CN105030973B - External application scalp care compositions, preparation with the refrigerant oil-control strengthen the hair effect of scalp and preparation method thereof - Google Patents
External application scalp care compositions, preparation with the refrigerant oil-control strengthen the hair effect of scalp and preparation method thereof Download PDFInfo
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Abstract
External application scalp care compositions, preparation with the refrigerant oil-control strengthen the hair effect of scalp and preparation method thereof, the invention discloses a kind of external medicine composition with the refrigerant oil-control strengthen the hair effect of scalp, the bulk drug matched by following weight parts is made：Witloof 30~60, radix scutellariae 20~60, selfheal 10~20, mulberry leaf 10~20, the fruit of medicinal cornel 10~20.The extract solution obtained after raw material compounding of the present invention through extraction is experimentally verified that non-stimulated to skin safe.Chinese medical extract and scalp care Essence not only have refrigerant, oil-control effect in itself, also with preferable strengthen the hair effect.The scalp care essence application method being prepared by extract of the present invention is simple, good absorbing effect.Easy, preparation method simplicity that the raw material of the present invention obtain, is easy to be esthetically acceptable to the consumers, has good application prospect and market prospects.
Description
Technical field
It is specifically a kind of that there is refrigerant scalp, oil-control and strengthen the hair work(the present invention relates to a kind of external nursing composition
The external application scalp care compositions of effect and the care formulations being prepared by the skin care compositions.
Background technology
Scalp care product effective object is head skin.Health scalp do not have itch, it is greasy, dry phenomena such as,
And scalp sebum secretion is moderate, follicular orifice will not be blocked.Easily sensitive and head skin is more slim, sebaceous glands density is relative
Larger, sebum secretion is vigorous, has essence different from face or body portion skin skin quality.In the market skin nursing products are a lot, but pin
To the product of scalp care but it is rarely found, the research for scalp health is also more rare.In addition people's scalp care consciousness is light
Thin, principal concern have ignored the importance of scalp health in the healthy with nursing above of hair.
Scalp is also a part for skin, and it has the structure similar with facial skin, but scalp is than facial skin more
Add fragile, more slim, the thickness of scalp is about 1.476 millimeters, and the thickness of skin is about 1.533 millimeters on cheek；
Scalp also has more sebaceous glands, and according to statistics, the sebaceous glands density on scalp is about 144~192/square centimeter, forehead
On be about 52~79/square centimeter, that on cheek is about then 42~78/square centimeter.This that is, even if
It is to be easiest to fuel-displaced forehead with face to compare, the sebaceous glands quantity of scalp also has as many as its twice.Scalp will more be focused on
Nursing, the problems such as scalp care product will be important to note that sensitivity.And commercially available conventional skin nursing products be also not particularly suited for it is special
Scalp skin quality.
At present, commercially available scalp care product is mainly combined with the hair care product such as shampoo and hair conditioner, is belonged to and is washed
Type product is removed, rinse-off products are limited in scalp residence time, and functional component addition is low, cause " scalp care product " can not
Real effect is played, is also easy to cause scalp tender subject.Summer weather is hot, dries；Summer scalp is easily led because of high temperature
The fuel-displaced excess of scalp is caused, how to recover scalp water and oil balance state, it is comfortably those skilled in the art's research to make scalp refrigerant
Focus.
The content of the invention
The primary and foremost purpose of the present invention is to propose a kind of external medicine composition with scalp oil-control and strengthen the hair effect.
Another object of the present invention is to propose a kind of preparation method of above-mentioned Chinese medicine composition.
The third object of the present invention is to propose a kind of scalp care preparation being prepared based on above-mentioned composition.
The present invention invention thinking be：
The present invention utilizes advanced biotechnology, with reference to the theory of traditional Chinese medical science of Chinese tradition, by witloof, radix scutellariae, selfheal, mulberry
Leaf and the fruit of medicinal cornel are effectively combined in together, form compound, and as active component, be prepared into scalp care preparation, it has
Having makes refrigerant scalp, oil-control and strengthen the hair and other effects.
Witloof：With clearing heat and detoxicating；The effect of inducing diuresis to remove edema.Cure mainly jaundice with damp-heat pathogen；Nephritic dropsy；Epigastric distending pain；Appetite
It is depressed.Also there is stomach invigorating and other effects.
