CN104959126A - Throat-clearing-and-nourishing composite adsorbent for cigarette filter and preparation method thereof - Google Patents
Throat-clearing-and-nourishing composite adsorbent for cigarette filter and preparation method thereof Download PDFInfo
- Publication number
- CN104959126A CN104959126A CN201510300535.5A CN201510300535A CN104959126A CN 104959126 A CN104959126 A CN 104959126A CN 201510300535 A CN201510300535 A CN 201510300535A CN 104959126 A CN104959126 A CN 104959126A
- Authority
- CN
- China
- Prior art keywords
- throat
- parts
- cigarette filter
- clearing
- adsorbent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention discloses a throat-clearing-and-nourishing composite adsorbent for a cigarette filter. The adsorbent is characterized by being prepared from the following raw materials by weight: 30 to 40 parts of polyvinyl alcohol, 3 to 5 parts of licorice, 2 to 4 parts of cape jasmine, 1 to 2 parts of tuber of dwarf lilyturf, 1 to 2 parts of boat-fruited sterculia, 0.05 to 0.1 part of sodium dodecyl sulfate, 5 to 10 parts of maize starch, 3 to 5 parts of sodium alginate, 0.3 to 0.5 part of a silane coupling agent A-151 and 5 to 10 parts of modified inorganic powder. The composite adsorbent for the cigarette filter can highly efficiently filter out and adsorb harmful substances in smoke and achieve the effect of reduction in tar and toxic matters, maintains the taste of smoke, is capable of clearing the throat, stopping pain, relieving cough and nourishing the throat and has health care efficacy.
Description
Technical field
The present invention relates to cigarette filter tip materials field, be specifically related to a kind of throat-clearing throat-moistening cigarette filter compound adsorbent and preparation method thereof.
Background technology
The diseases related caused along with smoking is more and more frequent, and the infringement of smoking to human body becomes common recognition.Main component tar, nicotine and CO etc. in cigarette smoke are all to human body poisonous and harmful, and wherein tar has carcinogenesis to people, and CO causes anoxic, and nicotine easily makes people produce dependence, can also benumb the respiratory center of people, cause angiocardiopathy etc.Filter tip can not only part harmful components in filtering flue gas, and can TPM in effectively catching cigarette mainstream flue gas, reduce tar content, reducing the harm of flue gas to health and environment, is therefore that cigarette is fallen Jiao, fallen harm and manage the most frequently used means to the improvement of cigarette filter tip materials.
At present, the filtering material generally used has Diacetate cellulose tow, polypropylene tows, active carbon, inorganic mineral fiber etc.Suitable filter tip material not only needs optionally to filter and adsorb the harmful substance in flue gas, reduce the stimulation of flue gas to oral cavity and the injury to health, also should be able to keep the mouthfeel of flue gas, retain harmless fragrance component, the development of filter tip material also has larger market prospects and practical value.
Summary of the invention
The object of this invention is to provide a kind of throat-clearing throat-moistening cigarette filter compound adsorbent, energy high efficiency filter and the harmful substance of adsorbing in flue gas, reach the effect of falling Jiao, toxicity reduction.
The present invention is achieved by the following technical solutions:
A kind of throat-clearing throat-moistening cigarette filter compound adsorbent, it is obtained by the raw material of following weight parts:
Polyvinyl alcohol 30-40, Radix Glycyrrhizae 3-5, cape jasmine 2-4, the tuber of dwarf lilyturf 1-2, sterculia seed 1-2, lauryl sodium sulfate 0.05-0.1, cornstarch 5-10, sodium alginate 3-5, silane coupling A-151 0.3-0.5, modified inorganic powder 5-10;
Described modified inorganic powder is obtained by the raw material of following weight parts: sodium-based montmorillonite 20-30, zeolite powder 4-6, citric acid 1-2, shitosan 0.1-0.2; Citric acid and shitosan add in suitable quantity of water by the preparation method of described modified inorganic powder, 60-80 DEG C is stirred until dissolve completely, more ultrasonic process 20-30min under adding sodium-based montmorillonite and the same temperature of zeolite powder, after filtration, filtration cakes torrefaction is complete, grinding evenly, to obtain final product.
A preparation method for throat-clearing throat-moistening cigarette filter compound adsorbent, comprises the following steps:
(1) Radix Glycyrrhizae, cape jasmine, the tuber of dwarf lilyturf, the sterculia seed and lauryl sodium sulfate are added first 70-80 DEG C of stirring 6-8h in suitable quantity of water, ultrasonic process 10-20min again, cooled and filtered removing filter residue, mix and stirring at normal temperature 4-6h with modified inorganic powder after the filtrate obtained is fully concentrated, complete in 70-80 DEG C of drying after filtration, obtain active powder after grinding evenly;
(2) first press solid-liquid weight ratio 1:15-1:20 polyvinyl alcohol and sodium alginate are mixed with water, 85-95 DEG C is stirred until dissolve completely, then the active powder added in cornstarch and (1) stirs 2-4h at same temperature, 10-15min is stirred under adding the same temperature of silane coupling A-151 again, finally add the BAS solidification process 12-24h of appropriate calcium chloride, obtain adsorbent matrix, the every 100mL of BAS of described calcium chloride contains 4g boric acid, 5g calcium chloride;
(3) by the adsorbent matrix use water cleaning for several times postlyophilization in (2), pulverizes and grind even after namely obtain throat-clearing throat-moistening cigarette filter compound adsorbent.
Advantage of the present invention is:
Using polyvinyl alcohol, cornstarch and sodium alginate as base material, with the inorganic particle compound of carrying active composition, first obtain the gel with grid cross-linked structure by solidification process, and the compatibility of gel and oils is improved with silane coupling A-151 modification, improve its adsorption capacity to tar ingredients in flue gas; High hole adsorbing base is obtained again by freeze drying, the compound adsorbent with high-specific surface area, high absorption property is obtained finally by pulverizing milled processed, pass through the composite of active component simultaneously, make this compound adsorbent can high efficiency filter and absorption flue gas in harmful substance, reach the effect of falling Jiao, toxicity reduction, keep the mouthfeel of flue gas simultaneously, also there is clearing pain relieving, effect that cough-relieving wets one's whistle, there is good health-care efficacy.
Detailed description of the invention
Non-limiting examples of the present invention is as follows:
A kind of throat-clearing throat-moistening cigarette filter compound adsorbent, is prepared from by the component raw material of following weight (kg):
Polyvinyl alcohol 35, Radix Glycyrrhizae 4, cape jasmine 3, the tuber of dwarf lilyturf 1.5, the sterculia seed 1.5, lauryl sodium sulfate 0.08, cornstarch 8, sodium alginate 4, silane coupling A-151 0.4, modified inorganic powder 8;
Described modified inorganic powder is obtained by the raw material of following weight parts: sodium-based montmorillonite 25, zeolite powder 5, citric acid 1.5, shitosan 0.15; Citric acid and shitosan add in suitable quantity of water by the preparation method of described modified inorganic powder, 80 DEG C are stirred until dissolve completely, more ultrasonic process 20min under adding sodium-based montmorillonite and the same temperature of zeolite powder, after filtration, filtration cakes torrefaction is complete, grinding evenly, to obtain final product.
The preparation method of throat-clearing throat-moistening cigarette filter compound adsorbent comprises the following steps:
(1) Radix Glycyrrhizae, cape jasmine, the tuber of dwarf lilyturf, the sterculia seed and lauryl sodium sulfate are added first 80 DEG C of stirring 6h in suitable quantity of water, ultrasonic process 10min again, cooled and filtered removing filter residue, mix and stirring at normal temperature 4h with modified inorganic powder after the filtrate obtained is fully concentrated, complete in 80 DEG C of dryings after filtration, obtain active powder after grinding evenly;
(2) first press solid-liquid weight ratio 1:15 polyvinyl alcohol and sodium alginate are mixed with water, 95 DEG C are stirred until dissolve completely, then the active powder added in cornstarch and (1) stirs 2h at same temperature, 10min is stirred under adding the same temperature of silane coupling A-151 again, finally add the BAS solidification process 12h of appropriate calcium chloride, obtain adsorbent matrix, wherein the every 100mL of the BAS of calcium chloride is containing 4g boric acid, 5g calcium chloride;
(3) by the adsorbent matrix use water cleaning for several times postlyophilization in (2), pulverizes and grind even after namely obtain throat-clearing throat-moistening cigarette filter compound adsorbent.
