CN103055789A - Reaction vessel negative pressure distilled water separating apparatus - Google Patents
Reaction vessel negative pressure distilled water separating apparatus Download PDFInfo
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- CN103055789A CN103055789A CN201210573205XA CN201210573205A CN103055789A CN 103055789 A CN103055789 A CN 103055789A CN 201210573205X A CN201210573205X A CN 201210573205XA CN 201210573205 A CN201210573205 A CN 201210573205A CN 103055789 A CN103055789 A CN 103055789A
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Abstract
The invention discloses a reaction vessel negative pressure distilled water separating apparatus which comprises a reaction vessel body. A separating apparatus is arranged in the reaction vessel body and comprises a distillation column, a condenser, a separator, a reception tank and a vacuum pump, wherein the reaction vessel body is communicated with the distillation column through a pipeline, the distillation column is communicated with an inlet of the condenser through a pipeline, an outlet of the condenser is communicated with the separator through a discharging pipe, one side of the separator is provided with a reflux inlet, the reflux inlet is communicated with the reaction vessel body through a reflux pipe, the bottom of the separator is provided with a water rising opening, the water rising opening is communicated with the reception tank through a water rising pipe, and the tops of the separator and the reception tank are respectively connected with the vacuum pump through pipelines. The apparatus provided by the invention overcomes the following problems in usage of a traditional reaction vessel separator: water is taken back to a reaction vessel with a solvent during two-phase separation by the traditional separator under the condition of a negative pressure, and a separation effect of a solvent and water is poor, which causes reduction in product yield, delay of reaction time, reduction in production efficiency and the like.
Description
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Technical field
The present invention relates to the reactor equipment technical field, be specifically related to a kind of reactor vacuum distillation water separation device.
Background technology
Two-phase fluid separation applications in vacuum distillation reaction system process, the solvent phase recycling, water separates fully, guarantees carrying out continuously of production, this shows, and separated from solvent is an important step of resource recycling.At present, enterprise usually adopts traditional separator to carry out two and is separated, two are separated and exist water to be brought back into phenomenon in the reactor with solvent under the conventional separators condition of negative pressure, solvent, moisture are from poor effect, caused reducing the yield of product, cause the time-delay in reaction time, reduce production efficiency.
Summary of the invention
The technical problem to be solved in the present invention provides a kind of reactor vacuum distillation water separation device, the present invention efficiently solves traditional reactor with separator in use, conventional separators two is separated and exists water to be brought back into problem in the reactor with solvent under condition of negative pressure, solvent, moisture are from poor effect, cause product yield to reduce, cause the time-delay in reaction time, and the problems such as reduction of production efficiency.
The present invention is achieved through the following technical solutions:
A kind of reactor vacuum distillation water separation device, comprise reactor body (1), it is characterized in that: described reactor body (1) is provided with separator, described separator comprises destilling tower (2), condenser (3), separator (4), groove (5) and vavuum pump (6), reactor body (1) is communicated with destilling tower (2) by pipeline, destilling tower (2) is communicated with condenser (3) import by pipeline, condenser (3) outlet is communicated with separator (4) by discharge nozzle (7), separator (4) one sides are provided with refluxing opening (41), refluxing opening (41) is communicated with reactor body (1) by return duct (9), separator (4) bottom is provided with premium on currency mouth (42), premium on currency mouth (42) is communicated with separator (4) by riser pipe (10) with groove (5), groove (5) top is connected with vavuum pump (6) by pipeline respectively.
The technical scheme that the present invention further solves is:
Be provided with fluid cushion plate (8) on the top inner wall of described separator (4) and discharge nozzle (7) junction.
The technical scheme that the present invention further solves is:
Described destilling tower (2) is provided with the visual windows (21) of being made by transparent material.
The present invention compared with prior art, has obvious advantage, the present invention adds separator at traditional reactor, can be according to different solvents proportion free adjustment, conveniently, strong operability, utilize self proportion different characteristics, the two-phase that successfully realizes not dissolving each other is separated fully, and simultaneously separator import is provided with a fluid cushion plate, avoid liquid that the impact of separation liquid level is affected separating effect, thereby improve the separating effect of two liquid phases.
Description of drawings
Fig. 1 is structural representation of the present invention.
The specific embodiment
As shown in Figure 1, the present invention includes and comprise reactor body 1, described reactor body 1 is provided with separator, described separator comprises destilling tower 2, condenser 3, separator 4, groove 5 and vavuum pump 6, reactor body 1 is communicated with destilling tower 2 by pipeline, destilling tower 2 is communicated with condenser 3 imports by pipeline, condenser 3 outlets are communicated with separator 4 by discharge nozzle 7, separator 4 one sides are provided with refluxing opening 41, refluxing opening 41 is communicated with reactor body 1 by return duct 9, separator 4 bottoms are provided with premium on currency mouth 42, premium on currency mouth 42 is communicated with groove 5 by riser pipe 10, separator 4, groove 5 tops are connected with vavuum pump 6 by pipeline respectively, are provided with fluid cushion plate 8 on the top inner wall of described separator 4 and discharge nozzle 7 junctions, and described destilling tower 2 is provided with the visual windows 21 of being made by transparent material.
Sketch the course of work of the present invention in conjunction with Fig. 1:
Reactor body 1 in course of reaction solvent and course of reaction in the water that produces, separate to advance condenser 3 through destilling tower 2, condenser 3 with two-phase liquid through discharge nozzle 7 through fluid cushion plate 8, overflow enters separator 4 light component solvents and water rapidly layering in separator 4, the light component solvent is on the upper strata, restructuring minute water is in lower floor, when liquid level reaches refluxing opening 41, solvent refluxing enters reactor body 1 and re-uses, the liquid that again distills according to the proportion difference produces water and enters riser pipe 10 by gravity through the premium on currency mouth and naturally flow into groove 5, negative pressure is provided by vavuum pump 6, and vavuum pump 6 offers respectively groove 5 by pipeline, separator 4 negative pressure.
The present invention has reached the foregoing invention purpose in sum.
Claims (3)
1. reactor vacuum distillation water separation device, comprise reactor body (1), it is characterized in that: described reactor body (1) is provided with separator, described separator comprises destilling tower (2), condenser (3), separator (4), groove (5) and vavuum pump (6), reactor body (1) is communicated with destilling tower (2) by pipeline, destilling tower (2) is communicated with condenser (3) import by pipeline, condenser (3) outlet is communicated with separator (4) by discharge nozzle (7), separator (4) one sides are provided with refluxing opening (41), refluxing opening (41) is communicated with reactor body (1) by return duct (9), separator (4) bottom is provided with premium on currency mouth (42), premium on currency mouth (42) is communicated with separator (4) by riser pipe (10) with groove (5), groove (5) top is connected with vavuum pump (6) by pipeline respectively.
2. a kind of reactor vacuum distillation water separation device according to claim 1 is characterized in that: be provided with fluid cushion plate (8) on the top inner wall of described separator (4) and discharge nozzle (7) junction.
3. a kind of reactor vacuum distillation water separation device according to claim 1 and 2, it is characterized in that: described destilling tower (2) is provided with the visual windows (21) of being made by transparent material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210573205XA CN103055789A (en) | 2012-12-26 | 2012-12-26 | Reaction vessel negative pressure distilled water separating apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210573205XA CN103055789A (en) | 2012-12-26 | 2012-12-26 | Reaction vessel negative pressure distilled water separating apparatus |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN103055789A true CN103055789A (en) | 2013-04-24 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201210573205XA Pending CN103055789A (en) | 2012-12-26 | 2012-12-26 | Reaction vessel negative pressure distilled water separating apparatus |
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| CN (1) | CN103055789A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105013424A (en) * | 2015-08-24 | 2015-11-04 | 王婧婧 | Production device for oil-soluble thermal reaction flavor |
| CN105272994A (en) * | 2015-11-09 | 2016-01-27 | 贝利化学（张家港）有限公司 | Reaction device |
| CN108392846A (en) * | 2018-04-28 | 2018-08-14 | 江苏宝盛龙城药业有限公司 | Vacuum distillation apparatus and technique |
| CN109395679A (en) * | 2018-11-02 | 2019-03-01 | 浙江六合工程技术有限公司 | Adjustable multipurpose way horizontal separator |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2820271Y (en) * | 2005-09-09 | 2006-09-27 | 北京普析通用仪器有限责任公司 | Multistage gas/liquid separator |
| KR20110011314A (en) * | 2009-07-28 | 2011-02-08 | 이규상 | Oil skimmer |
| CN202210086U (en) * | 2011-08-30 | 2012-05-02 | 中国海诚工程科技股份有限公司 | Measuring device for synthetic resin polymeric heat |
-
2012
- 2012-12-26 CN CN201210573205XA patent/CN103055789A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2820271Y (en) * | 2005-09-09 | 2006-09-27 | 北京普析通用仪器有限责任公司 | Multistage gas/liquid separator |
| KR20110011314A (en) * | 2009-07-28 | 2011-02-08 | 이규상 | Oil skimmer |
| CN202210086U (en) * | 2011-08-30 | 2012-05-02 | 中国海诚工程科技股份有限公司 | Measuring device for synthetic resin polymeric heat |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105013424A (en) * | 2015-08-24 | 2015-11-04 | 王婧婧 | Production device for oil-soluble thermal reaction flavor |
| CN105272994A (en) * | 2015-11-09 | 2016-01-27 | 贝利化学（张家港）有限公司 | Reaction device |
| CN108392846A (en) * | 2018-04-28 | 2018-08-14 | 江苏宝盛龙城药业有限公司 | Vacuum distillation apparatus and technique |
| CN109395679A (en) * | 2018-11-02 | 2019-03-01 | 浙江六合工程技术有限公司 | Adjustable multipurpose way horizontal separator |
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Application publication date: 20130424 |