Radix scutellariae：Bitter, it is cold in nature.Return lung, courage, spleen, large intestine, small intestinl channel.Major function：It is uncomfortable in chest to vomit for damp-warm syndrome, summer-heat and damp
Dislike, damp and hot feeling of fullness, rush down dysentery, jaundice, cough with lung heat, hyperpyrexia polydipsia, blood-head tells nosebleed, carbuncle sore tumefacting virus, fetal irritability.
Selfheal：Nature and flavor are pungent, bitter, tremble with fear.Return liver, gallbladder channel.Major function：It is dizzy for red eye, swell pain, mesh pearl nyctalgia, headache
It is dizzy, scrofula, goiter and tumor, acute mastitis, newborn addiction, swollen breasts.
Mulberry leaf：It is bitter, sweet, it is cold in nature.Return lung, Liver Channel.With dispelling wind and heat from the body, clearing away the lungheat and moisturizing, flat liver improving eyesight and cooling blood and hemostasis
The effect of.Major function：Anemopyretic cold, warm disease is from the beginning of cough with lung heat, liver-yang hyperactivity dizziness, hot eyes is dim-sighted, the cough of blood-heat bleeding
Blood, haematemesis.
The fruit of medicinal cornel：In meat etc., ripening fruits is Chinese medicine for nickname dogwood fruit, cornus officinalis sieb et zucc, mountain, for dizziness and tinnitus, soreness of waist and knee joint,
Impotence and seminal emission, enuresis frequent micturition, under uterine bleeding band, profuse sweating collapse.
To realize the purpose of the present invention, the present invention uses following concrete technical scheme：
A kind of external medicine composition with the refrigerant oil-control of scalp and strengthen the hair effect, wherein, the composition is by following
The bulk drug of weight is made：
Witloof 30~60, radix scutellariae 20~60, selfheal 10~20, mulberry leaf 10~20, the fruit of medicinal cornel 10~20.
The preferable weight of each bulk drug of composition is：
Witloof 40~60, radix scutellariae 40~60, selfheal 10~15, mulberry leaf 15~20, the fruit of medicinal cornel 15~20.
A kind of preparation method of above-mentioned external medicine composition, wherein, methods described step is as follows：
(1) each bulk drug is weighed according to above-mentioned weight, is well mixed after crushing respectively；
(2) plus percent by volume is that 60%~80% propane diols carries out ultrasonic extraction, and Extracting temperature is 40 DEG C~60 DEG C, when
Between be 30~60min, ultrasonic power is 300~500W；
(3) heating is stopped, extract solution prepared by step (2) filters after standing, then filters, and collects filtrate and produces.
The w/v g/mL of bulk drug and propane diols described in the step (2) is 1：8~1：12.
2~4 hours are stood in the step (3), after the filtering of 100~200 mesh, diatomite filter cake filters, the vacuum of suction filtration
Spend and produced for 0.06~0.1MPa, collection filtrate.
A kind of external application Chinese medicine extract with the refrigerant oil-control of scalp and strengthen the hair effect, wherein, the extract is by above-mentioned
Method extracts what is obtained.
Purposes of the said extracted thing in the external application scalp care preparation with the refrigerant oil-control of scalp and strengthen the hair effect is prepared.
A kind of external application scalp care preparation with the refrigerant oil-control of scalp and strengthen the hair effect, wherein, the preparation is by above-mentioned
Chinese medical extract and skin care field customary adjuvant are made.
A kind of external application scalp care compositions with the refrigerant oil-control of scalp and strengthen the hair effect, wherein, the composition is by A
Phase, B phases and C phase compositions, the A phases, B phases and C phases are made up of the raw material of following weight percentage：
A kind of preparation method of above-mentioned scalp care compositions, wherein, methods described comprises the following steps：
(1) A phases：Carbomer is uniformly sprinkling upon in water, stirred to being completely dissolved, adds A phase surplus stocks successively, stirring is equal
It is even, it is heated to 85 DEG C；
(2) when temperature is dropped to below 50 DEG C, B phase raw materials is added, are stirred；
(3) when temperature is dropped to below 45 DEG C, above-mentioned Chinese medical extract and C phase other raw materials is added, are stirred；Work as temperature
Degree drops to less than 40 DEG C, produces.
The preparation that above-mentioned raw materials and method are prepared is scalp care Essence.According to different, this external application using approach
Obtain active extract after scalp care compositions are extracted, it may also be fabricated which other external application scalp care preparations, as shampoo,
Hair conditioner etc., but above-mentioned formulation is not limited to, various differences can be made according to known method in scalp care product industrial circle
External preparation.
