CN105028868B - A kind of black onion black soya bean peptide chewable tablets of black garlic and preparation method thereof - Google Patents
A kind of black onion black soya bean peptide chewable tablets of black garlic and preparation method thereof Download PDFInfo
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Abstract
The invention discloses black onion black soya bean peptide chewable tablets of a kind of black garlic and preparation method thereof, which is made of the raw material of following parts by weight：7 11 parts of black garlic powder, 48 parts of black onion powder, 12 18 parts of black soya bean peptide zymolyte, 15 20 parts of konjaku flour, 20 50 parts of sucrose, 12 18 parts of synanthrin, 18 25 parts of fructose syrup, 0.8 1.5 parts of citric acid, 36 parts of sodium carboxymethylcellulose, 0 0.3 parts of essence, 0.9 1.1 parts of magnesium stearate.This method includes pretreatment of raw material, mixing preparation, makes the techniques such as softwood, wet granulation, drying, tabletting, sterilizing, packaging.The present invention chewable tablets surface is smooth, delicate mouthfeel, sweet and sour taste, palatability are good, easy to carry and edible, Storage and stability are preferable, without side-effects, and edible safety is higher, full of nutrition, the healthcare function with black-food；The manufacture craft of the present invention is simple, is easy to industrialized production.
Description
Technical field
The present invention relates to a kind of chewable tablets and preparation method thereof, and in particular to a kind of black onion black soya bean peptide chewable tablets of black garlic and
Its preparation method, belongs to functional food processing technique field.
Background technology
The allegro modern life and the social pressures of high competition make many people be in sub-health state, as people live
Horizontal and health care consciousness raising, consumer is growing day by day to convenient, fast, nutrition demand, and chewable tablets is as a kind of convenient
Instant snack food comes into being.
Black garlic is to pass through food made of spontaneous fermentation under certain temperature and humidity conditions with fresh raw garlic, and black garlic is not only
It is to remove acid, and on the basis of the original composition of raw garlic is remained, by promoting enzyme bioconversion, improves anti-oxidant work
Property, adds the nutrient composition contents such as amino acid, vitamin, polysaccharide, mineral matter, and generate Polyphenols, free amine group acids,
The effect of diallyl disulfide and diallyl trisulfide, β-carboline Alkaloids etc. are new component, has extremely strong
Anti-oxidant, the enhancing health-care effect such as physical, antifatigue.
Black onion is after fresh onion is pre-processed, to ferment what is obtained after a certain period of time under the conditions of constant temperature and humidity,
The penetrating odor of onion in itself is eliminated in fermentation process, enhances original physiological activity.Onion fermentation after organic sulfur compound,
Maillard reaction product, the enhancing of polyphenol isoreactivity component.Research show black onion have alleviate diabetes, hypoglycemic, reducing blood lipid,
Blood pressure lowering, suppress coagulating platelets, inhibit bacteria breeding, anti-aging, the formation for hindering nitrosamine, prevention and resistance cancer etc.
Physiological function.
Black soya bean peptide is the short chain being made of amino acid residue molecular that is obtained through protease hydrolytic using black soya bean albumen as raw material
Material.Science confirm Functional Polypeptides can not only play maintenance and improve protein nutrition condition, can also play weight-reducing body shaping,
The special physiological roles such as beautifying face and moistering lotion, norcholesterol, anti-oxidant, blood pressure lowering, improvement sleep, improvement angiocardiopathy, and
And it is beneficial to the absorption and digestion of the various electrolytes and minerals of human body.Black soya bean peptide has the health care of black soya bean and Functional Polypeptides concurrently at the same time
Effect.
Chinese patent CN102669527B discloses a kind of black garlic chewable tablet and preparation method thereof, and this method is with black big
Garlic ground-slag, xylitol and black rice flour for raw material through pelletizing, drying, whole grain, beat piece and black garlic chewable tablet be made, which makes black
Garlic, which is developed, to be applied, but the chewable tablets only has the health-care efficacy of black garlic and black rice.
At present, the chewable tablets using black garlic, black onion, black soya bean peptide as primary raw material has no report.
