CN104909833A - Shrinkage dot glaze and preparation method thereof - Google Patents

Shrinkage dot glaze and preparation method thereof Download PDF

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Publication number
CN104909833A
CN104909833A CN201510236232.1A CN201510236232A CN104909833A CN 104909833 A CN104909833 A CN 104909833A CN 201510236232 A CN201510236232 A CN 201510236232A CN 104909833 A CN104909833 A CN 104909833A
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China
Prior art keywords
parts
glaze
ball
mill
point reduction
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CN201510236232.1A
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Chinese (zh)
Inventor
林迪辉
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XIANFEN CERAMICS IND CO Ltd HUNAN
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XIANFEN CERAMICS IND CO Ltd HUNAN
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Priority to CN201510236232.1A priority Critical patent/CN104909833A/en
Publication of CN104909833A publication Critical patent/CN104909833A/en
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Abstract

The invention discloses a shrinkage dot glaze. The shrinkage dot glaze comprises, by mass, 100 parts of basic glaze and 15-25 parts of gaseous silicon, and the basic glaze comprises, by mass, 40-45 parts of potash feldspar, 15-20 parts of quartz, 8-10 parts of calcite, 3-5 parts of strontium carbonate, 1-2 parts of zinc oxide, 3-5 parts of barium carbonate, 6-8 parts of kaolin, 4-5 parts of talcum and 12-15 parts of zirconium silicate. A glaze layer formed by using the shrinkage dot glaze shrinks to form a dot-like effect, is beautiful and unique, has good artistic effects, and is highly collectable.

