CN105056575B - A kind of automatic liquid liquid abstraction instrument - Google Patents
A kind of automatic liquid liquid abstraction instrument Download PDFInfo
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- CN105056575B CN105056575B CN201510578022.0A CN201510578022A CN105056575B CN 105056575 B CN105056575 B CN 105056575B CN 201510578022 A CN201510578022 A CN 201510578022A CN 105056575 B CN105056575 B CN 105056575B
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Abstract
The present invention relates to chemical device field, more particularly to a kind of automatic liquid liquid abstraction instrument.It includes separatory funnel and the pipe-line system on separatory funnel, the separatory funnel at least includes two-layer inwall, the separatory funnel is divided into mezzanine space and inner space by least two-layer inwall, the inwall is provided with linked hole, the mezzanine space is communicated with the inner space by linked hole, the mezzanine space and inner space are at least each provided with an import and export, and the pipe-line system is communicated by importing and exporting with the separatory funnel.Separatory funnel of the present invention is designed to multilayer interior wall construction, and is communicated between inwall, facilitates jetting type extraction and air blowing type extraction, reasonable in design, substantially increases extraction efficiency, and inwall can be cleaned automatically, easy to use, improves operating efficiency.Present invention design is perfect, it is adaptable to various points of liquid processes, and practicality is the once huge innovation of liquid-liquid extraction greatly.
Description
Technical field
The present invention relates to chemical device field, more particularly to a kind of automatic liquid liquid abstraction instrument.
Background technology
Extraction, also known as solvent extraction or liquid-liquid extraction, also known as extracts, and is have different in a solvent using component in system
Solubility carrys out the unit operation of separating mixture.That is, it is to be dissolved in two kinds of solvents of immiscible (or slightly soluble) using material
The difference of degree or distribution coefficient, makes a kind of method of the solute substance from another solvent is transferred in solvent.Extensive use
In the industry such as chemistry, metallurgy, food, petroleum refining industry is common to.
The separate operation of the immiscible liquid of latter two will be extracted, is called a point liquid.Extraction and point liquid inevitably make
Use separatory funnel.At present, conventional separatory funnel design is simple, using single, comes for jetting type extraction and air blowing type extraction
Say, process is complicated, operation inconvenience.Furthermore, point liquid person of needing to use carries out Manual-cleaning.But, conventional separatory funnel shape is special
Different, Manual-cleaning is difficult to clean up.
The content of the invention
The technical problem to be solved in the present invention is how to overcome the deficiencies in the prior art, there is provided a kind of automatic liquid-liquid extraction
Instrument.
The technical scheme that uses to achieve the above object of the present invention is：A kind of automatic liquid liquid abstraction instrument, including separatory funnel
And the pipe-line system on separatory funnel, at least including two-layer inwall, the separatory funnel is by least for the separatory funnel
Two-layer inwall is divided into mezzanine space and inner space, the inwall to be provided with linked hole, and the mezzanine space is empty with the internal layer
Between communicated by linked hole, the mezzanine space and inner space are at least each provided with an import and export, and the pipe-line system is led to
Import and export are crossed to be communicated with the separatory funnel.
Further, described import and export is three, and the pipe-line system is imported and exported and the separatory funnel phase by three
It is logical.
Further, the separatory funnel includes two-layer inwall, and the separatory funnel is divided into interlayer empty by two-layer inwall
Between and inner space, the import and export are provided with three, and one import and export are communicated with the mezzanine space, described two turnover
Mouth is communicated with inner space.
Further, the import and export for being communicated with the mezzanine space are No. three import and export, and No. three import and export are provided with two
Individual spout, wherein spout is located at the inner surface of outside inwall at one, another place's spout is located at the outer surface of inner side inwall.
Further, two import and export for being communicated with inner space, respectively No. one is imported and exported and No. two import and export, described
No. two are imported and exported a parcel number import and export, and an import and export are provided with through hole, if described No. two are imported and exported bottom and are provided with
Dry spout.
Further, the pipe-line system includes three pipe-lines, is the first pipeline, the second pipeline and the 3rd pipe
Road, the pipe-line system includes four-way valve, triple valve, No. two triple valves, No. three triple valves, air pump, an inorganic salts addition pumps
And Unidirectional solenoid valve.
