CN104983608A - Mud pill particle-containing mask and preparation method thereof - Google Patents
Mud pill particle-containing mask and preparation method thereof Download PDFInfo
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Abstract
The invention provides a mud pill particle-containing mask. The mask is prepared from, by weight, 41.7-92.6 parts of water, 5-10 parts of glycerin, 4-8 parts of butylene glycol, 10-70 parts of mud pill particles, 0.05-0.2 parts of sodium hyaluronate, 0.2-0.5 parts of glucan, 0.4-1 part of carbomer940, 0.2-0.5 parts of triethanolamine, 0.2-0.5 parts of phenoxyethanol, 0.003-0.006 parts of an antiseptic N950, 0.002-0.05 parts of a solubilizer CO 40, and 0.001-0.004 parts of an essence. The invention also provides a preparation method of the mask. The mud pill particle-containing mask simultaneously has the water supplementing and moisturizing effects of gel masks and the deep cleansing effect of a mud mask, and the preparation method is simple, and is convenient for realizing industrial production.
Description
Technical field
The present invention relates to cosmetic field, be specifically related to a kind of facial film containing small muddy pill granule and preparation method thereof.
Background technology
Along with the progress of society, the improving constantly of living standards of the people, cosmetics become the necessary of people's life gradually from luxury goods, the mask product of showing one's talent in polyvoltine cosmetic of comforming in recent years is more and more subject to the favor of consumer.
Facial film refers to and applies human skin, play product that the is clean and effect of protection skin, its action principle is by the parcel of facial film to skin, allow skin and air insulated, make keratodermatitis obtain supplementing of moisture, wetting agent, nutrient and softening agent etc. contained in facial film, play the effect of soft skin; Facial film also has adsorption, and when peelling off facial film, can remove dirt, oils and fats and the acne on skin, careful pore, compact skin simultaneously, plays good clean skin and skin care effect.At cosmetic mask product apoplexy due to endogenous wind, there are mounted facial film, film forming facial film, powder facial film, gypsum facial mask, mud mask etc. at present.Mud film on market and facial film are all separately use, and be used alone mud film, use bothers and replenishing water and preserving moisture effect is not strong; Be used alone facial film, cleaning effect is not strong.
Summary of the invention
In order to overcome the deficiencies in the prior art, the object of the present invention is to provide a kind of facial film containing small muddy pill granule having excellent replenishing water and preserving moisture effect and cleaning effect concurrently, the present invention simultaneously also provides the preparation method of this facial film.
For solving the problem, the technical solution adopted in the present invention is as follows:
A facial film containing small muddy pill granule, it is made up of the following component according to parts by weight: water 41.7-92.6 part, glycerol 5-10 part, butanediol 4-8 part, small muddy pill granule 10-70 part, hyaluronate sodium 0.05-0.2 part, glucosan 0.2-0.5 part, carbopol 940 0.4-1 part, triethanolamine 0.2-0.5 part, phenoxyethanol 0.2-0.5 part, Liquid BPF 9500.003-0.006 part, solubilizing agent CO 400.002-0.05 part, essence 0.001-0.004 part;
Wherein, described small muddy pill granule is made up of the following component according to parts by weight: hydroxypropyl emthylcellulose 1-5 part, microcrystalline Cellulose 10-25 part, sucrose 12-18 part, lactose 20-30 part, mud film powder 15-35 part.
Wherein:
Hyaluronate sodium, it is natural moisture preserving agent, it can form the transparent hydration shell of one deck viscoelasticity at skin surface, this tunic has good water retention, the moisture of keratodermatitis can be increased, regulation of skin metabolism, increases skin wet smooth, fine and smooth tender, thus plays crease-resistant wrinkle resistant beauty and health care functions.
Glucosan, be natural soft skin agent, glucosan has film property, skin can be helped to keep moisture, have excellent moisture-keeping efficacy, have antioxidation, significantly can reduce wrinkle of skin, improve skin elasticity; The use skinfeel that product is good can be given.
Carbopol 940 is used as clear gel in the present invention, for making the substrate of gel facial film.
Triethanolamine, in the present invention as nertralizer, uses with carbopol 940 compatibility, thus reaches the effect of thickening and moisturizing.
Phenoxyethanol and Liquid BPF 950, use as antiseptic.
Solubilizing agent CO 40 is for essence solubilising.
