CN104941587A - Spirit-raising and tar-reducing type cigarette filter composite adsorbent and preparation method thereof - Google Patents
Spirit-raising and tar-reducing type cigarette filter composite adsorbent and preparation method thereof Download PDFInfo
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- CN104941587A CN104941587A CN201510300871.XA CN201510300871A CN104941587A CN 104941587 A CN104941587 A CN 104941587A CN 201510300871 A CN201510300871 A CN 201510300871A CN 104941587 A CN104941587 A CN 104941587A
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Abstract
The invention discloses a spirit-raising and tar-reducing type cigarette filter composite adsorbent, which is characterized by comprising the following raw materials in weight part: 30-40 parts of polyvinyl alcohol, 0.1-0.2 part of peppermint oil, 0.05-0.1 part of borneol, 0.5-1 part of walnut oil, 5-10 parts of starch maize, 3-5 parts of pine needle meal, 3-5 parts of sodium alginate, 0.4-0.6 part of silane coupling agent A-151, and 5-10 parts of modified inorganic powders. According to the invention, by means of the cigarette filter composite adsorbent, harmful substances in the flue gas can be efficiently filtered and absorbed, so that the tar-reducing and poison-reducing effects are realized. Meanwhile, the mouth feel of the flue gas is kept the same. The cigarette filter composite adsorbent also has the effects of refreshing the brain, dispelling the melancholy, easing the pain and removing the inflammation. Therefore, the cigarette filter composite adsorbent is good in health-care efficacy.
Description
Technical field
The present invention relates to cigarette filter tip materials field, be specifically related to one and refresh oneself and fall burnt odor tobacco filters compound adsorbent and preparation method thereof.
Background technology
The diseases related caused along with smoking is more and more frequent, and the infringement of smoking to human body becomes common recognition.Main component tar, nicotine and CO etc. in cigarette smoke are all to human body poisonous and harmful, and wherein tar has carcinogenesis to people, and CO causes anoxic, and nicotine easily makes people produce dependence, can also benumb the respiratory center of people, cause angiocardiopathy etc.Filter tip can not only part harmful components in filtering flue gas, and can TPM in effectively catching cigarette mainstream flue gas, reduce tar content, reducing the harm of flue gas to health and environment, is therefore that cigarette is fallen Jiao, fallen harm and manage the most frequently used means to the improvement of cigarette filter tip materials.
At present, the filtering material generally used has Diacetate cellulose tow, polypropylene tows, active carbon, inorganic mineral fiber etc.Suitable filter tip material not only needs optionally to filter and adsorb the harmful substance in flue gas, reduce the stimulation of flue gas to oral cavity and the injury to health, also should be able to keep the mouthfeel of flue gas, retain harmless fragrance component, the development of filter tip material also has larger market prospects and practical value.
Summary of the invention
The object of this invention is to provide one to refresh oneself and fall burnt odor tobacco filters compound adsorbent, can harmful substance in high efficiency filter and absorption flue gas, reach the effect of falling Jiao, toxicity reduction.
The present invention is achieved by the following technical solutions:
One is refreshed oneself and is fallen burnt odor tobacco filters compound adsorbent, and it is obtained by the raw material of following weight parts:
Polyvinyl alcohol 30-40, peppermint oil 0.1-0.2, borneol 0.05-0.1, walnut oil 0.5-1, cornstarch 5-10, pine needle meal 3-5, sodium alginate 3-5, silane coupling A-151 0.4-0.6, modified inorganic powder 5-10;
Described modified inorganic powder is obtained by the raw material of following weight parts: sodium-based montmorillonite 20-30, zeolite powder 4-6, citric acid 1-2, single stearine 0.1-0.2; Citric acid and single stearine add in suitable quantity of water by the preparation method of described modified inorganic powder, 10-20min is stirred prior to 60-80 DEG C, more ultrasonic process 20-30min under adding sodium-based montmorillonite and the same temperature of zeolite powder, after filtration, filtration cakes torrefaction is complete, grinding evenly, to obtain final product.