Before filter tip acetate fibres beam forming, by above-mentioned obtained adsorbent by fibre weight 20% addition be evenly sprinkling upon on the synnema of filter stick, be prepared into cigarette filter rod.Smoking result shows, sorbing material does not cause original suction taste style to change, and tarry matters in smoke reduction simultaneously 48%, nitrosamine reduction by 64%, CO reduce by 32%.
Claims (2)
1. a throat-clearing throat-moistening cigarette filter compound adsorbent, is characterized in that, it is obtained by the raw material of following weight parts:
Polyvinyl alcohol 30-40, Radix Glycyrrhizae 3-5, cape jasmine 2-4, the tuber of dwarf lilyturf 1-2, sterculia seed 1-2, lauryl sodium sulfate 0.05-0.1, cornstarch 5-10, sodium alginate 3-5, silane coupling A-151 0.3-0.5, modified inorganic powder 5-10;
Described modified inorganic powder is obtained by the raw material of following weight parts: sodium-based montmorillonite 20-30, zeolite powder 4-6, citric acid 1-2, shitosan 0.1-0.2; Citric acid and shitosan add in suitable quantity of water by the preparation method of described modified inorganic powder, 60-80 DEG C is stirred until dissolve completely, more ultrasonic process 20-30min under adding sodium-based montmorillonite and the same temperature of zeolite powder, after filtration, filtration cakes torrefaction is complete, grinding evenly, to obtain final product.
2. the preparation method of a kind of throat-clearing throat-moistening cigarette filter compound adsorbent according to claim 1, is characterized in that, comprise the following steps:
(1) Radix Glycyrrhizae, cape jasmine, the tuber of dwarf lilyturf, the sterculia seed and lauryl sodium sulfate are added first 70-80 DEG C of stirring 6-8h in suitable quantity of water, ultrasonic process 10-20min again, cooled and filtered removing filter residue, mix and stirring at normal temperature 4-6h with modified inorganic powder after the filtrate obtained is fully concentrated, complete in 70-80 DEG C of drying after filtration, obtain active powder after grinding evenly;
(2) first press solid-liquid weight ratio 1:15-1:20 polyvinyl alcohol and sodium alginate are mixed with water, 85-95 DEG C is stirred until dissolve completely, then the active powder added in cornstarch and (1) stirs 2-4h at same temperature, 10-15min is stirred under adding the same temperature of silane coupling A-151 again, finally add the BAS solidification process 12-24h of appropriate calcium chloride, obtain adsorbent matrix, the every 100mL of BAS of described calcium chloride contains 4g boric acid, 5g calcium chloride;
(3) by the adsorbent matrix use water cleaning for several times postlyophilization in (2), pulverizes and grind even after namely obtain throat-clearing throat-moistening cigarette filter compound adsorbent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510300535.5A CN104959126A (en) | 2015-06-05 | 2015-06-05 | Throat-clearing-and-nourishing composite adsorbent for cigarette filter and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510300535.5A CN104959126A (en) | 2015-06-05 | 2015-06-05 | Throat-clearing-and-nourishing composite adsorbent for cigarette filter and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104959126A true CN104959126A (en) | 2015-10-07 |
Family
ID=54213310
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510300535.5A Pending CN104959126A (en) | 2015-06-05 | 2015-06-05 | Throat-clearing-and-nourishing composite adsorbent for cigarette filter and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104959126A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115445578A (en) * | 2022-08-30 | 2022-12-09 | 南京植创生物技术研究院有限公司 | Composite montmorillonite particles for cigarette filter tip and preparation method and application thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1059267A (en) * | 1990-08-25 | 1992-03-11 | 长春冶金地质专科学校 | Specific adsorbent of cigarette tar and production technology |