The content of the invention
An object of the present invention is to provide a kind of black onion black soya bean peptide chewable tablets of black garlic, can improve garlic, onion, black
The comprehensive utilization ratio of beans peptide, strengthens the nutritional health function of product, easy to carry, easily storage.
The second object of the present invention is to provide the preparation method of above-mentioned chewable tablets, and technique is simple.
For achieving the above object, the black onion black soya bean peptide chewable tablets of black garlic of the invention, by the raw material of following parts by weight
It is made：7-11 parts of black garlic powder, onion powder 4-8 parts black, 12-18 parts of black soya bean peptide zymolyte, 15-20 parts of konjaku flour, sucrose 20-50
Part, 12-18 parts of synanthrin, 18-25 parts of fructose syrup, 0.8-1.5 parts of citric acid, 3-6 parts of sodium carboxymethylcellulose, essence 0-0.3
Part, 0.9-1.1 parts of magnesium stearate.
Preferably, the black onion black soya bean peptide chewable tablets of the black garlic, is made of the raw material of following parts by weight：Black garlic powder
9 parts, 6 parts of black onion powder, 15 parts of black soya bean peptide zymolyte, 15 parts of konjaku flour, 30 parts of sucrose, 15 parts of synanthrin, 20 parts of fructose syrup, lemon
1 part of lemon acid, 4 parts of sodium carboxymethylcellulose, 0.2 part of essence, 1 part of magnesium stearate.
The preparation method of the above-mentioned black onion black soya bean peptide chewable tablets of black garlic, including following procedure of processing：
A, black garlic powder and black onion powder are prepared：To be fermented complete black garlic, the peeling of black onion, be cleaned with circulating water and be removed table
The dust in face, 8-12h is dried in vacuo under the conditions of -0.1Mpa, 50-60 DEG C, through ultramicro grinding obtain 25-40 μm black garlic powder,
Black onion powder；
B, black soya bean peptide zymolyte is prepared：By black soya bean and water with material-water ratio 1:10-1:20 mashing, with food sodium hydroxide tune
Section pH is 8-9, adds 2-5% protease, 3.5-4h is digested under the conditions of 40-60 DEG C, is heated to 90-100 DEG C of enzyme deactivation 5-
10min, centrifugation, residue is 4-5 with food grade salt acid for adjusting pH, centrifugation, and taking precipitate adds 2 times of distillation water washings, centrifugations twice,
Merge supernatant, add 2-3% cyclodextrin, 60-70 DEG C of absorption 30-45min takes off hardship, vacuum-concentrcted, vacuum freeze drying
After obtain black soya bean peptide zymolyte；
C, softwood is made：Major ingredient black garlic powder, black onion powder, black soya bean peptide zymolyte are weighed by formula rate, adds auxiliary material evil spirit
Taro powder, sucrose, synanthrin, fructose syrup, citric acid, sodium carboxymethylcellulose, essence, put into mixer and are uniformly mixed, mixed
The edible ethanol that concentration is 40-90% is slowly added in compound material softwood is made, its hardness is pinched agglomerating with hand, and light pressure, which dissipates, is
It is accurate；
D, granulation and drying：The softwood that step C is obtained is spray-dried, and gained particle is crossed 20 mesh sieves, is placed 30-
60min makes edible ethanol volatilize completely, the dry 0.5-1h at 50-60 DEG C；
E, tabletting：Magnesium stearate is added after granulation, 30-45min is stood, in 10-15MPa condition lower sheetings；
F, sterilizing, packaging：Gained chewable tablets is subjected to ultraviolet disinfection 20-30min, is steeped after sterilizing using nitrogen charging single dose
Bonnet hot press seal mode or the bottled mode of multiple dose pack, preservation under room temperature.
Preferably, protease described in step B is in flavor protease, alkali protease or neutral proteinase
One kind.
Preferably, enzymatic hydrolysis condition is described in step B：The material-water ratio of black soya bean and water is 1:15-1:20, add 2-
3% protease, digests 3.5-4h under the conditions of 50-60 DEG C.
Preferably, the dosage of edible ethanol described in step C accounts for the 6-10% of mixed material weight.
