CN204816541U - Apparatus for producing of thermal response essence - Google Patents
Apparatus for producing of thermal response essence Download PDFInfo
- Publication number
- CN204816541U CN204816541U CN201520645204.0U CN201520645204U CN204816541U CN 204816541 U CN204816541 U CN 204816541U CN 201520645204 U CN201520645204 U CN 201520645204U CN 204816541 U CN204816541 U CN 204816541U
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- CN
- China
- Prior art keywords
- chromatographic column
- essence
- condenser
- kettle body
- reaction kettle
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- 238000006243 chemical reaction Methods 0.000 claims abstract description 48
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000012141 concentrate Substances 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims description 24
- 238000007599 discharging Methods 0.000 claims description 15
- 239000003480 eluent Substances 0.000 claims description 14
- 239000011229 interlayer Substances 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 5
- 239000003205 fragrance Substances 0.000 abstract description 7
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 235000013305 food Nutrition 0.000 abstract description 4
- 235000013361 beverage Nutrition 0.000 abstract description 2
- 239000002932 luster Substances 0.000 abstract description 2
- 238000004587 chromatography analysis Methods 0.000 abstract 3
- 230000015572 biosynthetic process Effects 0.000 abstract 1
- 238000010828 elution Methods 0.000 abstract 1
- 239000000796 flavoring agent Substances 0.000 description 4
- 239000007788 liquid Substances 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 230000002745 absorbent Effects 0.000 description 2
- 239000002250 absorbent Substances 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 230000001476 alcoholic effect Effects 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- 238000009835 boiling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000010410 layer Substances 0.000 description 1
- 238000010297 mechanical methods and process Methods 0.000 description 1
- 230000005226 mechanical processes and functions Effects 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
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- Fats And Perfumes (AREA)
Abstract
The utility model discloses an apparatus for producing of thermal response essence mainly comprises the conveying line between the reation kettle body, condenser, chromatography column, U type pipe, eluate storage tank, constant flow pump, buffer tank and concentrator and each part. In hot reaction sequence, the mixed steam that has fragrance of the internal production of reation kettle passes through condenser, chromatography column, U type pipe in proper order, flows back to at last to the internal formation of reation kettle to circulate, after the thermal response, the constant flow pump carries out the elution in going into the chromatography column according to certain velocity of flow pump with the eluate from the eluate storage tank, flows to the buffer tank, shifts at last and carry out the concentration in the concentrator, and the concentrate is essence promptly. The weak problem of thermal response essence intensity has been solved to the thermal response essence of the device production, and the essence product is transparent, water -soluble simultaneously, does not influence the color and luster of application product, can be applied to in various beverages and other food.
Description
Technical field
The utility model relates to a kind of technology of food processing field, particularly a kind of process units of hot reaction essence, can be used for the working system of hot reaction essence.
Background technology
Hot reaction essence mainly produces the process of fragrance and the essence developed by simulated foods in heating process, has fragrance true to nature, mellow in taste and the advantage such as high temperature resistant.The process units mainly reactor of current hot reaction essence, Zhejiang Province Green Crystal Flavor Co., Ltd discloses a kind of process units (CN203247245U) of thermal process flavourings, reaction kettle body and blending tank are organically combined, easy production technology, but this process units is not suitable for the production of clear shape hot reaction essence.
Summary of the invention
The purpose of this utility model is to overcome the deficiencies in the prior art, provides a kind of process units by thermal process flavourings, is applicable to the production of transparence thermal process flavourings.
For achieving the above object, the technical solution adopted in the utility model is: it is characterized in that described hot reaction essence process units is primarily of the transfer pipeline composition between reaction kettle body, condenser, chromatographic column, U-tube, eluent storage tank, constant flow pump, surge tank and inspissator and each parts; Described reaction kettle body is provided with mixed vapour outlet and return-flow catheter, and described condenser is provided with steam inlet and condensate outlet, and described chromatographic column is provided with charging aperture and discharging opening; Mixed vapour outlet on described reaction kettle body is connected with pipeline with the steam inlet on condenser, condensate outlet on described condenser is connected with pipeline with the charging aperture on chromatographic column, discharging opening on described chromatographic column and connecting by U-tube between return-flow catheter, the position of the discharging opening on described chromatographic column is higher than the position of the return-flow catheter on reaction kettle body; Described eluent storage tank is connected with pipeline with the charging aperture on chromatographic column, and centre is provided with constant flow pump; Discharging opening on described chromatographic column is also connected with surge tank, and during wash-out, eluent pumps into chromatographic column, flow in surge tank store through discharging opening, is then transferred in inspissator and concentrates.