Description

Point reduction glaze and preparation method thereof
Technical field
The present invention relates to a kind of point reduction glaze and preparation method thereof, belong to glaze preparing technical field.
Background technology
At present, in ceramic industry, the moulding of porcelain base is that the allotment of the base glaze of quality products makes porcelain more dazzling brilliant, the porcelain base of same moulding, often because glaze paint is different, and make the vision of human consumer produce different impacts, if make its glaze paint be shrunk to the glaze of point-like, its condition of surface is the daily edible vegetables " balsam pear " of people seemingly, the sub-light that this point reduction glaze has, and what have has gloss, decorate in vase class, cups and dishes class ceramic product, uniqueness attractive in appearance, have good artistic effect, product has reserve value.
Summary of the invention
Technical problem to be solved by this invention is the defect overcoming prior art, provides a kind of point reduction glaze, and its glaze layer is shrunk to point-like effect, uniqueness attractive in appearance, and have good artistic effect, product has reserve value.
In order to solve the problems of the technologies described above, technical scheme of the present invention is: a kind of point reduction glaze, its component and each component mass parts as follows:
Base glaze: 100 parts; Meteorological silicon: 15 parts-25 parts.
Component and each component mass parts of base glaze are as follows: potassium felspar sand: 40 parts-45 parts; Quartz: 15 parts-20 parts; Calcite: 8 parts-10 parts; Strontium carbonate powder: 3 parts-5 parts; Zinc oxide: 1 part-2 parts; Barium carbonate: 3 parts-5 parts; Kaolin: 6 parts-8 parts; Talcum: 4 parts-5 parts; Zirconium silicate: 12 parts-15 parts.
Be also 5/10000ths to millesimal carboxymethyl cellulose containing mass percent in the base glaze of 100%.
Also containing mass parts to be the aluminum oxide of 2 parts and mass parts the be quartz of 1 part in base glaze.
Present invention also offers a kind of preparation method of point reduction glaze, the step of the method is as follows:
A () is got the raw materials ready according to each component and each component mass parts;
B the material got ready is poured in ball mill and is added ball-milling medium and water carries out ball milling by (); Wherein, expect: the mass ratio=1:(0.5-0.6 of water), and the volume of the ball-milling medium added is the 1/3-1/2 of ball mill volume;
C () ball milling terminates after, unload and put glaze slip, measure glaze slip fineness, glaze slip fineness controls at 325 mesh screen residues: 0.02%-0.10%; The glaze slip of furnishing 37-38 degree Beaume again, gets the bright and clean base substrate of appearance and carries out glazing, under oxidizing atmosphere, fire finished product.
Further, in step (b), ball-milling medium adopts high alumina ballstone, according to greatly: in: the grating of little=1:2:1 mass ratio adds.
Further, in described step (b), the condition of Ball-milling Time, rotational speed of ball-mill and loading capacity is as follows: adopt 10kg ball mill, rotational speed of ball-mill is 60-62 rev/min, and Ball-milling Time was at 12 hours, and the loading capacity of ball mill is the raw material of 6kg; Adopt 500kg ball mill: rotational speed of ball-mill is 21 revs/min, Ball-milling Time 14 hours, and the loading capacity of ball mill is 300kg raw material.
Further, in described step (c), get the bright and clean base substrate of appearance and carry out glazing, glazing thickness is at 2.0-3.0mm.
After have employed technique scheme, by introducing meteorological silicon (magnesiumcarbonate) 15 parts-25 parts in base glaze, contracting glaze effect is fine, forms the even point-like of size, has prepared the point reduction glaze ceramic having artistic value, and had anti-skidding effect.
Embodiment
In order to make content of the present invention more easily be clearly understood, below according to specific embodiment, the present invention is further detailed explanation.
Embodiment one
A kind of point reduction glaze, its component and each component mass parts as follows:
Base glaze: 100 parts; Meteorological silicon: 15 parts.
Component and each component mass parts of base glaze are as follows: potassium felspar sand: 40 parts; Quartz: 15 parts; Calcite: 8 parts; Strontium carbonate powder: 3 parts; Zinc oxide: 1 part; Barium carbonate: 3 parts; Kaolin: 6 parts; Talcum: 4 parts; Zirconium silicate: 12 parts.
In the base glaze of 100%, also contain mass percent is the carboxymethyl cellulose of 5/10000ths.
Also containing mass parts to be the aluminum oxide of 2 parts and mass parts the be quartz of 1 part in base glaze.
The step of the preparation method of this point reduction glaze is as follows:
A () is got the raw materials ready according to each component and each component mass parts;
B the material got ready is poured in ball mill and is added ball-milling medium and water carries out ball milling by (); Wherein, expect: the mass ratio=1:(0.5-0.6 of water), and the volume of the ball-milling medium added is the 1/3-1/2 of ball mill volume;
