CN105106154B - A kind of person in middle and old age's sugar-free calcium tablet and preparation method thereof - Google Patents
A kind of person in middle and old age's sugar-free calcium tablet and preparation method thereof Download PDFInfo
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- CN105106154B CN105106154B CN201510589790.6A CN201510589790A CN105106154B CN 105106154 B CN105106154 B CN 105106154B CN 201510589790 A CN201510589790 A CN 201510589790A CN 105106154 B CN105106154 B CN 105106154B
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Abstract
The invention belongs to the preparation fields of calcium tablet, and in particular to a kind of person in middle and old age's sugar-free calcium tablet and preparation method thereof.The calcium tablet its raw material composition is calculated as by weight, 1160 ~ 1220 parts of calcium carbonate, 345 ~ 365 parts of D-sorbite, 25 parts of citric acid, 5 parts of purified water, 8.5 parts of edible alcohol, 635 ~ 647 parts of dextrin, 240 ~ 250 parts of maltodextrin, 3 ~ 4 parts of orange flavor, 0.5 ~ 1.0 part of Sucralose, 23 ~ 27 parts of magnesium stearate.The present invention increases the sugariness of calcium tablet using non-sugar sweetener, but not increases heat, and obtained product has the characteristics that low in calories, low temperature is anti-oxidant, sugar-free, easily absorbs.
Description
Technical field
The invention belongs to the preparation fields of calcium tablet, and in particular to a kind of person in middle and old age's sugar-free calcium tablet and preparation method thereof.
Background technology
The diet in China is formed based on plant food, and calcium content is few, and the abundant food of calcium content is few, and calcium-phosphorus ratio
Value is serious to be inverted, and is unfavorable for being absorbed and utilized for calcium, while there are a variety of calcium uptakes that are unfavorable for such as phytic acid content height in diet to utilize
Factor.At present, one of most effective measure for improving crowd's calcium intake is exactly to strengthen calcium in food.Though existing have numerous commercial cas
Preparation and the food for strengthening calcium, but it is most of expensive, it is difficult to it promotes, and the effect of supplemented calcium for most products in itself
And absorption rate also requires study.The calcium source used in commodity calcium preparation and condensed food at present mainly has calcium carbonate, lactic acid
Calcium, calcium citrate and calcium gluconate etc., wherein most commonly used is still calcium carbonate, because of its calcium content height, in condensed food
Usage amount it is few, without side-effects, inexpensive.
Due to food source, eating habit and diet structure etc., China's different age people diet calcium intake is general
The nutrient recommendations intake in the daily diet recommended less than Chinese Soclety of Nutrition（RNIs or AIs）Standard, the middle-aged and the old lack
Calcium is especially serious.But much there are the health cares for the phenomenon that blood fat is high, blood glucose is high, high blood pressure, the crowd being suitble to eat by the middle-aged and the old
Product must low sugar, low in calories.
Invention content
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide a kind of person in middle and old age's sugar-free calcium tablet and its preparation side
Method.The calcium tablet has the advantages that low in calories, low temperature is anti-oxidant, sugar-free, easily absorbs.
To achieve the above object, the present invention adopts the following technical scheme that：
A kind of person in middle and old age's sugar-free calcium tablet, raw material composition are calculated as by weight, 1160 ~ 1220 parts of calcium carbonate, D-sorbite
345 ~ 365 parts, 25 parts of citric acid, 5 parts of purified water, 8.5 parts of edible alcohol, 635 ~ 647 parts of dextrin, 240 ~ 250 parts of maltodextrin,
3 ~ 4 parts of orange flavor, 0.5 ~ 1.0 part of Sucralose, 23 ~ 27 parts of magnesium stearate.
Person in middle and old age's sugar-free calcium tablet, raw material composition is preferably 1200 parts of calcium carbonate by weight, D-sorbite
357 parts, 25 parts of citric acid, 5 parts of purified water, 8.5 parts of edible alcohol, 643 parts of dextrin, 245.8 parts of maltodextrin, orange flavor
3.5 parts, 0.7 part of Sucralose, 25 parts of magnesium stearate.