| CN102423132A (en) * | 2011-08-15 | 2012-04-25 | 武汉力诚生物科技有限公司 | Plant polysaccharide cigarette filter tip and preparation method thereof |
-
2015
- 2015-06-05 CN CN201510300535.5A patent/CN104959126A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1059267A (en) * | 1990-08-25 | 1992-03-11 | 长春冶金地质专科学校 | Specific adsorbent of cigarette tar and production technology |
| CN102423132A (en) * | 2011-08-15 | 2012-04-25 | 武汉力诚生物科技有限公司 | Plant polysaccharide cigarette filter tip and preparation method thereof |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115445578A (en) * | 2022-08-30 | 2022-12-09 | 南京植创生物技术研究院有限公司 | Composite montmorillonite particles for cigarette filter tip and preparation method and application thereof |
| CN115445578B (en) * | 2022-08-30 | 2024-03-01 | 南京植创生物技术研究院有限公司 | Composite montmorillonite particle for cigarette filter tip and preparation method and application thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104959127A (en) | Tranquillizing soothing health-care composite adsorbent for cigarette filter and preparation method thereof | |
| CN103932386B (en) | The low harmful element cigarette of selenium-enriched plant | |
| CN102266122A (en) | Smoking filter material using hemp straw active carbon | |
| CN104905409A (en) | Healthcare cigarette filter tip composite adsorbent with functions of relieving cough and reducing sputum and preparation method thereof | |
| CN112568242A (en) | Folium artemisiae argyi mosquito-repellent incense and preparation method thereof | |
| CN113273583A (en) | Plant extract bacteriostatic agent, bacteriostatic and odor-removing type health-care cat litter containing plant extract, and preparation method and application thereof | |
| CN104941608A (en) | Attenuated and tar-reducing cigarette filter composite adsorbent and preparation method thereof | |
| CN104957768A (en) | Health care cigarette filter tip composite adsorbent for promoting sleep and preparing method thereof | |
| CN104959126A (en) | Throat-clearing-and-nourishing composite adsorbent for cigarette filter and preparation method thereof | |
| CN104923187A (en) | Anti-inflammation sore-throat-relieving cigarette filter composite adsorbent and preparation method thereof | |
| CN102423137A (en) | Fructus phyllanthi extract for cigarettes and application thereof in cigarette filter tip | |
| CN104923170A (en) | Cigarette filter tip compound adsorbent for reducing toxicity and strengthening body and preparation method of cigarette filter tip compound adsorbent | |
| CN104923188A (en) | Cigarette filter tip composite adsorbent containing aloe vera gel and preparation method of cigarette filter tip composite adsorbent | |
| CN104941587A (en) | Spirit-raising and tar-reducing type cigarette filter composite adsorbent and preparation method thereof | |
| CN202514579U (en) | Cigarette filter | |
| CN105381487A (en) | Incense capable of expelling wind and removing cold and preparation method thereof | |
| CN104921301A (en) | Composite adsorbent with persimmon peel for cigarette filter tips and method for preparing composite adsorbent | |
| CN103695174B (en) | Violet porous particles and application thereof in cigarettes | |
| CN104921300A (en) | Immunity enhancing composite adsorbent for cigarette filter tips and method for preparing immunity enhancing composite adsorbent | |
| CN105011367A (en) | Composite adsorbent for heat-clearing fire-purging cigarette filter and preparation method thereof | |
| CN104957769A (en) | Lung clearing and health care cigarette filter tip composite adsorbent and preparing method thereof | |
| CN105011366A (en) | Composite adsorbent for health-care cigarette filter with function of relieving fatigue | |
| CN104921299A (en) | Cigarette filter composite absorbent with banana peel and preparing method thereof | |
| KR20120087519A (en) | Bio-green filter | |
| CN105962413A (en) | Cigarette filter stick achieving stable aroma |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20151007 |