CN104944446A - 一种印染废水中提取硝酸钾试剂的方法 - Google Patents
一种印染废水中提取硝酸钾试剂的方法 Download PDFInfo
- Publication number
- CN104944446A CN104944446A CN201510328937.6A CN201510328937A CN104944446A CN 104944446 A CN104944446 A CN 104944446A CN 201510328937 A CN201510328937 A CN 201510328937A CN 104944446 A CN104944446 A CN 104944446A
- Authority
- CN
- China
- Prior art keywords
- potassium nitrate
- printing
- dyeing wastewater
- saltpetre
- reagent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 title claims abstract description 72
- 238000000034 method Methods 0.000 title claims abstract description 42
- 239000002351 wastewater Substances 0.000 title claims abstract description 37
- 235000010333 potassium nitrate Nutrition 0.000 title claims abstract description 36
- 239000004323 potassium nitrate Substances 0.000 title claims abstract description 36
- 238000004043 dyeing Methods 0.000 title claims abstract description 34
- 239000003153 chemical reaction reagent Substances 0.000 title claims abstract description 17
- 238000007639 printing Methods 0.000 title abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 31
- 238000005406 washing Methods 0.000 claims abstract description 27
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 25
- 238000000502 dialysis Methods 0.000 claims abstract description 16
- 238000001728 nano-filtration Methods 0.000 claims abstract description 16
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000002425 crystallisation Methods 0.000 claims description 13
- 235000011187 glycerol Nutrition 0.000 claims description 12
- 238000001816 cooling Methods 0.000 claims description 11
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 10
- 239000012452 mother liquor Substances 0.000 claims description 10
- DPDMMXDBJGCCQC-UHFFFAOYSA-N [Na].[Cl] Chemical compound [Na].[Cl] DPDMMXDBJGCCQC-UHFFFAOYSA-N 0.000 claims description 7
- 238000011221 initial treatment Methods 0.000 claims description 7
- 229910001415 sodium ion Inorganic materials 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 239000006228 supernatant Substances 0.000 claims description 7
- 238000011282 treatment Methods 0.000 claims description 7
- FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 claims description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract description 5
- 238000000605 extraction Methods 0.000 abstract description 5
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 abstract description 3
- 238000001035 drying Methods 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 238000004064 recycling Methods 0.000 abstract description 2
- 238000005119 centrifugation Methods 0.000 abstract 1
- 238000005185 salting out Methods 0.000 abstract 1
- 230000001105 regulatory effect Effects 0.000 description 4
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 230000008025 crystallization Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229920006395 saturated elastomer Polymers 0.000 description 2
- VWDWKYIASSYTQR-UHFFFAOYSA-N sodium nitrate Chemical compound [Na+].[O-][N+]([O-])=O VWDWKYIASSYTQR-UHFFFAOYSA-N 0.000 description 2
- 241000370738 Chlorion Species 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 1
- AZFNGPAYDKGCRB-XCPIVNJJSA-M [(1s,2s)-2-amino-1,2-diphenylethyl]-(4-methylphenyl)sulfonylazanide;chlororuthenium(1+);1-methyl-4-propan-2-ylbenzene Chemical compound [Ru+]Cl.CC(C)C1=CC=C(C)C=C1.C1=CC(C)=CC=C1S(=O)(=O)[N-][C@@H](C=1C=CC=CC=1)[C@@H](N)C1=CC=CC=C1 AZFNGPAYDKGCRB-XCPIVNJJSA-M 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- IYNDLOXRXUOGIU-LQDWTQKMSA-M benzylpenicillin potassium Chemical compound [K+].N([C@H]1[C@H]2SC([C@@H](N2C1=O)C([O-])=O)(C)C)C(=O)CC1=CC=CC=C1 IYNDLOXRXUOGIU-LQDWTQKMSA-M 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 235000019504 cigarettes Nutrition 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000003317 industrial substance Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000005649 metathesis reaction Methods 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000007800 oxidant agent Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229940056360 penicillin g Drugs 0.000 description 1