A kind of preparation method of person in middle and old age's sugar-free calcium tablet as described above, includes the following steps：
（1）Dispensing：Raw material has been weighed respectively by formula rate；By load weighted calcium carbonate, dextrin, maltodextrin, trichlorine
After sucrose mixing 20min, mixture is made；
（2）Solution is prepared：By citric acid purifying water dissolution, add in edible alcohol and be deployed into citric acid solution；
（3）Mixing granulation：By step（1）Mixture obtained is placed in efficient wet granulator, adds in citric acid solution,
It is operated by efficient wet granulator S.O.P., the wet granular of 16 mesh is made；
（4）It is dry：HighefficientFluidbeddrier is first opened, then wet granular is slowly sent into HighefficientFluidbeddrier, temperature
At 65 DEG C, vapor tension control is down to less than 5% in 0.15MPa, drying to pellet moisture for control；
（5）Whole grain：Dried particle is sieved into whole grain with efficient pelletizing machine by 14 mesh；
（6）It is total mixed：Material after whole grain is added in two-dimensional motion mixer, adds in magnesium stearate, orange flavor, sorb
Sugar alcohol mixes 10min；
（7）Tabletting：Particle after mixing is placed in the hopper of rotary tablet machine and carries out tabletting, it is every in tableting processes
30min survey piece weights are primary, and control every is in 2.45 ~ 2.50g/ pieces.
The beneficial effects of the present invention are：
1）The present invention uses sorbierite and Sucralose as sweetener so that calcium tablet has the performances such as sugar-free, low heat value；It examines
Consider the easy moisture absorption of sorbierite, the present invention increases dextrin dosage, ensure that the drying of product；Not only it had been suitble to physical labourer but also had been suitble to
Brain worker is also suitable the special populations such as diabetic, the three high patients；It is a kind of inexpensive, high added value novel
Product；
2）The intake of invented food calcium is 470 ~ 475mg/d, and effect of supplemented calcium is apparent.
Specific embodiment
The present invention is further illustrated the present invention with the following example, but protection scope of the present invention is not limited to following reality
Apply example.
Embodiment 1
Person in middle and old age's sugar-free calcium tablet, raw material composition is calcium carbonate 1200g, D-sorbite 357g, citric acid 25g, purified water
5g, edible alcohol 8.5g, dextrin 643g, maltodextrin 245.8g, orange flavor 3.5g, Sucralose 0.7g, magnesium stearate
25g；
Preparation method, the specific steps are：
（1）Dispensing：Raw material has been weighed respectively by formula rate；By load weighted calcium carbonate, dextrin, maltodextrin, trichlorine
After sucrose mixing 20min, mixture is made；
（2）Solution is prepared：By citric acid purifying water dissolution, add in edible alcohol and be deployed into citric acid solution；
（3）Mixing granulation：By step（1）Mixture obtained is placed in efficient wet granulator, adds in citric acid solution,
It is operated by efficient wet granulator S.O.P., the wet granular of 16 mesh is made；
（4）It is dry：HighefficientFluidbeddrier is first opened, then wet granular is slowly sent into HighefficientFluidbeddrier, temperature
At 65 DEG C, vapor tension control is down to less than 5% in 0.15MPa, drying to pellet moisture for control；
（5）Whole grain：Dried particle is sieved into whole grain with efficient pelletizing machine by 14 mesh；
（6）It is total mixed：Material after whole grain is added in two-dimensional motion mixer, adds in magnesium stearate, orange flavor, sorb
Sugar alcohol mixes 10min；
（7）Tabletting：Particle after mixing is placed in the hopper of rotary tablet machine and carries out tabletting, it is every in tableting processes
30min surveys that piece weight is primary, and control every is made 1000 in 2.45 ~ 2.50g/ pieces；
The middle-aged and the old eats a piece of daily（2.50g/ piece）, the intake of calcium is 470 ~ 475mg/d, and effect of supplemented calcium is apparent.
