CN204932935U - A kind of automatic liquid liquid abstraction instrument - Google Patents
A kind of automatic liquid liquid abstraction instrument Download PDFInfo
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- CN204932935U CN204932935U CN201520704173.1U CN201520704173U CN204932935U CN 204932935 U CN204932935 U CN 204932935U CN 201520704173 U CN201520704173 U CN 201520704173U CN 204932935 U CN204932935 U CN 204932935U
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- export
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- liquid
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Abstract
The utility model relates to chemical device field, particularly relates to a kind of automatic liquid liquid abstraction instrument.It comprises separatory funnel and is positioned at the pipe-line system on separatory funnel, described separatory funnel at least comprises two-layer inwall, described separatory funnel is divided into mezzanine space and inner space by least two-layer inwall, described inwall is provided with linked hole, described mezzanine space is communicated by linked hole with described inner space, described mezzanine space and inner space are at least respectively provided with import and export, and described pipe-line system communicates with described separatory funnel by importing and exporting.The utility model separatory funnel is designed to multilayer interior wall construction, and communicates between inwall, facilitates jetting type extraction and air blowing type extraction, reasonable in design, substantially increases extraction efficiency, automatically can clean inwall, easy to use, improves operating efficiency.The utility model design is perfect, is applicable to various separatory process, and practicality is very big, is the once huge innovation of liquid-liquid extraction.
Description
Technical field
The utility model relates to chemical device field, particularly relates to a kind of automatic liquid liquid abstraction instrument.
Background technology
Extraction, also known as solvent extraction or liquid-liquid extraction, also known as extracting, is utilize component in system to have different solubility to carry out the unit operations of separating mixture in a solvent.That is, be the difference utilizing material solubility or distribution coefficient in the solvent of two kinds immiscible (or slightly solubles), make solute substance in a kind of solvent, transfer to method another solvent.Be widely used in the industry such as chemistry, metallurgy, food, be common to petroleum refining industry.
By the operation that liquid immiscible for extraction latter two separates, be called separatory.Extraction and separatory inevitably use separatory funnel.At present, conventional separatory funnel simplicity of design, uses single, and for jetting type extraction and air blowing type extraction, process is complicated, operation inconvenience.Moreover separatory needs user to carry out Manual-cleaning.But conventional separatory funnel shape is special, and Manual-cleaning not easily cleans up.
Summary of the invention
The technical problems to be solved in the utility model how to overcome the deficiencies in the prior art, provides a kind of automatic liquid liquid abstraction instrument.
The technical scheme that the utility model adopts for achieving the above object is: a kind of automatic liquid liquid abstraction instrument, comprise separatory funnel and be positioned at the pipe-line system on separatory funnel, described separatory funnel at least comprises two-layer inwall, described separatory funnel is divided into mezzanine space and inner space by least two-layer inwall, described inwall is provided with linked hole, described mezzanine space is communicated by linked hole with described inner space, described mezzanine space and inner space are at least respectively provided with import and export, and described pipe-line system communicates with described separatory funnel by importing and exporting.
Further, described import and export are three, and described pipe-line system is communicated with described separatory funnel by three import and export.
Further, described separatory funnel comprises two-layer inwall, and described separatory funnel is divided into mezzanine space and inner space by two-layer inwall, and described import and export are provided with three, described import and export communicate with described mezzanine space, and described two import and export communicate with inner space.
Further, the import and export communicated with described mezzanine space are No. three and import and export, and described No. three import and export are provided with two spouts, and wherein place's spout is positioned at the inner surface place of outside inwall, and another place's spout is positioned at the outer surface of inner side inwall.
Further, import and export with inner space for two that communicate, be respectively No. one and import and export and No. two import and export, import and export the described import and export of parcel for described No. two, described import and export are provided with through hole, and described No. two import and export bottoms are provided with several spouts.
Further, described pipe-line system comprises three pipe-lines, be the first pipeline, the second pipeline and the 3rd pipeline, described pipe-line system comprises cross valve, triple valve, No. two triple valves, No. three triple valves, air pump, inorganic salts add pump and Unidirectional solenoid valve.
Further, described first pipeline connects No. three import and export, is finally connecting described import and export through cross valve, No. two triple valves, air pump, No. three triple valves, triple valves.
Further, described second pipeline connects No. two import and export, and finally communicate with described No. three import and export through described cross valve, described second pipeline can external cleaning solution supplying unit.
Further, the external inorganic salts feed unit of described 3rd pipeline, more finally communicate with described import and export through inorganic salts interpolation pump, Unidirectional solenoid valve.
Further, a described triple valve can directly be connected with described cross valve, and described No. two triple valves directly can connect import and export.
