CN105067546A - High-temperature multispectral coupling optical-mechanical system - Google Patents
High-temperature multispectral coupling optical-mechanical system Download PDFInfo
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- CN105067546A CN105067546A CN201510516720.8A CN201510516720A CN105067546A CN 105067546 A CN105067546 A CN 105067546A CN 201510516720 A CN201510516720 A CN 201510516720A CN 105067546 A CN105067546 A CN 105067546A
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Abstract
The invention provides a high-temperature multispectral coupling optical-mechanical system. Simultaneous ultraviolet spectrum and lasers work is achieved in one measuring cell, and the prominent problems that an existing instrument is poor in measuring accuracy, simple in measuring component, low in sensitivity, high in lower detecting limit and the like are solved. The system comprises a gas pool assembly, an ultraviolet light emitting assembly, an ultraviolet light receiving assembly, a laser emitting assembly, a laser receiving assembly and a heating assembly, and the laser emitting assembly and the laser receiving assembly are located on the same side of the measuring cell and located at the upper end and the lower end of a gas pool respectively. The ultraviolet light emitting assembly and the ultraviolet light receiving assembly are mounted on the left side and the right side of the measuring cell respectively, and correspond to the center of the gas pool. A left/right reflector is provided with three through holes, namely, a large hole in the middle and small holes in the two sides, the large hole in the middle corresponds to the ultraviolet light emitting assembly or the ultraviolet light receiving assembly, and the small holes in the two sides correspond to the laser emitting assembly and the laser receiving assembly. A corresponding large hole is formed in the middle of the right/left reflector.
Description
Technical field
The invention belongs to flue gas analysis field, relate to the multispectral coupling optical-mechanical system of a kind of high temperature, measure achieve ultraviolet spectrum (200nm-400nm), laser (1000nm-10000nm) in same measuring cell while.
Background technology
Flue gas discharge continuous monitoring system (CEMS, ContinuousEmissionMonitoringSystem) refers to the important watch-dog of conduction factory desulphurization and denitration system operation with closed ring, is again the important monitoring equipment of fume emission simultaneously.Along with the continuous propelling of China's energy-saving and emission-reduction work, SO in gaseous contaminant
2, NO
x, NH
3deng concentration of emission more and more lower, originally single infrared absorption spectroscopies and single ultraviolet difference absorption spectroscopy techniques be both difficult to adapt to current hot and humid, low emission operating mode, can not realize again to while various ingredients measure.
Summary of the invention
The technical matters that the present invention solves is to provide the multispectral coupling optical-mechanical system of a kind of high temperature, and this system architecture is simply compact, installation adjustment operation is convenient, can achieve ultraviolet spectrum, laser works simultaneously.
The multispectral coupling optical-mechanical system of a kind of high temperature: comprise gas pond assembly, ultraviolet light emission and receiving unit, Laser emission and receiving unit and heating component, described gas pond assembly comprises measuring cell, adjusting part and left and right catoptron, Laser emission and receiving unit are all installed on measuring cell homonymy, and are located at the upper/lower terminal in gas pond respectively; Described ultraviolet light emission and receiving unit are installed on measuring cell arranged on left and right sides respectively, and the centre position in ultraviolet light emission gas pond corresponding to receiving unit; Left/right catoptron has three through holes, be respectively middle macropore and the aperture of both sides, the corresponding ultraviolet light emission of middle macropore or receiving unit, both sides aperture is corresponding Laser emission and receiving unit respectively; Also corresponding macropore is had in the middle of right/left catoptron.
Further design of the present invention is:
Adjustable component comprises trim ring and adjustment seat, and catoptron is pressed in adjustment seat by trim ring, and adjustment seat is arranged on measuring cell end by adjustment screw, and adjustment seat outside surface is designed to sphere.
Measuring cell cavity inner wall is mirror finish inwall.
Described measuring cell inner wall surface is provided with corrosion-inhibiting coating.
Described measuring cell adopts thermostable fluorine rubber seal rings for seal.
Ultraviolet emission assembly comprises light source and collimation group, and light source comprises deuterium lamp, deuterium lamp holder; Collimation group comprises collimation lens, mirror pipe and adjustable optic fibre coupling seat, for the ultraviolet divergence optical alignment of Optical Fiber Transmission is become directional light; Ultraviolet receiving unit comprises collector lens, mirror pipe and adjustable optic fibre coupling seat.
Laser emission assembly comprises lens combination, micrometer adjusting screw, fixed mount and fine motion frame; Laser pick-off assembly comprises collector lens, mirror pipe and photodetector.