In technique scheme, described reaction kettle body is also provided with dog-house, agitating device, temperature control interlayer, temperature sensor, drain hole, pressure sensor, safety valve; Described temperature controls can admittance deep fat, high-temperature steam or frozen water in interlayer.
In technique scheme, described condenser is the one in shell and tube condenser, jacket type condenser or coiler type condenser.
In technique scheme, described chromatographic column is also provided with temperature and controls interlayer composition; Described temperature controls chuck layer can lead to hot water or frozen water.
In thermal process reactor, the aromatic mixed vapour of band produced in reaction kettle body, successively through condenser, chromatographic column, U-tube, finally flows back in reaction kettle body and forms circulation; After thermal response terminates, eluent pumps in chromatographic column by certain flow rate and carries out wash-out by constant flow pump from eluent storage tank, and flow to surge tank, be finally transferred in inspissator and concentrate, concentrate is essence.
Hot reaction essence process units of the present utility model, compared with prior art, has following advantage:
1) this device makes the fragrance component produced in thermal process reactor adsorb in chromatographic column, by follow-up wash-out with concentrated, realizes concentrating hot reaction essence fragrance, increases essence intensity, solve the problem that hot reaction essence intensity is weak;
2) the utility model device is produced the essence obtained and can be obtained transparent, water miscible liquid essence excessively, does not affect the color and luster of application product, can be applicable in various beverage and other food.
Accompanying drawing explanation
Below in conjunction with accompanying drawing, detailed description of the invention of the present utility model is described in further detail.
Fig. 1 is the primary structure schematic diagram of the process units of thermal process flavourings of the present utility model.
Detailed description of the invention
Below in conjunction with instantiation, the technical solution of the utility model is described further.
Embodiment 1:
Primarily of the transfer pipeline composition between reaction kettle body 1, condenser 2, chromatographic column 3, U-tube 4, eluent storage tank 5, constant flow pump 6, surge tank 7 and inspissator 8 and each parts; Described reaction kettle body 1 is provided with mixed vapour outlet 19 and return-flow catheter 16; Described condenser 2 is provided with steam inlet 21 and condensate outlet 22; Described chromatographic column 3 is provided with charging aperture 31 and discharging opening 33; Described mixed vapour outlet 19 is connected with pipeline with steam inlet 21, described condensate outlet 22 is connected with pipeline with charging aperture 31, connect by U-tube 4 between described discharging opening 33 and return-flow catheter 16, the position of the discharging opening 33 on described chromatographic column 3 is higher than the position of the return-flow catheter 16 on reaction kettle body 1; Described eluent storage tank 5 is connected with pipeline with the charging aperture 31 on chromatographic column 3, and centre is provided with constant flow pump 6; Discharging opening 33 on described chromatographic column 3 is also connected with surge tank 7, and during wash-out, eluent pumps into chromatographic column 3, flow in surge tank 7 and stores, be then transferred in inspissator 8 and concentrate through discharging opening 33.
Reaction kettle body 1 is provided with dog-house 11 and agitating device 12, and thermal response raw material drops in reaction kettle body by dog-house 11, and feed liquid, under the stirring of agitating device 12, forms homogeneous reaction solution; Reaction kettle body 1 is provided with temperature simultaneously and controls interlayer 13, heated by the raw material of conduction oil to reaction kettle body 1 inside passing into high-temperature steam or high temperature in this interlayer, and maintain certain temperature and carry out thermal response, after arriving reaction end, reducing temperature by controlling to pass into frozen water in interlayer 13 in temperature, stopping thermal response; For controlling reaction temperature, reaction kettle body 1 is provided with temperature sensor 14, can measure and show reaction kettle body internal temperature; Reaction kettle body 1 is also provided with return-flow catheter 16, and this conduit stretches into reaction kettle body 1 inner chamber, avoids withdrawing fluid to flow down along reaction kettle body inwall, causes before its haptoreaction solution main body with regard to direct boiling after the heat of absorption inwall; Consider from the angle of safety, pressure sensor 17 and safety valve 18 are also equipped with in reaction kettle body 1 top, prevent because of line clogging or the too high danger causing reaction kettle body inner overpressure to bring of heating-up temperature.
Condenser 2 adopts shell and tube condenser.
Be filled with macroporous absorbent resin in chromatographic column 3, selective absorption is carried out to the fragrance component in condensate liquid, chromatographic column 3 is also provided with temperature and controls interlayer 32, pass into warm water in interlayer, the temperature of chromatographic column is controlled the optimal adsorption temperature at macroporous absorbent resin.