In the present invention, preferred scheme is that the described facial film containing small muddy pill granule is made up of the following component according to parts by weight: 56 parts, water, glycerol 8 parts, butanediol 5 parts, small muddy pill granule 30 parts, hyaluronate sodium 0.1 part, glucosan 0.3 part, carbopol 940 0.8 part, triethanolamine 0.2 part, phenoxyethanol 0.3 part, Liquid BPF 9500.005 parts, solubilizing agent CO 400.05 parts, 0.003 part, essence;
Wherein, described small muddy pill granule is made up of the following component according to parts by weight: hydroxypropyl emthylcellulose 2.4 parts, microcrystalline Cellulose 24 parts, sucrose 15.6 parts, lactose 27 parts, 20 parts, mud film powder.
The present invention also provides this to contain the preparation method of the facial film of small muddy pill granule, in turn includes the following steps:
1) water of formula ratio, glycerol, butanediol, hyaluronate sodium, glucosan are put into emulsifying pot homogenizing dispersed with stirring until dissolve completely, then constant temperature 75 ~ 85 DEG C;
2) step 1) process after, in emulsifying pot, add carbopol 940 in proportion, at 70-90 DEG C of temperature, homogenizing be stirred to material body fully dissolve after start cooling;
3) when pot kettle temperature to be emulsified is down to 35 ~ 45 DEG C, add the phenoxyethanol of formula ratio, Liquid BPF 950, solubilizing agent CO 40, essence, small muddy pill granule, triethanolamine, be stirred to and dissolve completely, filter, discharging;
4) leave standstill after discharging, subpackage, packaging.
Particularly, step 1) in time of constant temperature be 3-8min.
Particularly, it is also included in step 3) step that product detected after discharging.
Particularly, in step 3) first add small muddy pill granule and add triethanolamine again, and mixing speed is slowed to 18r/min.
Wherein, described small muddy pill granule is made according to following steps:
A, by the microcrystalline Cellulose of formula ratio, sucrose, lactose, mud film powder mix homogeneously, to be added to the water, to be heated to boiling, to be brewed into syrup; Then by fluid unit spraying dry, granule is made;
B, by the hydroxypropyl emthylcellulose of formula ratio in 5% ratio add in the ethanol of 95%, be stirred to and dissolve completely, obtained Coating Solution;
C, the Coating Solution obtained by step B is wrapped in extra-granular obtained by steps A by fluid bed side spray technique, makes small muddy pill granule.
Compared to existing technology, beneficial effect of the present invention is: the facial film containing small muddy pill granule of the present invention, have the replenishing water and preserving moisture effect of gel facial film and the deep layer cleaning effect of mud film concurrently: utilize gel facial film composition to provide sufficient moisture to skin, prevent water loss; Utilize oils and fats unnecessary in the ingredient adsorption pore of small muddy pill, promote that skin water oil balances and provides and enrich mineral.The present invention, by the selection for component and proportioning thereof, makes overall compositions obtain the functions such as good replenishing water and preserving moisture, cleaning skin, raising skin elasticity, easy to use; The present invention is applicable to various skin, nonirritant, and product cost is high; In addition, preparation method of the present invention is simple, easy to operate, is convenient to large-scale industrial production.
Below in conjunction with detailed description of the invention, the present invention is described in further detail.
Detailed description of the invention
In the specific embodiment of the present invention, all raw materials are all being buied on the market.
Embodiment 1
A facial film containing small muddy pill granule, it is made up of the following component according to parts by weight: 56 parts, water, glycerol 8 parts, butanediol 5 parts, small muddy pill granule 30 parts, hyaluronate sodium 0.1 part, glucosan 0.3 part, carbopol 940 0.8 part, triethanolamine 0.2 part, phenoxyethanol 0.3 part, Liquid BPF 9500.005 parts, solubilizing agent CO 400.05 parts, 0.003 part, essence;
Wherein, described small muddy pill granule is made up of the following component according to parts by weight: hydroxypropyl emthylcellulose 2.4 parts, microcrystalline Cellulose 24 parts, sucrose 15.6 parts, lactose 27 parts, 20 parts, mud film powder.
The preparation method of the above-mentioned facial film containing small muddy pill granule, in turn includes the following steps:
1) water of formula ratio, glycerol, butanediol, hyaluronate sodium, glucosan are put into emulsifying pot homogenizing dispersed with stirring until dissolve completely, then constant temperature 5min at the temperature of 80 DEG C;
2) step 1) process after, in emulsifying pot, add carbopol 940 in proportion, at 75 DEG C of temperature, homogenizing be stirred to material body fully dissolve after start cooling;
3) when pot kettle temperature to be emulsified is down to 45 DEG C, add the phenoxyethanol of formula ratio, Liquid BPF 950, solubilizing agent CO 40, essence, small muddy pill granule, triethanolamine, be stirred to and dissolve completely, filter, discharging, detect;
4) leave standstill after discharging, subpackage, packaging.
Particularly, in step 3) first add small muddy pill granule and add triethanolamine again, and mixing speed is slowed to 18r/min.
Wherein, described small muddy pill granule is made according to following steps:
A, by the microcrystalline Cellulose of formula ratio, sucrose, lactose, mud film powder mix homogeneously, to be added to the water, to be heated to boiling, to be brewed into syrup; Then by fluid unit spraying dry, granule is made;
B, by the hydroxypropyl emthylcellulose of formula ratio in 5% ratio add in the ethanol of 95%, be stirred to and dissolve completely, obtained Coating Solution;
C, the Coating Solution obtained by step B is wrapped in the outside of the granule obtained by steps A by fluid bed side spray technique, makes small muddy pill granule.
Embodiment 2
A facial film containing small muddy pill granule, it is made up of the following component according to parts by weight: 65 parts, water, glycerol 9 parts, butanediol 7 parts, small muddy pill granule 40 parts, hyaluronate sodium 0.2 part, glucosan 0.5 part, carbopol 940 1 part, triethanolamine 0.3 part, phenoxyethanol 0.2 part, Liquid BPF 9500.006 parts, solubilizing agent CO 400.03 parts, 0.002 part, essence;
Wherein, described small muddy pill granule is made up of the following component according to parts by weight: hydroxypropyl emthylcellulose 3 parts, microcrystalline Cellulose 20 parts, sucrose 16 parts, lactose 20 parts, 25 parts, mud film powder.
The preparation method of the above-mentioned facial film containing small muddy pill granule, in turn includes the following steps:
1) water of formula ratio, glycerol, butanediol, hyaluronate sodium, glucosan are put into emulsifying pot homogenizing dispersed with stirring until dissolve completely, then constant temperature 8min at the temperature of 75 DEG C;
2) step 1) process after, in emulsifying pot, add carbopol 940 in proportion, at 70 DEG C of temperature, homogenizing be stirred to material body fully dissolve after start cooling;
3) when pot kettle temperature to be emulsified is down to 45 DEG C, add the phenoxyethanol of formula ratio, Liquid BPF 950, solubilizing agent CO 40, essence, small muddy pill granule, triethanolamine, be stirred to and dissolve completely, filter, discharging, detect;
4) leave standstill after discharging, subpackage, packaging.
Particularly, in step 3) first add small muddy pill granule and add triethanolamine again, and mixing speed is slowed to 18r/min.
Wherein, described small muddy pill granule is made according to following steps:
A, by the microcrystalline Cellulose of formula ratio, sucrose, lactose, mud film powder mix homogeneously, to be added to the water, to be heated to boiling, to be brewed into syrup; Then by fluid unit spraying dry, granule is made;
B, by the hydroxypropyl emthylcellulose of formula ratio in 5% ratio add in the ethanol of 95%, be stirred to and dissolve completely, obtained Coating Solution;
C, the Coating Solution obtained by step B is wrapped in the outside of the granule obtained by steps A by fluid bed side spray technique, makes small muddy pill granule.
Embodiment 3
A facial film containing small muddy pill granule, it is made up of the following component according to parts by weight: 45 parts, water, glycerol 5 parts, butanediol 5 parts, small muddy pill granule 30 parts, hyaluronate sodium 0.05 part, glucosan 0.2 part, carbopol 940 0.4 part, triethanolamine 0.2 part, phenoxyethanol 0.3 part, Liquid BPF 9500.003 parts, solubilizing agent CO 400.002 parts, 0.003 part, essence;
Wherein, described small muddy pill granule is made up of the following component according to parts by weight: hydroxypropyl emthylcellulose 3 parts, microcrystalline Cellulose 18 parts, sucrose 12 parts, lactose 21 parts, 18 parts, mud film powder.
The preparation method of the above-mentioned facial film containing small muddy pill granule, in turn includes the following steps:
1) water of formula ratio, glycerol, butanediol, hyaluronate sodium, glucosan are put into emulsifying pot homogenizing dispersed with stirring until dissolve completely, then constant temperature 3min at the temperature of 85 DEG C;
2) step 1) process after, in emulsifying pot, add carbopol 940 in proportion, at 90 DEG C of temperature, homogenizing be stirred to material body fully dissolve after start cooling;
3) when pot kettle temperature to be emulsified is down to 35 DEG C, add the phenoxyethanol of formula ratio, Liquid BPF 950, solubilizing agent CO 40, essence, small muddy pill granule, triethanolamine, be stirred to and dissolve completely, filter, discharging, detect;
4) leave standstill after discharging, subpackage, packaging.