The utility model has the advantage of: the utility model separatory funnel is designed to multilayer interior wall construction, and communicates between inwall, facilitate jetting type extraction and air blowing type extraction, reasonable in design, substantially increase extraction efficiency.The utility model is designed with at least three import and export, and facilitate entering and passing in and out of gas and inorganic salt solution, the utility model can clean automatically to inwall, easy to use, improves operating efficiency.The utility model is provided with pipe-line system, and pipe-line system is controlled by triple valve and cross valve, use flexibly, greatly improves traditional liquid separation system.The utility model design is perfect, is applicable to various separatory process, and practicality is very big, is the once huge innovation of separatory.
Accompanying drawing explanation
Fig. 1 is the utility model structural representation.
Detailed description of the invention
As shown in Figure 1, a kind of automatic liquid liquid abstraction instrument, comprises separatory funnel 1 and is positioned at the pipe-line system 2 on separatory funnel 1, ensures that pipe-line system 2 carries liquids and gases timely in separatory funnel 1.Described separatory funnel 1 comprises two-layer inwall, described separatory funnel 1 is divided into mezzanine space 3 and inner space 4 by two-layer inwall, described inwall 11 is provided with linked hole 111, described mezzanine space 3 is communicated by linked hole 111 with described inner space 4, conveniently when air-flow and current enter inner space 4 from mezzanine space 3 by linked hole 111, thus realize jetting type extraction and air blowing type extraction.
Described separatory funnel 1 upper end is provided with stopper 5, described separatory funnel 1 is connected with described pipe-line system 2 by stopper 5, for convenience of the current of pipe-line system and entering of air-flow, described stopper 5 is provided with three import and export, comprises two of communicating with inner space 4 and imports and exports, be respectively No. one import and export 51 and No. two import and export 52, import and export the described import and export 51 of 52 parcels for described No. two, described import and export 51 are provided with through hole, communicate up and down, facilitate entering of air-flow current.Be provided with several spouts 521 bottom described No. two import and export 52, facilitate air-flow current to flow along the inner surface of inner side inwall 12, design ingenious.
The import and export communicated with described mezzanine space 3 are No. three and import and export 53, described No. three import and export 53 are provided with two spouts, wherein a place spout A is positioned at the inner surface place of outside inwall 11, another place spout B is positioned at the outer surface of inner side inwall 12, ensures that air-flow and liquid directly spray to the inner surface of outside inwall 11 from spout A.The current sprayed from spout B and air-flow directly can spray to the outer surface of inner side inwall 12.
Described pipe-line system 2 comprises three pipe-lines, be the first pipeline 21, second pipeline 22 and the 3rd pipeline 23, described pipe-line system comprises cross valve 24, triple valve 25, No. two triple valves 26, No. three triple valves 27, air pump 28, inorganic salts interpolation pump 29 and Unidirectional solenoid valve 210.
Described first pipeline 21 connects No. three and imports and exports 53, finally connect described No. one through cross valve 24, No. two triple valves 26, air pump 28, No. three triple valves 27, triple valve 25 again and import and export 51, facilitate air-flow to import and export 53 from No. three and enter mezzanine space 3, inner space 4 is entered again by linked hole 111, finally, 51 are imported and exported out from No. one, reasonable in design.
Described second pipeline 22 connects No. two and imports and exports 52, finally import and export 53 with described No. three through described cross valve 24 to communicate, second pipeline 22 is circumscribed with cleaning solution supplying unit 6, facilitate cleaning fluid and enter mezzanine space 3 from No. three import and export 53, midway, through spout A, B, is cleaned the inner surface of outside inwall 11.Cleaning fluid directly can spray to the outer surface of inner side inwall 12 from the current that spout B sprays, and cleans outer surface.
The external inorganic salts feed unit 7 of described 3rd pipeline 23, add pump 29 through inorganic salts again, Unidirectional solenoid valve 210 is is finally imported and exported 51 with described No. one and communicated, facilitate inorganic salts to import and export 51 from inorganic salts feed unit 7 through No. one and finally enter in the middle of inner space 4.
Flexible and changeable for ensureing pipe-line system 2, a described triple valve 25 can directly be connected with described cross valve 24, and described No. two triple valves 26 directly can connect No. one and import and export 51, ensure the variation of whole pipe-line system 2 circuit.
Workflow of the present utility model is as follows:
(1) during Jet-flow extraction, air pump 28 operates, the ac mouth of No. three triple valves 27 is connected, the ac of a triple valve 25 connects, the ac of No. two triple valves 26 connects the ac connection of cross valve 24, air is imported and exported 53 from No. three and is entered separatory funnel 1, 51 are imported and exported out from No. one, the liquid of mezzanine space 3 is pushed in inner space 4 through linked hole 111, then a triple valve 25 and No. two triple valves 26 convert path, ab is become from ac is logical, realize gas circuit to exchange, air imports and exports 53 out from No. three, 51 bottle inlets are imported and exported from No. one, liquid is shifted onto in mezzanine space 3 from inner space 4, so repeatedly, liquid in ectonexine bottle linked hole 111 not stop-spraying penetrate and shuttle back and forth, reach the effect of abundant hybrid extraction.
(2) when blowing afloat extraction, air pump 28 operates, the ac mouth of No. three triple valves 27 is connected, the ac of a triple valve 25 connects, the ac of No. two triple valves 26 connects the ac connection of cross valve 24, air is imported and exported 53 from No. three and is entered separatory funnel, 51 are imported and exported out from No. one, the liquid of mezzanine space 3 is pushed in inner space 4 through ectonexine bottle linked hole 111, gas circuit does not switch, gas constantly passes from ectonexine bottle linked hole 111, liquid in inner space 4, import and export 51 from No. one and get back to air pump 28, realize circulation to blow, reach rolling liquid, realize the object of extraction.
(3) during cleaning, the bc mouth of cross valve 24 is connected, open piston 13, the cleaning fluid of cleaning solution supplying unit 6 divides two-way to enter No. three import and export 53 from filter washing water inlet and No. two import and export 52 enter washer bottle wall bottle, and the inner surface of spout A to outside inwall 11 cleans.Cleaning fluid directly can spray to the outer surface of inner side inwall 12 from the current that spout B sprays, and cleans outer surface, and all waste water flows out through tapping piston 13 to be collected.
(4) the inorganic salts flow process that adds during extraction is that Unidirectional solenoid valve 210 is opened, and inorganic salts add the solution that pump 29 extracts inorganic salts feed unit 7, imports and exports 51 in separatory funnel by No. one.
Above-described embodiment, just in order to technical conceive of the present utility model and feature are described, its objective is and is one of ordinary skilled in the art can be understood content of the present utility model and implement according to this, can not limit protection domain of the present utility model with this.The change of every equivalence made according to the essence of the utility model content or modification, all should be encompassed in protection domain of the present utility model.
Claims (10)
1. an automatic liquid liquid abstraction instrument, comprise separatory funnel and be positioned at the pipe-line system on separatory funnel, it is characterized in that: described separatory funnel at least comprises two-layer inwall, described separatory funnel is divided into mezzanine space and inner space by least two-layer inwall, described inwall is provided with linked hole, described mezzanine space is communicated by linked hole with described inner space, described mezzanine space and inner space are at least respectively provided with import and export, and described pipe-line system communicates with described separatory funnel by importing and exporting.
2. a kind of automatic liquid liquid abstraction instrument according to claim 1, is characterized in that: described import and export are three, and described pipe-line system is communicated with described separatory funnel by three import and export.
3. a kind of automatic liquid liquid abstraction instrument according to claim 1 and 2, it is characterized in that: described separatory funnel comprises two-layer inwall, described separatory funnel is divided into mezzanine space and inner space by two-layer inwall, described import and export are provided with three, described import and export communicate with described mezzanine space, and described two import and export communicate with inner space.
4. a kind of automatic liquid liquid abstraction instrument according to claim 3, it is characterized in that: the import and export communicated with described mezzanine space are No. three and import and export, described No. three import and export are provided with two spouts, wherein place's spout is positioned at the inner surface place of outside inwall, and another place's spout is positioned at the outer surface of inner side inwall.
5. a kind of automatic liquid liquid abstraction instrument according to claim 3, it is characterized in that: import and export for two that communicate with inner space, be respectively No. one to import and export and No. two import and export, import and export the described import and export of parcel for described No. two, described import and export are provided with through hole, and described No. two import and export bottoms are provided with several spouts.
6. a kind of automatic liquid liquid abstraction instrument according to claim 1, it is characterized in that: described pipe-line system comprises three pipe-lines, be the first pipeline, the second pipeline and the 3rd pipeline, described pipe-line system comprises cross valve, triple valve, No. two triple valves, No. three triple valves, air pump, inorganic salts add pump and Unidirectional solenoid valve.
7. a kind of automatic liquid liquid abstraction instrument according to claim 6, is characterized in that: described first pipeline connects No. three import and export, is finally connecting described import and export through cross valve, No. two triple valves, air pump, No. three triple valves, triple valves.
8. a kind of automatic liquid liquid abstraction instrument according to claim 6, is characterized in that: described second pipeline connects No. two import and export, and finally communicate with described No. three import and export through described cross valve, described second pipeline can external cleaning solution supplying unit.
9. a kind of automatic liquid liquid abstraction instrument according to claim 6, is characterized in that: the external inorganic salts feed unit of described 3rd pipeline, more finally communicates with described import and export through inorganic salts interpolation pump, Unidirectional solenoid valve.
10. a kind of automatic liquid liquid abstraction instrument according to claim 6, it is characterized in that: a described triple valve can directly be connected with described cross valve, described No. two triple valves directly can connect import and export.
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CN201520704173.1U CN204932935U (en) | 2015-09-11 | 2015-09-11 | A kind of automatic liquid liquid abstraction instrument |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105056575A (en) * | 2015-09-11 | 2015-11-18 | 刘艾新 | Automatic liquid-liquid extraction instrument |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105056575A (en) * | 2015-09-11 | 2015-11-18 | 刘艾新 | Automatic liquid-liquid extraction instrument |
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Granted publication date: 20160106 Termination date: 20170911 |