The preparation method of Chinese medicine composition provided by the present invention is not limited to of the present invention, other routines in the art
Method can also realize described effect, and the method for the invention is that inventor recommends preferable preparation method.This scalp care Essence
Composition in addition to extract is not customary adjuvant, the optimum formula obtained for inventor through creative work, and formula each group divides it
Between cooperate with work.
Essence of the present invention recommends method：Daily after cleaning scalp, Essence is coated on scalp, gently
Forlement, treat that Essence fully absorbs, without in secondary cleaning.
The beneficial outcomes of the present invention：
The extract solution obtained after raw material compounding of the present invention through extraction is experimentally verified that non-stimulated to skin safe.Traditional Chinese medicine extraction
Thing and scalp care Essence not only have refrigerant, oil-control effect in itself, also with preferable strengthen the hair effect.Extracted by the present invention
The scalp care essence application method that thing is prepared is simple, good absorbing effect.Easy, preparation that the raw material of the present invention obtain
Method is easy, is easy to be esthetically acceptable to the consumers, has good application prospect and market prospects.
Brief description of the drawings
The rate of change of Fig. 1 test sections skin oil and fat content；
Relative change rate (the * p of Fig. 2 test sections skin oil and fat content<0.05).
Embodiment
Medicinal material used in the present embodiment can be commercially available from China Medicament Group Corp., meet People's Republic of China's medicine
2005 editions standards of allusion quotation.Other raw materials can be obtained by commercially available purchase, and the present invention is shown in Table 1 using the source of raw material, institute of the present invention
Instrument title and producer are shown in Table 2.
The raw material sources of table 1
The instrument title of table 2 and producer
The preparation of the scalp care Chinese medical extract of the present invention of embodiment 1
(1) bulk drug is weighed according to following weight parts proportioning；
60 grams of witloof, 60 grams of radix scutellariae, 15 grams of selfheal, 20 grams of mulberry leaf, 20 grams of the fruit of medicinal cornel, are crushed to 80 mesh respectively, and mixing is equal
It is even to obtain composition；
(2) in composition plus percent by volume is that 70% propane diols carries out ultrasonic extraction, Extracting temperature is 45 DEG C, and the time is
30min, ultrasonic power 500W, the w/v g/mL of the bulk drug and propane diols is 1：10；
(3) heating is stopped, extract solution prepared by step (2) stands 2 hours, and after the filtering of 200 mesh, diatomite filter cake filters
Supernatant, vacuum 0.06MPa, collect smoke filtrate and produce.
The preparation of the scalp care Chinese medical extract of the present invention of embodiment 2
(1) bulk drug is weighed according to following weight parts proportioning；
30 grams of witloof, 40 grams of radix scutellariae, 20 grams of selfheal, 15 grams of mulberry leaf, 10 grams of the fruit of medicinal cornel, are crushed to 100 mesh respectively, and mixing is equal
It is even to obtain composition；
(2) percent by volume is added to carry out ultrasonic extraction, Extracting temperature 60 for 80% propane diols above-mentioned important composition
DEG C, time 60min, ultrasonic power 300W, the w/v g/mL of the Chinese medicine composition and propane diols is 1：12；
(3) heating is stopped, extract solution prepared by step (2) stands 3 hours, and after the filtering of 100 mesh, diatomite filter cake filters
Supernatant, vacuum 0.1MPa, collect smoke filtrate and produce.
The preparation of the scalp care Chinese medical extract of the present invention of embodiment 3
(1) bulk drug is weighed according to following weight parts proportioning；
40 grams of witloof, 20 grams of radix scutellariae, 10 grams of selfheal, 10 grams of mulberry leaf, 15 grams of the fruit of medicinal cornel, are crushed to 60 mesh respectively, and mixing is equal
It is even to obtain composition；
(2) percent by volume is added to carry out ultrasonic extraction, Extracting temperature 40 for 60% propane diols above-mentioned important composition
DEG C, time 40min, ultrasonic power 400W, the w/v g/mL of the Chinese medicine composition and propane diols is 1：8；
(3) heating is stopped, extract solution prepared by step (2) stands 4 hours, and after the filtering of 100 mesh, diatomite filter cake filters
Supernatant, vacuum 0.06MPa, collect smoke filtrate and produce.