Beneficial effects of the present invention are as follows：
1st, chewable tablets surface of the invention is smooth, delicate mouthfeel, sweet and sour taste, palatability are good, easy to carry and edible, stores
Tibetan property and stability are preferable, are used suitable for wine assistant, remaining meal, leisure；
2nd, black garlic and black onion are food in itself, and black soya bean peptide eventually becomes amino acid or water, no secondary work through body metabolism
With, edible safety is high, and above-mentioned each raw material, by cooperating and promoting, the health-care efficacy of black-food greatly improves,
To be got well relative to the effect reached using a kind of raw material merely, while also there are the nutrition health-care functions of Functional Polypeptides；
3rd, the present invention retains preferably neutraceutical active ingredients in raw material, caters to consumer to health without extreme processing conditions
The demand of food；
4th, the present invention is metabolized, suitable diabetes, obesity trouble unrelated with insulin in vivo using synanthrin as sweetener
Eating for the special populations such as person, also acts on anti-caries；
5th, manufacture craft of the invention is simple, and manufacture cost is low, is suitable for industrialized production.
Embodiment
The present invention is described in further detail with reference to specific embodiment.
Embodiment 1
A kind of black onion black soya bean peptide chewable tablets of black garlic, is made of the raw material of following parts by weight：9 parts of black garlic powder, black onion powder 6
Part, 15 parts of black soya bean peptide zymolyte, 15 parts of konjaku flour, 30 parts of sucrose, 15 parts of synanthrin, 20 parts of fructose syrup, 1 part of citric acid, carboxylic first
4 parts of base sodium cellulosate, 0.2 part of essence, 1 part of magnesium stearate.
The preparation method of the above-mentioned black onion black soya bean peptide chewable tablets of black garlic, comprises the following steps：
A, black garlic powder and black onion powder are prepared：To be fermented complete black garlic, the peeling of black onion, be cleaned with circulating water and be removed table
The dust in face, 12h is dried in vacuo under the conditions of -0.1Mpa, 50 DEG C, and 25-40 μm of black garlic powder, black onion are obtained through ultramicro grinding
Powder；
B, black soya bean peptide zymolyte is prepared：By black soya bean and water with material-water ratio 1:20 mashing, with 1mol/L food sodium hydroxides
It is 8.5 to adjust pH, adds 2% flavor protease, digests 4h under the conditions of 50 DEG C, 100 DEG C of enzyme deactivation 8min are heated to, with 4000r/
Min centrifuges 20min, and residue is 4.5 with 1moL/L food grade salts acid for adjusting pH, and 20min, taking precipitate are centrifuged with 4000r/min
Add 2 times of distillation water washings, centrifugations twice, merge supernatant, add 3% cyclodextrin, 65 DEG C of absorption 30min take off hardship, vacuum decompression
Concentration, obtain black soya bean peptide zymolyte after vacuum freeze drying again；
C, softwood is made：Major ingredient black garlic powder, black onion powder, black soya bean peptide zymolyte are weighed by formula rate, adds auxiliary material evil spirit
Taro powder, sucrose, synanthrin, fructose syrup, citric acid, sodium carboxymethylcellulose, essence, put into mixer and are uniformly mixed, mixed
Softwood is made in the edible ethanol that the concentration for being slowly added to account for mixed material weight 9% in compound material is 60%, its hardness is pinched with hand
Agglomerating, light pressure is subject to dissipating；
D, granulation and drying：The softwood that step C is obtained is spray-dried, and gained particle is crossed 20 mesh sieves, and placing 50min makes
Edible ethanol volatilizees completely, the dry 0.5h at 60 DEG C；
E, tabletting：Magnesium stearate is added after granulation, 30min is stood, in 12MPa condition lower sheetings；
F, sterilizing, packaging：Gained chewable tablets is subjected to ultraviolet disinfection 30min, nitrogen charging single dose blister is used after sterilizing
Mode is sealed in formula hot pressing or the bottled mode of multiple dose packs, preservation under room temperature.
The color and luster of the chewable tablets, fragrance, mouthfeel, texture are evaluated respectively, evaluation criteria is shown in Table 1.
The black onion black soya bean peptide chewable tablets sensory evaluation scores table of 1 black garlic of table
Its specific sensory evaluation is as follows：Chewable tablets is in black, and color and luster is homogeneous, and shape is complete, and surface is smooth, has flavor water
Fruity, smell are coordinated, delicate mouthfeel, sweet and sour taste, and hardness is moderate.