Particularly, in step 3) first add small muddy pill granule and add triethanolamine again, and mixing speed is slowed to 18r/min.
Wherein, described small muddy pill granule is made according to following steps:
A, by the microcrystalline Cellulose of formula ratio, sucrose, lactose, mud film powder mix homogeneously, to be added to the water, to be heated to boiling, to be brewed into syrup; Then by fluid unit spraying dry, granule is made;
B, by the hydroxypropyl emthylcellulose of formula ratio in 5% ratio add in the ethanol of 95%, be stirred to and dissolve completely, obtained Coating Solution;
C, the Coating Solution obtained by step B is wrapped in the outside of the granule obtained by steps A by fluid bed side spray technique, makes small muddy pill granule.
Embodiment 4
A facial film containing small muddy pill granule, it is made up of the following component according to parts by weight: 50 parts, water, glycerol 7 parts, butanediol 6 parts, small muddy pill granule 45 parts, hyaluronate sodium 0.15 part, glucosan 0.4 part, carbopol 940 0.6 part, triethanolamine 0.5 part, phenoxyethanol 0.4 part, Liquid BPF 9500.004 parts, solubilizing agent CO 400.01 parts, 0.002 part, essence;
Wherein, described small muddy pill granule is made up of the following component according to parts by weight: hydroxypropyl emthylcellulose 2 parts, microcrystalline Cellulose 20 parts, sucrose 15 parts, lactose 24 parts, 28 parts, mud film powder.
The preparation method of the above-mentioned facial film containing small muddy pill granule, in turn includes the following steps:
1) water of formula ratio, glycerol, butanediol, hyaluronate sodium, glucosan are put into emulsifying pot homogenizing dispersed with stirring until dissolve completely, then constant temperature 4min at the temperature of 82 DEG C;
2) step 1) process after, in emulsifying pot, add carbopol 940 in proportion, at 78 DEG C of temperature, homogenizing be stirred to material body fully dissolve after start cooling;
3) when pot kettle temperature to be emulsified is down to 40 DEG C, add the phenoxyethanol of formula ratio, Liquid BPF 950, solubilizing agent CO 40, essence, small muddy pill granule, triethanolamine, be stirred to and dissolve completely, filter, discharging, detect;
4) leave standstill after discharging, subpackage, packaging.
Particularly, in step 3) first add small muddy pill granule and add triethanolamine again, and mixing speed is slowed to 18r/min.
Wherein, described small muddy pill granule is made according to following steps:
A, by the microcrystalline Cellulose of formula ratio, sucrose, lactose, mud film powder mix homogeneously, to be added to the water, to be heated to boiling, to be brewed into syrup; Then by fluid unit spraying dry, granule is made;
B, by the hydroxypropyl emthylcellulose of formula ratio in 5% ratio add in the ethanol of 95%, be stirred to and dissolve completely, obtained Coating Solution;
C, the Coating Solution obtained by step B is wrapped in the outside of the granule obtained by steps A by fluid bed side spray technique, makes small muddy pill granule.
Embodiment 5
A facial film containing small muddy pill granule, it is made up of the following component according to parts by weight: 50 parts, water, glycerol 7 parts, butanediol 6 parts, small muddy pill granule 45 parts, hyaluronate sodium 0.15 part, glucosan 0.4 part, carbopol 940 0.6 part, triethanolamine 0.5 part, phenoxyethanol 0.4 part, Liquid BPF 9500.004 parts, solubilizing agent CO 400.01 parts, 0.002 part, essence;
Wherein, described small muddy pill granule is made up of the following component according to parts by weight: hydroxypropyl emthylcellulose 2 parts, microcrystalline Cellulose 20 parts, sucrose 15 parts, lactose 24 parts, 28 parts, mud film powder.
The preparation method of the above-mentioned facial film containing small muddy pill granule, in turn includes the following steps:
1) water of formula ratio, glycerol, butanediol, hyaluronate sodium, glucosan are put into emulsifying pot homogenizing dispersed with stirring until dissolve completely, then constant temperature 6min at the temperature of 83 DEG C;
2) step 1) process after, in emulsifying pot, add carbopol 940 in proportion, at 87 DEG C of temperature, homogenizing be stirred to material body fully dissolve after start cooling;
3) when pot kettle temperature to be emulsified is down to 39 DEG C, add the phenoxyethanol of formula ratio, Liquid BPF 950, solubilizing agent CO 40, essence, small muddy pill granule, triethanolamine, be stirred to and dissolve completely, filter, discharging, detect;
4) leave standstill after discharging, subpackage, packaging.
