CN105013424A - Production device for oil-soluble thermal reaction flavor - Google Patents
Production device for oil-soluble thermal reaction flavor Download PDFInfo
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- CN105013424A CN105013424A CN201510521684.4A CN201510521684A CN105013424A CN 105013424 A CN105013424 A CN 105013424A CN 201510521684 A CN201510521684 A CN 201510521684A CN 105013424 A CN105013424 A CN 105013424A
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Abstract
The invention discloses a production device for oil-soluble thermal reaction flavor. The production device mainly comprises a reaction kettle body, a condenser, an extraction kettle, a buffer tank and conveying pipelines among the components, wherein mixed steam with aroma, generated during the thermal reaction process in the reaction kettle body sequentially passes through the condenser, extraction kettle and buffer tank, and finally flows back into the reaction kettle body to form a cycle; after the end of the thermal reaction, an oil phase in the extraction kettle is the flavor product. According to the device provided by the invention, aroma components generated during the thermal reaction process are separated and concentrated in the oil phase of the extraction tank, so that the aroma intensity of the obtained flavor is high; required aroma intensity or concentration multiple can be obtained through adjusting the rate of the oil phase to the water phase; the flavor is transparent, so that the color and lustre of the product are not influenced; moreover, the flavor produced by adopting the device is oil-soluble flavor which is high in heat resistance and suitable for candies, baked products and the like.
Description
Technical field
The present invention relates to a kind of technology of food processing field, particularly a kind of process units of oil-soluble hot reaction essence, can be used for the working system of hot reaction essence.
Background technology
Hot reaction essence mainly produces the process of fragrance and the essence developed by simulated foods in heating process, has fragrance true to nature, mellow in taste and the advantage such as high temperature resistant.The process units mainly reactor of current hot reaction essence, Zhejiang Province Green Crystal Flavor Co., Ltd discloses a kind of process units (CN203247245 U) of thermal process flavourings, reaction kettle body and blending tank are organically combined, easy production technology, but this process units is not suitable for the production of clear shape hot reaction essence.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, a kind of process units by thermal process flavourings is provided, is applicable to the production of transparence oil-soluble thermal process flavourings.
For achieving the above object, the technical solution used in the present invention is: a kind of process units of hot reaction essence, primarily of the transfer pipeline composition between reaction kettle body, condenser, extraction kettle, surge tank and each parts; Described reaction kettle body is provided with mixed vapour outlet and return-flow catheter, and described return-flow catheter stretches into reaction kettle body inner chamber; Described condenser is provided with steam inlet and condensate outlet; Described extraction kettle is provided with liquid distributor and material liquid outlet; Described surge tank is provided with feed conduit and discharging opening, and described feed conduit stretches into surge tank inner chamber; Described mixed vapour outlet is connected with steam inlet pipeline; Described condensate outlet is connected with liquid distributor pipeline, and described condensate outlet is also connected with return-flow catheter pipeline; Described material liquid outlet is connected with feed conduit pipeline; Described discharging opening is connected with return-flow catheter connecting pipe road, and pipeline is in " U " shape; The height of described liquid distributor lower section is higher than the height of feed conduit, and the height of feed conduit is higher than the height of return-flow catheter;
In technique scheme, described reaction kettle body is also provided with dog-house, agitating device, temperature control interlayer, temperature sensor, drain hole, pressure sensor and safety valve; Described temperature controls can admittance deep fat, high-temperature steam or frozen water in interlayer.
In technique scheme, described condenser is the one in shell and tube condenser, jacket type condenser or coiler type condenser.
In technique scheme, described extraction kettle is also provided with and controls interlayer by feed conduit and temperature; Described temperature controls can lead to hot water or frozen water in interlayer.
Hot reaction essence process units of the present invention, compared with prior art, has following advantage:
1) this device makes the oil phase of fragrance component in extractor produced in thermal process reactor realize isolation and identification, and the essence aroma strength obtained is strong, and by adjusting the ratio of oil phase and aqueous phase, obtains required aroma strength or cycles of concentration.
2) produce by apparatus of the present invention the essence obtained and present transparence, do not affect the color and luster of application product.
3) apparatus of the present invention produce the essence obtained is oil soluble perfume, and heat resistance is strong, the product such as be applicable to candy or cure.
4) condensed fluid flows to distributional effects through liquid distributor in extractor through condenser, condensed fluid is fully contacted with oil phase, realizes effective separation of fragrance.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the specific embodiment of the present invention is described in further detail.
Fig. 1 is the primary structure schematic diagram of oil-soluble thermal process flavourings process units of the present invention.
Detailed description of the invention
Below in conjunction with instantiation, technical scheme of the present invention is described further.
Embodiment 1:
Fig. 1 gives a kind of process units of oil-soluble thermal process flavourings, primarily of the transfer pipeline composition between reaction kettle body 1, condenser 2, extraction kettle 3, surge tank 4 and each parts.
Reaction kettle body 1 is provided with dog-house 11, and thermal response raw material drops in reaction kettle body thus, and feed liquid, under the stirring of agitating device 12, forms homogeneous reaction solution; Reaction kettle body 1 is provided with temperature simultaneously and controls interlayer 13, heated by the raw material of conduction oil to reaction kettle body 1 inside passing into high-temperature steam or high temperature in this interlayer, and maintain certain temperature and carry out thermal response, after arriving reaction end, temperature is reduced by controlling to pass into frozen water in interlayer 13 in temperature, stop thermal response, feed liquid is discharged from drain hole (15); For controlling reaction temperature, reaction kettle body 1 is provided with temperature sensor 14, can measure and show reaction kettle body internal temperature; Reaction kettle body 1 is also provided with return-flow catheter 16, and this conduit stretches into reaction kettle body inner chamber, avoids withdrawing fluid to flow down along reaction kettle body inwall, causes before its haptoreaction solution main body with regard to direct boiling after the heat of absorption inwall; Consider from the angle of safety, pressure sensor 17 and safety valve 18 are also equipped with in reaction kettle body top, prevent because of line clogging or the too high danger causing reaction kettle body inner overpressure to bring of heating-up temperature; The top of reaction kettle body 1 is provided with mixed vapour outlet 19, and be connected with reaction kettle body inner chamber and condenser 2, the mixed vapour containing fragrance component in thermal process reactor enters condenser 2 by this steam (vapor) outlet.
Steam inlet 21 on condenser 2 and the mixed vapour on reaction kettle body 1 are exported 19 and are connected by pipeline, and condensate outlet 22 is equipped with three-way valve 23, and condensate outlet 22 is connected with the return-flow catheter 16 on extraction kettle 3, reaction kettle body 1 respectively by pipeline.
Extraction kettle 3 is provided with feed conduit 31, is convenient to add aqueous phase and oil phase; Liquid distributor 32 is equipped with in the upper end of extraction kettle 3 inside, and this distributor is connected with condenser 2, instills the oil phase surface in extraction kettle 3, then enter oil phase and aqueous phase successively after the liquid got off through condenser 2 condensation enters liquid distributor 32 after being divided evenly; Extraction kettle 3 is provided with temperature and controls interlayer 33, passes into hot water improve extraction efficiency at this layer, passes into the separation that frozen water accelerates water-oil phase after extraction terminates.
Surge tank 4 is provided with feed conduit 41, and be connected with the material liquid outlet 34 of extraction kettle 3, this conduit stretches into surge tank inner chamber simultaneously, prevents feed liquid from flowing down formation channel along top tank structure; Surge tank discharging opening 42 is connected with pipeline with the return-flow catheter 16 on reaction kettle body 1, and in " U " shape, to form fluid-tight.
The height of liquid distributor 32 lower section is higher than the height of feed conduit 41, and the height of feed conduit 41 is higher than the height of return-flow catheter 16.
In actual mechanical process, the two-phase system of lower floor's aqueous phase, upper oil phase is formed by adding water and oil-dissolving solvent in extraction kettle 3, the condensate liquid got off through condenser 2 condensation is after oil phase, main aromatic components enters oil phase and is extracted, moisture then enters aqueous phase, and circulation enters in reaction kettle body 1 and proceeds thermal response.Thermal response terminates to be separated the water-oil phase in extraction kettle afterwards, and the oil phase obtained is essence product.
Finally, it is also to be noted that what enumerate above is only a specific embodiment of the present invention.Obviously, the invention is not restricted to above embodiment, many distortion can also be had.All distortion that those of ordinary skill in the art can directly derive from content disclosed by the invention or associate, all should think protection scope of the present invention.