Embodiment 2
A kind of black onion black soya bean peptide chewable tablets of black garlic, is made of the raw material of following parts by weight：7 parts of black garlic powder, black onion powder 8
Part, 12 parts of black soya bean peptide zymolyte, 18 parts of konjaku flour, 20 parts of sucrose, 18 parts of synanthrin, 25 parts of fructose syrup, 0.8 part of citric acid, carboxylic
3 parts of sodium carboxymethylcellulose pyce, 0.9 part of magnesium stearate.
The preparation method of the above-mentioned black onion black soya bean peptide chewable tablets of black garlic, including following procedure of processing：
A, black garlic powder and black onion powder are prepared：To be fermented complete black garlic, the peeling of black onion, be cleaned with circulating water and be removed table
The dust in face, 12h is dried in vacuo under the conditions of -0.1Mpa, 50 DEG C, and 25-40 μm of black garlic powder, black onion are obtained through ultramicro grinding
Powder；
B, black soya bean peptide zymolyte is prepared：By black soya bean and water with material-water ratio 1:10 mashing, with 1mol/L food sodium hydroxides
It is 8 to adjust pH, adds 3% alkali protease, digests 3.5h under the conditions of 50 DEG C, 100 DEG C of enzyme deactivation 5min are heated to, with 4000r/
Min centrifuges 20min, and residue is 4 with 1moL/L food grade salts acid for adjusting pH, centrifuges 20min with 4000r/min, taking precipitate adds 2
Times distillation water washing, centrifugation twice, merge supernatant, add 2% cyclodextrin, 60 DEG C absorption 40min take off hardship, vacuum decompression is dense
Contracting, obtain black soya bean peptide zymolyte after vacuum freeze drying again；
C, softwood is made：Major ingredient black garlic powder, black onion powder, black soya bean peptide zymolyte are weighed by formula rate, adds auxiliary material evil spirit
Taro powder, sucrose, synanthrin, fructose syrup, citric acid, sodium carboxymethylcellulose, essence, put into mixer and are uniformly mixed, mixed
Softwood is made in the edible ethanol that the concentration for being slowly added to account for mixed material weight 6% in compound material is 40%, its hardness is pinched with hand
Agglomerating, light pressure is subject to dissipating；
D, granulation and drying：The softwood that step C is obtained is spray-dried, and gained particle is crossed 20 mesh sieves, and placing 60min makes
Edible ethanol volatilizees completely, the dry 1h at 50 DEG C；
E, tabletting：Magnesium stearate is added after granulation, 40min is stood, in 10MPa condition lower sheetings；
F, sterilizing, packaging：Gained chewable tablets is subjected to ultraviolet disinfection 20min, nitrogen charging single dose blister is used after sterilizing
Mode is sealed in formula hot pressing or the bottled mode of multiple dose packs, preservation under room temperature.
Its specific sensory evaluation is as follows：Chewable tablets is in black, and color and luster is homogeneous, and shape is complete, and surface is smooth, and essence taste is not
Foot, smell are relatively coordinated, delicate mouthfeel, sweet and sour taste, and hardness is moderate.
Embodiment 3
A kind of black onion black soya bean peptide chewable tablets of black garlic, is made of the raw material of following parts by weight：11 parts of black garlic powder, black onion powder
4 parts, 18 parts of black soya bean peptide zymolyte, 20 parts of konjaku flour, 50 parts of sucrose, 12 parts of synanthrin, 18 parts of fructose syrup, 1.5 parts of citric acid, carboxylic
6 parts of sodium carboxymethylcellulose pyce, 0.3 part of essence, 1.1 parts of magnesium stearate.
