CN104959577A - Method for simulating growth of solidification structure of large ingot under slow cooling condition, and fusion casting experiment apparatus - Google Patents

Method for simulating growth of solidification structure of large ingot under slow cooling condition, and fusion casting experiment apparatus Download PDF

Info

Publication number
CN104959577A
CN104959577A CN201510164008.6A CN201510164008A CN104959577A CN 104959577 A CN104959577 A CN 104959577A CN 201510164008 A CN201510164008 A CN 201510164008A CN 104959577 A CN104959577 A CN 104959577A
Authority
CN
China
Prior art keywords
crucible
temperature
metal
heater
solidification
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201510164008.6A
Other languages
Chinese (zh)
Other versions
CN104959577B (en
Inventor
仲红刚
陈峥
赵静
俞基浩
李仁兴
翟启杰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
University of Shanghai for Science and Technology
Original Assignee
University of Shanghai for Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by University of Shanghai for Science and Technology filed Critical University of Shanghai for Science and Technology
Priority to CN201510164008.6A priority Critical patent/CN104959577B/en
Publication of CN104959577A publication Critical patent/CN104959577A/en
Application granted granted Critical
Publication of CN104959577B publication Critical patent/CN104959577B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Abstract

The invention discloses a method for simulating the growth of the solidification structure of a large ingot under a slow cooling condition, and a fusion casting experiment apparatus. Aiming at a solidification process of the large ingot, the influence on the growth of the solidification structure under different temperature gradients, different cooling speeds and different molten steel flow speeds can be researched through the simulation. An external field is introduced into a metal melt solidification process, so that the influence on the growth of the solidification structure by the external field can be researched. According to the invention, a growth process of the solidification structure of the large ingot under the slow cooling condition is simulated, simulation results are directly related to a large ingot solidification process, and the simulation results play an important role in determining the casting technology for the large ingot, adjusting parameters of related equipment, and improving defects of the solidification structure.

Description

Simulate method and the founding experimental provision of solidified structure growth under large ingot casting slow cooling condition
Technical field
The present invention relates to a kind of metal freezing method and experimental provision, particularly relate to a kind of large ingot solidification tissue growth method of simulation and experimental provision, be applied to the solidification technology field of metal solidification texture growth course thermal simulation technical field and large-sized casting ingot.
Background technology
Along with China's power industry, the develop rapidly of nuclear industry and petrochemical industry, increasing to the demand of heavy casting and forging, simultaneously also more and more higher to the quality requirements of heavy casting and forging.Large-sized casting ingot due to volume large, radiation processes is slow, and process of setting wants last from days, and the cooldown rate difference of ingot casting different parts is maximum reaches more than 100 times, and therefore the problem such as thick, the grain size of solidified structure and component distributing is uneven, shrinkage cavity shrinkage porosity is very serious.Not only affect the performance of final products, also often cause forging crack, heat treatment can not evenly wait a follow-up difficult problem.Strengthening forming core is the essential measure reducing these defects to produce more crystallization nuclei and to promote crystal grain to breed.Developing and solidify control method based on inside generation, homogenizing of outfield intensifying propagation, is the key obtaining good solidified structure.
Research at present to large-sized casting ingot process of setting, the following several approach of main employing: one is the method adopting numerical simulation, simulate the change procedure of the flow field of large ingot casting in process of setting, temperature field and solute field, adjust the parameters such as the shape of casting mold, pouring temperature, pouring type on this basis, Optimization Technology; Two is directly dissect large-scale or superhuge ingot casting.By observing the macrostructure of ingot casting, in conjunction with the regularity of distribution of the elements such as inside ingot C, S, and the distribution of shrinkage cavity and porosity and field trash and Formation rule etc., the principal element of the large Casting Ingot Solidification Process of research impact, as thermograde, free convection etc.But the cost of dissecting ingot casting is high, and research cycle is long, and the process of setting individual difference of large-sized casting ingot is large, and the rule of single ingot casting has certain limitation; Three is the nucleation and growth processes of crystal grain under the method simulation slow cooling condition of application numerical simulation, and by comparing different parameters, different model, on the impact of analog result, finds the model comparatively met with truth.
The factors such as the flowing of the solidified structures such as the grain size formed in the process of setting of metal, the tissue topography of dendrite, solute segregation and thermograde, cooldown rate and melt in ingot casting are relevant., in large-sized casting ingot process of setting, there is the features such as non-uniform temperature, cooldown rate is slow, melt convection is strong in relatively little ingot casting.Current existing experimental technique and equipment can not reappear the curing condition of large inside ingot, therefore, there is certain difficulty to the simulation that large ingot solidification is organized.
" method of pulse magneto liquid level vibration thinning metal solidification texture " of Shanghai University, patent publication No.: CN201010167538,2010.12.22.This technical operation is convenient, and remarkable to the solidified structure thinning effect of ingot casting, the mode of action is upper surface lattice coil being acted on metal bath, is contactless melt process, casting mold can be avoided the shielding action in magnetic field.Therefore, pulse magneto liquid level vibration refinement technology is extremely suitable for the application in die casting industrial production.But the experimental subjects in early stage is all based on small-sized ingot casting, its setting rate is very fast, lacks deep research for the impact of solidified structure under slow cooling condition.
Being familiar with solidified structure and solute Distribution feature under different curing condition, is realize the basis that large-sized casting ingot homogenizes.Be the curing condition such as thermograde, cooldown rate obtaining large inside ingot by the method for numerical simulation at present, the method utilizing ingot casting to dissect obtains partial coagulation tissue and solute Distribution situation.And curing condition is not combined with solidified structure, solute Distribution the process of setting analyzing ingot casting.
Summary of the invention
In order to solve prior art problem, the object of the invention is to the deficiency overcoming prior art existence, a kind of method and founding experimental provision of simulating solidified structure growth under large ingot casting slow cooling condition are provided, by controlling the cooldown rate of metal bath different directions, simulate the thermograde of zones of different in large Casting Ingot Solidification Process, and introduce outfield by outfield gatherer, carry out external field treatment to solidification of metal melt process, the present invention is that the solidified structure growth studying large inside ingot zones of different provides a kind of research means more effectively newly.
Create object for reaching foregoing invention, the present invention adopts following technical proposals:
A kind of method simulating solidified structure growth under large ingot casting slow cooling condition, raw metal is placed in crucible in body of heater, and crucible is placed in the body of heater vacuum environment of the body of heater final vacuum 10Pa of temperature-controllable, the calandria that 4 can control power output is respectively set in the periphery of crucible, come to carry out heating and temperaturel control to 4 sides of crucible respectively, concrete fusion-casting process is as follows:
A. in the Metal Melting stage, first raw metal is placed in crucible, then crucible is heated by controlling each calandria simultaneously, after raw metal is heated, forming metal bath;
B. in the metal freezing stage, provide temperature gradient conditions, cooldown rate, pressure flow field state for metal solidification texture growth course and apply any one assistant interventional mechanism or any several assistant interventional composition mechanism in the state of outfield, being specially:
1. control the not ipsilateral of each calandria to crucible to be respectively incubated, form the temperature required gradient of setting in crucible inside, realize the metal solidification texture thermal simulation experiment under customization temperature gradient conditions;
2. in the metal freezing stage, control the rate of temperature fall on each surface of crucible, the temperature of crucible 4 sides is maintained according to the state of temperature of the cooling curve of diverse location in large inside ingot process of setting, the cooldown rate of metal bath in crucible is controlled respectively, realizes the metal solidification texture thermal simulation experiment under controlled cooldown rate;
3. in the metal freezing stage, also utilize the integral level rotary reciprocating motion of body of heater, make metal bath inside produce forced convertion, realize the metal solidification texture thermal simulation experiment under the condition of setting flow field;
4. in solidification of metal melt process, also outfield is applied to metal bath and process, make metal bath inside produce concussion effect, realize the metal solidification texture thermal simulation experiment under setting condition of external field.The inventive method under the condition such as " under having temperature gradient conditions ", " under Different Cooling Conditions " and " under different molten steel flow velocitys ", imports outfield in solidification of metal melt process simultaneously, the impact that research outfield grows solidified structure.
The present invention simulates the process of solidified structure growth under large ingot casting slow cooling condition, the result of simulation and large Casting Ingot Solidification Process direct correlation, to determine large ingot casting casting technique, adjust relevant device parameter and improve solidified structure defect significant.
As the preferred technical scheme of the present invention, in the Metal Melting stage with in the metal freezing stage, raw metal and metal bath are all in the thermal environment of body of heater final vacuum 1Pa.
As the present invention's preferred technical scheme further, heating limits temperature 1800 DEG C; Thermograde in crucible is adjustable within the scope of 0 ~ 10 DEG C/cm; Calandria temperature-controlled precision remains on ± 0.5 DEG C within; Between 1600 ~ 1200 DEG C, the cooldown rate of crucible surface is controlled within the scope of 0 ~ 10 DEG C/min; The body of heater speed of rotation be 0 ~ 30 rev/min adjustable.
As the further optimal technical scheme of such scheme of the present invention, gather according to being not less than the temperature data of 10Hz frequency to 4 of crucible sides.
A kind of the present invention of enforcement simulates the founding experimental provision of the method for solidified structure growth under large ingot casting slow cooling condition, primarily of heating and atmosphere protection system, temperature control and temperature acquisition system and central controller composition, heating and atmosphere protection system mainly comprise and are arranged at crucible in the vacuum furnace shell of sealing and graphite protective sleeve, graphite protective sleeve is enclosed within the outside of crucible, corundum fine sand is tamped between graphite protective sleeve and crucible, raw metal is placed in crucible, temperature control and temperature acquisition system are made up of a series of temperature thermocouple and temperature data collecting system and temperature controller, temperature data collecting system and temperature controller are all connected with central controller signal, in vacuum furnace shell, 4 sides of graphite protective sleeve are respectively in the face of one group of graphite heating body, the operating current of each graphite heating body carries out independent control by temperature controller, each temperature thermocouple is arranged between each graphite heating body and crucible, in clearance space between vacuum furnace shell and graphite protective sleeve, all separate with thermal insulation board between adjacent often group graphite heating body, form a series of independently heating clamber respectively, temperature in each heating clamber is controlled by independently one group of graphite heating body of correspondence respectively, bottom surface between each heating clamber and end face are closed by heat insulation felt, temperature control is carried out according to the cooling curve of diverse location in large Casting Ingot Solidification Process by central controller, corresponding temperature gradient in crucible is set in different directions, realize the metal solidification texture thermal simulation experiment under customization temperature gradient conditions, central controller adjusts the power output of each graphite heater respectively by temperature controller, control the rate of temperature fall on each surface of crucible, realize the metal solidification texture thermal simulation experiment under setting condition of external field, raw metal and crucible are all in the thermal environment of vacuum 10Pa, be provided with body of heater rotary system, body of heater rotary system is made up of the swivel base be arranged at below the outside body of heater of vacuum furnace shell and power set, swivel base is driven to drive whole body of heater crankmotion by central controller controls power set, the metal bath inside in crucible is made to form forced convertion, realize the metal solidification texture thermal simulation experiment under the condition of setting flow field, be provided with outfield gatherer, outfield gatherer is utilized to import outfield to the metal bath in crucible, by central controller controls outfield gatherer, carry out under making solidification of metal melt process be in the outer field action of customization, realize the metal solidification texture thermal simulation experiment under setting condition of external field.