It is peripheral that described well heater is coated on gas pond, comprises heating plate, foamed heat insulating thermofin and crust from inside to outside successively.
the present invention has following effect compared to existing technology:
The invention provides the multispectral coupling optical-mechanical system of a kind of high temperature, this system works achieve ultraviolet spectrum (200nm-400nm), laser (1000nm-10000nm) in same measuring cell while, a system can detect Multicomponent simultaneously, both be applicable to current hot and humid, low emission operating mode, realized again Measurement and analysis while various ingredients.
The invention solves the outstanding problems such as existing tester measuring accuracy is poor, measurement component is simple, sensitivity is low, Monitoring lower-cut is high; Achieve different spectral technique information fusion, the gordian technique approach such as multi-wavelength polycomponent detects simultaneously, the highly sensitive monitoring of long light path.
Ultraviolet light unit and laser cell are designed in a system in present system, one is positioned at centre position, two ends, a position, design ingenious, neither affect the launching and receiving of ultraviolet spectrum, infrared laser multiple reflections back and forth between two catoptrons can be ensured again, be independent of each other.
Two kinds of unit combine in a system, and whole system is operated in 200 ° of C conditions of high temperature, should ensure its thermal stability, again integral sealing, and technical a lot of difficult point needs to solve.As: measuring cell cavity inner wall mirror finish and surface anticorrosion coating processing technique; Thermostable fluorine rubber seal and heat insulation treatment technology.
Accompanying drawing explanation
Fig. 1 is the structural representation of invention the present invention multispectral coupling ray machine System Implementation;
Fig. 2 is the structural representation of ultraviolet source assembly of the present invention;
Fig. 3 is the structural representation of Infrared laser emission assembly of the present invention;
Fig. 4 is the structural representation of right reflection mirror adjustment group of the present invention;
Fig. 5 is heater assembly structural representation of the present invention.
In figure: 101-Laser emission assembly, 102-laser pick-off assembly, 103-ultraviolet light emission assembly, 104-measuring cell, 105-catoptron group, 106-ultraviolet light receiving unit;
The coupling of 201-deuterium lamp holder, 202-ultraviolet spectrum ray machine, 203-optical fiber coupling head;
301-micrometer adjusting screw, 302-fixed mount, 303-fine motion frame, 304-lens combination;
401-trim ring, 402-right reflection mirror, 403-adjustment seat;
501-heating plate, 502-foamed heat insulating thermofin, 503-crust, 504-hydraucone.
Embodiment
Below in conjunction with accompanying drawing, the invention will be further described:
embodiment one:
The multispectral coupling optical-mechanical system of flue gas analysis of the present invention comprises gas pond assembly, ultraviolet light emission and receiving unit, Laser emission and receiving unit, heating component.
As shown in Figure 1, Laser emission and receiving unit comprise Laser emission assembly 101 and laser pick-off assembly 102; Ultraviolet light emission and receiving unit comprise ultraviolet light emission assembly 103, ultraviolet light receiving unit 106; Gas pond assembly comprises measuring cell 104, catoptron group 105(comprises catoptron and adjustable component) etc.Laser emission assembly and receiving unit are all installed on the left of measuring cell, and are located at the upper/lower terminal in gas pond respectively; Ultraviolet light emission and receiving unit are installed on measuring cell arranged on left and right sides respectively, and the centre position in ultraviolet light emission gas pond corresponding to receiving unit, the i.e. center-aisle in corresponding gas pond; Left reflection minor has three through holes, be respectively middle macropore and the aperture of both sides, the corresponding ultraviolet light emission of middle macropore or receiving unit, both sides aperture is corresponding Laser emission and receiving unit respectively; Also have macropore in the middle of right reflection mirror corresponding with macropore in the middle of left reflection minor, form ultraviolet light emission and receiving path.
As shown in Figure 2, ultraviolet light emission assembly 103 comprises light source and collimation group; Light source comprises deuterium lamp holder 201, ultraviolet spectrum coupling ray machine 202, spectrum coupling head 203.Taper light beam launched by deuterium lamp, and the Shang You state of deuterium lamp holder determines the screw hole of deuterium lamp flange, can realize, to the accurate real location of deuterium lamp, ensureing that deuterium lamp is operated in optimum condition by thermal Equilibrium Design simultaneously.Ultraviolet spectrum coupling ray machine is made up of coupled lens group, mirror pipe, adjustable optic fibre seat.Lens combination is by JGS1 and CAF
2ultraviolet light maximizes and is coupled in incident optical by bi-material optimal design.Ultraviolet light emission and receiving unit adopt symmetrical expression design, are made up of lens, mirror pipe, adjustable optic fibre seat.
As shown in Figure 3, Laser emission assembly is made up of micrometer adjusting screw 301, fixed mount 302, fine motion frame 303, lens combination 304, and lens material can select different infrared glasses according to the wavelength difference of laser instrument.
Gas pond assembly comprises measuring cell, draft tube/escape pipe, left and right (sphere) catoptron, adjustable component, and draft tube/escape pipe is designed to stainless-steel tube by screw thread fixation measuring pond.Left and right spherical reflector is arranged in measuring cell respectively by adjustable component, as shown in Figure 4, adjustable component comprises trim ring 401 and adjustment seat 403, and install as right reflection mirror 402 and be pressed in adjustment seat 403 through trim ring 401, adjustment seat is arranged on measuring cell end by adjustment screw.Adjustment seat one side is designed to sphere, by adjustment screw, can realize harmonizing to the three-dimensional of catoptron.
As shown in Figure 5, well heater comprises heating plate 501 from inside to outside successively, foamed heat insulating thermofin 502, crust 503 form, and the bottom of well heater is also provided with hydraucone 504 for lead-in wire.This well heater is coated on the periphery of measuring cell 104, the preferred 1mm of thickness of heating plate, the preferred 10mm of foamed board thickness, the preferred 0.8mm of skin thickness.Both homogeneous heating, profile were little, safe and reliable to ensure well heater by power density optimal design and special forming technique.
Laser emission and receiving unit, absorbed the long light path of laser to realize flue gas for more than 30 time by the whole laser roundtrip between two catoptrons that realizes of three-dimensional fine-tuning, and analyzed shoot laser by the detector of reception group.
embodiment two:
In this example, measuring cell material selection has good formed machining performance, corrosion stability and excellent weldability, medium tenacity aluminium alloy 5052, by smooth after grinding after inner wall surface finishing, inner wall surface does preservative treatment simultaneously, is beneficial to measurement gas flowing and reduces adsorption.For ensureing its thermal stability, again integral sealing, measuring cell adopts thermostable fluorine rubber seal rings for seal.In this example, all right set temperature sensor in group side, gas pond, temperature sensor is close to measuring cell outer wall, for measuring temperature in gas pond, to control heating-up temperature.
Claims (8)
1. the multispectral coupling optical-mechanical system of high temperature: comprise gas pond assembly, ultraviolet light emission and receiving unit, Laser emission and receiving unit and heating component, described gas pond assembly comprises measuring cell, adjusting part and left and right catoptron, it is characterized in that: Laser emission and receiving unit are all installed on measuring cell homonymy, and be located at the upper/lower terminal in gas pond respectively; Described ultraviolet light emission and receiving unit are installed on measuring cell arranged on left and right sides respectively, and the centre position in ultraviolet light emission gas pond corresponding to receiving unit; Left/right catoptron has three through holes, be respectively middle macropore and the aperture of both sides, the corresponding ultraviolet light emission of middle macropore or receiving unit, both sides aperture is corresponding Laser emission and receiving unit respectively; Also corresponding macropore is had in the middle of right/left catoptron.
2. the multispectral coupling optical-mechanical system of high temperature according to claim 1, it is characterized in that: adjustable component comprises trim ring and adjustment seat, catoptron is pressed in adjustment seat by trim ring, and adjustment seat is arranged on measuring cell end by adjustment screw, and adjustment seat outside surface is designed to sphere.
3. the multispectral coupling optical-mechanical system of high temperature according to claim 2, is characterized in that: measuring cell cavity inner wall is mirror finish inwall.
4. the multispectral coupling optical-mechanical system of high temperature according to claim 3, is characterized in that: described measuring cell inner wall surface is provided with corrosion-inhibiting coating.
5. the multispectral coupling optical-mechanical system of high temperature according to claim 4, is characterized in that: described measuring cell adopts thermostable fluorine rubber seal rings for seal.
6., according to the multispectral coupling optical-mechanical system of the arbitrary described high temperature of claim 1-5, it is characterized in that: ultraviolet emission assembly comprises light source and collimation group, and light source comprises deuterium lamp, deuterium lamp holder; Collimation group comprises collimation lens, mirror pipe and adjustable optic fibre coupling seat, for the ultraviolet divergence optical alignment of Optical Fiber Transmission is become directional light; Ultraviolet receiving unit comprises collector lens, mirror pipe and adjustable optic fibre coupling seat.