The preparation of the scalp care Essence of the present invention of embodiment 4
Component and dosage, are shown in Table 3
Table 3
Preparation method
(1) A phases：Carbomer is uniformly sprinkling upon in water, quickly stirred to being completely dissolved, A phase surplus stocks is added successively, stirs
Mix uniformly, be heated to 85 DEG C；
(2) when temperature is dropped to below 50 DEG C, B phase raw materials is added, are stirred；
(3) when temperature is dropped to below 45 DEG C, add embodiment 1 and prepare extract and C phases other raw materials, stir；
When temperature drops to less than 40 DEG C, produce.
The preparation of the scalp care Essence of the present invention of embodiment 5
Component and dosage, are shown in Table 4
Table 4
Preparation method
(1) A phases：Carbomer is uniformly sprinkling upon in water, quickly stirred to being completely dissolved, A phase surplus stocks is added successively, stirs
Mix uniformly, be heated to 85 DEG C；
(2) when temperature is dropped to below 50 DEG C, B phase raw materials is added, are stirred；
(3) when temperature is dropped to below 45 DEG C, add embodiment 2 and prepare extract and C phases other raw materials, stir；
When temperature drops to less than 40 DEG C, produce.
The preparation of the scalp care Essence of the present invention of embodiment 6
Component and dosage, are shown in Table 5
Table 5
Preparation method
(1) A phases：Carbomer is uniformly sprinkling upon in water, quickly stirred to being completely dissolved, A phase surplus stocks is added successively, stirs
Mix uniformly, be heated to 85 DEG C；
(2) when temperature is dropped to below 50 DEG C, B phase raw materials is added, are stirred；
(3) when temperature is dropped to below 45 DEG C, add embodiment 3 and prepare extract and C phases other raw materials, stir；
When temperature drops to less than 40 DEG C, produce.
Efficacy experiments of the present invention
First, refrigerant efficacy study-human trial
1st, experiment material
Experiment condition：100 volunteers are randomly selected, men and women is unlimited, and the age is unlimited；
Given the test agent：Embodiment 4 prepares scalp care Essence 100,50 grams/；
The tested time：Summer, i.e. 6~August part；
2nd, experimental method
Trial product is provided to 100 volunteers, appropriate amount of sample is taken after having cleaned scalp daily, is applied on scalp, massage
To fully absorbing, filled in questionnaires according to actual conditions.
3rd, interpretation of result
Questionnaire investigation result is counted, volunteer can substantially feel that scalp has accounting for 75%, feeling that scalp has for cooling effect
Certain cooling effect account for 22%, do not feel cooling effect account for 3%.Inventor utilizes elite prepared by embodiment 5,6
Liquid repeats above-mentioned experiment, and experimental result is the same as above-mentioned.
2nd, oil-control effect experiment
1st, experimental principle
Human experimentation, test population is formed by particular experiment crowd, the scalp that test subject is prepared using embodiment protects
Skin oil and fat changes of contents before and after reason Essence, so that it is determined that suppression fat effect of cosmetics (or functional component).
2nd, laboratory apparatus and sample
Laboratory apparatus：Skin oil and fat tester
Sample：Embodiment 4 prepares scalp care Essence.
3rd, Subject Population
Subject amounts to 30 people.Specific sex composition and age composition determine at random.It is bad anti-that if period has 2 people to occur
Should, then terminate test；As a result adverse reaction is not found.
4th, experimental method
1. selection subject's head skin is marked, tested using half a head, i.e. left side scalp smears sample, right side scalp
Any product is not smeared, is blank control.
2. technical staff uses skin oil and fat testerTest test position 3 times, average,
It is designated as initial value.
3. subject tries out sample and smears scalp test zone, other can not be smeared during test oil-control effect oil-control production
Product.
4. scalp care Essence latter hour, two hours, four hours is being used continuously in subject, used by technical staff
Skin oil and fat testerMeasurement 3 times, averages.
5. counting the numerical value measured, its skin oil and fat changes of contents rule is analyzed.
5th, result and analysis
Within test period, this test event screens 30 people and includes research altogether, is come off between no group, and in tested crowd not
There is obvious systemic adverse reactions or more than 3 grades of skin irritatin, therefore effective volunteer's number of this test is 30 people.
△=Tn-T0
Rate of change (%)=((Tn-T0)/T0) × 100, this value is lower, and skin is fewer with time secretion oil quantity.
Relative change rate (%)=(((Tn-T0)-(KTn-KT0))/T0) × 100, this value is lower, illustrates relative comparison
Group, test section skin oil and fat content are fewer.