C () ball milling terminates after, unload and put glaze slip, measure glaze slip fineness, glaze slip fineness controls at 325 mesh screen residues: 0.02%-0.10%; The glaze slip of furnishing 37-38 degree Beaume again, gets the bright and clean base substrate of appearance and carries out glazing, under oxidizing atmosphere, fire finished product.
In step (b), ball-milling medium adopts high alumina ballstone, according to greatly: in: the grating of little=1:2:1 mass ratio adds.
In step (b), the condition of Ball-milling Time, rotational speed of ball-mill and loading capacity is as follows: adopt 10kg ball mill, rotational speed of ball-mill is 60-62 rev/min, and Ball-milling Time was at 12 hours, and the loading capacity of ball mill is the raw material of 6kg.
In described step (c), get the bright and clean base substrate of appearance and carry out glazing, glazing thickness is at 2.0-3.0mm.
Embodiment two
A kind of point reduction glaze, its component and each component mass parts as follows:
Base glaze: 100 parts; Meteorological silicon: 25 parts.
Component and each component mass parts of base glaze are as follows: potassium felspar sand: 45 parts; Quartz: 20 parts; Calcite: 10 parts; Strontium carbonate powder: 5 parts; Zinc oxide: 2 parts; Barium carbonate: 5 parts; Kaolin: 8 parts; Talcum: 5 parts; Zirconium silicate: 15 parts.
In the base glaze of 100%, also contain mass percent is millesimal carboxymethyl cellulose.
Also containing mass parts to be the aluminum oxide of 2 parts and mass parts the be quartz of 1 part in base glaze.
The step of the preparation method of this point reduction glaze is as follows:
A () is got the raw materials ready according to each component and each component mass parts;
B the material got ready is poured in ball mill and is added ball-milling medium and water carries out ball milling by (); Wherein, expect: the mass ratio=1:(0.5-0.6 of water), and the volume of the ball-milling medium added is (1/3-1/2) of ball mill volume;
C () ball milling terminates after, unload and put glaze slip, measure glaze slip fineness, glaze slip fineness controls at 325 mesh screen residues: 0.02%-0.10%; The glaze slip of furnishing 37-38 degree Beaume again, gets the bright and clean base substrate of appearance and carries out glazing, under oxidizing atmosphere, fire finished product.
In step (b), ball-milling medium adopts high alumina ballstone, according to greatly: in: the grating of little=1:2:1 mass ratio adds.
In step (b), the condition of Ball-milling Time, rotational speed of ball-mill and loading capacity is as follows: adopt 500kg ball mill: rotational speed of ball-mill is 21 revs/min, Ball-milling Time 14 hours, and the loading capacity of ball mill is 300kg raw material.
In described step (c), get the bright and clean base substrate of appearance and carry out glazing, glazing thickness is at 2.0-3.0mm.
Embodiment three
A kind of point reduction glaze, its component and each component mass parts as follows:
Base glaze: 100 parts; Meteorological silicon: 20 parts.
Component and each component mass parts of base glaze are as follows: potassium felspar sand: 42 parts; Quartz: 18 parts; Calcite: 9 parts; Strontium carbonate powder: 4 parts; Zinc oxide: 1 part; Barium carbonate: 4 parts; Kaolin: 7 parts; Talcum: 4 parts; Zirconium silicate: 12 parts.
In the base glaze of 100%, also contain mass percent is millesimal carboxymethyl cellulose.
Also containing mass parts to be the aluminum oxide of 2 parts and mass parts the be quartz of 1 part in base glaze.
The step of the preparation method of this point reduction glaze is as follows:
A () is got the raw materials ready according to each component and each component mass parts;
B the material got ready is poured in ball mill and is added ball-milling medium and water carries out ball milling by (); Wherein, expect: the mass ratio=1:(0.5-0.6 of water), and the volume of the ball-milling medium added is the 1/3-1/2 of ball mill volume;
C () ball milling terminates after, unload and put glaze slip, measure glaze slip fineness, glaze slip fineness controls at 325 mesh screen residues: 0.02%-0.10%; The glaze slip of furnishing 37-38 degree Beaume again, gets the bright and clean base substrate of appearance and carries out glazing, under oxidizing atmosphere, fire finished product.
In step (b), ball-milling medium adopts high alumina ballstone, according to greatly: in: the grating of little=1:2:1 mass ratio adds.
In step (b), the condition of Ball-milling Time, rotational speed of ball-mill and loading capacity is as follows: adopt 10kg ball mill, rotational speed of ball-mill is 60-62 rev/min, and Ball-milling Time was at 12 hours, and the loading capacity of ball mill is the raw material of 6kg.
In described step (c), get the bright and clean base substrate of appearance and carry out glazing, glazing thickness is at 2.0-3.0mm.
Point reduction glaze contracting glaze effect prepared by above three embodiments is fine, forms the even point-like of size, has prepared the point reduction glaze ceramic having artistic value, and had anti-skidding effect.
Above-described specific embodiment; technical problem, technical scheme and beneficial effect that the present invention solves are further described; be understood that; the foregoing is only specific embodiments of the invention; be not limited to the present invention; within the spirit and principles in the present invention all, any amendment made, equivalent replacement, improvement etc., all should be included within protection scope of the present invention.

Claims (8)

1. a point reduction glaze, it is characterized in that its component and each component mass parts as follows:
Base glaze: 100 parts; Meteorological silicon: 15 parts-25 parts.
2. point reduction glaze according to claim 1, is characterized in that: component and each component mass parts of described base glaze are as follows: potassium felspar sand: 40 parts-45 parts; Quartz: 15 parts-20 parts; Calcite: 8 parts-10 parts; Strontium carbonate powder: 3 parts-5 parts; Zinc oxide: 1 part-2 parts; Barium carbonate: 3 parts-5 parts; Kaolin: 6 parts-8 parts; Talcum: 4 parts-5 parts; Zirconium silicate: 12 parts-15 parts.
3. point reduction glaze according to claim 2, is characterized in that: be also 5/10000ths to millesimal carboxymethyl cellulose containing mass percent in the base glaze of 100%.
4. point reduction glaze according to claim 2, is characterized in that: also containing mass parts to be the aluminum oxide of 2 parts and mass parts the be quartz of 1 part in described base glaze.
5. a preparation method for the point reduction glaze according to any one of Claims 1-4, is characterized in that the step of the method is as follows:
A () is got the raw materials ready according to each component and each component mass parts;
B the material got ready is poured in ball mill and is added ball-milling medium and water carries out ball milling by (); Wherein, expect: the mass ratio=1:(0.5-0.6 of water), and the volume of the ball-milling medium added is the 1/3-1/2 of ball mill volume;
C () ball milling terminates after, unload and put glaze slip, measure glaze slip fineness, glaze slip fineness controls at 325 mesh screen residues: 0.02%-0.10%; The glaze slip of furnishing 37-38 degree Beaume again, gets the bright and clean base substrate of appearance and carries out glazing, under oxidizing atmosphere, fire finished product.
6. the preparation method of point reduction glaze according to claim 5, is characterized in that: in step (b), and ball-milling medium adopts high alumina ballstone, according to greatly: in: the grating of little=1:2:1 mass ratio adds.
7. the preparation method of point reduction glaze according to claim 5: it is characterized in that: in described step (b), the condition of Ball-milling Time, rotational speed of ball-mill and loading capacity is as follows: adopt 10kg ball mill, rotational speed of ball-mill is 60-62 rev/min, Ball-milling Time was at 12 hours, and the loading capacity of ball mill is the raw material of 6kg; Adopt 500kg ball mill: rotational speed of ball-mill is 21 revs/min, Ball-milling Time 14 hours, and the loading capacity of ball mill is 300kg raw material.
8. the preparation method of point reduction glaze according to claim 5: it is characterized in that: in described step (c), get the bright and clean base substrate of appearance and carry out glazing, glazing thickness is at 2.0-3.0mm.
CN201510236232.1A 2015-05-11 2015-05-11 Shrinkage dot glaze and preparation method thereof Pending CN104909833A (en)

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Application Number Priority Date Filing Date Title
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Publication Number Publication Date
CN104909833A true CN104909833A (en) 2015-09-16

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108892537A (en) * 2018-07-27 2018-11-27 醴陵千汇实业有限公司 A kind of production method for having light glaze forming rice-shaped effect
CN109369145A (en) * 2018-12-04 2019-02-22 德化县宏顺陶瓷有限公司 Point reduction glaze ceramic and preparation method thereof
CN109384477A (en) * 2018-12-15 2019-02-26 醴陵陶润实业发展有限公司 Layer Black bottom white point reduction reacts glaze and preparation method thereof
CN109608044A (en) * 2018-12-04 2019-04-12 德化县宏顺陶瓷有限公司 Cracking glaze and preparation method thereof, be cracked the method for glaze ceramic with cracking glaze production

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101759440A (en) * 2009-12-18 2010-06-30 深圳市永丰源实业有限公司 Lead-free ceramic glaze and preparation process thereof
CN103030434A (en) * 2012-12-14 2013-04-10 潮州市荣华陶瓷制作有限公司 Novel ceramic glaze and preparation process thereof

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101759440A (en) * 2009-12-18 2010-06-30 深圳市永丰源实业有限公司 Lead-free ceramic glaze and preparation process thereof
CN103030434A (en) * 2012-12-14 2013-04-10 潮州市荣华陶瓷制作有限公司 Novel ceramic glaze and preparation process thereof

Non-Patent Citations (2)

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Title
刘钦志: "缩点釉的研究与应用", 《江苏陶瓷》 *
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108892537A (en) * 2018-07-27 2018-11-27 醴陵千汇实业有限公司 A kind of production method for having light glaze forming rice-shaped effect
CN109369145A (en) * 2018-12-04 2019-02-22 德化县宏顺陶瓷有限公司 Point reduction glaze ceramic and preparation method thereof
CN109608044A (en) * 2018-12-04 2019-04-12 德化县宏顺陶瓷有限公司 Cracking glaze and preparation method thereof, be cracked the method for glaze ceramic with cracking glaze production
CN109384477A (en) * 2018-12-15 2019-02-26 醴陵陶润实业发展有限公司 Layer Black bottom white point reduction reacts glaze and preparation method thereof

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