- 239000002957 persistent organic pollutant Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 235000010289 potassium nitrite Nutrition 0.000 description 1
- 239000004304 potassium nitrite Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- JQXXHWHPUNPDRT-WLSIYKJHSA-N rifampicin Chemical compound O([C@](C1=O)(C)O/C=C/[C@@H]([C@H]([C@@H](OC(C)=O)[C@H](C)[C@H](O)[C@H](C)[C@@H](O)[C@@H](C)\C=C\C=C(C)/C(=O)NC=2C(O)=C3C([O-])=C4C)C)OC)C4=C1C3=C(O)C=2\C=N\N1CC[NH+](C)CC1 JQXXHWHPUNPDRT-WLSIYKJHSA-N 0.000 description 1
- 229960001225 rifampicin Drugs 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 235000010344 sodium nitrate Nutrition 0.000 description 1
- 239000004317 sodium nitrate Substances 0.000 description 1
- 229940001516 sodium nitrate Drugs 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 230000000930 thermomechanical effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D9/00—Nitrates of sodium, potassium or alkali metals in general
- C01D9/16—Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Removal Of Specific Substances (AREA)
Abstract
Description
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201510328937.6A CN104944446B (zh) | 2015-06-13 | 2015-06-13 | 一种印染废水中提取硝酸钾试剂的方法 |
Applications Claiming Priority (1)
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---|---|---|---|
CN201510328937.6A CN104944446B (zh) | 2015-06-13 | 2015-06-13 | 一种印染废水中提取硝酸钾试剂的方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN104944446A true CN104944446A (zh) | 2015-09-30 |
CN104944446B CN104944446B (zh) | 2016-06-29 |
Family
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Application Number | Title | Priority Date | Filing Date |
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CN201510328937.6A Active CN104944446B (zh) | 2015-06-13 | 2015-06-13 | 一种印染废水中提取硝酸钾试剂的方法 |
Country Status (1)
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CN (1) | CN104944446B (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107601533A (zh) * | 2017-10-27 | 2018-01-19 | 安徽胜达化工科技有限公司 | 一种硝酸钾的结晶方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101734690A (zh) * | 2008-11-13 | 2010-06-16 | 常福松 | 一种溶剂萃取法制取硝酸钾的方法 |
-
2015
- 2015-06-13 CN CN201510328937.6A patent/CN104944446B/zh active Active
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101734690A (zh) * | 2008-11-13 | 2010-06-16 | 常福松 | 一种溶剂萃取法制取硝酸钾的方法 |
Non-Patent Citations (1)
Title |
---|
张罡等: "盐析结晶法制取硝酸钾研究", 《无机盐工业》 * |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107601533A (zh) * | 2017-10-27 | 2018-01-19 | 安徽胜达化工科技有限公司 | 一种硝酸钾的结晶方法 |
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CN104944446B (zh) | 2016-06-29 |
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Effective date of registration: 20201119 Address after: 225600 Jiangsu Province Yangzhou Gaoyou Economic Development Zone Dongting Lake Road Science and Technology Venture Center, Room 210, 2nd floor Patentee after: JIANGSU BOSIWEI INTELLECTUAL PROPERTY OPERATION Co.,Ltd. Address before: Gehu Lake Road Wujin District 213164 Jiangsu city of Changzhou province No. 1 Patentee before: CHANGZHOU University |
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Effective date of registration: 20201125 Address after: 224600 North of Port and Television Avenue, Xiangshui Coastal Economic Development Zone, Yancheng City, Jiangsu Province Patentee after: Xiangshui Huaqing Sewage Treatment Co.,Ltd. Address before: 225600 Jiangsu Province Yangzhou Gaoyou Economic Development Zone Dongting Lake Road Science and Technology Venture Center, Room 210, 2nd floor Patentee before: JIANGSU BOSIWEI INTELLECTUAL PROPERTY OPERATION Co.,Ltd. |
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Effective date of registration: 20240715 Address after: 224600 Coastal Economic Development Zone of Xiangshui County, Yancheng City, Jiangsu Province Patentee after: Fuda Lingang Water Supply and Drainage Co.,Ltd. in Xiangshui County Country or region after: China Address before: 224600 north side of Gangdian Avenue, coastal economic development zone, Xiangshui County, Yancheng City, Jiangsu Province Patentee before: Xiangshui Huaqing Sewage Treatment Co.,Ltd. Country or region before: China |
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