CN104959577B - Simulate the method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling - Google Patents

Simulate the method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling Download PDF

Info

Publication number
CN104959577B
CN104959577B CN201510164008.6A CN201510164008A CN104959577B CN 104959577 B CN104959577 B CN 104959577B CN 201510164008 A CN201510164008 A CN 201510164008A CN 104959577 B CN104959577 B CN 104959577B
Authority
CN
China
Prior art keywords
crucible
temperature
metal
solidified structure
conditions
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201510164008.6A
Other languages
Chinese (zh)
Other versions
CN104959577A (en
Inventor
仲红刚
陈峥
赵静
俞基浩
李仁兴
翟启杰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
University of Shanghai for Science and Technology
Original Assignee
University of Shanghai for Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by University of Shanghai for Science and Technology filed Critical University of Shanghai for Science and Technology
Priority to CN201510164008.6A priority Critical patent/CN104959577B/en
Publication of CN104959577A publication Critical patent/CN104959577A/en
Application granted granted Critical
Publication of CN104959577B publication Critical patent/CN104959577B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Manufacture And Refinement Of Metals (AREA)
  • Crucibles And Fluidized-Bed Furnaces (AREA)

Abstract

The method and founding experimental provision grown the invention discloses solidified structure under the conditions of a kind of big ingot casting slow cooling of simulation, for the process of setting of big ingot casting, the influence that the conditions such as analog study different temperatures gradient, different cooling and different molten steel flow velocitys grow to solidified structure, outfield, the influence that research outfield grows to solidified structure are imported during solidification of metal melt simultaneously.The present invention simulates the process that solidified structure under the conditions of big ingot casting slow cooling grows, the result of simulation and big Casting Ingot Solidification Process direct correlation, pair determines the casting technique of big ingot casting, adjustment relevant device parameter and to improve solidified structure defect significant.

