CN105011366A - Composite adsorbent for health-care cigarette filter with function of relieving fatigue - Google Patents

Composite adsorbent for health-care cigarette filter with function of relieving fatigue Download PDF

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Publication number
CN105011366A
CN105011366A CN201510300750.5A CN201510300750A CN105011366A CN 105011366 A CN105011366 A CN 105011366A CN 201510300750 A CN201510300750 A CN 201510300750A CN 105011366 A CN105011366 A CN 105011366A
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China
Prior art keywords
oil
health
fatigue
modified inorganic
powder
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Pending
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CN201510300750.5A
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Chinese (zh)
Inventor
杜威
郭杰
郑鸿雁
陶香君
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Chuzhou Cigarette Materials Factory
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Chuzhou Cigarette Materials Factory
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Priority to CN201510300750.5A priority Critical patent/CN105011366A/en
Publication of CN105011366A publication Critical patent/CN105011366A/en
Pending legal-status Critical Current

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Abstract

The invention discloses a composite adsorbent for a health-care cigarette filter with a function of relieving fatigue. The composite adsorbent is characterized by comprising following raw materials, by weight, 30 to 40 parts of polyving akohol, 0.1 to 0.2 part of wintergreen oil, 0.05 to 0.1 part of eucalyptus oil, 0.02 to 0.04 part of rhizoma acori graminei oil, 0.05 to 0.1 part of wheat germ oil, 0.5 to 1 part of walnut oil, 5 to 10 parts of corn starch, 3 to 5 parts of sodium alginate, 0.3 to 0.5 part of a silane coupling agent A-151, and 5 to 10 parts of modified inorganic powders. The composite adsorbent for the health-care cigarette filter has following beneficial effects: harmful substance in fuel gas can be efficiently filtered and absorbed in order to achieve effects of tar reduction and toxicity attenuation; smoke taste can be maintained; functions of relieving fatigue and inducing resuscitation are fulfilled; and fine health efficacy is obtained.

Description

A kind of fatigue-relieving health filter-tip of cigarette compound adsorbent and preparation method thereof
Technical field
The present invention relates to cigarette filter tip materials field, be specifically related to a kind of fatigue-relieving health filter-tip of cigarette compound adsorbent and preparation method thereof.
Background technology
The diseases related caused along with smoking is more and more frequent, and the infringement of smoking to human body becomes common recognition.Main component tar, nicotine and CO etc. in cigarette smoke are all to human body poisonous and harmful, and wherein tar has carcinogenesis to people, and CO causes anoxic, and nicotine easily makes people produce dependence, can also benumb the respiratory center of people, cause angiocardiopathy etc.Filter tip can not only part harmful components in filtering flue gas, and can TPM in effectively catching cigarette mainstream flue gas, reduce tar content, reducing the harm of flue gas to health and environment, is therefore that cigarette is fallen Jiao, fallen harm and manage the most frequently used means to the improvement of cigarette filter tip materials.
At present, the filtering material generally used has Diacetate cellulose tow, polypropylene tows, active carbon, inorganic mineral fiber etc.Suitable filter tip material not only needs optionally to filter and adsorb the harmful substance in flue gas, reduce the stimulation of flue gas to oral cavity and the injury to health, also should be able to keep the mouthfeel of flue gas, retain harmless fragrance component, the development of filter tip material also has larger market prospects and practical value.
Summary of the invention
The object of this invention is to provide a kind of fatigue-relieving health filter-tip of cigarette compound adsorbent, energy high efficiency filter and the harmful substance of adsorbing in flue gas, reach the effect of falling Jiao, toxicity reduction.
The present invention is achieved by the following technical solutions:
A kind of fatigue-relieving health filter-tip of cigarette compound adsorbent, it is obtained by the raw material of following weight parts:
Polyvinyl alcohol 30-40, wintergreen 0.1-0.2, eucalyptus oil 0.05-0.1, Rhizoma Acori Graminei oil 0.02-0.04, wheat-germ oil 0.05-0.1, walnut oil 0.5-1, cornstarch 5-10, sodium alginate 3-5, silane coupling A-151 0.3-0.5, modified inorganic powder 5-10;
Described modified inorganic powder is obtained by the raw material of following weight parts: sodium-based montmorillonite 20-30, zeolite powder 4-6, citric acid 1-2, single stearine 0.1-0.2; Citric acid and single stearine add in suitable quantity of water by the preparation method of described modified inorganic powder, 10-20min is stirred prior to 60-80 DEG C, more ultrasonic process 20-30min under adding sodium-based montmorillonite and the same temperature of zeolite powder, after filtration, filtration cakes torrefaction is complete, grinding evenly, to obtain final product.
A preparation method for fatigue-relieving health filter-tip of cigarette compound adsorbent, comprises the following steps:
(1) first wintergreen, eucalyptus oil, Rhizoma Acori Graminei oil, wheat-germ oil and walnut oil are mixed, then mix with modified inorganic powder, after stirring at normal temperature 2-4h, after grinding evenly, obtain active powder;
(2) first press solid-liquid weight ratio 1:15-1:20 polyvinyl alcohol and sodium alginate are mixed with water, 85-95 DEG C is stirred until dissolve completely, then the active powder added in cornstarch and (1) stirs 2-4h at same temperature, 10-15min is stirred under adding the same temperature of silane coupling A-151 again, finally add the BAS solidification process 12-24h of appropriate calcium chloride, obtain adsorbent matrix, the every 100mL of BAS of described calcium chloride contains 4g boric acid, 5g calcium chloride;
(3) by the adsorbent matrix use water cleaning for several times postlyophilization in (2), pulverizes and grind even after namely obtain fatigue-relieving cigarette filter compound adsorbent.
Advantage of the present invention is:
Using polyvinyl alcohol, cornstarch and sodium alginate as base material, with the inorganic particle compound of carrying active composition, first obtain the gel with grid cross-linked structure by solidification process, and the compatibility of gel and oils is improved with silane coupling A-151 modification, improve its adsorption capacity to tar ingredients in flue gas; High hole adsorbing base is obtained again by freeze drying, the compound adsorbent with high-specific surface area, high absorption property is obtained finally by pulverizing milled processed, pass through the composite of active component simultaneously, make this compound adsorbent can high efficiency filter and absorption flue gas in harmful substance, reach the effect of falling Jiao, toxicity reduction, keep the mouthfeel of flue gas simultaneously, also there is fatigue-relieving, the effect of inducing resuscitation of having one's ideas straightened out, there is good health-care efficacy.
Detailed description of the invention
Non-limiting examples of the present invention is as follows:
A kind of fatigue-relieving health filter-tip of cigarette compound adsorbent, is prepared from by the component raw material of following weight (kg):
Polyvinyl alcohol 35, wintergreen 0.15, eucalyptus oil 0.08, Rhizoma Acori Graminei oil 0.03, wheat-germ oil 0.08, walnut oil 0.8, cornstarch 8, sodium alginate 4, silane coupling A-151 0.4, modified inorganic powder 8;
Described modified inorganic powder is obtained by the raw material of following weight parts: sodium-based montmorillonite 25, zeolite powder 5, citric acid 1.5, single stearine 0.15; Citric acid and single stearine add in suitable quantity of water by the preparation method of described modified inorganic powder, 10min is stirred prior to 80 DEG C, more ultrasonic process 30min under adding sodium-based montmorillonite and the same temperature of zeolite powder, after filtration, filtration cakes torrefaction is complete, grinding evenly, to obtain final product.
The preparation method of fatigue-relieving health filter-tip of cigarette compound adsorbent comprises the following steps:
(1) first wintergreen, eucalyptus oil, Rhizoma Acori Graminei oil, wheat-germ oil and walnut oil are mixed, then mix with modified inorganic powder, after stirring at normal temperature 3h, after grinding evenly, obtain active powder;
(2) first press solid-liquid weight ratio 1:15 polyvinyl alcohol and sodium alginate are mixed with water, 95 DEG C are stirred until dissolve completely, then the active powder added in cornstarch and (1) stirs 2h at same temperature, 10min is stirred under adding the same temperature of silane coupling A-151 again, finally add the BAS solidification process 12h of appropriate calcium chloride, obtain adsorbent matrix, wherein the every 100mL of the BAS of calcium chloride is containing 4g boric acid, 5g calcium chloride;
(3) by the adsorbent matrix use water cleaning for several times postlyophilization in (2), pulverizes and grind even after namely obtain fatigue-relieving cigarette filter compound adsorbent.
Before filter tip acetate fibres beam forming, by above-mentioned obtained adsorbent by fibre weight 20% addition be evenly sprinkling upon on the synnema of filter stick, be prepared into cigarette filter rod.Smoking result shows, sorbing material does not cause original suction taste style to change, and tarry matters in smoke reduction simultaneously 61%, nitrosamine reduction by 57%, CO reduce by 26%.

