CN203469546U - Separation device for immiscible liquids with different densities - Google Patents
Separation device for immiscible liquids with different densities Download PDFInfo
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- CN203469546U CN203469546U CN201320605890.XU CN201320605890U CN203469546U CN 203469546 U CN203469546 U CN 203469546U CN 201320605890 U CN201320605890 U CN 201320605890U CN 203469546 U CN203469546 U CN 203469546U
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- separation device
- liquid separator
- liquid
- knockout
- different densities
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Abstract
The utility model discloses a separation device for immiscible liquids with different densities. The separation device comprises a reaction kettle (1), a condenser (2), a buffer tank (4) and a liquid separator (5). The condenser (2) is connected with the reaction kettle (1) and the liquid separator (5) through pipelines respectively. The buffer tank is located between the reaction kettle (1) and the liquid separator (5) and connected with the reaction kettle (1) and the liquid separator (5) through a backflow pipe (3). A discharging outlet (6) is formed in the upper portion of the liquid separator (5). A liquid outlet (7) is formed in the upper portion of the buffer tank (4). The separation device is used for achieving liquid backflow separation and separating two immiscible phases, liquids which are not beneficial to a reaction can be effectively eliminated, liquids which are beneficial to the reaction are made to flow back to a reactor, the stability of a reaction system is ensured, the height of the liquid level and the height of the backflow pipe are both adjustable, and the separation device can be applied to multi-system separation and can also enable any component in the liquid separator to flow back.
Description
Technical field
The utility model relates to a kind of different densities liquid separating appts that do not dissolve each other.
Background technology
At present at chemical field, often need to by two kinds do not dissolve each other, the fluid separation applications of different densities opens, but existing separation equipment separating effect is bad, and versatility is poor, can not meet the separated needs of multiple system.
Summary of the invention
Technical problem to be solved in the utility model is: a kind of different densities liquid separating appts that do not dissolve each other is provided.
For solving the problems of the technologies described above, the technical solution adopted in the utility model is:
A kind of different densities liquid separating appts that do not dissolve each other, comprise reactor (1), condenser (2), surge tank (4) and knockout (5), condenser (2) is connected with knockout (5) with reactor (1) respectively by pipeline, surge tank is positioned at the centre of reactor (1) and knockout (5), and connects by return duct (3); Knockout (5) top is provided with discharging opening (6), and surge tank (4) top is provided with liquid outlet (7).
In knockout (5), little density material liquid level is h1, and large density material liquid level is h2; The liquid level difference of discharging opening (6) and liquid outlet (7) is h3.
The utility model is for realizing backflow separatory, separated insoluble two-phase, can effectively remove reacting disadvantageous liquid also flowing back to reactor to reacting favourable liquid, guarantee the stability of reaction system, and liquid level and return duct height are all adjustable, both can be applied to arbitrary component that multiple system separation also can reflux in knockout.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, the specific embodiment of the present utility model is described in further detail.
Fig. 1 is structural representation of the present utility model.
The specific embodiment
Embodiment 1
As shown in Figure 1, a kind of different densities liquid separating appts that do not dissolve each other, comprise reactor (1), condenser (2), surge tank (4) and knockout (5), condenser (2) is connected with knockout (5) with reactor (1) respectively by pipeline, surge tank is positioned at the centre of reactor (1) and knockout (5), and connects by return duct (3); Knockout (5) top is provided with discharging opening (6), and surge tank (4) top is provided with liquid outlet (7).
In knockout (5), little density material liquid level is h1, and large density material liquid level is h2; The liquid level difference of discharging opening (6) and liquid outlet (7) is h3.
Embodiment 2
The present embodiment is Separation of Water and benzene in chemical process, effectively benzene is discharged water is refluxed.Water benzene vapour enters knockout 4 from reactor 1 through condenser 2 and carries out layering ，Shui lower floor benzene on upper strata, and benzene is emitted from discharging opening, and water flows into reactor from return duct 3.H wherein
1h
2h
3be related to that section, by calculating, is obtained by Bernoulli equation:
(h
1+ h
2-h
3) * ρ
water=h
1* ρ
benzene+ h
2* ρ
water
ρ wherein
water=1, ρ
benzene=0.88
h
3=0.12?h
1
By measuring h
1height, can determine h
3height can determine that the height of return duct guarantees that water can reflux.
The above, it is only preferred embodiment of the present utility model, be not the utility model to be done to the restriction of other form, any those skilled in the art may utilize the technology contents of above-mentioned announcement to be changed or be modified as the equivalent embodiment of equivalent variations.But every technical solutions of the utility model content that do not depart from, any simple modification, equivalent variations and the remodeling above embodiment done according to technical spirit of the present utility model, still belong to the protection domain of technical solutions of the utility model.
Claims (1)
1. the different densities liquid separating appts that do not dissolve each other, it is characterized in that, comprise reactor (1), condenser (2), surge tank (4) and knockout (5), condenser (2) is connected with knockout (5) with reactor (1) respectively by pipeline, surge tank is positioned at the centre of reactor (1) and knockout (5), and connects by return duct (3); Knockout (5) top is provided with discharging opening (6), and surge tank (4) top is provided with liquid outlet (7).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320605890.XU CN203469546U (en) | 2013-09-29 | 2013-09-29 | Separation device for immiscible liquids with different densities |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320605890.XU CN203469546U (en) | 2013-09-29 | 2013-09-29 | Separation device for immiscible liquids with different densities |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203469546U true CN203469546U (en) | 2014-03-12 |
Family
ID=50217965
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201320605890.XU Expired - Fee Related CN203469546U (en) | 2013-09-29 | 2013-09-29 | Separation device for immiscible liquids with different densities |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203469546U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105013424A (en) * | 2015-08-24 | 2015-11-04 | 王婧婧 | Production device for oil-soluble thermal reaction flavor |
| CN105056871A (en) * | 2015-08-24 | 2015-11-18 | 王婧婧 | Production device for thermal reaction essence |
-
2013
- 2013-09-29 CN CN201320605890.XU patent/CN203469546U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105013424A (en) * | 2015-08-24 | 2015-11-04 | 王婧婧 | Production device for oil-soluble thermal reaction flavor |
| CN105056871A (en) * | 2015-08-24 | 2015-11-18 | 王婧婧 | Production device for thermal reaction essence |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140312 Termination date: 20150929 |
|
| EXPY | Termination of patent right or utility model |