7. the multispectral coupling optical-mechanical system of high temperature according to claim 6, is characterized in that: Laser emission assembly comprises lens combination, micrometer adjusting screw, fixed mount and fine motion frame; Laser pick-off assembly comprises collector lens, mirror pipe and photodetector.
8. the multispectral coupling optical-mechanical system of high temperature according to claim 7, is characterized in that: it is peripheral that described well heater is coated on gas pond, comprises heating plate, foamed heat insulating thermofin and crust from inside to outside successively.
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Cited By (6)
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CN105739104A (en) * | 2016-05-10 | 2016-07-06 | 力合科技(湖南)股份有限公司 | Multi-beam coupling device and detection air chamber |
CN107561034A (en) * | 2016-06-30 | 2018-01-09 | 株式会社堀场制作所 | Gas concentration measuring apparatus |
CN108398396A (en) * | 2018-02-28 | 2018-08-14 | 南京国电环保科技有限公司 | A kind of double light path high temperature lighting apparatus components of ultraviolet reflectance formula |
CN112098338A (en) * | 2020-09-14 | 2020-12-18 | 西南石油大学 | Well head foam content detection sensor |
CN113008814A (en) * | 2021-02-22 | 2021-06-22 | 山东省科学院海洋仪器仪表研究所 | Device and method for detecting water vapor concentration by using dual lasers |
CN113281300A (en) * | 2021-05-21 | 2021-08-20 | 中国人民解放军战略支援部队航天工程大学 | Measuring device for high-sensitivity measurement of weak absorption gas parameters in narrow environment |
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CN202092953U (en) * | 2011-06-03 | 2011-12-28 | 天津市蓝宇科工贸有限公司 | Direct insertion type smoke ultraviolet differential probe with on-line calibration optical path |
CN203798726U (en) * | 2014-04-23 | 2014-08-27 | 南京国电环保科技有限公司 | Smoke concentration analysis meter optical-mechanical system with universal bulb mechanism |
CN203798723U (en) * | 2014-04-23 | 2014-08-27 | 南京国电环保科技有限公司 | Smoke concentration analysis meter optical-mechanical system with deuterium lamp fine adjustment mechanism |
CN104568836A (en) * | 2015-01-26 | 2015-04-29 | 南京国电环保科技有限公司 | Low-concentration and multi-component gas detection method based on integration of multiple spectrum technologies |
CN204924925U (en) * | 2015-08-21 | 2015-12-30 | 南京国电环保科技有限公司 | Multispectral coupling optical -mechanical system of high temperature |
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CN1439880A (en) * | 2003-01-21 | 2003-09-03 | 中国科学院安徽光学精密机械研究所 | Method and apparatus for real time remote determining multiple pollutants in vehicle exhaust |
CN202092953U (en) * | 2011-06-03 | 2011-12-28 | 天津市蓝宇科工贸有限公司 | Direct insertion type smoke ultraviolet differential probe with on-line calibration optical path |
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Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105739104A (en) * | 2016-05-10 | 2016-07-06 | 力合科技(湖南)股份有限公司 | Multi-beam coupling device and detection air chamber |
CN107561034A (en) * | 2016-06-30 | 2018-01-09 | 株式会社堀场制作所 | Gas concentration measuring apparatus |
CN108398396A (en) * | 2018-02-28 | 2018-08-14 | 南京国电环保科技有限公司 | A kind of double light path high temperature lighting apparatus components of ultraviolet reflectance formula |
CN108398396B (en) * | 2018-02-28 | 2021-04-09 | 南京国电环保科技有限公司 | Ultraviolet reflection type double-optical-path high-temperature optical-mechanical assembly |
CN112098338A (en) * | 2020-09-14 | 2020-12-18 | 西南石油大学 | Well head foam content detection sensor |
CN112098338B (en) * | 2020-09-14 | 2022-03-08 | 西南石油大学 | Well head foam content detection sensor |
CN113008814A (en) * | 2021-02-22 | 2021-06-22 | 山东省科学院海洋仪器仪表研究所 | Device and method for detecting water vapor concentration by using dual lasers |
CN113281300A (en) * | 2021-05-21 | 2021-08-20 | 中国人民解放军战略支援部队航天工程大学 | Measuring device for high-sensitivity measurement of weak absorption gas parameters in narrow environment |
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