Description

Simulate the method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling
Technical field
The present invention relates to a kind of metal freezing method and experimental provision, and big ingot solidification tissue is simulated more particularly to one kind Growing method and experimental provision, applied to metal solidification texture growth course thermal simulation technical field and the solidification skill of large-sized casting ingot Art field.
Background technology
With China's power industry, the rapid development of nuclear industry and petrochemical industry is more next to the demand of heavy casting and forging It is bigger, while also to the quality requirements more and more higher of heavy casting and forging.For large-sized casting ingot because volume is big, radiation processes are slow, solidification Process lasts a couple of days, the cooldown rate difference maximum of ingot casting different parts is up to more than 100 times, therefore solidified structure is thick, brilliant Grain size and the problems such as component distributing is uneven, shrinkage cavity shrinkage porosity it is extremely serious.The performance of final products is not only influenceed, is also often resulted in Forging crack, heat treatment can not uniformly wait follow-up problem.Strengthen forming core to produce more crystallization nucleis and promote crystal grain to breed It is the essential measure for reducing these defects.Develop the solidification control method that homogenizes based on internal generation, outfield intensifying propagation, be Obtain the key of good solidified structure.
At present to the research of large-sized casting ingot process of setting, mainly using following several approach:First, using numerical simulation Method, the change procedure of flow field of the big ingot casting in process of setting, temperature field and solute field is simulated, adjusts casting mold on this basis Shape, pouring temperature, the parameter such as pouring type, optimize technique;Second, directly dissect large-scale or ultra-large type ingot casting.Pass through sight The macrostructure of ingot casting is examined, with reference to the regularity of distribution of the elements such as inside ingot C, S, and the distribution of shrinkage cavity and porosity and field trash And rule etc. is formed, research influences the principal element of big Casting Ingot Solidification Process, such as thermograde, free convection etc..But dissect The cost of ingot casting is high, and research cycle is grown, and the process of setting individual difference of large-sized casting ingot is big, and the rule of single ingot casting has one Fixed limitation;Third, using the forming core and growth course of crystal grain under the conditions of the method simulation slow cooling of numerical simulation, pass through and compare Different parameters, influence of the different models to analog result, find with truth compared with the model met.
The solidified structures such as the grain size that is formed in the process of setting of metal, the tissue topography of dendrite, solute segregation and casting The factor such as flowing of thermograde, cooldown rate and melt is relevant in ingot.Relatively small ingot casting, deposit in large-sized casting ingot process of setting Non-uniform temperature, cooldown rate is slow, melt convection is strong the features such as.Current existing experimental method and equipment can not reappear big casting Certain difficulty be present in the curing condition inside ingot, therefore, the simulation to big ingot solidification tissue.
Shanghai University《The method of pulse magneto liquid level vibration thinning metal solidification texture》, patent publication No.: CN201010167538,2010.12.22.The technical operation is convenient, effect side notable to the solidified structure thinning effect of ingot casting Formula is that lattice coil is acted on to the upper surface of metal bath, is handled for contactless melt, can avoid casting mold to magnetic field Shielding action.Therefore, pulse magneto liquid level vibration refinement technology is quite suitable for molding the application in industrial production.But early stage Experimental subjects based on small-sized ingot casting, its setting rate is very fast, and the influence for solidified structure under the conditions of slow cooling lacks depth The research entered.
Recognize solidified structure and solute Distribution feature under different curing conditions, be to realize the basis that large-sized casting ingot homogenizes. It is currently the curing conditions such as thermograde, the cooldown rate that big inside ingot has been obtained with the method for numerical simulation, utilizes ingot casting The method of dissection has obtained partially solidified tissue and solute Distribution situation.Without curing condition and solidified structure, solute point Cloth combines the process of setting of analysis ingot casting.
The content of the invention
In order to solve prior art problem, it is an object of the present invention to overcome the deficiencies of the prior art, and to provide one kind The method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling are simulated, by controlling metal bath different directions Cooldown rate, simulate the thermogrades of different zones in big Casting Ingot Solidification Process, and outfield is introduced by outfield gatherer, External field treatment is carried out to solidification of metal melt process, the present invention carries to study the growth of the solidified structure of big inside ingot different zones A kind of new more efficiently research meanses are supplied.
Purpose is created to reach foregoing invention, the present invention uses following technical proposals:
A kind of method simulated solidified structure under the conditions of big ingot casting slow cooling and grown, metal raw is placed in the crucible in body of heater Material, and crucible is placed in the body of heater final vacuum 10Pa body of heater vacuum environment of temperature-controllable, set 4 in the periphery of crucible The individual calandria that can control power output respectively, to be heated respectively to 4 sides of crucible and temperature control, specific founding Process is as follows:
A. in the Metal Melting stage, raw metal is placed in crucible first, then by controlling each calandria simultaneously Crucible is heated, raw metal is formed metal bath after being heated;
B. in the metal freezing stage, temperature gradient conditions, cooldown rate, pressure are provided for metal solidification texture growth course Flow field state and any one assistant interventional mechanism in application outfield state or any several assistant interventional composition mechanisms, specifically For:
1. controlling each calandria to be incubated the not ipsilateral of crucible respectively, it is internally formed in crucible needed for setting Thermograde, realize the metal solidification texture thermal simulation experiment under customization temperature gradient conditions;
2. in the metal freezing stage, the rate of temperature fall on each surface of control crucible, make the temperature of 4 sides of crucible according to big The state of temperature of the cooling curve of diverse location is maintained in inside ingot process of setting, the cooling to metal bath in crucible Speed is respectively controlled, and realizes the metal solidification texture thermal simulation experiment under controllable cooldown rate;
3. in the metal freezing stage, also using the integral level rotary reciprocating motion of body of heater, make to produce inside metal bath Forced convertion, realize the metal solidification texture thermal simulation experiment under setting flow field condition;
4. during solidification of metal melt, outfield also is applied to metal bath and handled, make to produce inside metal bath Raw concussion effect, realizes the metal solidification texture thermal simulation experiment under setting condition of external field.The inventive method is coagulated in metal bath During Gu under the conditions of " having under temperature gradient conditions ", " under Different Cooling Conditions " and " under different molten steel flow velocitys " etc., simultaneously Import outfield, the influence that research outfield grows to solidified structure.
The present invention simulates the process of solidified structure growth under the conditions of big ingot casting slow cooling, the result of simulation and big ingot solidification mistake Journey direct correlation, pair determine big ingot casting casting technique, adjustment relevant device parameter and the solidified structure defect that improves have it is important Meaning.
As currently preferred technical scheme, in the Metal Melting stage and in the metal freezing stage, make raw metal It is in metal bath in body of heater final vacuum 1Pa thermal environment.
The technical scheme further preferred as the present invention, 1800 DEG C of heating limits temperature;Thermograde in crucible is 0 It is adjustable in the range of ~ 10 DEG C/cm;Calandria temperature-controlled precision is maintained within ± 0.5 DEG C;Between 1600 ~ 1200 DEG C, crucible surface Cooldown rate it is controllable in the range of 0 ~ 10 DEG C/min;The body of heater speed of rotation is 0 ~ 30 rev/min adjustable.
As the further preferred technical scheme of such scheme of the present invention, according to 4 not less than 10Hz frequencies to crucible The temperature data of side is acquired.
The founding experimental provision for the method that solidified structure grows, main under the conditions of a kind of big ingot casting slow cooling of implementation present invention simulation To be made up of heating and atmosphere protection system, temperature control and temperature acquisition system and central controller, heating and atmosphere protection system The main crucible and graphite protective sleeve for including being arranged in the vacuum furnace shell of sealing, graphite protective sleeve are enclosed on the outside of crucible, Corundum fine sand is tamped between graphite protective sleeve and crucible, raw metal is placed in crucible, and temperature control and temperature acquisition system are by one Serial temperature thermocouple and temperature data collecting system and temperature controller composition, temperature data collecting system and temperature controller all with center Controller signals connect, and in vacuum furnace shell, 4 sides of graphite protective sleeve face one group of graphite heating body, each graphite respectively The operating current of calandria is independently controlled by temperature controller, and each temperature thermocouple is arranged in each graphite heating body and earthenware Between crucible, in the clearance space between vacuum furnace shell and graphite protective sleeve, between every group of adjacent graphite heating body with every Hot plate separates, and forms a series of independent heating chambers respectively, and the temperature in each heating chamber is respectively by corresponding independent one group Graphite heating body is controlled, and the bottom surface and top surface between each heating chamber are closed by heat insulation felt, by central controller according to big casting The cooling curve of diverse location carrys out temperature control in ingot process of setting, sets corresponding temperature gradient in crucible in different directions, realizes The metal solidification texture thermal simulation experiment under temperature gradient conditions is customized, central controller adjusts each graphite by temperature controller respectively The power output of heater, the rate of temperature fall on each surface of control crucible, realize the metal solidification texture heat under setting condition of external field Simulated experiment, raw metal are in vacuum 10Pa thermal environment with crucible, provided with body of heater rotary system, body of heater rotation System is made up of the swivel base and power set being arranged at outside vacuum furnace shell below body of heater, is moved by central controller controls Power apparatus drives swivel base to drive whole body of heater crankmotion, the metal bath in crucible is internally formed pressure pair Stream, the metal solidification texture thermal simulation experiment under setting flow field condition is realized, provided with outfield gatherer, imported and filled using outfield The metal bath put into crucible imports outfield, by central controller controls outfield gatherer, makes solidification of metal melt mistake Journey is under the outer field action of customization and carried out, and realizes the metal solidification texture thermal simulation experiment under setting condition of external field.