As the preferred technical scheme of the present invention, the importing coil of outfield gatherer is arranged at vacuum furnace shell inside, imports coil at furnace interior controllable lift, and for importing coil configuration cooling system.
As the present invention's preferred technical scheme further, the cooling system importing coil is water-cooling system, and make water flowing cooling in importing coil, cooling water flow is regulated according to the height of pipe outer wall temperature.
As the further optimal technical scheme of such scheme of the present invention, heat insulation felt is carbon felt.
The present invention compared with prior art, has following apparent outstanding substantive distinguishing features and remarkable advantage:
1. the process of setting of large ingot casting is a complicated process, the growth course of solidified structure is both by the impact in temperature field, flow field, affect again the formation of the defects such as large ingot casting shrinkage cavity and porosity and gross segregation, the present invention can simulate large ingot solidification tissue growth process, result is directly associated with the solidified structure of ingot casting, to the process of setting controlling large ingot casting, improve the solidified structure of large ingot casting, realize large-sized casting ingot composition and homogenize significant;
2. the present invention is by changing cooling condition, reproduce thermograde and the cooldown rate of zones of different in large Casting Ingot Solidification Process, study the growth course of large inside ingot zones of different solidified structure, for development solidifies control method based on inside generation, homogenizing of outfield intensifying propagation, realize homogenizing of large-sized casting ingot and foundation and reference are provided.
Accompanying drawing explanation
Fig. 1 is the founding experimental provision schematic diagram that the preferred embodiment of the present invention simulates large ingot solidification tissue growth.
Fig. 2 is the sectional view in A-A direction in Fig. 1.
Fig. 3 is the large ingot casting sample sampling core position view prepared in a preferred embodiment of the invention.
Fig. 4 is the sectional view in B-B direction in Fig. 3.
Fig. 5 is the thermal simulation temperature control curve map that the preferred embodiment of the present invention adopts.
Fig. 6 is that the large ingot casting center of the preferred embodiment of the present invention is without the thermal simulation ingot casting central section photo under temperature gradient conditions.
Fig. 7 is the thermal simulation ingot casting edge cross-section photographs of the large ingot casting of the preferred embodiment of the present invention near ingot casting edge.
Detailed description of the invention
Details are as follows for the preferred embodiments of the present invention:
In the present embodiment, see Fig. 1 ~ Fig. 7, a kind of founding experimental provision of simulating solidified structure growing method under large ingot casting slow cooling condition, primarily of heating and atmosphere protection system, temperature control and temperature acquisition system, body of heater rotary system and central controller composition, heating and atmosphere protection system mainly comprise and are arranged at crucible 7 in the vacuum furnace shell 1 of sealing and graphite protective sleeve 3, graphite protective sleeve 3 is enclosed within the outside of crucible 7, corundum fine sand 8 is tamped between graphite protective sleeve 3 and crucible 7, raw metal is placed on 7 li, crucible, temperature control and temperature acquisition system are made up of a series of temperature thermocouple 6 and temperature data collecting system 4 and temperature controller, temperature data collecting system 4 and temperature controller are all connected with central controller signal, in vacuum furnace shell 1, 4 sides of graphite protective sleeve 3 are respectively in the face of one group of graphite heating body 2, the operating current of each graphite heating body 2 carries out independent control by temperature controller, each temperature thermocouple 6 is arranged between each graphite heating body 2 and crucible 7, in clearance space between vacuum furnace shell 1 and graphite protective sleeve 3, all separate with thermal insulation board 12 between adjacent often group graphite heating body 2, form a series of independently heating clamber 11 respectively, temperature in each heating clamber 11 is controlled by independently one group of graphite heating body 2 of correspondence respectively, bottom surface between each heating clamber 11 and end face are closed in case loses heat by heat insulation felt 5, heat insulation felt 5 is carbon felt, temperature control is carried out according to the cooling curve of diverse location in large Casting Ingot Solidification Process by central controller, corresponding temperature gradient in crucible 7 is set in different directions, realize the metal solidification texture thermal simulation experiment under customization temperature gradient conditions, central controller adjusts the power output of each graphite heater 2 respectively by temperature controller, control the rate of temperature fall on each surface of crucible 7, realize the metal solidification texture thermal simulation experiment under setting condition of external field, it is in the thermal environment of 10Pa that raw metal and crucible 7 are all in vacuum, be provided with body of heater rotary system, body of heater rotary system is made up of the swivel base 10 be arranged at below the outside body of heater of vacuum furnace shell 1 and power set, swivel base 10 is driven to drive whole body of heater crankmotion by central controller controls power set, the metal bath inside in crucible 7 is made to form forced convertion, realize the metal solidification texture thermal simulation experiment under the condition of setting flow field, body of heater rotary system is by motor, mechanical drive train unify spacing part composition, under three phase alternating current motor drives, whole body of heater crankmotion is driven by swivel base 10, molten steel inside is made to form forced convertion, be provided with outfield gatherer 9, outfield gatherer 9 is utilized to import outfield to the metal bath in crucible 7, by central controller controls outfield gatherer 9, carry out under making solidification of metal melt process be in the outer field action of customization, realize the metal solidification texture thermal simulation experiment under setting condition of external field, the importing coil of outfield gatherer 9 is arranged at vacuum furnace shell 1 inside, import coil at furnace interior controllable lift, for when preventing work because hyperthermia radiation causes losing efficacy, to importing coil configuration cooling system, the cooling system importing coil is water-cooling system, make water flowing cooling in importing coil, cooling water flow is regulated according to the height of pipe outer wall temperature.
In the present embodiment; see Fig. 1 ~ Fig. 7; a kind of experimental provision of simulating solidified structure growth under large ingot casting slow cooling condition; mainly comprise by heating and atmosphere protection system, temperature control and temperature acquisition system, body of heater rotary system and outfield import system four systems, this equipment specific implementation method is as follows:
A. raw metal is made the block of suitable size, after acid pickling and rust removing, put into the crucible 7 of cuboid, the inner cavity size of crucible 7 is long 150mm, wide 100mm, high 230mm, once experiment raw metal is about 20Kg, break when heating for preventing crucible 7, crucible 7 overcoat has a graphite protective sleeve 3, crucible 7 and graphite protective sleeve 3 centre high-purity corundum fine sand 8 tamp, with thermal insulation board, whole furnace chamber is divided into four heating clambers 11, the top of each heating clamber 11 and bottom are all closed with carbon felt, it is in the vacuum environment of 10Pa that raw metal and cuboid crucible 7 entirety are in vacuum,
B. arrange the power output of graphite heater 2, atmosphere temperature in heating furnace according to 10Hz frequency collection data, can be heated to 1550 DEG C by temperature acquisition system, is incubated 120 minutes, raw metal is melted completely;
C. according to the different resample area of large inside ingot simulated in Fig. 3 with Fig. 4, according to the cooling process of each graphite heater 2 of the temperature curve setting in Fig. 5, control the cooling velocity of crucible 7 not coplanar, the metal bath in crucible 7 is solidified under different thermogrades;
D. cooling is continued according to setting curve, until be down to room temperature, completely after cooling, open vent valve, open bell, sample is taken out, after pre-grinding, polishing, hydrochloric acid solution with 50% soaks 30 minutes at the temperature of 80 DEG C, use absolute alcohol clean surface rapidly after taking out, observe and statistical experiment result, as shown in Figure 6 and Figure 7, the structure refinement of ingot casting center and peripheral, crystal grain is even.
Raw metal is placed in crucible 7 by the present embodiment, and raw metal and crucible 7 are in the vacuum environment be well incubated.Four side temperature of crucible 7 by faced by four independently graphite heating body 2 control.Graphite heating body 2 jointly heating makes the raw metal in crucible 7 be fused into metal bath completely.Temperature control is carried out according to the cooling curve of diverse location in large Casting Ingot Solidification Process in four sides of crucible 7, thus can in the inner formation temperature gradient of crucible 7.By adjusting the power output of graphite heating body 2, form different cooldown rates at the two ends of crucible 7.The integral level of body of heater is utilized to be rotated in the forced convertion of metal bath inside generation.In addition, outfield gatherer 9 can be placed in the top of metal bath, external field treatment is carried out to solidification of metal melt process.
The present embodiment achieves the solidified structure thermal simulation under temperature gradient conditions, according to the numerical result in large Casting Ingot Solidification Process temperature field, by adjusting the power output of graphite heater 2, control the rate of temperature fall on each surface of crucible 7, formation temperature gradient in metal bath in crucible 7, is convenient to the impact that research thermograde grows solidified structure; The present embodiment, for the feature that in large-sized casting ingot process of setting, between ingot casting regional, cooldown rate difference is large, controls graphite heating body 2 with different rates cooling, realizes the solidified structure thermal simulation under different cooling rate; The present embodiment utilizes the integral level of body of heater to rotate research forced convertion to the impact of solidified structure, is rotated in molten steel produces forced convertion by body of heater integral level, and the convection current of simulation molten steel is on the impact of solidified structure; The present embodiment utilizes outfield gatherer 9 to import outfield in solidification of metal melt process, the impact that research outfield grows large Casting Ingot Solidification Process.
By reference to the accompanying drawings the embodiment of the present invention is illustrated above; but the invention is not restricted to above-described embodiment; multiple change can also be made according to the object of innovation and creation of the present invention; change, the modification made under all Spirit Essences according to technical solution of the present invention and principle, substitute, combination, to simplify; all should be the substitute mode of equivalence; as long as goal of the invention according to the invention; only otherwise deviating from the present invention simulates the method for solidified structure growth and the know-why of founding experimental provision and inventive concept under large ingot casting slow cooling condition, all protection scope of the present invention is belonged to.