Further, first pipeline connects No. three import and export, by four-way valve, No. two triple valves, air pump, No. three
Triple valve, a triple valve finally connect an import and export.
Further, second pipeline connects No. two import and export, is finally passed in and out with described No. three by the four-way valve
Mouth is communicated, and second pipeline can external cleaning solution supplying unit.
Further, the external inorganic salts feed unit of the 3rd pipeline, then by inorganic salts addition pump, Unidirectional solenoid valve
Finally communicated with an import and export.
Further, a triple valve directly can be connected with the four-way valve, and No. two triple valves can directly connect
Connect an import and export.
The advantage of the invention is that：Separatory funnel of the present invention is designed to multilayer interior wall construction, and is communicated between inwall, convenient
Jetting type extraction and air blowing type extraction, it is reasonable in design, substantially increase extraction efficiency.The present invention is designed with least three turnover
Mouthful, facilitating the entrance and turnover of gas and inorganic salt solution, the present invention can automatically be cleaned to inwall, easy to use, be carried
Operating efficiency high.The present invention is provided with pipe-line system, and pipe-line system is controlled by triple valve and four-way valve, uses spirit
It is living, greatly improve traditional liquid separation system.Present invention design is perfect, it is adaptable to various points of liquid processes, and practicality is very big,
It is the once huge innovation of point liquid.
Brief description of the drawings
Fig. 1 is schematic structural view of the invention.
Specific embodiment
As shown in figure 1, a kind of automatic liquid liquid abstraction instrument, including separatory funnel 1 and the pipeline system on separatory funnel 1
System 2, it is ensured that pipe-line system 2 in separatory funnel 1 timely to conveying liquids and gases.The separatory funnel 1 includes two-layer inwall,
The separatory funnel 1 is divided into mezzanine space 3 and inner space 4, the inwall 11 to be provided with linked hole 111, institute by two-layer inwall
Mezzanine space 3 is stated to be communicated by linked hole 111 with the inner space 4, it is convenient when air-flow and current pass through connection from mezzanine space 3
Through hole 111 enters inner space 4, so as to realize jetting type extraction and air blowing type extraction.
The upper end of the separatory funnel 1 is provided with stopper 5, and the separatory funnel 1 is connected by stopper 5 with the pipe-line system 2,
For convenience of the entrance of the current and air-flow of pipe-line system, the stopper 5 is provided with three import and export, including is communicated with inner space 4
Two import and export, respectively No. one import and export 51 and No. two import and export 52, it is described No. two import and export 52 parcel described No. one enter
Outlet 51, imports and exports 51 for described No. one and is provided with through hole, communicates up and down, facilitates the entrance of air-flow current.Described No. two are imported and exported 52
Bottom is provided with several spouts 521, facilitates air-flow current to be flowed along the inner surface of inner side inwall 12, designs ingenious.
The import and export communicated with the mezzanine space 3 are No. three and import and export 53, import and export 53 for described No. three and be provided with two sprays
Mouthful, wherein spout A is located at the inner surface of outside inwall 11 at one, another place's spout B is located at the outer surface of inner side inwall 12,
Ensure that air-flow and liquid directly spray to the inner surface of outside inwall 11 from spout A.The current and air-flow sprayed from spout B can be direct
Spray to the outer surface of inner side inwall 12.
The pipe-line system 2 includes three pipe-lines, is the first pipeline 21, the second pipeline 22 and the 3rd pipeline 23,
The pipe-line system includes four-way valve 24, a triple valve 25, two triple valve 26, No. three triple valves 27, air pumps 28, inorganic salts
Addition pump 29 and Unidirectional solenoid valve 210.
First pipeline 21 connects No. three and imports and exports 53, then by 24, No. two triple valves 26 of four-way valve, air pump 28, three
Number 27, triple valve 25 of triple valve finally connects described No. one and imports and exports 51, facilitates air-flow to import and export 53 from No. three and enters folder
Sheaf space 3, then inner space 4 is entered by linked hole 111, finally, 51 are imported and exported from No. one out, it is reasonable in design.