As currently preferred technical scheme, the importing coil of outfield gatherer is arranged inside vacuum furnace shell, is led Enter coil in furnace interior controllable lift, and to import coil configuration cooling system.
The technical scheme further preferred as the present invention, the cooling system for importing coil is water-cooling system, makes lead-in wire Water flowing is cooled down in circle, and cooling water flow is adjusted according to the height of pipe outer wall temperature.
As the further preferred technical scheme of such scheme of the present invention, heat insulation felt is carbon felt.
The present invention compared with prior art, has following obvious prominent substantive distinguishing features and remarkable advantage:
1. the process of setting of big ingot casting is a complicated process, the growth course of solidified structure is both by temperature field, flow field Influence, the formation for the defects of affecting big ingot casting shrinkage cavity and porosity and gross segregation again, the present invention can simulate big ingot solidification Tissue growth process, as a result directly it is associated with the solidified structure of ingot casting, the process of setting to controlling big ingot casting, improves big ingot casting Solidified structure, it is significant to realize that large-sized casting ingot composition homogenizes;
2. the present invention by changing cooling condition, reproduce in big Casting Ingot Solidification Process the thermograde of different zones and Cooldown rate, the growth course of big inside ingot different zones solidified structure is studied, be that development is based on internal generation, outfield intensifying The solidification control method that homogenizes of propagation, realizes that homogenizing for large-sized casting ingot provides foundation and reference.
Brief description of the drawings
Fig. 1 is the founding experimental provision schematic diagram that the preferred embodiment of the present invention simulates big ingot solidification tissue growth.
Fig. 2 be along Fig. 1 in A-A directions sectional view.
Fig. 3 is the big ingot casting sample sampling core position view prepared in a preferred embodiment of the invention.
Fig. 4 be along Fig. 3 in B-B directions sectional view.
Fig. 5 is the thermal simulation temperature control curve map that the preferred embodiment of the present invention uses.
Fig. 6 is that the big ingot casting center of the preferred embodiment of the present invention is shone without the thermal simulation ingot casting central section under temperature gradient conditions Piece.
Fig. 7 is thermal simulation ingot casting edge cross-section photographs of the big ingot casting of the preferred embodiment of the present invention close to ingot casting edge.
Embodiment
Details are as follows for the preferred embodiments of the present invention:
In the present embodiment, referring to Fig. 1 ~ Fig. 7, solidified structure growing method is molten under the conditions of a kind of big ingot casting slow cooling of simulation Experimental provision is cast, is mainly controlled by heating and atmosphere protection system, temperature control and temperature acquisition system, body of heater rotary system and center Device composition, heating and atmosphere protection system mainly include the crucible 7 and graphite protective sleeve 3 being arranged in the vacuum furnace shell 1 of sealing, Graphite protective sleeve 3 is enclosed on the outside of crucible 7, and corundum fine sand 8 is tamped between graphite protective sleeve 3 and crucible 7, and raw metal is placed In crucible 7, temperature control and temperature acquisition system are by a series of temperature thermocouples 6 and temperature data collecting system 4 and temperature controller group Into, temperature data collecting system 4 and temperature controller are all connected with central controller signal, in vacuum furnace shell 1, graphite protective sleeve 3 4 sides face one group of graphite heating body 2 respectively, the operating current of each graphite heating body 2 carries out independent control by temperature controller System, each temperature thermocouple 6 is arranged between each graphite heating body 2 and crucible 7, vacuum furnace shell 1 and graphite protective sleeve 3 it Between clearance space in, separated, formed respectively a series of independent with thermal insulation board 12 between every group of adjacent graphite heating body 2 Heating chamber 11, the temperature in each heating chamber 11 are controlled by corresponding one group of independent graphite heating body 2 respectively, each heating chamber 11 Between bottom surface and top surface by heat insulation felt 5 close to prevent lose heat, heat insulation felt 5 is carbon felt, by central controller according to The cooling curve of diverse location carrys out temperature control in big Casting Ingot Solidification Process, sets corresponding temperature gradient in crucible 7 in different directions, The metal solidification texture thermal simulation experiment under customization temperature gradient conditions is realized, central controller is adjusted respectively respectively by temperature controller The power output of graphite heater 2, the rate of temperature fall on 7 each surface of control crucible, realize the metal freezing under setting condition of external field Thermal simulation experiment is organized, raw metal is in crucible 7 in the thermal environment that vacuum is 10Pa, rotates system provided with body of heater System, body of heater rotary system is made up of the swivel base 10 and power set being arranged at below the outside body of heater of vacuum furnace shell 1, in Centre controller controls power set to drive swivel base 10 to drive whole body of heater crankmotion, makes the metal in crucible 7 Melt is internally formed forced convertion, realizes the metal solidification texture thermal simulation experiment under setting flow field condition, body of heater rotary system It is made up of motor, machine driven system and spacing part, under three phase alternating current motor driving, is