In formula, Tn --- tested region changes over time numerical value
T0 --- tested region initial value
KTn --- white space changes over time numerical value
KT0 --- white space initial value
As can be seen from Table 6, within 4 weeks test periods, after subject uses scalp care Essence, skin oil and fat content
It is in rise trend；Normal distribution analysis is carried out to data group using the softwares of SigmaStat 3.5, statistical result meets normal state point
Cloth, significance analysis is carried out to data using paired t-test method, at the 4th week, experimental group data relative comparison group, existed aobvious
Write sex differernce (p<0.05).
The statistical result (n=30) of scalp fat content before and after the product use of table 6
The rate of change value of scalp fat content and relative change rate see Fig. 1 and Fig. 2.
As seen from Figure 1, in test period 4h, after subject uses test sample, test section skin oil and fat content
It is in rise trend, but rate of change is below control group in 1h, 2h and 4h, illustrates that test section skin oil and fat content is few
In control group.
As seen from Figure 2, in test period 4h, after subject uses test sample, test section skin oil and fat content
Equal relative change rate is negative value in 1h, 2h and 4h, illustrates that test section skin oil and fat content is less than control group, and
Significant difference (p during 4h be present<0.05), i.e., sample has oil-control effect.Inventor utilizes Essence prepared by embodiment 5,6
Above-mentioned experiment is repeated, experimental result is the same as above-mentioned.
3rd, strengthen the hair effect-human experimentation
1st, experiment material
Experiment condition：Select the age in one full year of life 25 one full year of life~45, skin of head health without allergy or scar and without local system
The hair loss patient 72 of system property other diseases, male 48, women 24.
Given the test agent：Embodiment 4 prepares scalp care Essence 72,150 grams/；
The tested time：Summer, i.e. 6~August part；
2nd, experimental method
Volunteer is divided into two big groups, i.e. sample sets, blank group；24 males, 12 women are respectively included in each big group,
Six groups are separated into per big group, 6 people are randomly choosed per group.The situation tracking of advanced wardrobe hair health status, allows whole aspirations
Person is after first 15 days clean scalp according to personal habits, and after hair natural air drying, hair is combed daily with the oak comb of offer
Under 10, each number of shaving one's head of record, form is aggregated into.
Sample sets, according to personal habits, after cleaning scalp daily, appropriate Essence is taken, Essence is applied to scalp, pressed
Rub to fully absorbing, without cleaning again；Start to count for the 16th day in experiment, volunteer treated hair natural air drying every five days
Afterwards, combed with oak under hair 10, each number of shaving one's head of record, be aggregated into form.If to be done in time when there is adverse reaction
Record easy to remember, and the progress of termination test.
Blank group, according to personal habits, after cleaning scalp daily, hair natural air drying is treated, start to calculate for the 16th day in experiment
Rise, volunteer was combed under hair 10 every five days with oak, each number of shaving one's head of record, was aggregated into form.
This experiment amounts to three months, the first step 15 days by a definite date, second step 45 days by a definite date；In this experiment, volunteer can not be with
Meaning changes shampoo, and shampoo is selected according to respective custom, until experiment terminates.
3rd, interpretation of result
The sample sets of table 7 front and rear alopecia number on probation
The blank group of table 8 front and rear alopecia number on probation
According to above table, preparing nursing elite liquid energy using embodiment 4 reduces the quantity of trier's hair loss, illustrates to implement
Example 4, which prepares nursing Essence, strengthen the hair effect.The Essence that inventor is prepared using embodiment 5,6 repeats above-mentioned experiment, experiment
As a result with above-mentioned.
4th, human body patch is tested
First, test objective
Human experimentation, test population is formed by particular experiment crowd, test subject uses cosmetics (and cosmetics work(
Effect composition) the front and rear possibility for causing human body skin adverse reaction.
2nd, test material
Spot tries device：The production of Beijing North doctor's management of investment Co., Ltd, circular, diameter 12mm.
Spot tries thing：Example 4 prepares Essence 0.025g.
3rd, Subject Population and testing time
Effective subject amounts to 30 people, and specific sex composition and age composition determine (to meet 2007 at random《Cosmetics health
Specification》Include, exclusion standard.
Test the time started：On 06 03rd, 2014 on 06 05th, 2014.
4th, experimental method
1st, subject is selected by subject enrollment standard, number is 30.