Refresh oneself and fall a preparation method for burnt odor tobacco filters compound adsorbent, comprise the following steps:
(1) first by peppermint oil, borneol and walnut oil mixing and stirring, then mix with modified inorganic powder, after stirring at normal temperature 2-4h, after grinding evenly, obtain active powder;
(2) first press solid-liquid weight ratio 1:15-1:20 polyvinyl alcohol and sodium alginate are mixed with water, 85-95 DEG C is stirred until dissolve completely, then the active powder added in cornstarch, pine needle meal and (1) stirs 2-4h at same temperature, 10-15min is stirred under adding the same temperature of silane coupling A-151 again, finally add the BAS solidification process 12-24h of appropriate calcium chloride, obtain adsorbent matrix, the every 100mL of BAS of described calcium chloride contains 4g boric acid, 5g calcium chloride;
(3) by the adsorbent matrix use water cleaning for several times postlyophilization in (2), pulverizes and grind even after namely obtain to refresh oneself and fall burnt odor tobacco filters compound adsorbent.
Advantage of the present invention is:
Using polyvinyl alcohol, cornstarch and sodium alginate as base material, with inorganic particle and the pine needle meal compound of carrying active composition, first obtain the gel with grid cross-linked structure by solidification process, and the compatibility of gel and oils is improved with silane coupling A-151 modification, improve its adsorption capacity to tar ingredients in flue gas; High hole adsorbing base is obtained again by freeze drying, the compound adsorbent with high-specific surface area, high absorption property is obtained finally by pulverizing milled processed, pass through the composite of active component simultaneously, make this compound adsorbent can high efficiency filter and absorption flue gas in harmful substance, reach the effect of falling Jiao, toxicity reduction, keep the mouthfeel of flue gas simultaneously, also there is the Xie Yu that refreshes oneself, effect of easing pain and diminishing inflammation, has good health-care efficacy.
Detailed description of the invention
Non-limiting examples of the present invention is as follows:
One is refreshed oneself and is fallen burnt odor tobacco filters compound adsorbent, is prepared from by the component raw material of following weight (kg):
Polyvinyl alcohol 35, peppermint oil 0.15, borneol 0.08, walnut oil 0.8, cornstarch 8, pine needle meal 4, sodium alginate 4, silane coupling A-151 0.5, modified inorganic powder 8;
Described modified inorganic powder is obtained by the raw material of following weight parts: sodium-based montmorillonite 25, zeolite powder 5, citric acid 1.5, single stearine 0.15; Citric acid and single stearine add in suitable quantity of water by the preparation method of described modified inorganic powder, 10min is stirred prior to 80 DEG C, more ultrasonic process 30min under adding sodium-based montmorillonite and the same temperature of zeolite powder, after filtration, filtration cakes torrefaction is complete, grinding evenly, to obtain final product.
The preparation method falling burnt odor tobacco filters compound adsorbent that refreshes oneself comprises the following steps:
(1) first by peppermint oil, borneol and walnut oil mixing and stirring, then mix with modified inorganic powder, after stirring at normal temperature 3h, after grinding evenly, obtain active powder;
(2) first press solid-liquid weight ratio 1:15 polyvinyl alcohol and sodium alginate are mixed with water, 95 DEG C are stirred until dissolve completely, then the active powder added in cornstarch, pine needle meal and (1) stirs 2h at same temperature, 10min is stirred under adding the same temperature of silane coupling A-151 again, finally add the BAS solidification process 12h of appropriate calcium chloride, obtain adsorbent matrix, wherein the every 100mL of the BAS of calcium chloride is containing 4g boric acid, 5g calcium chloride;
(3) by the adsorbent matrix use water cleaning for several times postlyophilization in (2), pulverizes and grind even after namely obtain to refresh oneself and fall burnt odor tobacco filters compound adsorbent.