Second pipeline 22 connects No. two and imports and exports 52, and finally 53 are imported and exported with described No. three by the four-way valve 24
Communicate, cleaning solution supplying unit 6 is circumscribed with the second pipeline 22, facilitate cleaning fluid and 53 into interlayer sky are imported and exported from No. three
Between 3, midway through spout A, B, the inner surface to outside inwall 11 is cleaned.The current that cleaning fluid sprays from spout B can be straight
The outer surface for spraying to inner side inwall 12 is connect, outer surface is cleaned.
The external inorganic salts feed unit 7 of 3rd pipeline 23, then by inorganic salts addition pump 29, Unidirectional solenoid valve 210
Finally 51 are imported and exported with described No. one to communicate, facilitate inorganic salts to import and export 51 by No. one from inorganic salts feed unit 7 and finally enter
Enter in the middle of inner space 4.
Flexible and changeable to ensure pipe-line system 2, a triple valve 25 directly can be connected with the four-way valve 24, described
No. two triple valves 26 can be directly connected to No. one and import and export 51, it is ensured that the whole circuit of pipe-line system 2 variation.
Workflow of the invention is as follows：
(1) during Jet-flow extraction, air pump 28 is operated, and No. three ac of triple valve 27 mouthfuls of connections a, ac for triple valve 25 is connected,
No. two ac of triple valve 26 connect the ac connections of four-way valve 24, and air imports and exports 53 and enter separatory funnel 1, enters from No. one from No. three
Outlet 51 out, the liquid of mezzanine space 3 is pushed into inner space 4 by linked hole 111, then a He of triple valve 25
No. two triple valves 26 convert path, and ab is changed into from ac is logical, realize that gas circuit is exchanged, and air imports and exports 53 from No. three out, from No. one
51 bottle inlets are imported and exported, liquid is shifted onto in mezzanine space 3 from inner space 4, so repeatedly, liquid is in ectonexine bottle UNICOM
Stop-spraying is not shot through shuttle in hole 111, reaches the effect for being sufficiently mixed extraction.
(2) when blowing afloat extraction, air pump 28 is operated, and No. three ac of triple valve 27 mouthfuls of connections a, ac for triple valve 25 is connected,
No. two ac of triple valve 26 connect the ac connections of four-way valve 24, and air imports and exports 53 and enter separatory funnel, enters from No. one from No. three
Outlet 51 out, the liquid of mezzanine space 3 is pushed into inner space 4 by ectonexine bottle linked hole 111, and gas circuit is not cut
Change, gas is constantly passed through from ectonexine bottle linked hole 111, by the liquid in inner space 4, import and export 51 from No. one and return to
Air pump 28, realizes that circulation is blown, and reaches rolling liquid, realizes the purpose of extraction.
(3) when cleaning, bc mouthful of four-way valve 24 connection, opening piston 13, the cleaning fluid of cleaning solution supplying unit 6 is from cleaning
Liquid entrance point two-way enter No. three import and export 53 and No. two import and export 52 into bottle wall is cleaned in bottle, spout A is to outside inwall 11
Inner surface cleaned.The current that cleaning fluid sprays from spout B can directly spray to the outer surface of inner side inwall 12, to appearance
Face is cleaned, and all waste water flow out through tapping piston 13 to be collected.
(4) when extracting plus inorganic salts flow is that Unidirectional solenoid valve 210 is opened, and inorganic salts addition pump 29 extracts inorganic salts
The solution of feed unit 7, by an import and export 51 to separatory funnel.
Above-described embodiment simply to illustrate that technology design of the invention and feature, the purpose is to be to allow in the art
Those of ordinary skill will appreciate that present disclosure and implement according to this that it is not intended to limit the scope of the present invention.It is all
It is the equivalent change or modification made according to the essence of present invention, should all covers within the scope of the present invention.
Claims (7)
1. a kind of automatic liquid liquid abstraction instrument, including separatory funnel and the pipe-line system on separatory funnel, it is characterised in that：
The separatory funnel at least includes two-layer inwall, and the separatory funnel is divided into mezzanine space and internal layer empty by least two-layer inwall
Between, the inwall is provided with linked hole, and the mezzanine space is communicated with the inner space by linked hole, the mezzanine space and
Inner space is at least each provided with an import and export, and the pipe-line system is communicated by importing and exporting with the separatory funnel；It is described
It is three to import and export, and the pipe-line system is communicated by three import and export with the separatory funnel；The separatory funnel includes two
Layer inwall, the separatory funnel is divided into mezzanine space and inner space by two-layer inwall, and the import and export are provided with three, described
One in import and export communicates with the mezzanine space, and two in the import and export communicate with inner space；With inner space
Two import and export for communicating, respectively No. one is imported and exported and No. two import and export, and described No. two are imported and exported a parcel number turnover
Mouthful, import and export for described No. one and be provided with through hole, import and export bottom for described No. two and be provided with several spouts.
