CN111249768A

CN111249768A - Extraction equipment convenient to chemical reagent processing

Info

Publication number: CN111249768A
Application number: CN202010263751.8A
Authority: CN
Inventors: 孙海侠
Original assignee: Individual
Current assignee: Individual
Priority date: 2020-04-07
Filing date: 2020-04-07
Publication date: 2020-06-09

Abstract

The invention provides extraction equipment convenient for processing chemical reagents, and relates to the technical field of chemical equipment. This extraction equipment convenient to chemical reagent processing, the on-line screen storage device comprises a base, the both sides fixed mounting at base top has the support frame, and the inboard fixed mounting of two support frames has the holding frame, be provided with the reaction tube on the holding frame, the right side fixed mounting of reaction tube has the interpolation pipe. This extraction equipment convenient to chemical reagent processing, aerating device passes through manual control, close sealed lid promptly, extrude the piston downwards, and realize the leading-in of liquid through connecting the return bend, and steerable extrusion piston's effort size, realize the speed that control solvent added, the inner space of reaction tube and reagent pipe communicates with each other through the through-hole, the inside of being convenient for air current and rivers from entering into the reagent pipe in the middle of the inside of reaction tube, realize the extraction operation, the setting of shower nozzle, be convenient for spray water to the lateral wall of reaction tube on, be convenient for wash the surface department of lateral wall.

Description

Extraction equipment convenient to chemical reagent processing

Technical Field

The invention relates to the technical field of chemical equipment, in particular to extraction equipment convenient for processing chemical reagents.

Background

Extraction, also known as solvent extraction or liquid-liquid extraction, also known as extraction, is a unit operation that separates mixtures by utilizing the different solubilities of components in the system in a solvent. That is, the method is a method of transferring a solute substance from one solvent to another solvent by utilizing the difference in solubility or partition coefficient of the substance in two solvents which are not soluble (or slightly soluble) with each other. The method is widely applied to chemical, metallurgical, food and other industries and is generally applied to petroleum refining industry. The operation of separating the two immiscible liquids after extraction is called liquid separation.

The extraction and the separating inevitably use separating funnel, and present separating funnel design is simple, uses singly, is difficult to realize better extraction separating to the liquid of different grade type, and the operation is comparatively inconvenient, moreover, generally will carry out manual washing to the funnel after separating, because conventional separating funnel shape is specific, is not convenient for wash.

Disclosure of Invention

Technical problem to be solved

Aiming at the defects of the prior art, the invention provides extraction equipment convenient for processing chemical reagents, and solves the problem that the extraction equipment is difficult to realize better extraction and liquid separation on different types of liquid.

(II) technical scheme

In order to achieve the purpose, the invention is realized by the following technical scheme: the utility model provides an extraction equipment convenient to chemical reagent processing, includes the base, the both sides fixed mounting at base top has the support frame, and the inboard fixed mounting of two support frames has the holding frame, be provided with the reaction tube on the holding frame, the right side fixed mounting of reaction tube has the addition pipe, the entry of reaction tube and addition pipe is provided with first sealed the pad and the sealed pad of second respectively, the reaction tube communicates with each other through connecting bend between with the addition pipe.

The right side of adding the pipe communicates with each other has the feed liquor pipe, the top of feed liquor pipe is provided with aerating device, the inside of reaction tube is provided with the reagent pipe, the bottom of reaction tube is provided with out the liquid device, the bottom of reagent pipe communicates with each other has the connector, the through-hole has evenly been seted up to the side of connector, the top of reaction tube communicates with each other has communicating pipe, the top of reagent pipe communicates with each other has the liquid inlet head.

Preferably, be equipped with the bifurcated pipe on communicating pipe, the bifurcated pipe runs through first sealed the inside that fills up and extend to the reaction tube, the inlet header includes middle part pipe and lateral part pipe, the lateral part pipe is located the both sides of middle part pipe, the intercommunicating pore has been seted up with lateral part pipe relevant position to the both sides of middle part pipe.