driven entirely by swivel base 10 Body of heater crankmotion, makes molten steel be internally formed forced convertion, provided with outfield gatherer 9, using outfield gatherer 9 to Metal bath in crucible 7 imports outfield, by central controller controls outfield gatherer 9, makes solidification of metal melt process Carried out under outer field action in customization, realize the metal solidification texture thermal simulation experiment under setting condition of external field, outfield imports The importing coil of device 9 is arranged inside vacuum furnace shell 1, imports coil in furnace interior controllable lift, during to prevent work because Hyperthermia radiation causes to fail, and to importing coil configuration cooling system, the cooling system for importing coil is water-cooling system, makes lead-in wire Water flowing is cooled down in circle, and cooling water flow is adjusted according to the height of pipe outer wall temperature.
In the present embodiment, referring to Fig. 1 ~ Fig. 7, the experiment dress that solidified structure grows under the conditions of a kind of big ingot casting slow cooling of simulation Put, it is main to include by heating and atmosphere protection system, temperature control and temperature acquisition system, body of heater rotary system and outfield introgressive line System four systemses, the equipment specific implementation method are as follows:
A., raw metal is made to the block of suitable size, after acid pickling and rust removing, is put into the crucible 7 of cuboid, crucible 7 Interior chamber size be long 150mm, wide 100mm, high 230mm, once experiment raw metal about 20Kg, to prevent crucible 7 from adding Ruptured when hot, be cased with a graphite protective sleeve 3 outside crucible 7, filled out among crucible 7 and graphite protective sleeve 3 with high-purity corundum fine sand 8 It is real, whole furnace chamber is divided into four heating chambers 11 with thermal insulation board, the top and bottom of each heating chamber 11 are closed with carbon felt, gold Belong to raw material and cuboid crucible 7 in the vacuum environment that vacuum is 10Pa;
B., the power output of graphite heater 2 is set, and temperature acquisition system be able to will add according to 10Hz frequency collection data Atmosphere temperature is heated to 1550 DEG C in hot stove, is incubated 120 minutes, is completely melt raw metal;
C. according to the different sampling regions of the big inside ingot simulated in Fig. 3 and Fig. 4, set according to the temperature curve in Fig. 5 The cooling process of fixed each graphite heater 2, controls the cooling velocity of the different faces of crucible 7, makes the metal bath in crucible 7 in difference Thermograde under solidify;
D. continue to cool according to setting curve, until being down to room temperature, completely after cooling, open vent valve, open bell, will Sample takes out, and after pre-grinding, polishing, is soaked 30 minutes at a temperature of 80 DEG C with 50% hydrochloric acid solution, is used rapidly after taking-up Absolute alcohol cleans surface, observes simultaneously statistical experiment result, as shown in Figure 6 and Figure 7, the structure refinement of ingot casting center and peripheral, Crystal grain is uniform.
Raw metal is placed in crucible 7 by the present embodiment, and raw metal is in the vacuum environment being well incubated with crucible 7 In.Four side temperature of crucible 7 by face of four independent graphite heating bodies 2 control.Graphite heating body 2 heats jointly The raw metal in crucible 7 is set to be completely melt into metal bath.Four sides of crucible 7 according in big Casting Ingot Solidification Process not Cooling curve with position carrys out temperature control, it is possible thereby to be internally formed thermograde in crucible 7.By adjusting graphite heating body 2 Power output, different cooldown rates is formed at the both ends of crucible 7.It is rotated in using the integral level of body of heater inside metal bath Caused forced convertion.Furthermore it is possible to outfield gatherer 9 is placed in the top of metal bath, to solidification of metal melt process Carry out external field treatment.
The present embodiment realizes the solidified structure thermal simulation under temperature gradient conditions, according to big Casting Ingot Solidification Process temperature The numerical result of field, by adjusting the power output of graphite heater 2, the rate of temperature fall on 7 each surface of control crucible, in earthenware Thermograde is formed in metal bath in crucible 7, is easy to study the influence that thermograde grows solidified structure;The present embodiment pin To the characteristics of cooldown rate difference is big between ingot casting regional in large-sized casting ingot process of setting, control graphite heating body 2 is not with Same rate cools, and realizes the solidified structure thermal simulation under different cooling rate;The present embodiment is rotated using the integral level of body of heater Influence of the forced convertion to solidified structure is studied, is rotated in by body of heater integral level in molten steel and produces forced convertion, simulates steel Influence of the liquid convection current to solidified structure;The present embodiment imports outfield using outfield gatherer 9 in solidification of metal melt process, grinds Study carefully the influence that outfield grows to big Casting Ingot Solidification Process.
The embodiment of the present invention is illustrated above in conjunction with accompanying drawing, but the invention is not restricted to above-described embodiment, can be with A variety of changes are made according to the purpose of the innovation and creation of the present invention, under all Spirit Essence and principle according to technical solution of the present invention Change, modification, replacement, combination, the simplification made, should be equivalent substitute mode, as long as meeting the goal of the invention of the present invention, only Otherwise the method and the technical principle of founding experimental provision that solidified structure grows under the conditions of the big ingot casting slow cooling of present invention simulation And inventive concept, belong to protection scope of the present invention.