Certain density alcoholic solution is stored as eluent in eluent storage tank 5.
In actual mechanical process, in the thermal response stage, pass through Valve controlling, make the aromatic mixed vapour of band produced in reaction kettle body 1 successively through condenser 2, chromatographic column 3, U-tube 4, finally to flow back in reaction kettle body 1 and form circulation, the fragrance component in condensate liquid in chromatographic column by macroporous resin adsorption; After thermal response terminates, alcoholic solution pumps in chromatographic column by certain flow rate and carries out wash-out by constant flow pump 6 from eluent storage tank 5, and then flow to surge tank 7, be finally transferred in inspissator 8 and concentrate, concentrate is essence product.
Finally, it is also to be noted that what enumerate above is only a specific embodiment of the present utility model.Obviously, the utility model is not limited to above embodiment, can also have many distortion.All distortion that those of ordinary skill in the art can directly derive from content disclosed in the utility model or associate, all should think protection domain of the present utility model.
Claims (4)
1. a process units for hot reaction essence, is characterized in that described hot reaction essence process units is primarily of the transfer pipeline composition between reaction kettle body (1), condenser (2), chromatographic column (3), U-tube (4), eluent storage tank (5), constant flow pump (6), surge tank (7) and inspissator (8) and each parts; Described reaction kettle body (1) is provided with mixed vapour outlet (19) and return-flow catheter (16), and described return-flow catheter (16) stretches into reaction kettle body inner chamber; Described condenser (2) is provided with steam inlet (21) and condensate outlet (22); Described chromatographic column (3) is provided with charging aperture (31) and discharging opening (33); Described mixed vapour outlet (19) is connected with pipeline with steam inlet (21), described condensate outlet (22) is connected with pipeline with charging aperture (31), connect by U-tube (4) between described discharging opening (33) and return-flow catheter (16), the position of the discharging opening (33) on described chromatographic column (3) is higher than the position of the return-flow catheter (16) on reaction kettle body (1); Described eluent storage tank (5) is connected with pipeline with the charging aperture (31) on chromatographic column (3), and centre is provided with constant flow pump (6); Discharging opening (33) on described chromatographic column (3) is also connected with surge tank (7), and during wash-out, eluent pumps into chromatographic column (3), stores, be then transferred in inspissator (8) and concentrate in discharging opening (33) flow to surge tank (7).
2. the process units of hot reaction essence according to claim 1, described reaction kettle body (1) is also provided with dog-house (11), agitating device (12), temperature control interlayer (13), temperature sensor (14), drain hole (15), pressure sensor (17), safety valve (18); Described temperature controls can admittance deep fat, high-temperature steam or frozen water in interlayer (13).
3. the process units of hot reaction essence according to claim 1, described condenser (2) is the one in shell and tube condenser, jacket type condenser or coiler type condenser.
4. the process units of hot reaction essence according to claim 1, described chromatographic column (3) is also provided with temperature and controls interlayer (32) composition; Described temperature controls can lead to hot water or frozen water in interlayer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520645204.0U CN204816541U (en) | 2015-08-25 | 2015-08-25 | Apparatus for producing of thermal response essence |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201520645204.0U CN204816541U (en) | 2015-08-25 | 2015-08-25 | Apparatus for producing of thermal response essence |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN204816541U true CN204816541U (en) | 2015-12-02 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201520645204.0U Active CN204816541U (en) | 2015-08-25 | 2015-08-25 | Apparatus for producing of thermal response essence |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN204816541U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108998245A (en) * | 2018-08-30 | 2018-12-14 | 王婧婧 | A kind of preparation method of wine taste essence |
| CN109090700A (en) * | 2018-09-20 | 2018-12-28 | 云南中烟工业有限责任公司 | A kind of high efficiency preparation method and purposes of coffee absolute oil |
-
2015
- 2015-08-25 CN CN201520645204.0U patent/CN204816541U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108998245A (en) * | 2018-08-30 | 2018-12-14 | 王婧婧 | A kind of preparation method of wine taste essence |
| CN109090700A (en) * | 2018-09-20 | 2018-12-28 | 云南中烟工业有限责任公司 | A kind of high efficiency preparation method and purposes of coffee absolute oil |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Yang Yirong Inventor before: Wang Jingjing |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20171228 Address after: 361028 Xinchang Road, Haicang Xinyang Industrial Zone, Xiamen, Fujian Province, No. 30 Patentee after: Xiamen Zhongkun Chemical Co., Ltd. Address before: 237364 Anhui County of Jinzhai city of Lu'an Province Tang Jiahui town streets two groups Patentee before: Wang Jingjing |