CN205412940U - Reation kettle inhales useless liquid device that divides - Google Patents
Reation kettle inhales useless liquid device that divides Download PDFInfo
- Publication number
- CN205412940U CN205412940U CN201620054595.3U CN201620054595U CN205412940U CN 205412940 U CN205412940 U CN 205412940U CN 201620054595 U CN201620054595 U CN 201620054595U CN 205412940 U CN205412940 U CN 205412940U
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- CN
- China
- Prior art keywords
- outlet
- pipe
- outlet pipe
- distributing device
- liquor separator
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 239000007788 liquid Substances 0.000 title claims abstract description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 37
- 239000002699 waste material Substances 0.000 claims description 12
- 238000004064 recycling Methods 0.000 claims description 7
- 239000000126 substance Substances 0.000 abstract description 3
- 239000003039 volatile agent Substances 0.000 abstract 1
- 239000007789 gas Substances 0.000 description 9
- 239000000498 cooling water Substances 0.000 description 8
- 238000000034 method Methods 0.000 description 4
- 230000008569 process Effects 0.000 description 3
- 239000002912 waste gas Substances 0.000 description 3
- 230000008676 import Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 230000002411 adverse Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 230000001112 coagulating effect Effects 0.000 description 1
- 230000019771 cognition Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
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- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The utility model belongs to the technical field of the chemical industry equipment, a reation kettle inhales useless liquid device that divides is related to, including the interchanger that has a liquid outlet with connect in the knockout of liquid outlet, knockout one side is equipped with the liquid level pipe, be equipped with outlet pipe, well outlet pipe and lower outlet pipe on the knockout from top to bottom in proper order, liquid level pipe go up the export with well outlet pipe gets into the height such as position of knockout, the bottom and a catch basin of knockout is connected to the outlet pipe down, be equipped with a shut -off valve on the well outlet pipe, be equipped with a governing valve down on the outlet pipe. The utility model discloses can adjust the dynamic balance of drainage, accomplish water oil separating, carry out the processing of volatiles.
Description
Technical field
This utility model relates to technical field of chemical, particularly to a kind of reactor waste suction liquid distributing device.
Background technology
Reactor is reaction vessel conventional in Chemical Manufacture, typically have mixing, heat, the function such as evaporation.In some thermal responses, carry out having the relatively low solvent of a large amount of boiling point or reactant volatilization along with reaction and become waste gas, it is therefore desirable to discharge reactor and cause kettle to burst in order to avoid pressure raises.Waste gas first has to carry out cooling liquefaction at discharge reactor, is the most just avoided that waste gas is directly discharged into atmospheric pollution environment.
The escaping gas produced in reactor is water cooled after coagulating, and wherein formation oil reservoir is floated on above water layer by non-water-soluble fractions, and both separately to process will use liquor separator.My department have developed a kind of reactor waste-absorbing device by gas-vapor mix heat exchange, and owing to the water yield is relatively big, liquor separator needs to be discharged by water layer at any time, in order to adapt to quantity-produced requirement, needs to improve liquor separator pipeline.
This utility model is contemplated to provide a kind of new liquid distributing device.
Utility model content
Main purpose of the present utility model is to provide a kind of reactor waste suction liquid distributing device.
This utility model is achieved through the following technical solutions above-mentioned purpose: a kind of reactor waste suction liquid distributing device, including there is the exchanger of liquid outlet and being connected to the liquor separator of described liquid outlet, described liquor separator side is provided with liquid level tube, upper outlet pipe, middle outlet pipe and lower outlet from top to bottom it is sequentially provided with on described liquor separator, the position that the upper outlet of described liquid level tube enters liquor separator with described middle outlet pipe is contour, described lower outlet connects bottom and a catch basin of liquor separator, described middle outlet pipe is provided with a shut-off valve, and described lower outlet is provided with a flow speed control valve.
Concrete, described upper outlet pipe and middle outlet manifold enter a recycling can.
Concrete, described exchanger also has inlet, water inlet, outlet, internal channel and outer tunnel, described internal channel and outer tunnel are completely cut off by tube wall, and described inlet and liquid outlet are connected by described internal channel, and described water inlet and outlet are connected by described outer tunnel.
Further, described inlet is connected to above reactor by an exhaustor, and described exhaustor separates the return pipe of a described outlet of connection.
Further, described return pipe is provided with a mixing chamber with the intersection of exhaustor.
Further, described water inlet connects described catch basin by a water inlet pipe.
Further, described water inlet pipe is provided with a water pump.
Using technique scheme, technical solutions of the utility model provide the benefit that: can regulate the dynamic equilibrium of draining, complete oil-water separation, carry out the process of volatile component.
Accompanying drawing explanation
Fig. 1 is the front view of this device；
Fig. 2 is the detail view at mixing chamber；
Fig. 3 is the A-A sectional view in Fig. 2；
Fig. 4 is the detail view at liquor separator.
In figure, numeral represents:
1-exchanger, 11-internal channel, 12-outer tunnel, 11a-inlet, 11b-liquid outlet, 12a-water inlet, 12b-outlet, 1a-return pipe；
2-reactor, 2a-exhaustor；
3-catch basin, 3a-water inlet pipe；
4-liquor separator, 41-liquid level tube, 42a-upper outlet pipe, 42b-middle outlet pipe, outlet under 42c-；
5-mixing chamber, 51-mistress, 511-exports, 52-inner chamber, 521-jet pipe；
6-water pump；
7-recycling can；
8a-flow speed control valve, 8b-shut-off valve.
Detailed description of the invention
Below in conjunction with specific embodiment, this utility model is described in further detail.
As shown in Figure 1, a kind of reactor waste suction liquid distributing device, including the exchanger 1 with internal channel 11 and outer tunnel 12, internal channel 11 and outer tunnel 12 are completely cut off by tube wall, internal channel 11 has inlet 11a and liquid outlet 11b, outer tunnel 12 has water inlet 12a and outlet 12b, inlet 11a is connected to above reactor 2 by an exhaustor 2a, exhaustor 2a separates the return pipe 1a of a connection outlet 12b, water inlet 12a connects a catch basin 3 by a water inlet pipe 3a, and liquid outlet 11b connects a liquor separator 4.The Volatile Gas produced in reactor 2 is known from experience through exhaustor 2a, exchanger 1 internal channel 11 is entered again from inlet 11a, cooling water from catch basin 3 then passes from outer tunnel 12 and imports inlet 1a simultaneously, gas by internal channel 11, finally flows to liquor separator 4 and carries out separatory together with after cooling water mixing.Cooling water serves not only as heat exchange low-temperature receiver, also exists as solvent.Volatilization gas potentially includes water-soluble component and water insoluble component, owing to it has higher temperature, mixes latter aspect with cooling water and heat exchange can be occurred to condense, and on the other hand component can be separated because of the dissolubility difference to water.Owing to gas is fully contacted with water, therefore heat exchange is relatively more abundant, and condensation is more thorough, saves the energy, it is to avoid gas is in the problem of workshop disperse.
As shown in Figure 1 to Figure 3, the intersection of return pipe 1a and exhaustor 2a is provided with a mixing chamber 5, mixing chamber 5 has the mistress 51 of connection exhaustor 2a and the inner chamber 52 connecting return pipe 1a, mistress 51 has the outlet 511 of connection inlet 1a, inner chamber 52 is positioned at mistress 51 and is provided with some jet pipes 521 side by side, the mouth of pipe export-oriented 511 of jet pipe 521.The mouth of pipe sectional area summation of jet pipe 521 sectional area less than return pipe 1a, so when cooling water flow velocity after return pipe 1a enters jet pipe 52 greatly speeds up, according to bernoulli principle, pressure at the mouth of pipe reduces, and the Volatile Gas cognition produced in reactor 2 allows its pressure raise, therefore, under the effect of pressure differential, volatilization gas is inhaled into mistress 71.Cooling water can form jet after multiple jet pipes 521, and each jet is fully contacted with the gas of surrounding, so can accelerate heat exchange, prevents aqueous vapor adverse current.
As it is shown in figure 1, water inlet pipe 3a is provided with a water pump 6.Water pump 6 makes cooling water draw water from catch basin 3 and enter exchanger 1.Cooling water is easier to cavitation phenomenons after heat exchange, and this position that water pump 6 is in can reduce cavitation and damage the risk of water pump 6.
As shown in Figure 1 and Figure 4, liquor separator 4 side is provided with liquid level tube 41, upper outlet pipe 42a, middle outlet pipe 42b and lower outlet 42c from top to bottom it is sequentially provided with on liquor separator 4, the position that the upper outlet of liquid level tube 41 enters liquor separator 4 with middle outlet pipe 42b is contour, lower outlet 42c connects bottom and the catch basin 3 of liquor separator 4, and lower outlet 42c is provided with a flow speed control valve 8a；Upper outlet pipe 42a and middle outlet pipe 42b imports a recycling can 7；Middle outlet pipe 42b is provided with a shut-off valve 8b.Closing shut-off valve 8b, the liquid flowed out through exchanger 1 can produce layering, wherein water layer under, oil reservoir is upper；Make water-oil interface can indicate in liquid level tube 41 by regulation flow speed control valve 8a aperture, catch basin 3 can be expelled back into from lower outlet 42c after water enters liquor separator 4, owing to oil reservoir floats over above water layer, so oil reservoir will not leave liquor separator 4 from lower outlet 42c, and recycling can 7 can be entered from upper outlet pipe 42a overflow；After reactor 2 power cut-off, first close flow speed control valve 8a, make water-oil interface be higher than liquid level tube 41 peak, switch off the pump 6 immediately, open shut-off valve 8b and allow oil reservoir all flow into recycling can 7, finally open flow speed control valve 8a and liquor separator 4 is emptied.The most just can complete oil-water separation, carry out the process of volatile component.
Above-described is only embodiments more of the present utility model.For the person of ordinary skill of the art, on the premise of creating design without departing from this utility model, it is also possible to making some deformation and improvement, these broadly fall into protection domain of the present utility model.
Claims (7)
1. a reactor waste suction liquid distributing device, including there is the exchanger of liquid outlet and being connected to the liquor separator of described liquid outlet, described liquor separator side is provided with liquid level tube, it is characterized in that: on described liquor separator, be from top to bottom sequentially provided with upper outlet pipe, middle outlet pipe and lower outlet, the position that the upper outlet of described liquid level tube enters liquor separator with described middle outlet pipe is contour, described lower outlet connects bottom and a catch basin of liquor separator, described upper outlet pipe and middle outlet manifold enter a recycling can, described middle outlet pipe is provided with a shut-off valve, described lower outlet is provided with a flow speed control valve.
Reactor waste suction liquid distributing device the most according to claim 1, it is characterised in that: described upper outlet pipe and middle outlet manifold enter a recycling can.
Reactor waste suction liquid distributing device the most according to claim 1, it is characterized in that: described exchanger also has inlet, water inlet, outlet, internal channel and outer tunnel, described internal channel and outer tunnel are completely cut off by tube wall, described inlet and liquid outlet are connected by described internal channel, and described water inlet and outlet are connected by described outer tunnel.
Reactor waste suction liquid distributing device the most according to claim 3, it is characterised in that: described inlet is connected to above reactor by an exhaustor, and described exhaustor separates the return pipe of a described outlet of connection.
Reactor waste suction liquid distributing device the most according to claim 4, it is characterised in that: described return pipe is provided with a mixing chamber with the intersection of exhaustor.
Reactor waste suction liquid distributing device the most according to claim 3, it is characterised in that: described water inlet connects described catch basin by a water inlet pipe.
Reactor waste suction liquid distributing device the most according to claim 6, it is characterised in that: described water inlet pipe is provided with a water pump.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620054595.3U CN205412940U (en) | 2016-01-20 | 2016-01-20 | Reation kettle inhales useless liquid device that divides |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201620054595.3U CN205412940U (en) | 2016-01-20 | 2016-01-20 | Reation kettle inhales useless liquid device that divides |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN205412940U true CN205412940U (en) | 2016-08-03 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201620054595.3U Expired - Fee Related CN205412940U (en) | 2016-01-20 | 2016-01-20 | Reation kettle inhales useless liquid device that divides |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN205412940U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111514833A (en) * | 2020-06-15 | 2020-08-11 | 天津长芦汉沽盐场有限责任公司 | Tetrabromobisphenol A liquid separation operation method |
-
2016
- 2016-01-20 CN CN201620054595.3U patent/CN205412940U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111514833A (en) * | 2020-06-15 | 2020-08-11 | 天津长芦汉沽盐场有限责任公司 | Tetrabromobisphenol A liquid separation operation method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20160803 |