Preferably, the ends of the bifurcated pipe, the side pipe and the connecting bent pipe are provided with inclined edges, and the inclined edges are tightly attached to the inner wall of the reaction pipe.

Preferably, aerating device includes trachea, piston, tracheal one end is run through and is added the pipe and extend to the inside that the sealed pad of second, the one end of piston extends to tracheal outside, and the other end passes through the left and right sides overlap joint of extrusion piece and trachea inner wall.

Preferably, one end of the liquid inlet pipe, which is far away from the adding pipe, is movably connected with a sealing cover, and scales are arranged on the surface of the adding pipe.

Preferably, the liquid outlet device comprises an extension pipe and a control valve core, the extension pipe is communicated with the reaction pipe and is provided with a through groove matched with the control valve core, the control valve core is rotatably arranged on the extension pipe, and the control valve core is provided with a one-way through hole.

(III) advantageous effects

The invention provides extraction equipment convenient for processing chemical reagents. The method has the following beneficial effects:

1. this extraction equipment convenient to chemical reagent processing, aerating device passes through manual control, close sealed lid promptly, extrude the piston downwards, and realize the leading-in of liquid through connecting the return bend, and steerable extrusion piston's effort size, thereby realize the speed that control solvent added, the inner space of reaction tube and reagent pipe communicates with each other through the through-hole, the inside of being convenient for air current and rivers from entering into the reagent pipe in the middle of the inside of reaction tube, realize the extraction operation, the setting of shower nozzle, be used for on the lateral wall with water injection to the reaction tube, be convenient for wash the surface department of lateral wall.

2. This extraction equipment convenient to chemical reagent processing sets up the scale, and the solvent can accurately add the solvent to in will letting in the solvent that adds the intraductal reaction of effectively letting in through aerating device, the setting of first sealed pad and second sealed pad can prevent that reaction tube and adding the inside gas from revealing, plays sealed effect, the setting on slope limit, makes the inner wall of pipeline can be hugged closely to liquid, prevents because the liquid level of liquid is crossed the phenomenon that produces the splash and splash excessively.

Drawings

FIG. 1 is a front view of the structure of the present invention;

FIG. 2 is an enlarged view of a portion of the structure of FIG. 1;

FIG. 3 is a schematic view of the liquid outlet device of the present invention.

In the figure: the device comprises a base 1, a support frame 2, a clamping frame 3, a reaction tube 4, an adding tube 5, a first sealing gasket 6, a second sealing gasket 7, a connecting bent tube 8, a liquid inlet tube 9, an air charging device 10, an air tube 101, a piston 102, a reagent tube 11, a liquid outlet device 12, an extension tube 121, a control valve core 122, a one-way through hole 123, a connector 13, a through hole 14, a communicating tube 15, a liquid inlet head 16, a bifurcated tube 17, a middle tube 18, a side tube 19, an inclined edge 20, a sealing cover 21, a scale 22 and a spray tube 23.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The embodiment of the invention provides extraction equipment convenient for processing chemical reagents, which comprises a base 1, wherein support frames 2 are fixedly arranged on two sides of the top of the base 1, clamping frames 3 are fixedly arranged on the inner sides of the two support frames 2, a reaction tube 4 is arranged on each clamping frame 3, an addition tube 5 is fixedly arranged on the right side of each reaction tube 4, a first sealing gasket 6 and a second sealing gasket 7 are respectively arranged at the inlets of each reaction tube 4 and the addition tube 5, the first sealing gasket 6 and the second sealing gasket 7 are arranged, so that gas leakage in the reaction tubes 4 and the addition tubes 5 can be prevented, a sealing effect is achieved, and the reaction tubes 4 and the addition tubes 5 are communicated through a connecting bent tube 8.

The right side of the adding pipe 5 is communicated with a liquid inlet pipe 9, one end of the liquid inlet pipe 9, which is far away from the adding pipe 5, is movably connected with a sealing cover 21, the surface of the adding pipe 5 is provided with scales 22, the scales 22 are arranged, a solvent can be accurately added into the solvent, the solvent introduced into the adding pipe 5 is effectively introduced into the reaction pipe 4 through an inflating device 10, the top of the liquid inlet pipe 9 is provided with the inflating device 10, the inflating device 10 is arranged for introducing the viscous solvent into the reagent pipe through a through hole 14 to realize subsequent extraction, the inflating device 10 comprises a gas pipe 101 and a piston 102, one end of the gas pipe 101 penetrates through the adding pipe 5 and extends into the second sealing gasket 7, one end of the piston 102 extends to the outer side of the gas pipe 101, the other end of the gas pipe is overlapped with the left side and the right side of the inner wall of the gas pipe 101 through an extrusion block, the inflating device 10 is manually controlled, and can control the acting force of the extruding piston 102, realize the control of the adding speed of the solvent, the inside of the reaction tube 4 is provided with a reagent tube 11, the bottom of the reaction tube 4 is provided with a liquid outlet device 12, the liquid outlet device 12 comprises an extension tube 121 and a control valve core 122, the extension tube 121 is communicated with the reaction tube 4, and is provided with a through groove matched with the control valve core 122, the control valve core 122 is rotatably arranged on the extension tube 121, the control valve core 122 is provided with a one-way through hole 123, when the control valve core 122 rotates, the one-way through hole 123 is communicated with the extension tube 121, the liquid can be led out from the extension tube 121, when the one-way through hole 123 is rotated to be vertical to the extension tube 121, the extension tube 121 can be sealed, the bottom of the reagent tube 11 is communicated with a connector 13, the connector 13 is used for leading the common liquid into the reagent tube 11 for the subsequent extraction, the side of the connector, the reaction tube 4 is communicated with the inner space of the reagent tube 11 through the through hole 14, so that air flow and water flow enter the inner part of the reagent tube 11 from the middle of the inner part of the reaction tube 4, and extraction operation is realized, the concrete process of extraction is that a communicating tube 15 is communicated with the top of the liquid reaction tube 4 through a connector 13, a bifurcated tube 17 is arranged on the communicating tube 15, one end of the bifurcated tube 17 is communicated with a spray head 23, the spray head 23 is arranged and used for spraying water to the side wall of the reaction tube 4, so that the surface of the side wall is convenient to clean, the bifurcated tube 17 penetrates through the first sealing gasket 6 and extends to the inner part of the reaction tube 4, the liquid inlet head 16 comprises a middle tube 18 and a side tube 19, the side tube 19 is positioned at two sides of the middle tube 18, communicating holes are arranged at the two sides of the middle tube 18 and the corresponding position of the side tube 19, the top of the reagent tube 11 is communicated with the liquid inlet head 16, the, the inclined edge 20 is tightly attached to the inner wall of the reaction tube 4, and the arrangement of the inclined edge 20 enables liquid to be tightly attached to the inner wall of the pipeline, so that the phenomenon that water splash is splashed due to too low liquid level of the liquid is prevented.

The working principle is as follows: when extraction is needed, a common solvent can be introduced into the reaction tube 4 through the connector, the control valve on the communicating tube 15 is closed, the sealing cover 21 is covered, liquid is not placed in the adding tube 5, at the moment, the piston 102 is moved up and down manually, circulating air blowing to the reagent tube 11 is achieved, the solvent in the reagent tube 11 is rolled, the purpose of extraction is achieved, viscous liquid can be added through the adding tube 5 and the air charging device 10, the control valve is closed, all liquid in the adding tube 5 is introduced into the reaction tube 11 through the through hole 14 through the air charging device 10, circulating air charging is continued, extraction is achieved, liquid separation can be achieved through the liquid outlet device 12 according to pressure difference after extraction is finished, and through the arrangement of the spray head 23, the surface of the side wall of the reaction tube 4 can be cleaned.

In summary, in the extraction apparatus for facilitating chemical reagent processing, the gas filling device 10 is manually controlled to close the sealing cover 21, press the piston 102 downward, and achieve liquid introduction through the connecting elbow 8, and the force of the pressing piston 102 can be controlled to achieve controlling the speed of solvent addition, the reaction tube 4 is communicated with the inner space of the reagent tube 11 through the through hole 14, so as to facilitate the gas flow and water flow entering the inner part of the reagent tube 11 from the middle of the inner part of the reaction tube 4, thereby achieving extraction operation, and the nozzle 23 is arranged to facilitate the water spraying onto the side wall of the reaction tube 4, so as to facilitate cleaning the surface of the side wall.