2. a kind of automatic liquid liquid abstraction instrument according to claim 1, it is characterised in that：With entering that the mezzanine space is communicated
It is No. three import and export to export, and No. three import and export are provided with two spouts, wherein spout is located at the inner surface of outside inwall at one
Place, another place's spout is located at the outer surface of inner side inwall.
3. a kind of automatic liquid liquid abstraction instrument according to claim 1, it is characterised in that：The pipe-line system includes three pipes
Road circuit, is the first pipeline, the second pipeline and the 3rd pipeline, the pipe-line system include four-way valve, triple valve, No. two
Triple valve, No. three triple valves, air pump, inorganic salts addition pump and Unidirectional solenoid valves.
4. a kind of automatic liquid liquid abstraction instrument according to claim 3, it is characterised in that：First pipeline connects No. three and enters
Outlet, a turnover is finally being connected by four-way valve, No. two triple valves, air pump, No. three triple valves, a triple valves
Mouthful.
5. a kind of automatic liquid liquid abstraction instrument according to claim 3, it is characterised in that：Second pipeline connects No. two and enters
Outlet, finally communicates, the external cleaning solution supplying unit of the second pipeline by the four-way valve with No. three import and export.
6. a kind of automatic liquid liquid abstraction instrument according to claim 3, it is characterised in that：The external inorganic salts of 3rd pipeline
Feed unit, then finally communicated with an import and export by inorganic salts addition pump, Unidirectional solenoid valve.
7. a kind of automatic liquid liquid abstraction instrument according to claim 3, it is characterised in that：A number triple valve is directly and institute
Four-way valve connection is stated, No. two triple valves are directly connected to an import and export.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510578022.0A CN105056575B (en) | 2015-09-11 | 2015-09-11 | A kind of automatic liquid liquid abstraction instrument |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510578022.0A CN105056575B (en) | 2015-09-11 | 2015-09-11 | A kind of automatic liquid liquid abstraction instrument |
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| Publication Number | Publication Date |
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| CN105056575A CN105056575A (en) | 2015-11-18 |
| CN105056575B true CN105056575B (en) | 2017-05-31 |
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| CN201510578022.0A Active CN105056575B (en) | 2015-09-11 | 2015-09-11 | A kind of automatic liquid liquid abstraction instrument |
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Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105510235A (en) * | 2015-12-30 | 2016-04-20 | 北京万维盈创科技发展有限公司 | Portable automatic infrared lampblack detection system and automatic detection method |
| CN111249768A (en) * | 2020-04-07 | 2020-06-09 | 孙海侠 | Extraction equipment convenient to chemical reagent processing |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN2655230Y (en) * | 2003-11-20 | 2004-11-10 | 陈玉昆 | Chemical reactor for multi-element automatic chemical analyzer |
| JP5305382B2 (en) * | 2008-09-30 | 2013-10-02 | 独立行政法人日本原子力研究開発機構 | Counterflow emulsion flow continuous liquid-liquid extraction device |
| CN104001561A (en) * | 2014-06-07 | 2014-08-27 | 段作敏 | Separating funnel for extraction and extraction instrument based on separating funnel |
| CN104014381A (en) * | 2014-06-24 | 2014-09-03 | 济南盛泰电子科技有限公司 | Separating funnel for extraction and extraction instrument based on separating funnel |
| CN204932935U (en) * | 2015-09-11 | 2016-01-06 | 刘艾新 | A kind of automatic liquid liquid abstraction instrument |
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Effective date of registration: 20170803 Address after: Yang Road Chengyang District Chengyang Street Jingkou Shandong province Qingdao city community Wen 266000 No. 1193 Patentee after: QINGDAO SHUNXIN ELECTRONIC SCIENCE AND TECHNOLOGY CO., LTD. Address before: Xia Road Chengyang District Shandong 266000 Qingdao Shengtai home B District No. 169 Patentee before: Liu Aixin |