that longitudinal SEM photo of cotton fiber after oxidation, can find out in figure, cotton fiber surface occur along fiber axis to striped, and longitudinal stripe is deepened and is become irregular.
Figure 3 shows that the rear longitudinal SEM photo of cotton fiber after silk protein solution process of oxidation, can find out in figure, the longitudinal stripe on oxidized cotton fiber its surface after silk protein solution process disappears substantially, and surface becomes smooth, smooth.
Embodiment 2
For the characteristic of cotton, optimize cotton oxidation processing technique, employing sodium metaperiodate is oxidant, and consumption is 5g/L, and temperature controls at about 55 DEG C, and carry out isothermal holding 1 hours, pH value remains between 6, guarantees the optimum state that dialdehyde cellulose is formed.
By well-oxygenated COTTON FABRIC dipping silk protein solution, the consumption of silk protein solution is 20g/L, adopts polyurethane to be crosslinking agent simultaneously, consumption is 30g/L, and adjust ph is 7,95 DEG C of low temperature drying 2min, then under 165 DEG C of conditions, bake 3min, make protein molecule be cross-linked film forming at fabric face.
After sizing, carry out air soft finish, by the beating of air, the backbone of fabric is broken up, obtain feel soft as silk fabrics.
Carry out calendering arrangement, improve the gloss of fabric face.
Embodiment 3
For the characteristic of cotton, optimize cotton oxidation processing technique, employing sodium metaperiodate is oxidant, and consumption is 5g/L, and temperature controls at about 53 DEG C, and carry out isothermal holding 1 hours, pH value remains between 6, guarantees the optimum state that dialdehyde cellulose is formed.
By well-oxygenated COTTON FABRIC dipping silk protein solution, the consumption of silk protein solution is 20g/L, adopts polyurethane to be crosslinking agent simultaneously, consumption is 30g/L, and adjust ph is 6,95 DEG C of low temperature drying 2min, then under 165 DEG C of conditions, bake 3min, make protein molecule be cross-linked film forming at fabric face.
After sizing, carry out air soft finish, by the beating of air, the backbone of fabric is broken up, obtain feel soft as silk fabrics.
Carry out calendering arrangement, improve the gloss of fabric face.
Finally, also it should be noted that, term " comprises ", " comprising " or its any other variant are intended to contain comprising of nonexcludability, thus make to comprise the process of a series of key element, method, article or equipment and not only comprise those key elements, but also comprise other key elements clearly do not listed, or also comprise by the intrinsic key element of this process, method, article or equipment.
Claims (6)
1. cotton surpasses the manufacture method that flexible silk albumen imitates a color-woven fabric, it is characterized in that, comprising:
(1), to cotton carry out oxidation processes, employing sodium metaperiodate is oxidant, and temperature controls, at about 50 ~ 55 DEG C, to carry out isothermal holding, and pH value remains between 5 ~ 6;
(2), by well-oxygenated COTTON FABRIC dipping silk protein solution, adopt polyurethane to be crosslinking agent, adjust ph is 6 ~ 7, and low temperature drying, then bakes, and makes protein molecule be cross-linked film forming at fabric face simultaneously;
(3), carry out air soft finish, by the beating of air, the backbone of fabric is broken up.
2. cotton according to claim 1 surpasses the manufacture method that flexible silk albumen imitates a color-woven fabric, it is characterized in that: the consumption of described sodium metaperiodate is 5g/L, and the time of isothermal holding is 1 hour.
3. cotton according to claim 1 surpasses the manufacture method that flexible silk albumen imitates a color-woven fabric, it is characterized in that: the consumption of silk protein solution is 20g/L.
4. cotton according to claim 1 surpasses the manufacture method that flexible silk albumen imitates a color-woven fabric, it is characterized in that: the consumption of polyurethane is 30g/L.
5. cotton according to claim 1 surpasses the manufacture method that flexible silk albumen imitates a color-woven fabric, it is characterized in that: in described step (2), and the temperature of low temperature drying is 95 DEG C, and drying time is 2min.
6. cotton according to claim 1 surpasses the manufacture method that flexible silk albumen imitates a color-woven fabric, it is characterized in that: in described step (2), under 165 DEG C of conditions, bake 3min.
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| CN201510511331.6A CN105133287A (en) | 2015-08-19 | 2015-08-19 | Manufacture method for all-cotton super-soft silk-protein silk-like yarn-dyed fabric |
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| CN201510511331.6A CN105133287A (en) | 2015-08-19 | 2015-08-19 | Manufacture method for all-cotton super-soft silk-protein silk-like yarn-dyed fabric |
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Cited By (4)
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|---|---|---|---|---|
| CN107313261A (en) * | 2017-08-09 | 2017-11-03 | 青岛大学 | A kind of method of the plain enzyme of reinforcing fiber to bafta biopolishing effect |
| CN107881783A (en) * | 2017-11-29 | 2018-04-06 | 苏州大学 | A kind of protein modified method of pure-cotton fabric |
| CN107956118A (en) * | 2017-11-29 | 2018-04-24 | 江苏宝缦家纺科技有限公司 | A kind of fibroin method of modifying of pure-cotton fabric |
| CN110184817A (en) * | 2019-05-14 | 2019-08-30 | 苏州法比瑞纺织科技有限公司 | The manufacturing method of the super protein modified color brocade fabric lining of flexible silk |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107313261A (en) * | 2017-08-09 | 2017-11-03 | 青岛大学 | A kind of method of the plain enzyme of reinforcing fiber to bafta biopolishing effect |
| CN107881783A (en) * | 2017-11-29 | 2018-04-06 | 苏州大学 | A kind of protein modified method of pure-cotton fabric |
| CN107956118A (en) * | 2017-11-29 | 2018-04-24 | 江苏宝缦家纺科技有限公司 | A kind of fibroin method of modifying of pure-cotton fabric |
| CN110184817A (en) * | 2019-05-14 | 2019-08-30 | 苏州法比瑞纺织科技有限公司 | The manufacturing method of the super protein modified color brocade fabric lining of flexible silk |
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