And, set up scale 22, the solvent can accurately add the solvent to in will letting in the solvent that adds in the pipe 5 effectively lets in the reaction tube 4 through aerating device 10, the setting of first sealed pad 6 and second sealed pad 7 can prevent that the inside gas of reaction tube 4 and interpolation pipe 5 from revealing, plays sealed effect, the setting of slope limit 20 makes the inner wall of pipeline can be hugged closely to liquid, prevents to produce the phenomenon that the splash splashes because the liquid level of liquid is low excessively.

It should be noted that, in this document, terms such as "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.

Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims

1. An extraction equipment convenient to chemical reagent processing, includes base (1), its characterized in that: the device comprises a base (1), supporting frames (2) are fixedly mounted on two sides of the top of the base (1), clamping frames (3) are fixedly mounted on the inner sides of the two supporting frames (2), reaction tubes (4) are arranged on the clamping frames (3), an adding tube (5) is fixedly mounted on the right side of each reaction tube (4), a first sealing gasket (6) and a second sealing gasket (7) are respectively arranged at inlets of the reaction tubes (4) and the adding tube (5), and the reaction tubes (4) and the adding tube (5) are communicated through connecting bent tubes (8); the right side of adding pipe (5) communicates with each other has feed liquor pipe (9), the top of feed liquor pipe (9) is provided with aerating device (10), the inside of reaction tube (4) is provided with reagent pipe (11), the bottom of reaction tube (4) is provided with out liquid device (12), the bottom of reagent pipe (11) communicates with each other has connector (13), through-hole (14) have evenly been seted up to the side of connector (13), the top of reaction tube (4) communicates with each other has communicating pipe (15), the top of reagent pipe (11) communicates with each other has into liquid head (16).

2. An extraction apparatus to facilitate chemical processing according to claim 1, wherein: be equipped with bifurcated pipe (17) on communicating pipe (15), and inlay on one side of communicating pipe (15) and be provided with control flap, the one end of bifurcated pipe (17) communicates with each other there is shower nozzle (23), bifurcated pipe (17) run through first sealed pad (6) and extend to the inside of reaction tube (4), it includes middle part pipe (18) and lateral part pipe (19) to advance liquid head (16), lateral part pipe (19) are located the both sides of middle part pipe (18), the intercommunicating pore has been seted up with lateral part pipe (19) relevant position to the both sides of middle part pipe (18).

3. An extraction apparatus to facilitate chemical processing according to claim 1, wherein: the end parts of the bifurcated pipe (17), the side pipe (19) and the connecting bent pipe (8) are all provided with inclined edges (20), and the inclined edges (20) are tightly attached to the inner wall of the reaction pipe (4).

4. An extraction apparatus to facilitate chemical processing according to claim 1, wherein: aerating device (10) are including trachea (101), piston (102), the one end of trachea (101) is run through and is added pipe (5) and extend to the inside of the sealed pad (7) of second, the one end of piston (102) extends to the outside of trachea (101), and the other end passes through the left and right sides overlap joint of extrusion piece and trachea (101) inner wall.

5. An extraction apparatus to facilitate chemical processing according to claim 1, wherein: one end, far away from the adding pipe (5), of the liquid inlet pipe (9) is movably connected with a sealing cover (21), and scales (22) are arranged on the surface of the adding pipe (5).

6. An extraction apparatus to facilitate chemical processing according to claim 1, wherein: the liquid outlet device (12) comprises an extension pipe (121) and a control valve core (122), the extension pipe (121) is communicated with the reaction pipe (4), a through groove matched with the control valve core (122) is formed in the extension pipe, the control valve core (122) is rotatably arranged on the extension pipe (121), and a one-way through hole (123) is formed in the control valve core (122).