Particularly, in step 3) first add small muddy pill granule and add triethanolamine again, and mixing speed is slowed to 18r/min.
Wherein, described small muddy pill granule is made according to following steps:
A, by the microcrystalline Cellulose of formula ratio, sucrose, lactose, mud film powder mix homogeneously, to be added to the water, to be heated to boiling, to be brewed into syrup; Then by fluid unit spraying dry, granule is made;
B, by the hydroxypropyl emthylcellulose of formula ratio in 5% ratio add in the ethanol of 95%, be stirred to and dissolve completely, obtained Coating Solution;
C, the Coating Solution obtained by step B is wrapped in the outside of the granule obtained by steps A by fluid bed side spray technique, makes small muddy pill granule.
Experimental example
The facial film containing small muddy pill granule of Example 1-5, adopts the method for tester's vision self-appraisal to evaluate its performance:
1, measure of merit:
Adhesive film type mud mask of the present invention meets the indices in " the cosmetics health specification 2012 editions " of country's promulgation, said composition is not containing any noxious substance, by the said goods directly by the mode that sticks 25-40 year between, tried out by the puzzled office women of skin for a long time, trier totally 150 people.Trier's general health is good, do not have suckling or pregnancy, have glossy, the microgroove that shows or redness at face, the colour of skin is obscure.Trier endorsed comprehensive informed consent document.
Operational approach: 150 triers are divided into 5 groups at random, the product of above-described embodiment 1 ~ 5 is given respectively 5 groups of triers to use, each product at least uses 14 days, after 14 days, self-appraisal is carried out to test effect, experimenter's self-appraisal adopts the clinical evaluation of skin quality, the visual scoring system with 1-10 point provided in table 1.
The clinical score of table 1 skin quality
| Clinical assessment | Mark |
| Glossy | 1-10 |
| Microgroove | 1-10 |
| Red and swollen | 1-10 |
| Obscure | 1-10 |
Note: 1=does not improve (minimum possible mark), 2-9=improvement in various degree, and 10=greatly improves (the highest possible mark)
Trier uses tested products to carry out self-appraisal and test skin surface moisture to test effect after 14 days, calculates average.Test result is in table 2.
Skin quality test result after table 2 uses 14 days
| Project | Glossy | Microgroove | Red and swollen | Obscure |
| Embodiment 1 | 10 | 9 | 9 | 9 |
| Embodiment 2 | 8 | 7 | 8 | 9 |
| Embodiment 3 | 8 | 9 | 9 | 8 |
| Embodiment 4 | 9 | 7 | 8 | 6 |
| Embodiment 5 | 8 | 9 | 7 | 9 |
All experimenters (100%) report there is good tolerance to skin.All experimenters (100%) represent the facial film liking use to contain small muddy pill granule, easy to use relative to common mud mask, docile property is good, can reduce oils and fats by skin, again can replenishing water and preserving moisture, and 98% can continue regularly to use after the research phase of 14 days.
Glossy, microgroove and the red and swollen scoring at test position are higher, show test article to the deep layer cleaning of skin and replenishing water and preserving moisture effect better, it is mainly reflected in gel facial film containing small muddy pill granule and makes mud mask can be docile in face well by gel substrate, make facial skin absorb effective ingredient and moisture equably, bring comfort to user; Make mud film powder be released after small muddy pill particles by heat, absorb the oils and fats that skin is unnecessary, make skin cleaning dry and comfortable; Face pack prescription of the present invention has the effect of excellent removal dirt, and keep the skin wet nutrient, and compact level and smooth skin, bright color, and then improve skin problem.As can be seen from Table 1, the effect of the facial film containing small muddy pill granule of embodiment 1 is optimum.
2, skin surface moisture test
In above-mentioned experimenter, randomly draw 5 experimenters carry out the test of skin surface moisture, the operating ambient temperature of experimenter is 22-24 DEG C, and relative humidity is 46%-55%.Concrete method of testing is as follows: adopt the skin moisture content of CorneometerCM820 moisture of skin measuring instrument before tested site tests 5 experimenters use mask product, then the mask product of embodiment 1-5 is given respectively 5 experimenters to use, use rear and use latter one hour to carry out measurement skin surface moisture at tested position, tested position is the abundant forehead of sebaceous gland, and the unit of skin moisture content is au (arbitraryunit).Concrete data are in table 3.