Before filter tip acetate fibres beam forming, by above-mentioned obtained adsorbent by fibre weight 20% addition be evenly sprinkling upon on the synnema of filter stick, be prepared into cigarette filter rod.Smoking result shows, sorbing material does not cause original suction taste style to change, and tarry matters in smoke reduction simultaneously 58%, nitrosamine reduction by 57%, CO reduce by 25%.
Claims (2)
1. refresh oneself and fall a burnt odor tobacco filters compound adsorbent, it is characterized in that, it is obtained by the raw material of following weight parts:
Polyvinyl alcohol 30-40, peppermint oil 0.1-0.2, borneol 0.05-0.1, walnut oil 0.5-1, cornstarch 5-10, pine needle meal 3-5, sodium alginate 3-5, silane coupling A-151 0.4-0.6, modified inorganic powder 5-10;
Described modified inorganic powder is obtained by the raw material of following weight parts: sodium-based montmorillonite 20-30, zeolite powder 4-6, citric acid 1-2, single stearine 0.1-0.2; Citric acid and single stearine add in suitable quantity of water by the preparation method of described modified inorganic powder, 10-20min is stirred prior to 60-80 DEG C, more ultrasonic process 20-30min under adding sodium-based montmorillonite and the same temperature of zeolite powder, after filtration, filtration cakes torrefaction is complete, grinding evenly, to obtain final product.
2. according to claim 1 a kind of refresh oneself the preparation method of burnt odor tobacco filters compound adsorbent falls, it is characterized in that, comprise the following steps:
(1) first by peppermint oil, borneol and walnut oil mixing and stirring, then mix with modified inorganic powder, after stirring at normal temperature 2-4h, after grinding evenly, obtain active powder;
(2) first press solid-liquid weight ratio 1:15-1:20 polyvinyl alcohol and sodium alginate are mixed with water, 85-95 DEG C is stirred until dissolve completely, then the active powder added in cornstarch, pine needle meal and (1) stirs 2-4h at same temperature, 10-15min is stirred under adding the same temperature of silane coupling A-151 again, finally add the BAS solidification process 12-24h of appropriate calcium chloride, obtain adsorbent matrix, the every 100mL of BAS of described calcium chloride contains 4g boric acid, 5g calcium chloride;
(3) by the adsorbent matrix use water cleaning for several times postlyophilization in (2), pulverizes and grind even after namely obtain to refresh oneself and fall burnt odor tobacco filters compound adsorbent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510300871.XA CN104941587A (en) | 2015-06-05 | 2015-06-05 | Spirit-raising and tar-reducing type cigarette filter composite adsorbent and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510300871.XA CN104941587A (en) | 2015-06-05 | 2015-06-05 | Spirit-raising and tar-reducing type cigarette filter composite adsorbent and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107185022A (en) * | 2017-06-13 | 2017-09-22 | 四川建源节能科技有限公司 | A kind of air purifying preparation and its reparation technology |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1059267A (en) * | 1990-08-25 | 1992-03-11 | 长春冶金地质专科学校 | Specific adsorbent of cigarette tar and production technology |
| CN102423132A (en) * | 2011-08-15 | 2012-04-25 | 武汉力诚生物科技有限公司 | Plant polysaccharide cigarette filter tip and preparation method thereof |
-
2015
- 2015-06-05 CN CN201510300871.XA patent/CN104941587A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1059267A (en) * | 1990-08-25 | 1992-03-11 | 长春冶金地质专科学校 | Specific adsorbent of cigarette tar and production technology |
| CN102423132A (en) * | 2011-08-15 | 2012-04-25 | 武汉力诚生物科技有限公司 | Plant polysaccharide cigarette filter tip and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107185022A (en) * | 2017-06-13 | 2017-09-22 | 四川建源节能科技有限公司 | A kind of air purifying preparation and its reparation technology |
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Application publication date: 20150930 |
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