Claims (8)

1. a kind of method that solidified structure grows under the conditions of big ingot casting slow cooling of simulation, it is characterised in that in the crucible in body of heater Raw metal is placed, and crucible is placed in the body of heater final vacuum 10Pa body of heater vacuum environment of temperature-controllable, in crucible Periphery 4 calandrias that can control power output respectively are set, to be heated respectively to 4 sides of crucible and temperature control System, specific fusion-casting process are as follows:
A. in the Metal Melting stage, raw metal is placed in crucible first, then by controlling each calandria simultaneously to earthenware Crucible is heated, and raw metal is formed metal bath after being heated;
B. in the metal freezing stage, temperature gradient conditions, cooldown rate is provided for metal solidification texture growth course, forces flow field State and the combination for applying any one assistant interventional mechanism or any several assistant interventional mechanism in the state of outfield, it is each described Assistant interventional mechanism is as follows:
1. controlling each calandria to be incubated the not ipsilateral of crucible respectively, the required temperature ladder of setting is internally formed in crucible Degree, realize the metal solidification texture thermal simulation experiment under customization temperature gradient conditions;
2. in the metal freezing stage, the rate of temperature fall on each surface of control crucible, make 4 side temperature of crucible according in big ingot casting The state of temperature of the cooling curve of diverse location is maintained in portion's process of setting, to the metal bath of diverse location in crucible Cooldown rate is respectively controlled, and realizes the metal solidification texture thermal simulation experiment under controllable cooldown rate;
3. in the metal freezing stage, also using the integral level rotary reciprocating motion of body of heater, make to produce pressure inside metal bath Convection current, realize the metal solidification texture thermal simulation experiment under setting flow field condition;
4. during solidification of metal melt, outfield also is applied to metal bath and handled, makes to produce shake inside metal bath The effect of swinging, realize the metal solidification texture thermal simulation experiment under setting condition of external field.
2. the method that solidified structure grows under the conditions of big ingot casting slow cooling is simulated according to claim 1, it is characterised in that:In gold Belong to smelt stage and in the metal freezing stage, raw metal and metal bath is in body of heater final vacuum 10Pa guarantor In warm environment.
3. the method that solidified structure grows under the conditions of the big ingot casting slow cooling of simulation according to claim 1 or claim 2, it is characterised in that: 1800 DEG C of heating limits temperature;Thermograde in crucible is adjustable in the range of 0~10 DEG C/cm;Calandria temperature-controlled precision is kept Within ± 0.5 DEG C;Between 1600~1200 DEG C, the cooldown rate of crucible surface is controllable in the range of 0~10 DEG C/min;Stove The body speed of rotation is 0~30 rev/min adjustable.
4. the method that solidified structure grows under the conditions of the big ingot casting slow cooling of simulation according to claim 1 or claim 2, it is characterised in that: The temperature data of 4 sides of crucible is acquired according to the data acquiring frequency not less than 10Hz.
5. the founding experiment dress for the method that solidified structure grows under the conditions of the big ingot casting slow cooling of simulation described in a kind of implementation claim 1 Put, be mainly made up of heating and atmosphere protection system, temperature control and temperature acquisition system and central controller, the heating and atmosphere Protection system mainly includes the crucible (7) and graphite protective sleeve (3) being arranged in the vacuum furnace shell (1) of sealing, and the graphite is protected Sheath (3) is enclosed on the outside of the crucible (7), and corundum fine sand is tamped between the graphite protective sleeve (3) and the crucible (7) (8), it is inner to be placed on the crucible (7) for raw metal, the temperature control and temperature acquisition system by a series of temperature thermocouples (6) and Temperature data collecting system (4) and temperature controller composition, the temperature data collecting system (4) and the temperature controller all with it is described in Entreat controller signals connection, it is characterised in that:In the vacuum furnace shell (1), 4 sides point of the graphite protective sleeve (3) Not Mian Dui one group of graphite heating body (2), the operating current of each graphite heating body (2) carries out independent control by the temperature controller System, each temperature thermocouple (6) are arranged between each graphite heating body (2) and the crucible (7), described true In clearance space between empty furnace shell (1) and the graphite protective sleeve (3), between graphite heating body (2) described in adjacent every group Separated with thermal insulation board (12), form a series of independent heating chambers (11) respectively, the temperature in each heating chamber (11) Graphite heating body (2) control as described in corresponding independent one group respectively, bottom surface and top surface between each heating chamber (11) By heat insulation felt (5) close, by the central controller according to the cooling curve of diverse location in big Casting Ingot Solidification Process come Temperature control, the interior corresponding temperature gradient of the crucible (7) is set in different directions, realizes that the metal under customization temperature gradient conditions coagulates Gu tissue thermal simulation experiment, the central controller adjusts the output work of each graphite heater (2) by temperature controller respectively Rate, the rate of temperature fall on the crucible (7) each surface is controlled, realize that the metal solidification texture thermal simulation under controllable cooldown rate is real To test, raw metal is in vacuum 10Pa thermal environment with the crucible (7), provided with body of heater rotary system, the stove Body rotary system is made up of the swivel base (10) and power set being arranged at below the outside body of heater of vacuum furnace shell (1), passes through institute Power set described in central controller controls are stated to drive the swivel base (10) to drive whole body of heater crankmotion, are made Metal bath in the crucible (7) is internally formed forced convertion, realizes the metal solidification texture hot-die under setting flow field condition Draft experiment, provided with outfield gatherer (9), led using metal bath of the outfield gatherer (9) into the crucible (7) Enter outfield, by outfield gatherer (9) described in the central controller controls, solidification of metal melt process is in customization Carried out under outer field action, realize the metal solidification texture thermal simulation experiment under setting condition of external field.
6. founding experimental provision according to claim 5, it is characterised in that:The importing coil of the outfield gatherer (9) It is internal to be arranged at the vacuum furnace shell (1), the importing coil is cold for the importing coil configuration in furnace interior controllable lift But system.
7. founding experimental provision according to claim 6, it is characterised in that:The cooling system for importing coil is water cooling system System, makes water flowing cooling in the importing coil, and cooling water flow is adjusted according to the height of pipe outer wall temperature.
8. the founding experimental provision according to any one in claim 5~7, it is characterised in that:The heat insulation felt (5) is carbon Felt.
CN201510164008.6A 2015-04-09 2015-04-09 Simulate the method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling Active CN104959577B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510164008.6A CN104959577B (en) 2015-04-09 2015-04-09 Simulate the method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510164008.6A CN104959577B (en) 2015-04-09 2015-04-09 Simulate the method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling

Publications (2)

Publication Number Publication Date
CN104959577A CN104959577A (en) 2015-10-07
CN104959577B true CN104959577B (en) 2017-11-10

Family

ID=54213754

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510164008.6A Active CN104959577B (en) 2015-04-09 2015-04-09 Simulate the method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling

Country Status (1)

Country Link
CN (1) CN104959577B (en)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105290376B (en) * 2015-10-30 2017-12-12 广东工业大学 The smelting-casting equipment of low silver-colored hypoeutectic lead-free solder and the method using its manufacture solder
CN105483830A (en) * 2015-11-30 2016-04-13 上海大学 Method and apparatus for measuring flow velocity of interdendritic fluid under convection condition
CN106890985B (en) * 2017-04-25 2018-02-16 北京航空航天大学 It is a kind of to be used to manufacture the method that the casting device without shrinkage cavity casting is cast
CN107876718B (en) * 2017-11-20 2019-12-31 辽宁科技大学 Experimental device and experimental method for simulating slow solidification of extra-thick plate
CN108693210B (en) * 2018-05-25 2020-10-30 武汉钢铁有限公司 Equipment and method for testing relation between cooling rate of cooling wall and thermal shock
CN108982578B (en) * 2018-07-31 2021-05-11 马鞍山尚元冶金科技有限公司 Method for simulating molten steel solidification process
CN108961972B (en) * 2018-07-31 2020-10-16 马鞍山尚元冶金科技有限公司 Molten steel solidification simulator
CN109183157A (en) * 2018-09-26 2019-01-11 大连理工大学 It is a kind of for studying the Fluid Dynamics device and application method of solidification of metal melt behavior
CN109405999B (en) * 2018-10-24 2020-11-10 中国计量大学 Simulation experiment device for monitoring temperature change of outer wall of coal gasifier
CN109211422B (en) * 2018-10-24 2020-07-28 中国计量大学 Use method of simulation experiment device based on coal gasifier outer wall temperature monitoring
CN110000365A (en) * 2019-04-30 2019-07-12 唐山学院 The heat simulation and device of big ingot solidification tissue based on high throughput experiment
CN110243489B (en) * 2019-07-01 2020-09-11 西北工业大学 Device and method for measuring three-dimensional temperature field in solidification process of electromagnetic suspension melt
CN112297868B (en) * 2019-07-26 2022-05-27 浙江吉智新能源汽车科技有限公司 Active heating control method and device for hybrid excitation motor
CN113817910B (en) * 2021-10-08 2023-04-07 昆山晶微新材料研究院有限公司 Homogenization treatment device, casting equipment and preparation method of high-homogeneity cast ingot
CN114406246B (en) * 2022-03-10 2024-06-25 湖南东方钪业股份有限公司 Temperature-control retarding casting die and process for scandium precipitation and enrichment of aluminum-scandium intermediate alloy

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP3121672B2 (en) * 1992-04-17 2001-01-09 昭和電線電纜株式会社 Monitoring and measuring device for mold temperature
JP3121721B2 (en) * 1993-04-28 2001-01-09 新日本製鐵株式会社 Method and apparatus for solidifying simulation of metal material
CN101075287B (en) * 2007-06-26 2012-05-02 上海大学 Physical simulating method and device during continuous-casting billet coagulation tissue growth process
KR101235613B1 (en) * 2011-02-24 2013-02-21 현대제철 주식회사 Simulating apparatus for solidified layer thickness using water model mold
CN104226952A (en) * 2014-01-02 2014-12-24 上海大学 Metal solidification process simulation method
CN203972826U (en) * 2014-04-02 2014-12-03 上海大学 A kind of liquid surface fluctuation device

Also Published As

Publication number Publication date
CN104959577A (en) 2015-10-07

Similar Documents

Publication Publication Date Title
CN104959577B (en) Simulate the method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling
CN204867366U (en) Multi -functional high gradient vacuum induction directional solidification single crystal casting stove
CN103131980B (en) Method for realizing fine crystal solidification by controlling spherical crystal stabilization
CN100384568C (en) Control method and device for continuous metal monocrystal casting process
CN105290380A (en) Design method of internal baffle for directional solidification blade casting system
CN109396400A (en) A kind of large-scale complex thin-wall fine grain casting integrated molding method and apparatus
CN105964990B (en) A kind of directional freeze method of externally-applied magnetic field control freckle defect
CN110000365A (en) The heat simulation and device of big ingot solidification tissue based on high throughput experiment
CN105583366A (en) Precision casting method for thin-wall high-temperature alloy floating wall tiles
CN102879130A (en) Continuous-casting casting powder comprehensive heat transfer heat flow testing method
CN105973664A (en) Solidified sample high-flux preparation method
CN104353795A (en) Continuous directional solidification technology adopting temperature gradient crystallizer
CN111375746A (en) High-temperature alloy single crystal blade directional solidification method based on solid-liquid interface steady control
CN103008623A (en) Method for refining crystal grains by utilizing strong magnetic field and special metal solidification casting device thereof
CN105177715A (en) Method for controlling stray crystal formation
CN101767190B (en) Physical simulation method and physical simulation device for double-roll continuous casting thin strip solidification
CN103898347A (en) Preparation device and preparation method of lotus-type porous metal
CN104028733B (en) The regulate and control method of Ti-Zr-Nb-Cu-Be system amorphous composite material tissue and regulation device
CN104480527B (en) Full-power control ingot casting process for polycrystalline silicon ingot furnace
CN106929699B (en) A kind of large volume high-alloying aluminium alloy melt treatment device and method
CN205241766U (en) Bulky high alloy aluminum alloy fuse -element processing apparatus
CN114888254B (en) Experimental device and method for simulating continuous casting crystallizer to feed steel belt
CN104416162A (en) Rapid alloy solidification equipment and automatic control method thereof
CN203737962U (en) Refining device for metal solidification structure
CN214517527U (en) Directional solidification device

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant