CN104922006B - A kind of red wine clay mask and preparation method thereof - Google Patents
A kind of red wine clay mask and preparation method thereof Download PDFInfo
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- CN104922006B CN104922006B CN201510401587.1A CN201510401587A CN104922006B CN 104922006 B CN104922006 B CN 104922006B CN 201510401587 A CN201510401587 A CN 201510401587A CN 104922006 B CN104922006 B CN 104922006B
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Abstract
The invention discloses a kind of red wine clay mask, which is a kind of dosage form that coats and can be thrown off after drying, including following components：Deionized water, wine extract, ethyl alcohol, polyvinyl alcohol, glycerine, butanediol, dimethyl silicone polymer, polysorbate20, aminomethyl propanol, Phenoxyethanol, Sensiva SC50, hydroxyethyl cellulose and cellulose gum.The invention also discloses a kind of preparation methods of red wine clay mask.Liquor-making byproduct red wine mud is applied to personal care articles field by the present invention, and a kind of peelable red wine clay mask easily used has been made, and the red wine clay mask is mild, has the multiple efficacies such as skin lightening, moisturizing, exfoliating, and energy skin nutrition makes skin exquisiteness gloss.
Description
Technical field
The invention belongs to cosmetic fields, are related to a kind of strippable facial mask, more particularly, to a kind of red wine clay mask and
Its preparation method.
Background technology
By-product namely usually said grape vinasse of the red wine mud from red wine brewing process, are that red wine ferments
The purees obtained after former wine, skin slag, crystallization winestone is removed afterwards, and powdery is obtained after the techniques such as drying, sterilizing, crushing, screening
Object.
At present, people are concentrated mainly on food and herding field to the utilization of red wine mud, and using red wine mud as skin
Skin nursing product applies to that personal care product field is also at the early-stage, but it contains there are many ingredient to skin beneficiating, increasingly
It is concerned by people.The fragrance of the peculiar red wine of red wine mud contains abundant wine yeast active matter, Red Wine Polyphenols, tartaric acid, fibre
The nutritional ingredients such as dimension element, vitamin and trace element.Wherein wine yeast active matter includes amino acid, peptides, functional polysaccharide
Deng with anti-oxidant and skin whitening effect；Red Wine Polyphenols has effects that oxidation resistant；Tartaric acid constituents can remove old angle
Matter improves skin metabolism；The effect of vitamin and the nutritious skin of trace element.Red wine mud is not widely used in individual at present
Nursing field mainly can not preferably reside in skin surface due to being directly coated with red wine mud, using trouble, not easy to operate,
It acquires a certain degree of difficulty simultaneously on preparation stability.
The content of the invention
It is a kind of coating the purpose of the invention is to overcome the deficiencies of the prior art and provide a kind of red wine clay mask
The dosage form that can be thrown off after drying, the red wine clay mask is mild, has the multiple efficacies such as skin lightening, moisturizing, exfoliating, can nutrition skin
Skin makes skin exquisiteness gloss.
Another object of the present invention is to provide a kind of preparation method of above-mentioned red wine clay mask.
Realizing a kind of technical solution of above-mentioned purpose is：A kind of red wine clay mask includes the component of following parts by weight：
A kind of above-mentioned red wine clay mask, wherein, the hydroxyethyl cellulose and cellulose gum are thickener, the hydroxyl
The ratio of ethyl cellulose and cellulose gum is 5：2.
Above-mentioned raw materials are commercial product.
The present invention also provides a kind of preparation methods of red wine clay mask, comprise the following steps：
A, the 2/3 of deionized water is weighed, polyvinyl alcohol is added in 2/3 deionized water, 60 DEG C is heated with stirring to, makes
Polyvinyl alcohol is dissolved completely in 2/3 deionized water；
B, hydroxyethyl cellulose and cellulose gum are uniformly mixed, are then uniformly mixed glycerine and butanediol, then will
The mixture of hydroxyethyl cellulose and cellulose gum adds in the solution that step A obtains after being disperseed with the mixed liquor of glycerine and butanediol
In, stirring makes it be dissolved completely in the solution that step A obtains, is then heated to 70-75 DEG C；
C, by dimethyl silicone polymer and polysorbate -20 after mixing, 70-75 DEG C is heated to, is then added to B
It in the material that step obtains, stirs evenly, then cools down；
D, wine extract is added in remaining deionized water, stirred evenly；
E, when the material that step C obtains is cooled to 40 DEG C, material that D steps obtain is added in into the material that step C obtains
In, and stir evenly；
F, aminomethyl propanol, ethyl alcohol, Phenoxyethanol and Sensiva SC50 are sequentially added in the material that E steps obtain,
It discharges after being uniformly mixed.
The preparation method of above-mentioned red wine clay mask, wherein, in step B, the hydroxyethyl cellulose and cellulose gum are equal
For thickener, the ratio of the hydroxyethyl cellulose and cellulose gum is 5：2.
Employ a kind of technical solution of red wine clay mask of the present invention, compared with prior art, red wine mud of the invention
Facial mask uses peelable gel rubber system, adds the wine extract of high-content, possesses pleasant fragrance, there is refrigerant sense, Ke Yiyou
Anti-oxidant, whitening, removal cutin are imitated, nutrition skin improves skin metabolism, selects polyvinyl alcohol and hydroxyethyl cellulose, fiber
Plain glue builds gel rubber system and its space structure, adds in ethyl alcohol enhancing volatility, arrange in pairs or groups glycerine and butanediol control facial mask use
The peelable time afterwards.
It is a test to gel rubber system since high-content wine extract has centainly ionic, meanwhile, low
After temperature is freezed, gel is present with avalanche phenomenon.The reasonably combined emulsifier of the present invention, polyalcohol, active matter ratio, distribute work rationally
Skill solves the problems, such as its low temperature avalanche.And the present invention is matched by specific thickener, ensures red wine mud homodisperse
Meanwhile it is stable in the presence of in system.
A kind of technical solution of the preparation method of red wine clay mask using the present invention, can preferably improve gel rubber system
Stability, while to the salubrious moisturizing of skin, there is good anti-oxidant whitening effect.
Description of the drawings
Fig. 1 is that the skin of the red wine clay mask in each embodiment senses the radar map of test result；
Fig. 2 is the test result figure using the dermal melanin inhibiting rate before and after the red wine clay mask in each embodiment；
Fig. 3 is the test result figure using the skin moisture content before and after the red wine clay mask in each embodiment.
Specific embodiment
The present inventor is in order to preferably understand technical scheme, below by specifically real
It applies example and is described in detail with reference to attached drawing：
Table 1
The red wine clay mask of embodiment 1-4 is prepared according to the raw material proportioning of table 1.
In each raw material, deionized water uses and prepared by the deionized water apparatus for preparation of safe model DW 100；Grape wine
Extract produces for the evergreen bio tech ltd in Ningxia Helan, trade name red wine mud；Ethyl alcohol is Jiangsu prosperity functionalization
Learn limited company's production, trade name absolute ethyl alcohol；Polyvinyl alcohol select Japan can Li Le companies, trade name PVA
217；The peaceful Chemical Manufacture of glycerine selection section, trade name Glycerine 99.5%；Butanediol selects U.S. OXEA productions, commodity
Entitled 1,3-BG；Dimethyl silicone polymer selects Dow Corning Corporation's production, trade name PMX200-50cst；Polysorbate-
20 select the production of standing grain major company, trade name Tween 20；Aminomethyl propanol selects DOW Chemical production, trade name AMP-
ULTRA PC 2000；Phenoxyethanol and Sensiva SC50 select German Shu Mei companies to produce, trade name euxyl PE
9010；Hydroxyethyl cellulose selects the production of company of sub- Silan, trade name Natrosol 250HHR；Cellulose gum selects sub- scholar
Lan companies produce, trade name Aqualon CMC 7MF.
Red wine clay mask provided by the invention is prepared by following steps：
A, the 2/3 of deionized water is weighed, polyvinyl alcohol is added in 2/3 deionized water, 60 DEG C is heated with stirring to, makes
Polyvinyl alcohol is dissolved completely in 2/3 deionized water；
B, hydroxyethyl cellulose and cellulose gum are uniformly mixed, are then uniformly mixed glycerine and butanediol, then will
The mixture of hydroxyethyl cellulose and cellulose gum adds in the solution that step A obtains after being disperseed with the mixed liquor of glycerine and butanediol
In, stirring makes it be dissolved completely in the solution that step A obtains, is then heated to 70-75 DEG C；
C, by dimethyl silicone polymer and polysorbate -20 after mixing, 70-75 DEG C is heated to, is then added to B
It in the material that step obtains, stirs evenly, then cools down；
D, wine extract is added in remaining deionized water, stirred evenly；
E, when the material that step C obtains is cooled to 40 DEG C, material that D steps obtain is added in into the material that step C obtains
In, and stir evenly；
F, aminomethyl propanol, ethyl alcohol, Phenoxyethanol and Sensiva SC50 are sequentially added in the material that E steps obtain,
It discharges after being uniformly mixed.
Hydroxyethyl cellulose and cellulose gum are thickener.
Accelerated stability test is carried out to the red wine clay mask of the above-mentioned embodiment 1-4 prepared, successively at -15 DEG C, 5
DEG C, it at 40 DEG C and 49 DEG C, tests 30 days, 60 days and 90 days respectively, tests the stability of the red wine clay mask of the present invention, stability
Accelerated test is as shown in table 2：
Table 2
Accelerated stability test the results show in table 2：The red wine clay mask of the present invention has excellent stability, Ke Yiman
The demand listed enough.
Skin sense evaluation test is carried out to the red wine clay mask of the above-mentioned embodiment 1-4 prepared, 30 people of number is tested, in sense
In official's evaluation experimental room, after the 30min that sits quietly, subject uses own control evaluation method, and test volume is everyone 10g red wine mud face
Film, carries out face evaluation and test on probation, and skin senses test result as shown in table 3 and Fig. 1：
Table 3
It is shown in table 3 in the radar map of the skin sensing test result of skin sensing test result and Fig. 1：The red wine clay mask of the present invention
Use feeling it is comfortable, film forming and remove sex expression it is good.The red wine clay mask of the present invention is using peelable gel rubber system, addition
The wine extract of high-content possesses pleasant fragrance, there is refrigerant sense, can effectively anti-oxidant, whitening, removal cutin, nutrition
Skin improves skin metabolism, and polyvinyl alcohol is selected to build gel rubber system and its space knot with hydroxyethyl cellulose, cellulose gum
Structure, adds in ethyl alcohol enhancing volatility, and collocation glycerine and butanediol control facial mask use the rear peelable time.Due to high-content grape
Wine extract has centainly ionic, is a test to gel rubber system, meanwhile, after sharp freezing, gel, which is present with, to be collapsed
It collapses phenomenon.The reasonably combined emulsifier of the present invention, polyalcohol, active matter ratio, distribute technique rationally and solve its low temperature avalanche
Problem.And the present invention is matched by specific thickener, ensures that red wine mud while homodisperse, is stable in the presence of system
In.
System MPA10 skin evaluation appts are tested by German CK companies Multi probes, in 23 ± 2 DEG C of temperature, humidity 50 ±
Under 10% test condition, using two indexs of dermal melanin and moisture of skin as evaluation criterion, to manufactured embodiment 1 to 4
Red wine clay mask carry out arm cycle efficacy assessment, experiment middle left and right hand inner forearm mark 4 × 4cm2Test area,
It is interregional every 2cm.Test product and blank control are randomly dispersed on left and right inboard arm, specification subject by 2.0 ±
0.1mg samples/cm2Dosage be spread evenly across in trial zone, adhere to using daily.The wherein test knot of dermal melanin content
Fruit is as shown in table 4, and the result of calculation of dermal melanin inhibiting rate is as shown in table 5 and Fig. 2, the contrast test knot of skin moisture content
Fruit is as shown in table 6 and Fig. 3.
Table 4
Table 5
The result of calculation and figure of the test result of dermal melanin content in table 4, the dermal melanin inhibiting rate in table 5
It is shown in the result of calculation figure of dermal melanin inhibiting rate in 2：Red wine clay mask of the present invention has good whitening effect, right
Dermal melanin test result showed the red wine clay mask using embodiment 1 to 4 after 4 weeks, and dermal melanin content significantly reduces,
Dermal melanin content is considerably less than blank group, and the inhibiting rate of dermal melanin is higher than blank group.
Table 6
It is shown in skin moisture content test result figure in skin moisture content test result and Fig. 3 in table 6：This hair
Bright red wine clay mask has good moistening effect.After embodiment 1 to 4 being used to moisture of skin test display, moisture content of skin
It significantly improves, moisture content of skin is apparently higher than blank group.
It can be seen that the red wine clay mask of the present invention is with the addition of the wine extract of high-content, the red wine clay mask
Matter is mild, has the multiple efficacies such as skin lightening, moisturizing, exfoliating, and energy skin nutrition makes skin exquisiteness gloss, has good anti-
Aoxidize whitening effect.
Those of ordinary skill in the art it should be appreciated that more than embodiment be intended merely to illustrate the present invention,
And be not used as limitation of the invention, as long as in the spirit of the present invention, the change to embodiment described above
Change, modification will all fall in the range of claims of the present invention.
Claims (3)
1. a kind of red wine clay mask, which is characterized in that include the component of following parts by weight：
The hydroxyethyl cellulose and cellulose gum are thickener, and the ratio of the hydroxyethyl cellulose and cellulose gum is 5：
2。
2. a kind of preparation method of red wine clay mask as described in claim 1, which is characterized in that comprise the following steps：
A, the 2/3 of deionized water is weighed, polyvinyl alcohol is added in 2/3 deionized water, is heated with stirring to 60 DEG C, makes poly- second
Enol is dissolved completely in 2/3 deionized water；
B, hydroxyethyl cellulose and cellulose gum are uniformly mixed, are then uniformly mixed glycerine and butanediol, then by hydroxyl second
The mixture of base cellulose and cellulose gum is added in after being disperseed with the mixed liquor of glycerine and butanediol in the solution that step A obtains,
Stirring, makes it be dissolved completely in the solution that step A obtains, is then heated to 70-75 DEG C；
C, by dimethyl silicone polymer and polysorbate -20 after mixing, 70-75 DEG C is heated to, is then added to step B
It in obtained material, stirs evenly, then cools down；
D, wine extract is added in remaining deionized water, stirred evenly；
E, when the material that step C obtains is cooled to 40 DEG C, the material that D steps obtain is added in the material that step C obtains, and
It stirs evenly；
F, aminomethyl propanol, ethyl alcohol, Phenoxyethanol and Sensiva SC50 are sequentially added in the material that E steps obtain, stirred
It discharges after mixing.
3. the preparation method of red wine clay mask as claimed in claim 2, which is characterized in that in step B, the hydroxy ethyl fiber
Element and cellulose gum are thickener, and the ratio of the hydroxyethyl cellulose and cellulose gum is 5：2.
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| CN201510401587.1A CN104922006B (en) | 2015-07-09 | 2015-07-09 | A kind of red wine clay mask and preparation method thereof |
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| CN104922006B true CN104922006B (en) | 2018-05-18 |
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Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105147568A (en) * | 2015-10-15 | 2015-12-16 | 庄琪娟 | Active grape wine lees mask and production method thereof |
| KR101667937B1 (en) * | 2016-01-05 | 2016-10-24 | 한국콜마주식회사 | Cosmetics composition of peel-off type pack and method preparing the same |
| CN105878158A (en) * | 2016-04-15 | 2016-08-24 | 覃碧 | Tearing pearl powder mask |
| CN105832631A (en) * | 2016-04-15 | 2016-08-10 | 覃碧 | Manufacturing method of pearl powder peel-off face mask |
| CN106377465A (en) * | 2016-11-22 | 2017-02-08 | 郑州兰茜生物工程有限公司 | Facial mask with moisture retaining, nourishing and physical therapy effects and preparation method thereof |
| CN106389225A (en) * | 2016-11-22 | 2017-02-15 | 郑州兰茜生物工程有限公司 | Red wine moisturizing nutrient facial mask and preparation method thereof |
| CN106473984A (en) * | 2016-11-22 | 2017-03-08 | 郑州兰茜生物工程有限公司 | Anti-ageing facial film of a kind of red wine elite moisture-keeping nutrient and preparation method thereof |
| CN108354848B (en) * | 2018-03-01 | 2021-09-14 | 北方民族大学 | Wine lees mask and preparation method thereof |
| CN112972302A (en) * | 2021-02-06 | 2021-06-18 | 澳宝化妆品（惠州）有限公司 | Tear-off facial mask capable of quickly forming film and preparation method thereof |
| CN113546020A (en) * | 2021-09-06 | 2021-10-26 | 范月琴 | Preparation method of grape wine mud mask and grape wine mud mask |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1342453A (en) * | 2000-09-07 | 2002-04-03 | 莱雅公司 | Cosmetic composition and its application used as skin cleaning pack |
| CN102100648A (en) * | 2009-12-21 | 2011-06-22 | 上海子夏投资管理有限公司 | Preparation method of red wine hyaluronic acid face mask |
-
2015
- 2015-07-09 CN CN201510401587.1A patent/CN104922006B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1342453A (en) * | 2000-09-07 | 2002-04-03 | 莱雅公司 | Cosmetic composition and its application used as skin cleaning pack |
| CN102100648A (en) * | 2009-12-21 | 2011-06-22 | 上海子夏投资管理有限公司 | Preparation method of red wine hyaluronic acid face mask |
Non-Patent Citations (1)
| Title |
|---|
| APIVITA Instant Lifting Mask with red wine;Kalen0106;《http://www.cosdna.com/chs/cosmetic_979034586.html》;20100605;第1-2页表格部分 * |
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Inventor after: Mo Juanying Inventor after: Song Chunxiao Inventor after: Wang Feifei Inventor after: Ma Xiao Inventor after: Gao Shaoyang Inventor after: Guo Zhenyu Inventor after: He Li Inventor before: Gao Shaoyang Inventor before: Mo Juanying Inventor before: Zhou Yanfu Inventor before: Su Wenrou Inventor before: He Li |
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Effective date of registration: 20180408 Address after: 650000 Kunming hi tech Zone, Yunnan Province, Department of medicine No. 53 Applicant after: KUNMING BOTANEE BIOLOGICAL TECHNOLOGY Co.,Ltd. Applicant after: SHANGHAI BEITAINI BIOTECHNOLOGY CO., LTD. Applicant after: KUNMING BOTANEE BIOLOGICAL TECHNOLOGY Co.,Ltd. Shanghai branch Address before: 200335 Shanghai city Changning District Admiralty Road No. 999 Building 2 room 709 Applicant before: SHANGHAI BEITAINI BIOTECHNOLOGY CO., LTD. |
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Address after: 650106 No. 53, Ke Yan Road, hi tech Zone, Kunming, Yunnan. Co-patentee after: SHANGHAI BEITAINI BIOTECHNOLOGY CO., LTD. Patentee after: Yunnan Beitani Biotechnology Group Co., Ltd. Co-patentee after: Yunnan Beitani Biotechnology Group Co., Ltd. Shanghai Branch Address before: 650000 Kunming hi tech Zone, Yunnan Province, Department of medicine No. 53 Co-patentee before: SHANGHAI BEITAINI BIOTECHNOLOGY CO., LTD. Patentee before: KUNMING BOTANEE BIOLOGICAL TECHNOLOGY Co.,Ltd. Co-patentee before: KUNMING BOTANEE BIOLOGICAL TECHNOLOGY Co.,Ltd. Shanghai branch |