Claims (8)

1. the method for solidified structure growth under the large ingot casting slow cooling condition of simulation, it is characterized in that, raw metal is placed in crucible in body of heater, and crucible is placed in the body of heater vacuum environment of the body of heater final vacuum 10Pa of temperature-controllable, the calandria that 4 can control power output is respectively set in the periphery of crucible, come to carry out heating and temperaturel control to 4 sides of crucible respectively, concrete fusion-casting process is as follows:
A. in the Metal Melting stage, first raw metal is placed in crucible, then crucible is heated by controlling each calandria simultaneously, after raw metal is heated, forming metal bath;
B. in the metal freezing stage, provide temperature gradient conditions, cooldown rate, pressure flow field state for metal solidification texture growth course and apply any one assistant interventional mechanism or any several assistant interventional composition mechanism in the state of outfield, being specially:
1. control the not ipsilateral of each calandria to crucible to be respectively incubated, form the temperature required gradient of setting in crucible inside, realize the metal solidification texture thermal simulation experiment under customization temperature gradient conditions;
2. in the metal freezing stage, control the rate of temperature fall on each surface of crucible, 4 of crucible side temperature are maintained according to the state of temperature of the cooling curve of diverse location in large inside ingot process of setting, the cooldown rate of the metal bath of diverse location in crucible is controlled respectively, realizes the metal solidification texture thermal simulation experiment under controlled cooldown rate;
3. in the metal freezing stage, also utilize the integral level rotary reciprocating motion of body of heater, make metal bath inside produce forced convertion, realize the metal solidification texture thermal simulation experiment under the condition of setting flow field;
4. in solidification of metal melt process, also outfield is applied to metal bath and process, make metal bath inside produce concussion effect, realize the metal solidification texture thermal simulation experiment under setting condition of external field.
2. simulate the method for solidified structure growth under large ingot casting slow cooling condition according to claim 1, it is characterized in that: in the Metal Melting stage with in the metal freezing stage, raw metal and metal bath are all in the thermal environment of body of heater final vacuum 1Pa.
3. according to claim 1 or 2, simulate the method for solidified structure growth under large ingot casting slow cooling condition, it is characterized in that: heating limits temperature 1800 DEG C; Thermograde in crucible is adjustable within the scope of 0 ~ 10 DEG C/cm; Calandria temperature-controlled precision remains on ± 0.5 DEG C within; Between 1600 ~ 1200 DEG C, the cooldown rate of crucible surface is controlled within the scope of 0 ~ 10 DEG C/min; The body of heater speed of rotation be 0 ~ 30 rev/min adjustable.
4. according to claim 1 or 2, simulating the method for solidified structure growth under large ingot casting slow cooling condition, it is characterized in that: gather according to being not less than the temperature data of 10Hz frequency to 4 of crucible sides.
5. one kind implements the claims the founding experimental provision of the method simulating solidified structure growth under large ingot casting slow cooling condition described in 1, primarily of heating and atmosphere protection system, temperature control and temperature acquisition system and central controller composition, described heating and atmosphere protection system mainly comprise and are arranged at crucible (7) in the vacuum furnace shell (1) of sealing and graphite protective sleeve (3), described graphite protective sleeve (3) is enclosed within the outside of described crucible (7), corundum fine sand (8) is tamped between described graphite protective sleeve (3) and described crucible (7), it is inner that raw metal is placed on described crucible (7), described temperature control and temperature acquisition system are made up of a series of temperature thermocouple (6) and temperature data collecting system (4) and temperature controller, described temperature data collecting system (4) and described temperature controller are all connected with described central controller signal, it is characterized in that: in described vacuum furnace shell (1), 4 sides of described graphite protective sleeve (3) are respectively in the face of one group of graphite heating body (2), the operating current of each described graphite heating body (2) carries out independent control by described temperature controller, each described temperature thermocouple (6) is arranged between each described graphite heating body (2) and described crucible (7), in clearance space between described vacuum furnace shell (1) and described graphite protective sleeve (3), thermal insulation board (12) is all used to separate between the adjacent described graphite heating body of often group (2), form a series of independently heating clamber (11) respectively, temperature in each described heating clamber (11) is controlled by the independently graphite heating body (2) described in a group of correspondence respectively, bottom surface between each described heating clamber (11) and end face are closed by heat insulation felt (5), temperature control is carried out according to the cooling curve of diverse location in large Casting Ingot Solidification Process by described central controller, the interior corresponding temperature gradient of described crucible (7) is set in different directions, realize the metal solidification texture thermal simulation experiment under customization temperature gradient conditions, described central controller adjusts the power output of each described graphite heater (2) respectively by temperature controller, control the rate of temperature fall on described crucible (7) each surface, realize the metal solidification texture thermal simulation experiment under setting condition of external field, raw metal and described crucible (7) are all in the thermal environment of vacuum 10Pa, be provided with body of heater rotary system, described body of heater rotary system is made up of the swivel base (10) be arranged at below vacuum furnace shell (1) outside body of heater and power set, described swivel base (10) is driven to drive whole body of heater crankmotion by power set described in described central controller controls, the metal bath inside in described crucible (7) is made to form forced convertion, realize the metal solidification texture thermal simulation experiment under the condition of setting flow field, be provided with outfield gatherer (9), described outfield gatherer (9) is utilized to import outfield to the metal bath in described crucible (7), by outfield gatherer (9) described in described central controller controls, carry out under making solidification of metal melt process be in the outer field action of customization, realize the metal solidification texture thermal simulation experiment under setting condition of external field.
6. one kind implements the claims founding experimental provision described in 5, it is characterized in that: the importing coil in described outfield gatherer (9) is arranged at described vacuum furnace shell (1) inside, described importing coil, at furnace interior controllable lift, is described importing coil configuration cooling system.
7. implement the claims a founding experimental provision described in 6, it is characterized in that: the cooling system of described importing coil is water-cooling system, make water flowing cooling in described importing coil, cooling water flow is regulated according to the height of pipe outer wall temperature.
8. implement the claims a founding experimental provision described in any one in 5 ~ 7, it is characterized in that: described heat insulation felt (5) is carbon felt.
CN201510164008.6A 2015-04-09 2015-04-09 Simulate the method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling Active CN104959577B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510164008.6A CN104959577B (en) 2015-04-09 2015-04-09 Simulate the method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510164008.6A CN104959577B (en) 2015-04-09 2015-04-09 Simulate the method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling

Publications (2)

Publication Number Publication Date
CN104959577A true CN104959577A (en) 2015-10-07
CN104959577B CN104959577B (en) 2017-11-10

Family

ID=54213754

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201510164008.6A Active CN104959577B (en) 2015-04-09 2015-04-09 Simulate the method and founding experimental provision that solidified structure grows under the conditions of big ingot casting slow cooling

Country Status (1)

Country Link
CN (1) CN104959577B (en)

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105290376A (en) * 2015-10-30 2016-02-03 广东工业大学 Fusion casting equipment for low-silver hypo eutectic lead-free solder and method for manufacturing solder through fusion casting equipment
CN105483830A (en) * 2015-11-30 2016-04-13 上海大学 Method and apparatus for measuring flow velocity of interdendritic fluid under convection condition
CN106890985A (en) * 2017-04-25 2017-06-27 北京航空航天大学 It is a kind of for manufacturing casting device and method without shrinkage cavity casting
CN107876718A (en) * 2017-11-20 2018-04-06 辽宁科技大学 For simulating the experimental provision and experimental method of special heavy plate slow-set
CN108693210A (en) * 2018-05-25 2018-10-23 武汉钢铁有限公司 Cooling wall cooling rate and thermal shock relation test equipment and test method
CN108961972A (en) * 2018-07-31 2018-12-07 马鞍山尚元冶金科技有限公司 Steel liquid solidification simulator
CN108982578A (en) * 2018-07-31 2018-12-11 马鞍山尚元冶金科技有限公司 A method of simulation solidification of molten steel process
CN109183157A (en) * 2018-09-26 2019-01-11 大连理工大学 It is a kind of for studying the Fluid Dynamics device and application method of solidification of metal melt behavior
CN109211422A (en) * 2018-10-24 2019-01-15 中国计量大学 Application method based on coal gasifier outside wall temperature monitoring imitative experimental appliance
CN109405999A (en) * 2018-10-24 2019-03-01 中国计量大学 A kind of imitative experimental appliance of pair of coal gasifier outside wall temperature variation monitoring
CN110243489A (en) * 2019-07-01 2019-09-17 西北工业大学 A kind of electromagnetic suspension melt process of setting three-dimensional temperature field measurement device and method
CN112297868A (en) * 2019-07-26 2021-02-02 浙江吉智新能源汽车科技有限公司 Active heating control method and device for hybrid excitation motor
CN113817910A (en) * 2021-10-08 2021-12-21 昆山晶微新材料研究院有限公司 Homogenization treatment device, casting equipment and preparation method of high-homogeneity cast ingot
CN114406246A (en) * 2022-03-10 2022-04-29 湖南东方钪业股份有限公司 Temperature-control slow-setting casting die and process for scandium precipitation and enrichment of aluminum-scandium intermediate alloy

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05293619A (en) * 1992-04-17 1993-11-09 Showa Electric Wire & Cable Co Ltd Instrument for monitoring and measuring temperature in mold
JPH0798289A (en) * 1993-04-28 1995-04-11 Nippon Steel Corp Method and apparatus for simulating solidification of metal material
CN101075287A (en) * 2007-06-26 2007-11-21 上海大学 Physical simulating method and device during continuous-casting billet coagulation tissue growth process
KR20120097066A (en) * 2011-02-24 2012-09-03 현대제철 주식회사 Simulating apparatus for solidified layer thickness using water model mold
CN203972826U (en) * 2014-04-02 2014-12-03 上海大学 A kind of liquid surface fluctuation device
CN104226952A (en) * 2014-01-02 2014-12-24 上海大学 Metal solidification process simulation method

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH05293619A (en) * 1992-04-17 1993-11-09 Showa Electric Wire & Cable Co Ltd Instrument for monitoring and measuring temperature in mold
JPH0798289A (en) * 1993-04-28 1995-04-11 Nippon Steel Corp Method and apparatus for simulating solidification of metal material
CN101075287A (en) * 2007-06-26 2007-11-21 上海大学 Physical simulating method and device during continuous-casting billet coagulation tissue growth process
KR20120097066A (en) * 2011-02-24 2012-09-03 현대제철 주식회사 Simulating apparatus for solidified layer thickness using water model mold
CN104226952A (en) * 2014-01-02 2014-12-24 上海大学 Metal solidification process simulation method
CN203972826U (en) * 2014-04-02 2014-12-03 上海大学 A kind of liquid surface fluctuation device

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
仲红刚: "连铸坯凝固过程热模拟研究", 《中国博士学位论文全文数据库(工程科技Ⅰ辑)》 *