The preparation method of the above-mentioned black onion black soya bean peptide chewable tablets of black garlic, including following procedure of processing：
A, black garlic powder and black onion powder are prepared：To be fermented complete black garlic, the peeling of black onion, be cleaned with circulating water and be removed table
The dust in face, 12h is dried in vacuo under the conditions of -0.1Mpa, 50 DEG C, and 25-40 μm of black garlic powder, black onion are obtained through ultramicro grinding
Powder；
B, black soya bean peptide zymolyte is prepared：By black soya bean and water with material-water ratio 1:15 mashing, with 1mol/L food sodium hydroxides
It is 9 to adjust pH, adds 5% neutral proteinase, digests 3.5h under the conditions of 40 DEG C, 90 DEG C of enzyme deactivation 10min are heated to, with 4000r/
Min centrifuges 20min, and residue is 5 with 1moL/L food grade salts acid for adjusting pH, centrifuges 20min with 4000r/min, taking precipitate adds 2
Times distillation water washing, centrifugation twice, merge supernatant, add 2% cyclodextrin, 70 DEG C absorption 45min take off hardship, vacuum decompression is dense
Contracting, obtain black soya bean peptide zymolyte after vacuum freeze drying again；
C, softwood is made：Major ingredient black garlic powder, black onion powder, black soya bean peptide zymolyte are weighed by formula rate, adds auxiliary material evil spirit
Taro powder, sucrose, synanthrin, fructose syrup, citric acid, sodium carboxymethylcellulose, essence, put into mixer and are uniformly mixed, mixed
Softwood is made in the edible ethanol that the concentration for being slowly added to account for mixed material weight 10% in compound material is 90%, its hardness is pinched with hand
Agglomerating, light pressure is subject to dissipating；
D, granulation and drying：The softwood that step C is obtained is spray-dried, and gained particle is crossed 20 mesh sieves, and placing 30min makes
Edible ethanol volatilizees completely, the dry 45min at 55 DEG C；
E, tabletting：Magnesium stearate is added after granulation, 45min is stood, in 15MPa condition lower sheetings；
F, sterilizing, packaging：Gained chewable tablets is subjected to ultraviolet disinfection 30min, nitrogen charging single dose blister is used after sterilizing
Mode is sealed in formula hot pressing or the bottled mode of multiple dose packs, preservation under room temperature.
Its specific sensory evaluation is as follows：Chewable tablets is in black, and color and luster is homogeneous, and shape is complete, and surface is smooth, is had light
Essence fruity, smell are coordinated, delicate mouthfeel, sweet and sour taste, and hardness is moderate.
Claims (5)
1. a kind of black onion black soya bean peptide chewable tablets of black garlic, it is characterised in that be made of the raw material of following parts by weight：Black garlic powder 7-11
Part, onion powder 4-8 parts black, 12-18 parts of black soya bean peptide zymolyte, 15-20 parts of konjaku flour, 20-50 parts of sucrose, 12-18 parts of synanthrin, fruit
18-25 parts of glucose slurry, 0.8-1.5 parts of citric acid, 3-6 parts of sodium carboxymethylcellulose, 0-0.3 parts of essence, magnesium stearate 0.9-1.1
Part；It is prepared by following steps：
A, black garlic powder and black onion powder are prepared：To be fermented complete black garlic, the peeling of black onion, be cleaned with circulating water and be removed surface
Dust, 8-12h is dried in vacuo under the conditions of -0.1Mpa, 50-60 DEG C, and 25-40 μm of black garlic powder, Hei Yang is obtained through ultramicro grinding
Green onion powder；
B, black soya bean peptide zymolyte is prepared：By black soya bean and water with material-water ratio 1:10-1:20 mashing, pH is adjusted with food sodium hydroxide
For 8-9,2-5% protease is added, 3.5-4h is digested under the conditions of 40-60 DEG C, is heated to 90-100 DEG C of enzyme deactivation 5-10min, from
The heart, residue are 4-5 with food grade salt acid for adjusting pH, centrifugation, and taking precipitate adds 2 times of distillation water washings, centrifugations twice, merges supernatant
Liquid, addition 2-3% cyclodextrin, 60-70 DEG C of absorption 30-45min take off hardship, black soya bean are obtained after vacuum-concentrcted, vacuum freeze drying
Peptide zymolyte；
C, softwood is made：Weigh major ingredient black garlic powder, black onion powder, black soya bean peptide zymolyte by formula rate, add auxiliary material konjaku flour,
Sucrose, synanthrin, fructose syrup, citric acid, sodium carboxymethylcellulose, essence, put into mixer and are uniformly mixed, in mixed material
In be slowly added to the edible ethanol that concentration is 40-90% softwood be made, its hardness pinched with hand it is agglomerating, subject to light pressure dissipates；
D, granulation and drying：The softwood that step C is obtained is spray-dried, and gained particle is crossed 20 mesh sieves, and placing 30-60 min makes
Edible ethanol volatilizees completely, the dry 0.5-1h at 50-60 DEG C；
E, tabletting：Magnesium stearate is added after granulation, 30-45min is stood, in 10-15MPa condition lower sheetings；
F, sterilizing, packaging：Gained chewable tablets is subjected to ultraviolet disinfection 20-30min, nitrogen charging single dose blister formula is used after sterilizing
Mode is sealed in hot pressing or the bottled mode of multiple dose packs, preservation under room temperature.
2. the black onion black soya bean peptide chewable tablets of black garlic as claimed in claim 1, it is characterised in that by the raw material system of following parts by weight
Into：9 parts of black garlic powder, 6 parts of black onion powder, 15 parts of black soya bean peptide zymolyte, 15 parts of konjaku flour, 30 parts of sucrose, 15 parts of synanthrin, high fructose corn
20 parts of slurry, 1 part of citric acid, 4 parts of sodium carboxymethylcellulose, 0.2 part of essence, 1 part of magnesium stearate.
3. the black onion black soya bean peptide chewable tablets of black garlic as claimed in claim 1 or 2, it is characterised in that protease described in step B
One kind in flavor protease, alkali protease or neutral proteinase.
4. the black onion black soya bean peptide chewable tablets of black garlic as claimed in claim 1 or 2, it is characterised in that digest bar described in step B
Part is：The material-water ratio of black soya bean and water is 1:15-1:20,2-3% protease is added, 3.5-4h is digested under the conditions of 50-60 DEG C.
5. the black onion black soya bean peptide chewable tablets of black garlic as claimed in claim 1 or 2, it is characterised in that second is eaten described in step C
The dosage of alcohol accounts for the 6-10% of mixed material weight.
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| CN105285104B (en) * | 2015-11-23 | 2019-08-23 | 徐州工程学院 | A kind of black onion health care yoghourt of low fat Low lactose milk black garlic and preparation method thereof |
| CN105238670B (en) * | 2015-11-23 | 2018-07-27 | 徐州工程学院 | A kind of black onion health-care vinegar of compound blank corn and preparation method thereof |
| CN105410915B (en) * | 2015-12-03 | 2018-03-30 | 广东益生康生物科技有限公司 | A kind of black garlic soybean peptide oral liquid and preparation method thereof |
| CN106072568A (en) * | 2016-07-04 | 2016-11-09 | 徐州工程学院 | A kind of Bulbus Allii Cepae nutrient chewable tablet and preparation method thereof |
| CN107912777A (en) * | 2017-12-31 | 2018-04-17 | 山东禹泽医药科技有限公司 | A kind of compound peptide product with antioxidation |
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| CN112890206A (en) * | 2021-01-28 | 2021-06-04 | 麦和(广州)实业有限公司 | Black bean oligopeptide embedded substance and preparation method thereof |
| CN112980638A (en) * | 2021-04-16 | 2021-06-18 | 徐州工程学院 | Composite black fermented fruit wine and preparation method thereof |
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| CN101606566A (en) * | 2008-06-18 | 2009-12-23 | 刁媛媛 | The preparation method and the application of a kind of functional chewing and mouthful disintegrating tablet candy |
| KR101331991B1 (en) * | 2011-05-09 | 2013-11-25 | 허승재 | Functional black garlic pill and manufacturing method thereof |
| CN102302165B (en) * | 2011-07-20 | 2013-02-13 | 徐州绿之野生物食品有限公司 | Fermented black garlic residue powder and preparation method thereof |
| CN102669527B (en) * | 2012-05-25 | 2013-09-25 | 徐州绿之野生物食品有限公司 | Black garlic chewing tablets and preparation method thereof |
| CN103445105A (en) * | 2013-01-05 | 2013-12-18 | 徐州绿之野生物食品有限公司 | Black garlic chewable tablet and preparation method thereof |
| CN103734639A (en) * | 2013-12-23 | 2014-04-23 | 天津市傲绿农副产品集团股份有限公司 | Preparation method of chewable black garlic tablet |
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