2nd, from qualified patch material, sample is put into spot examination device (amount of samples is 0.020g~0.025g), control
Hole is blank (not putting any material).Sample and blank control are affixed on to the forearm song side of subject, is gently pressed and is allowed to palm
Equably it is pasted on skin, continues 24h.
3rd, 30min is spaced after removing spot examination device, dermoreaction is observed after impression disappearance.
4th, 24h and 48h is observed once again respectively after patch test, observes dermoreaction.
5th, skin adverse reaction grade scale is shown in Table 9：
5th, experimental result
The skin adverse reaction of table 9 is classified
Table 10 takes out 0.5 hour observation result of spot examination device
Table 11 removes 24 hours observation results of spot examination device
Table 12 removes 48 hours observation results of spot examination device
Explained according to skin closure type patch test results：Occurs the number of 1 grade of skin adverse reaction in 30 subjects
More than 5, or the number of 2 grades of skin adverse reactions is more than 2, or any 13 grades or more than 3 grades skin adverse reactions occurs
When, judge that tested material has adverse reaction to human body.
Skin closure type patch test results are shown in Table 10,11 and 12, are shown according to result, sample is to human body skin without bad
Reaction.The product that inventor is prepared using other embodiment repeats above-mentioned experiment, and experimental result is the same as above-mentioned.
Claims (10)
- A kind of 1. external medicine composition with the refrigerant oil-control of scalp and strengthen the hair effect, it is characterised in that the external application Chinese medicine The bulk drug that composition is matched by following weight parts is made：Witloof 30~60, radix scutellariae 20~60, selfheal 10~20, mulberry leaf 10~20, Fructus Corni 10~20.
- 2. external medicine composition as claimed in claim 1, it is characterised in that the bulk drug matched by following weight parts is made：Witloof 40~60, radix scutellariae 40~60, selfheal 10~15, mulberry leaf 15~20, Fructus Corni 15~20.
- A kind of 3. preparation method of the external medicine composition of claim 1 or 2, it is characterised in that the preparation method step It is rapid as follows：(1) each bulk drug is weighed according to the weight of claim 1 or 2, is well mixed after crushing respectively；(2) plus percent by volume is that 60%~80% propane diols carries out ultrasonic extraction, and Extracting temperature is 40 DEG C~60 DEG C, and the time is 30~60min, ultrasonic power are 300~500W；(3) heating is stopped, extract solution prepared by step (2) filters after standing, then filters, and collects filtrate and produces.
- 4. preparation method as claimed in claim 3, it is characterised in that bulk drug described in the step (2) and propane diols W/v g/mL is 1：8~1：12.
- 5. preparation method as claimed in claim 3, it is characterised in that 2~4 hours are stood in the step (3), 100~200 After mesh filtering, diatomite filter cake filters, and the vacuum of suction filtration is 0.06~0.1MPa, collects filtrate and produces.
- A kind of 6. external application Chinese medicine extract with the refrigerant oil-control of scalp and strengthen the hair effect, it is characterised in that the external application Chinese medicine Extract is extracted to obtain by any one methods described in claim 3 to 5.
- 7. external application Chinese medicine extract described in claim 6 is preparing the shield of the external application scalp with the refrigerant oil-control of scalp and strengthen the hair effect Manage the purposes in preparation.
- A kind of 8. external application scalp care preparation with the refrigerant oil-control of scalp and strengthen the hair effect, it is characterised in that the external application head Skin care formulations external application Chinese medicine extract and skin care field customary adjuvant as described in claim 6 are made.
- A kind of 9. external application scalp care compositions with the refrigerant oil-control of scalp and strengthen the hair effect, it is characterised in that the external application Scalp care compositions are made up of A phases, B phases and C phase compositions, the A phases, B phases and C phases the raw material of following weight percentage：0.25~0.50wt% of B phase sodium hydroxides
- A kind of 10. preparation method of external application scalp care compositions described in claim 9, it is characterised in that the preparation method Comprise the following steps：(1) A phases：Carbomer is uniformly sprinkling upon in water, stirred to being completely dissolved, A phase surplus stocks is added successively, stirs, It is heated to 85 DEG C；(2) when temperature is dropped to below 50 DEG C, B phase raw materials is added, are stirred；(3) when temperature is dropped to below 45 DEG C, external application Chinese medicine extract and C phase other raw materials described in claim 6 is added, are stirred Uniformly；When temperature drops to less than 40 DEG C, produce.
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