Embodiment 2
Person in middle and old age's sugar-free calcium tablet, raw material composition is calcium carbonate 1181g, D-sorbite 365g, citric acid 25g, purified water
5g, edible alcohol 8.5g, dextrin 647g, maltodextrin 250g, orange flavor 4g, Sucralose 1.0g, magnesium stearate 27g；
Preparation method, the specific steps are：
（1）Dispensing：Raw material has been weighed respectively by formula rate；By load weighted calcium carbonate, dextrin, maltodextrin, trichlorine
After sucrose mixing 20min, mixture is made；
（2）Solution is prepared：By citric acid purifying water dissolution, add in edible alcohol and be deployed into citric acid solution；
（3）Mixing granulation：By step（1）Mixture obtained is placed in efficient wet granulator, adds in citric acid solution,
It is operated by efficient wet granulator S.O.P., the wet granular of 16 mesh is made；
（4）It is dry：HighefficientFluidbeddrier is first opened, then wet granular is slowly sent into HighefficientFluidbeddrier, temperature
At 65 DEG C, vapor tension control is down to less than 5% in 0.15MPa, drying to pellet moisture for control；
（5）Whole grain：Dried particle is sieved into whole grain with efficient pelletizing machine by 14 mesh；
（6）It is total mixed：Material after whole grain is added in two-dimensional motion mixer, adds in magnesium stearate, orange flavor, sorb
Sugar alcohol mixes 10min；
（7）Tabletting：Particle after mixing is placed in the hopper of rotary tablet machine and carries out tabletting, it is every in tableting processes
30min surveys that piece weight is primary, and control every is made 1000 in 2.45 ~ 2.50g/ pieces.
Embodiment 3
A kind of person in middle and old age's sugar-free calcium tablet, raw material composition are calculated as by weight, calcium carbonate 1220g, D-sorbite 345g, lemon
Lemon acid 25g, purified water 5g, edible alcohol 8.5g, dextrin 635g, maltodextrin 248.5g, orange flavor 3g, Sucralose
0.5g, magnesium stearate 23g；
Preparation method, the specific steps are：
（1）Dispensing：Raw material has been weighed respectively by formula rate；By load weighted calcium carbonate, dextrin, maltodextrin, trichlorine
After sucrose mixing 20min, mixture is made；
（2）Solution is prepared：By citric acid purifying water dissolution, add in edible alcohol and be deployed into citric acid solution；
（3）Mixing granulation：By step（1）Mixture obtained is placed in efficient wet granulator, adds in citric acid solution,
It is operated by efficient wet granulator S.O.P., the wet granular of 16 mesh is made；
（4）It is dry：HighefficientFluidbeddrier is first opened, then wet granular is slowly sent into HighefficientFluidbeddrier, temperature
At 65 DEG C, vapor tension control is down to less than 5% in 0.15MPa, drying to pellet moisture for control；
（5）Whole grain：Dried particle is sieved into whole grain with efficient pelletizing machine by 14 mesh；
（6）It is total mixed：Material after whole grain is added in two-dimensional motion mixer, adds in magnesium stearate, orange flavor, sorb
Sugar alcohol mixes 10min；
（7）Tabletting：Particle after mixing is placed in the hopper of rotary tablet machine and carries out tabletting, it is every in tableting processes
30min surveys that piece weight is primary, and control every is made 1000 in 2.45 ~ 2.50g/ pieces.
Conditional filtering is tested：
1）The screening experiment result of auxiliary material
The screening experiment result of 1 auxiliary material of table
2）The adjusting of sour-sweet sense
Citric acid amount can cover the astringent taste of calcium carbonate.In oxide spinel calcium dosage, auxiliary material（Sweetener, magnesium stearate）With
Measure it is constant in the case of, devise 3 different citric acid amounts, each tested number is carried out by 1000 (2.5g/ pieces) is made, to tablet
Mouthfeel examined or check, the results are shown in Table 2.The result shows that No. 2 experiment sour and sweet palatabilities, effect are preferable.
Influence of the dosage of 2 citric acid of table to mouthfeel
3）Three batches of scale up test verify data
This product process stabilizing is reliable, enlarged experiment is carried out according to the production technology of trial test, to the production technology drafted
Carry out process certification and bias correction.Amplify 12 times with this technique by formula ratio, pass through 3 batch scale up test, theoretical yield, reality
As a result the scale up test technical data such as border must measure, yield rate prove that Product Process is stablized.Concrete condition see the table below 3.
3 three batches of scale up test verification data of table
* purified water and edible alcohol dosage are added according to 12 times of amplifications
4）Efficacy assessments
The adult's invented food Nutrition intake situation table of table 4
The foregoing is merely presently preferred embodiments of the present invention, all equivalent changes done according to scope of the present invention patent with
Modification should all belong to the covering scope of the present invention.
Claims (1)
1. a kind of person in middle and old age's sugar-free calcium tablet, it is characterised in that：Its raw material composition is calcium carbonate 1200g, D-sorbite 357g, lemon
Lemon acid 25g, purified water 5g, edible alcohol 8.5g, dextrin 643g, maltodextrin 245.8g, orange flavor 3.5g, Sucralose
0.7g, magnesium stearate 25g；
Preparation method, the specific steps are：
（1）Dispensing：Raw material has been weighed respectively by formula rate；By load weighted calcium carbonate, dextrin, maltodextrin, Sucralose
After mixing 20min, mixture is made；
（2）Solution is prepared：By citric acid purifying water dissolution, add in edible alcohol and be deployed into citric acid solution；
（3）Mixing granulation：By step（1）Mixture obtained is placed in efficient wet granulator, citric acid solution is added in, by height
The operation of wet granulator S.O.P. is imitated, the wet granular of 16 mesh is made；
（4）It is dry：HighefficientFluidbeddrier is first opened, then wet granular is slowly sent into HighefficientFluidbeddrier, temperature control
At 65 DEG C, vapor tension control is down to less than 5% in 0.15MPa, drying to pellet moisture；
（5）Whole grain：Dried particle is sieved into whole grain with efficient pelletizing machine by 14 mesh；
（6）It is total mixed：Material after whole grain is added in two-dimensional motion mixer, adds in magnesium stearate, orange flavor, sorbose
Alcohol mixes 10min；
（7）Tabletting：Particle after mixing is placed in the hopper of rotary tablet machine and carries out tabletting, per 30min in tableting processes
Survey that piece weight is primary, and control every is made 1000 in 2.45 ~ 2.50g/ pieces.
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| CN201510589790.6A CN105106154B (en) | 2015-09-17 | 2015-09-17 | A kind of person in middle and old age's sugar-free calcium tablet and preparation method thereof |
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| CN105106154B true CN105106154B (en) | 2018-06-29 |
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| CN106265725B (en) * | 2015-05-14 | 2021-02-09 | 北京科信必成医药科技发展有限公司 | Calcium carbonate taste-masking granules and preparation method thereof |
| CN106619750A (en) * | 2017-02-17 | 2017-05-10 | 王左良 | Ginkgol biloba osteocalcin hard capsules and preparation method thereof |
| CN108721236A (en) * | 2018-06-12 | 2018-11-02 | 贡享本草（永泰）生物科技有限公司 | A kind of roxburgh anoectochilus terminal bud chewable tablets and preparation method thereof |
| CN109846901A (en) * | 2019-04-03 | 2019-06-07 | 江西安顺堂生物科技有限公司 | It is a kind of to promote bone growth, anti-caries, the preparation and preparation process for supplementing calcium |
| CN110122880A (en) * | 2019-06-19 | 2019-08-16 | 安徽康博特保健食品有限公司 | A kind of calcium and magnesium piece health food and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1199611A (en) * | 1997-05-15 | 1998-11-25 | 北京路德有限责任公司 | Calcium replenishing chewing tablet |
| CN1565233A (en) * | 2003-06-18 | 2005-01-19 | 上海同利实业有限公司 | Sugar-free candy compositions for replenishing the calcium and its preparation process |
| CN103845357A (en) * | 2013-12-09 | 2014-06-11 | 浙江佐力药业股份有限公司 | Vitamin D calcium chewable tablet for calcium supplementation of children and preparation method thereof |
| CN104738609A (en) * | 2013-12-28 | 2015-07-01 | 大连美乐生物技术开发有限公司 | Calcium tablet and preparation method thereof |
-
2015
- 2015-09-17 CN CN201510589790.6A patent/CN105106154B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1199611A (en) * | 1997-05-15 | 1998-11-25 | 北京路德有限责任公司 | Calcium replenishing chewing tablet |
| CN1565233A (en) * | 2003-06-18 | 2005-01-19 | 上海同利实业有限公司 | Sugar-free candy compositions for replenishing the calcium and its preparation process |
| CN103845357A (en) * | 2013-12-09 | 2014-06-11 | 浙江佐力药业股份有限公司 | Vitamin D calcium chewable tablet for calcium supplementation of children and preparation method thereof |
| CN104738609A (en) * | 2013-12-28 | 2015-07-01 | 大连美乐生物技术开发有限公司 | Calcium tablet and preparation method thereof |
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