Claims (4)
1. a process units for oil-soluble hot reaction essence, is characterized in that described hot reaction essence process units is primarily of the transfer pipeline composition between reaction kettle body (1), condenser (2), extraction kettle (3), surge tank (4) and each parts; Described reaction kettle body (1) is provided with mixed vapour outlet (19) and return-flow catheter (16), and described return-flow catheter (16) stretches into reaction kettle body inner chamber; Described condenser (2) is provided with steam inlet (21) and condensate outlet (22); Described extraction kettle (3) is provided with liquid distributor (32) and material liquid outlet (34); Described surge tank (4) is provided with feed conduit (41) and discharging opening (42), and described feed conduit (41) stretches into surge tank inner chamber; Described mixed vapour outlet (19) is connected with pipeline with steam inlet (21); Described condensate outlet (22) is connected with pipeline with liquid distributor (32), and described condensate outlet (22) is also connected with pipeline with return-flow catheter (16); Described material liquid outlet (34) is connected with pipeline with feed conduit (41); Described discharging opening (42) is connected with return-flow catheter (16) connecting pipe road, and pipeline is in " U " shape; The height of described liquid distributor (32) lower section is higher than the height of feed conduit (41), and the height of feed conduit (41) is higher than the height of return-flow catheter (16).
2. the process units of oil-soluble hot reaction essence according to claim 1, described reaction kettle body (1) is also provided with dog-house (11), agitating device (12), temperature control interlayer (13), temperature sensor (14), drain hole (15), pressure sensor (17) and safety valve (18) composition; Described temperature controls interlayer (13) can admittance deep fat, high-temperature steam or frozen water.
3. the process units of oil-soluble hot reaction essence according to claim 1, described condenser (2) is the one in shell and tube condenser, jacket type condenser or coiler type condenser.
4. the process units of oil-soluble hot reaction essence according to claim 1, described extraction kettle (3) is also provided with and is made up of feed conduit (31) and temperature control interlayer (33); Described temperature controls can lead to hot water or frozen water in interlayer (33).
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CN201510521684.4A CN105013424A (en) | 2015-08-24 | 2015-08-24 | Production device for oil-soluble thermal reaction flavor |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109077344A (en) * | 2018-09-01 | 2018-12-25 | 王婧婧 | A kind of preparation method of milk-taste essence |
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US20020122754A1 (en) * | 1999-03-23 | 2002-09-05 | Ryzhkov Vladislav Andeevitch | Method and device for producing higher fullerenes and nanotubes |
CN103055789A (en) * | 2012-12-26 | 2013-04-24 | 淮安万邦香料工业有限公司 | Reaction vessel negative pressure distilled water separating apparatus |
CN203291851U (en) * | 2013-05-15 | 2013-11-20 | 山东轻工业学院 | Reaction device of quick reflux condensation |
CN203469546U (en) * | 2013-09-29 | 2014-03-12 | 青岛和兴精细化学有限公司 | Separation device for immiscible liquids with different densities |
CN203525685U (en) * | 2013-10-18 | 2014-04-09 | 淄博恒久聚氨酯科技股份有限公司 | Condensing recovery device of polyurethane reaction kettle |
CN204952891U (en) * | 2015-08-25 | 2016-01-13 | 王婧婧 | Apparatus for producing of oil solubility thermal response essence |
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2015
- 2015-08-24 CN CN201510521684.4A patent/CN105013424A/en active Pending
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
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US20020122754A1 (en) * | 1999-03-23 | 2002-09-05 | Ryzhkov Vladislav Andeevitch | Method and device for producing higher fullerenes and nanotubes |
CN103055789A (en) * | 2012-12-26 | 2013-04-24 | 淮安万邦香料工业有限公司 | Reaction vessel negative pressure distilled water separating apparatus |
CN203291851U (en) * | 2013-05-15 | 2013-11-20 | 山东轻工业学院 | Reaction device of quick reflux condensation |
CN203469546U (en) * | 2013-09-29 | 2014-03-12 | 青岛和兴精细化学有限公司 | Separation device for immiscible liquids with different densities |
CN203525685U (en) * | 2013-10-18 | 2014-04-09 | 淄博恒久聚氨酯科技股份有限公司 | Condensing recovery device of polyurethane reaction kettle |
CN204952891U (en) * | 2015-08-25 | 2016-01-13 | 王婧婧 | Apparatus for producing of oil solubility thermal response essence |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109077344A (en) * | 2018-09-01 | 2018-12-25 | 王婧婧 | A kind of preparation method of milk-taste essence |
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Application publication date: 20151104 |