CN105067740B - 一种仿生催化环己酮气液相氧化制备ε‑己内酯的产物分析方法 - Google Patents
一种仿生催化环己酮气液相氧化制备ε‑己内酯的产物分析方法 Download PDFInfo
- Publication number
- CN105067740B CN105067740B CN201510455899.0A CN201510455899A CN105067740B CN 105067740 B CN105067740 B CN 105067740B CN 201510455899 A CN201510455899 A CN 201510455899A CN 105067740 B CN105067740 B CN 105067740B
- Authority
- CN
- China
- Prior art keywords
- caprolactone
- cyclohexanone
- gas
- liquid phase
- phase oxidation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (1)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510455899.0A CN105067740B (zh) | 2015-07-29 | 2015-07-29 | 一种仿生催化环己酮气液相氧化制备ε‑己内酯的产物分析方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510455899.0A CN105067740B (zh) | 2015-07-29 | 2015-07-29 | 一种仿生催化环己酮气液相氧化制备ε‑己内酯的产物分析方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN105067740A CN105067740A (zh) | 2015-11-18 |
CN105067740B true CN105067740B (zh) | 2017-03-15 |
Family
ID=54497161
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201510455899.0A Active CN105067740B (zh) | 2015-07-29 | 2015-07-29 | 一种仿生催化环己酮气液相氧化制备ε‑己内酯的产物分析方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN105067740B (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109991352A (zh) * | 2019-04-09 | 2019-07-09 | 上海实朴检测技术服务有限公司 | 测定土壤中己二酸的方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10055653A1 (de) * | 2000-11-10 | 2002-05-16 | Basf Ag | Verfahren zur Oxidation von Ketonen und Aldehyden mit Wasserstoffperoxid über eine Baeyer-Villiger-Oxidation |
CN1994930A (zh) * | 2006-12-27 | 2007-07-11 | 沈阳工业大学 | 处理仿生催化氧化环己烷制环己酮过程中洗涤酸水的方法 |
CN103450144A (zh) * | 2013-09-12 | 2013-12-18 | 中山大学 | 一种仿生催化环己酮氧化制备ε-己内酯的方法 |
GB2512836A (en) * | 2013-04-08 | 2014-10-15 | Givaudan Sa | Novel process |
CN104557847A (zh) * | 2015-01-09 | 2015-04-29 | 武汉理工大学 | 一种用阳离子催化法解聚聚已内酯的生产方法 |
-
2015
- 2015-07-29 CN CN201510455899.0A patent/CN105067740B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE10055653A1 (de) * | 2000-11-10 | 2002-05-16 | Basf Ag | Verfahren zur Oxidation von Ketonen und Aldehyden mit Wasserstoffperoxid über eine Baeyer-Villiger-Oxidation |
CN1994930A (zh) * | 2006-12-27 | 2007-07-11 | 沈阳工业大学 | 处理仿生催化氧化环己烷制环己酮过程中洗涤酸水的方法 |
GB2512836A (en) * | 2013-04-08 | 2014-10-15 | Givaudan Sa | Novel process |
CN103450144A (zh) * | 2013-09-12 | 2013-12-18 | 中山大学 | 一种仿生催化环己酮氧化制备ε-己内酯的方法 |
CN104557847A (zh) * | 2015-01-09 | 2015-04-29 | 武汉理工大学 | 一种用阳离子催化法解聚聚已内酯的生产方法 |
Non-Patent Citations (3)
Title |
---|
Remarkable differences between benzaldehyde and isobutyraldehyde as coreductant in the performance toward the iron(III) porphyrins-catalyzed aerobic BaeyereVilliger oxidation of cyclohexanone, kinetic and mechanistic features;Hong-Yun Lan et al.;《Tetrahedron》;20131231;第69卷;4241-4246页 * |
环己烷氧化产物的气相色谱一质谱分析;陆慧宁 等;《质谱学报》;20041031;第25卷;73-74页 * |
环己酮氧化合成ε-己内酯的催化研究;南爱斌;《中国优秀硕士学位论文全文数据库 工程科技I辑》;20130715(第7期);B016-20 * |
Also Published As
Publication number | Publication date |
---|---|