Table 3 skin surface moisture test data
| Tested products | Use front au | Use rear au | Use rear 1h au |
| Embodiment 1 | 38.0 | 78.6 | 74.0 |
| Embodiment 2 | 34.0 | 72.6 | 67.1 |
| Embodiment 3 | 34.0 | 69.8 | 61.5 |
| Embodiment 4 | 36.0 | 49.4 | 40.6 |
| Embodiment 5 | 35.5 | 54.6 | 45.4 |
As shown in Table 3, facial film containing small muddy pill granule of the present invention has excellent replenishing water and preserving moisture effect, its reason is, the present invention adds multiple wetting agent in gel substrate, make product of the present invention have excellent moistening effect, be heated when facial film spreads on facial skin and small muddy pill granule is released, the mud film of small muddy pill granule can adsorb dirt and the excess oil of pore depths, allow skin can better absorb nutrition and moisture, make skin continue to keep water profit bullet sliding.
Above-mentioned embodiment is only the preferred embodiment of the present invention; can not limit the scope of protection of the invention with this, change and the replacement of any unsubstantiality that those skilled in the art does on basis of the present invention all belong to the present invention's scope required for protection.
Claims (6)
1. the facial film containing small muddy pill granule, is characterized in that: it is made up of the following component according to parts by weight: water 41.7-92.6 part, glycerol 5-10 part, butanediol 4-8 part, small muddy pill granule 10-70 part, hyaluronate sodium 0.05-0.2 part, glucosan 0.2-0.5 part, carbopol 940 0.4-1 part, triethanolamine 0.2-0.5 part, phenoxyethanol 0.2-0.5 part, Liquid BPF 950 0.003-0.006 part, solubilizing agent CO 40 0.002-0.05 part, essence 0.001-0.004 part;
Wherein, described small muddy pill granule is made up of the following component according to parts by weight: hydroxypropyl emthylcellulose 1-5 part, microcrystalline Cellulose 10-25 part, sucrose 12-18 part, lactose 20-30 part, mud film powder 15-35 part.
2. the facial film containing small muddy pill granule according to claim 1, is characterized in that: it is made up of the following component according to parts by weight: it is made up of the following component according to parts by weight: 56 parts, water, glycerol 8 parts, butanediol 5 parts, small muddy pill granule 30 parts, hyaluronate sodium 0.1 part, glucosan 0.3 part, carbopol 940 0.8 part, triethanolamine 0.2 part, phenoxyethanol 0.3 part, Liquid BPF 950 0.005 parts, solubilizing agent CO 400.05 parts, 0.003 part, essence;
Wherein, described small muddy pill granule is made up of the following component according to parts by weight: hydroxypropyl emthylcellulose 2.4 parts, microcrystalline Cellulose 24 parts, sucrose 15.6 parts, lactose 27 parts, 20 parts, mud film powder.
3. a preparation method for the facial film containing small muddy pill granule according to claim 1, is characterized in that: in turn include the following steps:
1) water of formula ratio, glycerol, butanediol, hyaluronate sodium, glucosan are put into emulsifying pot homogenizing dispersed with stirring until dissolve completely, then constant temperature 75 ~ 85 DEG C;
2) step 1) process after, in emulsifying pot, add carbopol 940 in proportion, at 70-90 DEG C of temperature, homogenizing be stirred to material body fully dissolve after start cooling;
3) when pot kettle temperature to be emulsified is down to 35 ~ 45 DEG C, add the phenoxyethanol of formula ratio, Liquid BPF 950, solubilizing agent CO 40, essence, small muddy pill granule, triethanolamine, be stirred to and dissolve completely, filter, discharging;
4) leave standstill after discharging, subpackage, packaging.
4. preparation method according to claim 3, is characterized in that: step 1) in time of constant temperature be 3-8min.
5. preparation method according to claim 3, is characterized in that: it is also included in step 3) step that product detected after discharging.
6. preparation method according to claim 3, is characterized in that: in step 3) first add small muddy pill granule and add triethanolamine again, and mixing speed is slowed to 18r/min.
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| CN110478282A (en) * | 2019-09-11 | 2019-11-22 | 黑龙江省科学院火山与矿泉研究所 | A kind of multi-functional volcanic slurry cleaning mud film and preparation method thereof and application method |
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