CN105086559A - Mold-proof preparation special for oil paint and preparation method thereof - Google Patents
Mold-proof preparation special for oil paint and preparation method thereof Download PDFInfo
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- CN105086559A CN105086559A CN201510475860.5A CN201510475860A CN105086559A CN 105086559 A CN105086559 A CN 105086559A CN 201510475860 A CN201510475860 A CN 201510475860A CN 105086559 A CN105086559 A CN 105086559A
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Abstract
The invention discloses a mold-proof preparation special for oil paint and relates to the technical field of chemical engineering manufacturing. The mold-proof preparation comprises 60-80 parts of water, 8-10 parts of sodium glutamate, 6-8 parts of ammonium propionate, 6-8 parts of polymeric guanidine, 3-5 parts of chlorhexidine, 7-10 parts of acrylic ester, 1-3 parts of ethylene glycol, 5-8 parts of hypochlorous acid, 6-8 parts of a green tea extract, 3-5 parts of mint leach liquor, 5-7 parts of pepper leach liquor, 6-8 parts of fresh ginger leach liquor and 6-10 parts of garlic leach liquor. The mold-proof preparation has the advantages that the technological process is simple, the raw material ratio is reasonable, the multi-component compound type mold removal mold-proof agent is obtained and can kill all common molds, kill spore activity and restrain mold regeneration, and can be used as the mold removal mold-proof agent for indoor and outdoor building walls, metal or wooden structures and furniture, the molds are completely killed on the basis that the original wall or other decoration structures are not damaged, the inherent color of the structure is recovered, and the mold-proof preparation is environmentally friendly, free of toxicity, efficient, high in market value and convenient to use and popularize.
Description
Technical field
The present invention relates to chemistry painting industry preparing technical field, be specifically related to a kind of paint special mildewproof preparation and preparation method thereof.
Background technology
After coating goes mouldy; viscosity and loss of adhesion can be caused; the mildew of coating surface not only makes coating lose protection and decoration functions; mould is scattered in the environment; also to environment; usual interpolation Coating Antifungal Agents prepares mould-repellant coating, from the effective ways that mould corrodes, prepares mould-repellant coating can be widely applied to as higher singularity industries of hygienic requirements such as food, Gourmet Powder Factory, slaughterhouse, food processing plant, pharmacy, beverage, wine brewing with Coating Antifungal Agents.
Coating Antifungal Agents refers to a kind of preparation adding in coating and prepare mould-repellant coating.Have efficient, wide spectrum, anti-algae, stable, the feature of environmental protection, traditional mould inhibitor quality is also bad, and major cause is that material choice is unreasonable, and preparation method's tradition, the mould inhibitor anti-mold effect of preparation is also relatively poor.
Summary of the invention:
Technical problem to be solved by this invention is to provide a kind of formula rationally, and production technique is simple, and material choice is reasonable, paint special mildewproof preparation that anti-mold effect is good and preparation method thereof.
Technical problem to be solved by this invention realizes by the following technical solutions:
A kind of paint special mildewproof preparation, is characterized in that: be made up of following raw material:
Water 60-80 part, Sodium Glutamate 8-10 part, propionic acid ammonium 6-8 part, polymeric guanidine 6-8 part, chlorhexidine 3-5 part, acrylate 7-10 part, ethylene glycol 1-3 part, hypochlorous acid 5-8 part, green tea extractive liquor 6-8 part, peppermint vat liquor 3-5 part, pepper vat liquor 5-7 part, ginger vat liquor 6-8 part, garlic extraneous liquid 6-10 part.
The preferred component of each raw material is: 65 parts, water, Sodium Glutamate 9 parts, propionic acid ammonium 7 parts, polymeric guanidine 7 parts, chlorhexidine 4 parts, acrylate 8 parts, ethylene glycol 2 parts, hypochlorous acid 6 parts, green tea extractive liquor 7 parts, peppermint vat liquor 4 parts, pepper vat liquor 6 parts, ginger vat liquor 7 parts, garlic extraneous liquid 8 parts.
Polymeric guanidine in described component, adopts following steps to be prepared:
A, polymerization: methyl acrylate and N-Methyl pyrrolidone are with volume ratio 1:(1-3) join in reaction unit, temperature controls at 80-85 DEG C, reaction times 35-45 minute;
B, ester amine exchange: adding under protection of inert gas atmosphere with methyl acrylate mol ratio is 1:(3-5) Guanidinium carbonate; and add propionic acid 4-6 kilogram during every batch reaction; temperature of reaction remains on 80-85 DEG C; when temperature starts to decline; proved response completes; continue to be cooled to temperature to be 40-45 DEG C and can to filter, be drying to obtain.
Another object of the present invention is to provide a kind of method that the present invention of preparation paints special mildewproof preparation, it is characterized in that comprising the following steps:
(1) Sodium Glutamate, propionic acid ammonium, polymeric guanidine are added to the water, are warming up to 60 ~ 80 DEG C, are uniformly mixed;
(2) chlorhexidine, acrylate, ethylene glycol and hypochlorous acid are carried out pre-mixing, be uniformly mixed;
(3) product of step (1) is added in the product of step (2), be uniformly mixed, react 1 ~ 3 hour;
(4) be cooled to room temperature, add green tea extractive liquor, peppermint vat liquor, pepper vat liquor, ginger vat liquor, garlic extraneous liquid, after being uniformly mixed finished product.
The invention has the beneficial effects as follows: present invention process flow process is succinct, reasonable raw material proportioning, the present invention is the compound mildew-eliminating and mildew-preventing agent of a kind of many components, all common moulds can be killed, kill the regeneration of spore active also mould fungus inhibition, can be used for the mildew-eliminating and mildew-preventing agent of indoor and outdoor construction wall, metal or wooden structures and furniture, on the basis not destroying original body of wall or other decorating structures, thoroughly kill mould, recover structure inherent colour, environment-protecting asepsis, efficient, marketable value is high, is convenient to promote and use.
Embodiment
The technique means realized to make the present invention, creation characteristic, reaching object and effect is easy to understand, below in conjunction with specific embodiment, setting forth the present invention further.
Embodiment 1
Take water 60g, Sodium Glutamate 8g, propionic acid ammonium 6g, polymeric guanidine 6g, chlorhexidine 3g, acrylate 7g, ethylene glycol 1g, hypochlorous acid 5g, green tea extractive liquor 6g, peppermint vat liquor 3g, pepper vat liquor 5g, ginger vat liquor 6g, garlic extraneous liquid 6g.
Polymeric guanidine in described component, adopts following steps to be prepared:
A, polymerization: methyl acrylate and N-Methyl pyrrolidone are with volume ratio 1:(1-3) join in reaction unit, temperature controls at 80-85 DEG C, reaction times 35-45 minute;
B, ester amine exchange: adding under protection of inert gas atmosphere with methyl acrylate mol ratio is 1:(3-5) Guanidinium carbonate; and add propionic acid 4-6 kilogram during every batch reaction; temperature of reaction remains on 80-85 DEG C; when temperature starts to decline; proved response completes; continue to be cooled to temperature to be 40-45 DEG C and can to filter, be drying to obtain.
Preparation method is as follows:
(1) Sodium Glutamate, propionic acid ammonium, polymeric guanidine are added to the water, are warming up to 60 ~ 80 DEG C, are uniformly mixed;
(2) chlorhexidine, acrylate, ethylene glycol and hypochlorous acid are carried out pre-mixing, be uniformly mixed;
(3) product of step (1) is added in the product of step (2), be uniformly mixed, react 1 ~ 3 hour;
(4) be cooled to room temperature, add green tea extractive liquor, peppermint vat liquor, pepper vat liquor, ginger vat liquor, garlic extraneous liquid, after being uniformly mixed finished product.
Embodiment 2
Take water 65kg, Sodium Glutamate 9kg, propionic acid ammonium 7kg, polymeric guanidine 7kg, chlorhexidine 4kg, acrylate 8kg, ethylene glycol 2kg, hypochlorous acid 6kg, green tea extractive liquor 7kg, peppermint vat liquor 4kg, pepper vat liquor 6kg, ginger vat liquor 7kg, garlic extraneous liquid 8kg.
Polymeric guanidine in described component, adopts following steps to be prepared:
A, polymerization: methyl acrylate and N-Methyl pyrrolidone are with volume ratio 1:(1-3) join in reaction unit, temperature controls at 80-85 DEG C, reaction times 35-45 minute;
B, ester amine exchange: adding under protection of inert gas atmosphere with methyl acrylate mol ratio is 1:(3-5) Guanidinium carbonate; and add propionic acid 4-6 kilogram during every batch reaction; temperature of reaction remains on 80-85 DEG C; when temperature starts to decline; proved response completes; continue to be cooled to temperature to be 40-45 DEG C and can to filter, be drying to obtain.
Preparation method is as follows:
(1) Sodium Glutamate, propionic acid ammonium, polymeric guanidine are added to the water, are warming up to 60 ~ 80 DEG C, are uniformly mixed;
(2) chlorhexidine, acrylate, ethylene glycol and hypochlorous acid are carried out pre-mixing, be uniformly mixed;
(3) product of step (1) is added in the product of step (2), be uniformly mixed, react 1 ~ 3 hour;
(4) be cooled to room temperature, add green tea extractive liquor, peppermint vat liquor, pepper vat liquor, ginger vat liquor, garlic extraneous liquid, after being uniformly mixed finished product.
More than show and describe ultimate principle of the present invention and principal character and advantage of the present invention.The technician of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and specification sheets just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (4)
1. paint a special mildewproof preparation, it is characterized in that: be made up of following raw material:
Water 60-80 part, Sodium Glutamate 8-10 part, propionic acid ammonium 6-8 part, polymeric guanidine 6-8 part, chlorhexidine 3-5 part, acrylate 7-10 part, ethylene glycol 1-3 part, hypochlorous acid 5-8 part, green tea extractive liquor 6-8 part, peppermint vat liquor 3-5 part, pepper vat liquor 5-7 part, ginger vat liquor 6-8 part, garlic extraneous liquid 6-10 part.
2. one paint special mildewproof preparation according to claim 1, it is characterized in that, the preferred component of each raw material is: 65 parts, water, Sodium Glutamate 9 parts, propionic acid ammonium 7 parts, polymeric guanidine 7 parts, chlorhexidine 4 parts, acrylate 8 parts, ethylene glycol 2 parts, hypochlorous acid 6 parts, green tea extractive liquor 7 parts, peppermint vat liquor 4 parts, pepper vat liquor 6 parts, ginger vat liquor 7 parts, garlic extraneous liquid 8 parts.
3. one paint special mildewproof preparation according to claim 1, is characterized in that: the polymeric guanidine in described component, adopts following steps to be prepared:
A, polymerization: methyl acrylate and N-Methyl pyrrolidone are with volume ratio 1:(1-3) join in reaction unit, temperature controls at 80-85 DEG C, reaction times 35-45 minute;
B, ester amine exchange: adding under protection of inert gas atmosphere with methyl acrylate mol ratio is 1:(3-5) Guanidinium carbonate; and add propionic acid 4-6 kilogram during every batch reaction; temperature of reaction remains on 80-85 DEG C; when temperature starts to decline; proved response completes; continue to be cooled to temperature to be 40-45 DEG C and can to filter, be drying to obtain.
4. prepare a kind of method of painting special mildewproof preparation in claim 1 or 2, it is characterized in that, comprise the following steps:
(1) Sodium Glutamate, propionic acid ammonium, polymeric guanidine are added to the water, are warming up to 60 ~ 80 DEG C, are uniformly mixed;
(2) chlorhexidine, acrylate, ethylene glycol and hypochlorous acid are carried out pre-mixing, be uniformly mixed;
(3) product of step (1) is added in the product of step (2), be uniformly mixed, react 1 ~ 3 hour;
(4) be cooled to room temperature, add green tea extractive liquor, peppermint vat liquor, pepper vat liquor, ginger vat liquor, garlic extraneous liquid, after being uniformly mixed finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510475860.5A CN105086559A (en) | 2015-08-05 | 2015-08-05 | Mold-proof preparation special for oil paint and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510475860.5A CN105086559A (en) | 2015-08-05 | 2015-08-05 | Mold-proof preparation special for oil paint and preparation method thereof |
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| CN105086559A true CN105086559A (en) | 2015-11-25 |
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| CN201510475860.5A Pending CN105086559A (en) | 2015-08-05 | 2015-08-05 | Mold-proof preparation special for oil paint and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3083428A1 (en) * | 2018-07-05 | 2020-01-10 | Centre Scientifique Et Technique Du Batiment (Cstb) | COATING COMPOSITIONS WITH FUNGISTATIC AND / OR FUNGICIDAL PROPERTIES |
| CN113265212A (en) * | 2021-05-28 | 2021-08-17 | 陕西省石油化工研究设计院 | Anti-corrosion and anti-mildew agent for cigarette glue and preparation method and application thereof |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102657281A (en) * | 2012-04-12 | 2012-09-12 | 广汉隆达饲料有限公司 | Dispersion type liquid mildew inhibitor and preparation method thereof |
-
2015
- 2015-08-05 CN CN201510475860.5A patent/CN105086559A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102657281A (en) * | 2012-04-12 | 2012-09-12 | 广汉隆达饲料有限公司 | Dispersion type liquid mildew inhibitor and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3083428A1 (en) * | 2018-07-05 | 2020-01-10 | Centre Scientifique Et Technique Du Batiment (Cstb) | COATING COMPOSITIONS WITH FUNGISTATIC AND / OR FUNGICIDAL PROPERTIES |
| CN113265212A (en) * | 2021-05-28 | 2021-08-17 | 陕西省石油化工研究设计院 | Anti-corrosion and anti-mildew agent for cigarette glue and preparation method and application thereof |
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Application publication date: 20151125 |
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