CN105067740A (zh) | 2015-11-18 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Grabner et al. | A chemo-enzymatic tandem reaction in a mixture of deep eutectic solvent and water in continuous flow | |
Vanoye et al. | Reinvestigation of the organocatalyzed aerobic oxidation of aldehydes to acids | |
Pieber et al. | Selective olefin reduction in thebaine using hydrazine hydrate and O2 under intensified continuous flow conditions | |
CN105067740B (zh) | 一种仿生催化环己酮气液相氧化制备ε‑己内酯的产物分析方法 | |
Li et al. | Two-stage flow synthesis of coumarin via O-acetylation of salicylaldehyde | |
CN111056934B (zh) | 一种微反应器内制备α-羟基酮光引发剂的方法 | |
CN108707126B (zh) | 采用微通道反应装置合成甲基丙烯酸缩水甘油酯的方法 | |
CN103214446B (zh) | 一种色满酮衍生物的不对称合成方法 | |
WO2011086135A1 (en) | Acylations in micro reaction systems | |
Yan et al. | Tetramethylammonium neodecanoate as a recyclable catalyst for acidolysis reaction of epichlorohydrin with neodecanoic acid | |
Matsumoto et al. | One-Pot Sequential 1, 4-and 1, 2-Reductions of α, β-Unsaturated δ-Lactones to the Corresponding δ-Lactols with CuCl and NaBH4 in Methanol | |
CN102794198A (zh) | 用于乙醇羰基化合成丙酸的催化剂的制备方法及其应用 | |
CN106591387A (zh) | 一种基于微通道反应器一步酶催化合成哌啶甲酸的方法 | |
Yan et al. | Highly efficient two‐stage ring‐opening of epichlorohydrin with carboxylic acid in a microreaction system | |
He et al. | Heteropoly acid-catalyzed three-component aza-Diels–Alder reaction in a continuous micro-flow system | |
McCaw et al. | Delivering enhanced efficiency in the synthesis of α-diazosulfoxides by exploiting the process control enabled in Flow | |
CN105566278A (zh) | 一种利用微反应装置连续制备ε-己内酯的方法 | |
TWI448458B (zh) | 環氧丙烷的製程 | |
CN112876330B (zh) | 一种利用微通道反应装置连续制备联苄的方法 | |
Ding et al. | Highly Efficient Oxidation of Toluene to Benzoic Acid Catalyzed by N-Hydroxyphthalimide and Oxime in PEG-1000-based dicationic ionic liquid | |
CN113248461A (zh) | 一种羟基氧杂环烷烃衍生物的制备方法 | |
CN109988143A (zh) | 一种通过生物质多元醇制备功能化手性环状碳酸酯的方法 | |
CN114907201B (zh) | 一种合成2-甲萘醌的绿色合成方法 | |
EP4041712B1 (en) | A continuous flow synthesis method for the manufacture of isoniazid | |
Piringer et al. | Enantioselective Syntheses of 3, 4‐Dihydropyrans Employing Isochalcogenourea‐Catalyzed Formal (4+ 2)‐Cycloadditions of Allenoates |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right |
Effective date of registration: 20210112 Address after: 255035 no.3482 Baoshan Road, high tech Zone, Zibo City, Shandong Province Patentee after: ZIBO ZHENGDA POLYURETHANE Co.,Ltd. Address before: 516081 room 205, building a, R & D building, No.5, Keji Road, science and Technology Innovation Park, Dayawan West District, Huizhou City, Guangdong Province Patentee before: HUIZHOU RESEARCH INSTITUTE, SUN YAT-SEN University |
|
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20230407 Address after: 256400 Maqiao Industrial Park, Huantai County, Zibo City, Shandong Province Patentee after: Shandong Shangzheng New Material Technology Co.,Ltd. Address before: 255035 no.3482 Baoshan Road, high tech Zone, Zibo City, Shandong Province Patentee before: ZIBO ZHENGDA POLYURETHANE Co.,Ltd. |
|
TR01 | Transfer of patent right |