Claims (2)

1. a fatigue-relieving health filter-tip of cigarette compound adsorbent, is characterized in that, it is obtained by the raw material of following weight parts:
Polyvinyl alcohol 30-40, wintergreen 0.1-0.2, eucalyptus oil 0.05-0.1, Rhizoma Acori Graminei oil 0.02-0.04, wheat-germ oil 0.05-0.1, walnut oil 0.5-1, cornstarch 5-10, sodium alginate 3-5, silane coupling A-151 0.3-0.5, modified inorganic powder 5-10;
Described modified inorganic powder is obtained by the raw material of following weight parts: sodium-based montmorillonite 20-30, zeolite powder 4-6, citric acid 1-2, single stearine 0.1-0.2; Citric acid and single stearine add in suitable quantity of water by the preparation method of described modified inorganic powder, 10-20min is stirred prior to 60-80 DEG C, more ultrasonic process 20-30min under adding sodium-based montmorillonite and the same temperature of zeolite powder, after filtration, filtration cakes torrefaction is complete, grinding evenly, to obtain final product.
2. the preparation method of a kind of fatigue-relieving health filter-tip of cigarette compound adsorbent according to claim 1, is characterized in that, comprise the following steps:
(1) first wintergreen, eucalyptus oil, Rhizoma Acori Graminei oil, wheat-germ oil and walnut oil are mixed, then mix with modified inorganic powder, after stirring at normal temperature 2-4h, after grinding evenly, obtain active powder;
(2) first press solid-liquid weight ratio 1:15-1:20 polyvinyl alcohol and sodium alginate are mixed with water, 85-95 DEG C is stirred until dissolve completely, then the active powder added in cornstarch and (1) stirs 2-4h at same temperature, 10-15min is stirred under adding the same temperature of silane coupling A-151 again, finally add the BAS solidification process 12-24h of appropriate calcium chloride, obtain adsorbent matrix, the every 100mL of BAS of described calcium chloride contains 4g boric acid, 5g calcium chloride;
(3) by the adsorbent matrix use water cleaning for several times postlyophilization in (2), pulverizes and grind even after namely obtain fatigue-relieving cigarette filter compound adsorbent.
CN201510300750.5A 2015-06-05 2015-06-05 Composite adsorbent for health-care cigarette filter with function of relieving fatigue Pending CN105011366A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1059267A (en) * 1990-08-25 1992-03-11 长春冶金地质专科学校 Specific adsorbent of cigarette tar and production technology
CN1081853A (en) * 1993-07-03 1994-02-16 彭宗禹 Healthy cigarette holders for reducing nicotine
WO2007086078A2 (en) * 2006-01-30 2007-08-02 Panacea Biotec Ltd. Novel pharmaceutical compositions and process of preparation thereof
CN101785581A (en) * 2009-01-23 2010-07-28 石永江 Smoking-cessation and health-care cigarette holders and using method thereof
CN103566882A (en) * 2013-09-29 2014-02-12 安徽金叶炭素科技有限公司 High-adsorptivity modified activated carbon and preparation method thereof
CN104437371A (en) * 2014-11-20 2015-03-25 安徽天泰环保科技有限公司 Composite porous activated carbon flue gas adsorbent and preparation method thereof

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1059267A (en) * 1990-08-25 1992-03-11 长春冶金地质专科学校 Specific adsorbent of cigarette tar and production technology
CN1081853A (en) * 1993-07-03 1994-02-16 彭宗禹 Healthy cigarette holders for reducing nicotine
WO2007086078A2 (en) * 2006-01-30 2007-08-02 Panacea Biotec Ltd. Novel pharmaceutical compositions and process of preparation thereof
CN101785581A (en) * 2009-01-23 2010-07-28 石永江 Smoking-cessation and health-care cigarette holders and using method thereof
CN103566882A (en) * 2013-09-29 2014-02-12 安徽金叶炭素科技有限公司 High-adsorptivity modified activated carbon and preparation method thereof
CN104437371A (en) * 2014-11-20 2015-03-25 安徽天泰环保科技有限公司 Composite porous activated carbon flue gas adsorbent and preparation method thereof

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Application publication date: 20151104