Cited By (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105290376A (en) * 2015-10-30 2016-02-03 广东工业大学 Fusion casting equipment for low-silver hypo eutectic lead-free solder and method for manufacturing solder through fusion casting equipment
CN105483830A (en) * 2015-11-30 2016-04-13 上海大学 Method and apparatus for measuring flow velocity of interdendritic fluid under convection condition
CN106890985A (en) * 2017-04-25 2017-06-27 北京航空航天大学 It is a kind of for manufacturing casting device and method without shrinkage cavity casting
CN107876718A (en) * 2017-11-20 2018-04-06 辽宁科技大学 For simulating the experimental provision and experimental method of special heavy plate slow-set
CN108693210A (en) * 2018-05-25 2018-10-23 武汉钢铁有限公司 Cooling wall cooling rate and thermal shock relation test equipment and test method
CN108693210B (en) * 2018-05-25 2020-10-30 武汉钢铁有限公司 Equipment and method for testing relation between cooling rate of cooling wall and thermal shock
CN108961972B (en) * 2018-07-31 2020-10-16 马鞍山尚元冶金科技有限公司 Molten steel solidification simulator
CN108982578A (en) * 2018-07-31 2018-12-11 马鞍山尚元冶金科技有限公司 A method of simulation solidification of molten steel process
CN108961972A (en) * 2018-07-31 2018-12-07 马鞍山尚元冶金科技有限公司 Steel liquid solidification simulator
CN109183157A (en) * 2018-09-26 2019-01-11 大连理工大学 It is a kind of for studying the Fluid Dynamics device and application method of solidification of metal melt behavior
CN109211422A (en) * 2018-10-24 2019-01-15 中国计量大学 Application method based on coal gasifier outside wall temperature monitoring imitative experimental appliance
CN109405999A (en) * 2018-10-24 2019-03-01 中国计量大学 A kind of imitative experimental appliance of pair of coal gasifier outside wall temperature variation monitoring
CN109405999B (en) * 2018-10-24 2020-11-10 中国计量大学 Simulation experiment device for monitoring temperature change of outer wall of coal gasifier
CN110243489A (en) * 2019-07-01 2019-09-17 西北工业大学 A kind of electromagnetic suspension melt process of setting three-dimensional temperature field measurement device and method
CN110243489B (en) * 2019-07-01 2020-09-11 西北工业大学 Device and method for measuring three-dimensional temperature field in solidification process of electromagnetic suspension melt
CN112297868A (en) * 2019-07-26 2021-02-02 浙江吉智新能源汽车科技有限公司 Active heating control method and device for hybrid excitation motor
CN112297868B (en) * 2019-07-26 2022-05-27 浙江吉智新能源汽车科技有限公司 Active heating control method and device for hybrid excitation motor
CN113817910A (en) * 2021-10-08 2021-12-21 昆山晶微新材料研究院有限公司 Homogenization treatment device, casting equipment and preparation method of high-homogeneity cast ingot
CN114406246A (en) * 2022-03-10 2022-04-29 湖南东方钪业股份有限公司 Temperature-control slow-setting casting die and process for scandium precipitation and enrichment of aluminum-scandium intermediate alloy

Also Published As

Publication number Publication date
CN104959577B (en) 2017-11-10

Similar Documents

Publication Publication Date Title
CN104959577A (en) Method for simulating growth of solidification structure of large ingot under slow cooling condition, and fusion casting experiment apparatus
CN110280746A (en) The method that a kind of high-strength ultrasonic wave added in list source casts big specification 2XXX line aluminium alloy billet
CN103131980B (en) Method for realizing fine crystal solidification by controlling spherical crystal stabilization
CN106041008B (en) A kind of continuous cast mold adjacent corner molten steel initial solidification simulator and method
CN102528002A (en) Process and device for high-temperature alloy fine-grain casting with composite electromagnetic fields
CN103464706A (en) Method and device for continuously casting and preparing high-oriented uniform fine-crystalline structure
CN109396400A (en) A kind of large-scale complex thin-wall fine grain casting integrated molding method and apparatus
CN105568018A (en) Directional magnesium alloy solidification device and method for directionally solidifying magnesium alloy through directional magnesium alloy solidification device
CN104353795A (en) Continuous directional solidification technology adopting temperature gradient crystallizer
CN103008623A (en) Method for refining crystal grains by utilizing strong magnetic field and special metal solidification casting device thereof
CN105177715A (en) Method for controlling stray crystal formation
CN110000365A (en) The heat simulation and device of big ingot solidification tissue based on high throughput experiment
CN105033213B (en) Simulating device for casting blanks in continuous casting chamfering crystallizer and application of simulating device
CN105964990A (en) Directional solidification method with external magnetic field for controlling freckle defect
CN101767190A (en) Physical simulation method and physical simulation device for double-roll continuous casting thin strip solidification
CN105014033A (en) Method for simulating solidification structure growth process of continuous cast billet
CN203972802U (en) A kind of continuous casting billet solidifies treating apparatus
CN102078947B (en) Method for calculating heat flow density in solidification heat transfer process of continuous casting crystallizer
CN105014035A (en) Device for simulating initial solidification of liquid steel in crystallizer
CN109513900A (en) Ingot casting part electromagnetic pump low-pressure casting process and part electromagnetic pump low-pressure casting process
CN108326262A (en) A kind of superpower travelling-magnetic-field continuous processing apparatus for directional solidification of alloy-steel casting
CN108326263A (en) A kind of superpower travelling-magnetic-field continuous processing directional freeze method of alloy-steel casting
CN107020358B (en) Device for simulating solidification structure and unsteady state heat flow of casting blank surface layer in crystallizer
CN103645200B (en) The method of ��-XAFS technology in site measurement scorification crystal growth microtexture and miniature crystal growing furnace
CN104593707B (en) A kind of regulate and control AlCoCrFeNi high-entropy alloy tissue method

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant