CN202983257U - Toluene distillation separation device - Google Patents

Toluene distillation separation device Download PDF

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Publication number
CN202983257U
CN202983257U CN 201220572680 CN201220572680U CN202983257U CN 202983257 U CN202983257 U CN 202983257U CN 201220572680 CN201220572680 CN 201220572680 CN 201220572680 U CN201220572680 U CN 201220572680U CN 202983257 U CN202983257 U CN 202983257U
Authority
CN
China
Prior art keywords
gas
liquid
liquid separator
condenser
toluene
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN 201220572680
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Chinese (zh)
Inventor
谭建平
王俊华
金标
邓炜
袁庆庆
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nantong Tendenci Chemical Co Ltd
Original Assignee
Nantong Tendenci Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Nantong Tendenci Chemical Co Ltd filed Critical Nantong Tendenci Chemical Co Ltd
Priority to CN 201220572680 priority Critical patent/CN202983257U/en
Application granted granted Critical
Publication of CN202983257U publication Critical patent/CN202983257U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model discloses a toluene distillation separation device which comprises a rectifying tower (1), a condenser (2) and a gas-liquid separator (3), wherein the condenser (2) is arranged above the gas-liquid separator (3), the top of the rectifying tower (1) is communicated with the upper portion of the gas-liquid separator (3),a liquid phase connector (3a) in the middle of the gas-liquid separator and the rectifying tower (1) are communicated to form external backflow, and a liquid phase connector (3b) in the bottom of the gas-liquid separator (3) is communicated with a water separating device (4) through pipelines. The toluene distillation separation device is simple and reasonable in structure and high in separating efficiency during toluene separation.

Description

A kind of toluene distillation separator
Technical field
The utility model belongs to the chemical plant installations field, relates in particular to a kind of toluene distillation separator.
Background technology
The distillation principle is utilized the difference of each component volatilization degree in liquid mixture, liquid mixture is partly vaporized and make the vapor portion condensation thereupon, thereby realizing the separation of its contained component, is widely used in the separating-purifying in chemical industry.Adopt the distillation principle to carry out separating-purifying and just need a cover separated device.When separation of methylbenzene, the distillation mode of the interior backflow that traditional separated device adopts, so-called interior reflux type is exactly namely that condenser is built-in, directly condenser is arranged on the top of rectifying column; But can bring a problem, the azeotropic gas of some toluene and water directly is back to the reduction that causes distillation efficiency in rectifying column downwards after meeting condenser.
Summary of the invention
Content of the present utility model is the shortcoming that overcomes prior art, separates the high a kind of separated device of efficient when a kind of piptonychia benzene is provided.
For solving the problems of the technologies described above, concrete technical scheme of the present utility model is as follows:
A kind of toluene distillation separator comprises rectifying column and condenser, it is characterized in that: comprise that also one can divide the gas-liquid separator of water, described condenser is arranged on the top of Gas and liquid flow diverter, and described rectifying column top is connected with gas-liquid separator top by pipeline; The formation exteenal reflux that is connected with rectifying column of described Gas and liquid flow diverter middle part liquid phase interface; The liquid-phase outlet of described Gas and liquid flow diverter bottom is connected with division box by pipeline.
The utility model is simple and reasonable, can efficiently toluene distillation be separated, and has higher practicality.
Description of drawings
Fig. 1 is structural representation of the present utility model.
The specific embodiment
Below in conjunction with accompanying drawing, the utility model is further described.
As shown in Figure 1, the utility model comprises rectifying column 1, is connected by the top of pipeline with gas-liquid separator 3 at rectifying column 1 top, and a condenser 2 is set at the top of gas-liquid separator 3.The described gas-liquid separator middle part liquid phase interface 3a formation exteenal reflux that is connected with rectifying column 1; Gas-liquid separator 3 bottoms arrange a division box 4 carry out toluene and standing separation, division box 4 is connected with the liquid-phase outlet 3b of gas-liquid separator by pipeline.During rectifying, in rectifying column 1, the mist of toluene and water rises in gas-liquid separator 3, and after condenser 2 was cooling, downward liquid flow was put in division box 4 through the liquid-phase outlet 3b of gas-liquid separator stream; Condensate liquid is back to circulation distillation in rectifying column 1 by gas-liquid separator middle part liquid phase interface 3a after minute water.Division box 4 can be separated water and toluene, has just completed the disengaging of toluene.
The utility model is simple and reasonable, has higher separated efficient during separation of methylbenzene, has greatly improved productivity ratio.

Claims (1)

1. toluene distillation separator, comprise rectifying column (1) and condenser (2), it is characterized in that: comprise that also one can divide the gas-liquid separator (3) of water, described condenser (2) is arranged on the top of Gas and liquid flow diverter (3), and described rectifying column (1) top is connected with gas-liquid separator (3) top by pipeline; Described Gas and liquid flow diverter middle part liquid phase interface (3a) the formation exteenal reflux that is connected with rectifying column (1); The liquid-phase outlet (3b) of described Gas and liquid flow diverter bottom is connected with division box (4) by pipeline.
CN 201220572680 2012-11-02 2012-11-02 Toluene distillation separation device Expired - Fee Related CN202983257U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201220572680 CN202983257U (en) 2012-11-02 2012-11-02 Toluene distillation separation device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201220572680 CN202983257U (en) 2012-11-02 2012-11-02 Toluene distillation separation device

Publications (1)

Publication Number Publication Date
CN202983257U true CN202983257U (en) 2013-06-12

Family

ID=48554483

Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201220572680 Expired - Fee Related CN202983257U (en) 2012-11-02 2012-11-02 Toluene distillation separation device

Country Status (1)

Country Link
CN (1) CN202983257U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103432762A (en) * 2013-08-29 2013-12-11 张家港市三联化工科技有限公司 Water separating device of S-2-methyl chloropropionate

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103432762A (en) * 2013-08-29 2013-12-11 张家港市三联化工科技有限公司 Water separating device of S-2-methyl chloropropionate

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20130612

Termination date: 20161102