CN203355321U - Simple distillation and rectification device - Google Patents
Simple distillation and rectification device Download PDFInfo
- Publication number
- CN203355321U CN203355321U CN 201320422826 CN201320422826U CN203355321U CN 203355321 U CN203355321 U CN 203355321U CN 201320422826 CN201320422826 CN 201320422826 CN 201320422826 U CN201320422826 U CN 201320422826U CN 203355321 U CN203355321 U CN 203355321U
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- valve
- distillation
- shell
- cooling water
- rectifying column
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Abstract
The utility model provides a simple distillation and rectification device, wherein the distillation operation and rectification operation are performed in the same unit, so that the operation is simple, the production efficiency is high, the utilization rate of equipment is high, and the energy is saved.
Description
Technical field
The utility model provides a kind of simple distillation rectifier unit, belongs to chemical industry, pharmaceutical equipment field.
Background technology
In organic synthesis, often, with distillation and distillation operation, generally in different unit operations, carry out respectively, complicated operation, production efficiency is low, and utilization rate of equipment and installations is low, and wastes energy.
Summary of the invention
Technical problem to be solved in the utility model is, a kind of simple distillation rectifier unit is provided, and distillation and distillation operation carry out in same unit, and simple to operate, production efficiency is high, and utilization rate of equipment and installations is high, and the saving energy.
The utility model is achieved in that 1 is distillation still, the 2nd, and rectifying column, the 3rd, shell and tube condenser, the 4th, receiving tank, the 5th, distillation still air intake valve, the 6th, distillation still venthole valve, the 7th, distillation valve, the 8th, rectifying valve, the 9th, rectifying column cooling water inlet valve, the 10th, rectifying column cooling water flowing water Valve, the 11st, shell and tube condenser cooling water inlet valve, the 12nd, shell and tube condenser cooling water flowing water Valve, the 13rd, distillate baiting valve.
Distillation still (1) is joined with distillation still air intake valve (5) and distillation still venthole valve (6) respectively, in distillation still (1) outlet, with distillation valve (7), with an end of rectifying valve (8), is connected respectively; The other end of rectifying valve (8) is connected with the bottom of rectifying column (2), the top of rectifying column (2) with the distillation valve (7) the other end be connected after, with the top of condenser (3), be connected, the bottom of condenser (3) is connected with receiving tank (4) by distillate baiting valve (13) again; Rectifying column (2) is connected with rectifying column cooling water flowing water Valve (10) with rectifying column cooling water inlet valve (9) respectively; Shell and tube condenser (3) is connected with shell and tube condenser cooling water flowing water Valve (12) with shell and tube condenser cooling water inlet valve (11) respectively.
The distillation rectifier unit of said structure, distillation and distillation operation carry out in same unit, and simple to operate, production efficiency is high, and utilization rate of equipment and installations is high, and saves the energy.
The accompanying drawing explanation
Accompanying drawing is structural representation of the present utility model.
In accompanying drawing: the 1st, distillation still, the 2nd, rectifying column, the 3rd, shell and tube condenser, the 4th, receiving tank, the 5th, distillation still air intake valve, the 6th, distillation still venthole valve, the 7th, distillation valve, the 8th, the rectifying valve, the 9th, rectifying column cooling water inlet valve, the 10th, rectifying column cooling water flowing water Valve, the 11st, shell and tube condenser cooling water inlet valve, the 12nd, shell and tube condenser cooling water flowing water Valve, the 13rd, distillate baiting valve.
The specific embodiment
Below in conjunction with accompanying drawing, concrete structure of the present utility model is described.
As shown in drawings, the distillation rectifier unit of the utility model, it is by distillation still (1), rectifying column (2), shell and tube condenser (3), receiving tank (4), distillation still air intake valve (5), distillation still venthole valve (6), distillation valve (7), rectifying valve (8), rectifying column cooling water inlet valve (9), rectifying column cooling water flowing water Valve (10), shell and tube condenser cooling water inlet valve (11), shell and tube condenser cooling water flowing water Valve (12), distillate baiting valve (13) forms.
Distillation still (1) is joined with distillation still air intake valve (5) and distillation still venthole valve (6) respectively, in distillation still (1) outlet, with distillation valve (7), with an end of rectifying valve (8), is connected respectively; The other end of rectifying valve (8) is connected with the bottom of rectifying column (2), the top of rectifying column (2) with the distillation valve (7) the other end be connected after, with the top of shell and tube condenser (3), be connected, the bottom of shell and tube condenser (3) is connected with receiving tank (4) by distillate baiting valve (13) again; Rectifying column (2) is connected with rectifying column cooling water flowing water Valve (10) with rectifying column cooling water inlet valve (9) respectively; Shell and tube condenser (3) is connected with shell and tube condenser cooling water flowing water Valve (12) with shell and tube condenser cooling water inlet valve (11) respectively.
When carrying out distillation procedure, close rectifying valve (8), open distillation valve (7), and then open distillation still air intake valve (5) and distillation still venthole valve (6), passing into steam heats distillation still, vaporizing liquid in distillation still, enter shell and tube condenser (3) by the outlet of distillation still upper end and distillation valve (7), open shell and tube condenser cooling water inlet valve (11) simultaneously, shell and tube condenser cooling water flowing water Valve (12) and distillate baiting valve (13), distillate enters in receiving tank (4) by distillate baiting valve (13) after condensation.
When rectifying, close distillation valve (7), open rectifying valve (8), the distillate gas enters in rectifying column (2), open rectifying column cooling water inlet valve (9) and rectifying column cooling water flowing water Valve (10) simultaneously, and regulate and open size, make distillate keep certain reflux ratio, the distillate gas enters shell and tube condenser (3) by the rectifying column top, and distillate enters in receiving tank (4) by distillate baiting valve (13) after condensation.
Claims (1)
1. one kind is distilled rectifier unit, it is characterized in that, it is by distillation still (1), rectifying column (2), shell and tube condenser (3), receiving tank (4), distillation still air intake valve (5), distillation still venthole valve (6), distillation valve (7), rectifying valve (8), rectifying column cooling water inlet valve (9), rectifying column cooling water flowing water Valve (10), shell and tube condenser cooling water inlet valve (11), shell and tube condenser cooling water flowing water Valve (12), distillate baiting valve (13) forms;
Distillation still (1) is joined with distillation still air intake valve (5) and distillation still venthole valve (6) respectively, in distillation still (1) outlet, with distillation valve (7), with an end of rectifying valve (8), is connected respectively; The other end of rectifying valve (8) is connected with the bottom of rectifying column (2), the top of rectifying column (2) with the distillation valve (7) the other end be connected after, with the top of shell and tube condenser (3), be connected, the bottom of shell and tube condenser (3) is connected with receiving tank (4) by distillate baiting valve (13) again; Rectifying column (2) is connected with rectifying column cooling water flowing water Valve (10) with rectifying column cooling water inlet valve (9) respectively; Shell and tube condenser (3) is connected with shell and tube condenser cooling water flowing water Valve (12) with shell and tube condenser cooling water inlet valve (11) respectively.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201320422826 CN203355321U (en) | 2013-07-17 | 2013-07-17 | Simple distillation and rectification device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201320422826 CN203355321U (en) | 2013-07-17 | 2013-07-17 | Simple distillation and rectification device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203355321U true CN203355321U (en) | 2013-12-25 |
Family
ID=49803147
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201320422826 Expired - Fee Related CN203355321U (en) | 2013-07-17 | 2013-07-17 | Simple distillation and rectification device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203355321U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105733814A (en) * | 2016-04-07 | 2016-07-06 | 广西贵港市宏利生物能源科技有限公司 | Distilling production method for sandalwood essential oil and equipment |
-
2013
- 2013-07-17 CN CN 201320422826 patent/CN203355321U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105733814A (en) * | 2016-04-07 | 2016-07-06 | 广西贵港市宏利生物能源科技有限公司 | Distilling production method for sandalwood essential oil and equipment |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170324 Address after: 274000 Heze high tech Zone, Shandong, No. 1666 Kunming Road Patentee after: Shandong Jia Ming Bang Pharmaceutical Co. Ltd. Address before: 274500 the Yellow River Road, Dongming, Shandong, Heze Patentee before: Shandong Fangming Pharmaceutical Group Co., Ltd. |
|
| TR01 | Transfer of patent right | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131225 Termination date: 20170717 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |