CN104887561A - Hydrogel eye-care mask comprising medical marine organism components - Google Patents
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Abstract
The present invention discloses a hydrogel eye-care mask comprising medical marine organism components, which comprises a backing layer, a hydrogel layer and an anti-sticky layer. The backing layer is prepared by pharmaceutical-grade non-woven fabrics. The hydrogel layer comprises the following components in mass part: 0.1-0.5 part of carbomer, 0.03-0.06 part of carboxymethyl chitosan, 0.01-0.1 part of plant essential oil, 0.01-0.03 part of peppermint oil, 0.01-0.03 part of borneol, 8-10 parts of propylene glycol, 3-5 parts of alcohol, 0.4-0.6 part of polyvinylpyrrolidone, 0.4-0.6 part of carboxymethylcellulose sodium, 0.1-0.2 part of disodium ethylene diamine tetraacetate, and 0.08-0.12 part of sodium benzoate. The anti-sticky layer is prepared by PC release paper. According to the technical scheme of the invention, the carbomer is adopted as the main gel skeleton of the hydrogel eye-care mask. Meanwhile, the carboxymethyl chitosan having the bacteriostasis effect is added, and the plant essential oil, the peppermint oil, the borneol and other components are added at the same time to prepare the hydrogel layer. Therefore, the hydrogel eye-care mask is capable of relieving the eye fatigue.
Description
Technical field
The present invention relates to field of medical accessory, specifically a kind of hydrogel eye paste of medical marine natural product.
Background technology
At present, universal along with electronic products such as computer, TV, mobile phones, the time that people's eyes are had a rest is shorter and shorter, and the symptom of the eyes discomforts such as eyes are dry and astringent, swelling that cause most people to have, even causes the consequence of vision degradation; Simultaneously working clan is often facing to display work, and the overtime work of even also staying up late had, very easily causes eye strain, at around eyes generation black eye, eye pouch and wrinkle, has a strong impact on the health of mankind's eye and attractive in appearance.Therefore, problems is solved extremely urgent.
Market there are the cosmetics such as a lot of eye sticker, eye mask, eye cream, mainly based on whitening, moisturizing, nourishing, Firm.In these products, major part is containing chemical composition, not only makes eyes can not get original maintenance effect, can stimulate eyes on the contrary.
Summary of the invention
The object of the present invention is to provide a kind of hydrogel eye paste of medical marine natural product, there is eye strain of releiving, refrigerant improving eyesight, anti-inflammation, invigorate blood circulation, antipyretic, the effect such as blood pressure lowering and slow down aging.
For achieving the above object, the invention provides following technical scheme:
A hydrogel eye paste for medical marine natural product, is made up of backing layer, hydrogel layer and adherent layer; The non-woven fabrics of pharmaceutical grade that what described backing layer adopted is; Described hydrogel layer comprises carbomer 0.1-0.5 part, carboxymethyl chitosan 0.03-0.06 part, plants essential oil 0.01-0.1 part, Oleum menthae 0.01-0.03 part, Borneolum Syntheticum 0.01-0.03 part, propylene glycol 8-10 part, ethanol 3-5 part, polyvinylpyrrolidone 0.4-0.6 part, sodium carboxymethyl cellulose 0.4-0.6 part, disodiumedetate 0.1-0.2 part and sodium benzoate 0.08-0.12 part according to the raw material of quality hundred number; What described adherent layer adopted is PC release paper.
As the further scheme of the present invention: described plants essential oil comprises Flos Rosae Rugosae quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil and Fructus Citri Limoniae quintessence oil.
As the further scheme of the present invention: the preparation method of described hydrogel layer, comprises the following steps:
(1) carbomer gel, oil phase, aqueous phase and ethanol phase is prepared first respectively:
1) carbomer gel: the carbomer appropriate amount of deionized water of getting 0.1-0.5 part is soaked swelling, is then neutralized to pH=7 and obtains carbomer gel;
2) oil phase: take propylene glycol 8-10 part, adds polyvinylpyrrolidone 0.4-0.6 part, sodium carboxymethyl cellulose 0.4-0.6 part, plants essential oil 0.01-0.1 part, disodiumedetate 0.1-0.2 part successively, stirs, obtain oil phase;
3) aqueous phase: take carboxymethyl chitosan 0.03-0.06 part, add appropriate amount of deionized water, stir, obtain aqueous phase;
4) ethanol phase: take ethanol 3-5 part, adds Oleum menthae 0.01-0.03 part, Borneolum Syntheticum 0.01-0.03 part successively, stirs, obtain ethanol phase;
(2) then successively oil phase, aqueous phase, ethanol are put in carbomer gel mutually and stir, add sodium benzoate 0.08-0.12 part, then add appropriate amount of deionized water and dissolve;
(3) finally solution is stirred and obtain hydrogel.
As the further scheme of the present invention: in described step 1), the quality of the deionized water added is 20-100 times of carbomer; In described step 3), the quality of the deionized water added is 22-60 times of carboxymethyl chitosan.
As the further scheme of the present invention: adopt poloxamer or chitin to replace carbomer.
Compared with prior art, the invention has the beneficial effects as follows:
The present invention for major gel skeleton with medical grade carbomer, adds the natural marine organism material carboxymethyl chitosan with bacteriostasis, adds plants essential oil, Oleum menthae, Borneolum Syntheticum etc. simultaneously, prepare the hydrogel layer of eye paste.
This hydrogel layer can make around eyes keep moistening and nice and cool fast and enduringly, reduces the temperature of circumference of eyes, impels circumference of eyes vasoconstriction, the sense of discomfort that improvement eye too much causes, temporarily play effect of releive eye strain and refrigerant improving eyesight; Carboxymethyl chitosan has fungistatic effect, plants essential oil add the absorption that the fragrance that not only can increase product can also promote skin; After using, not only there is no the residual of colloid substance, non-stimulated to skin, but also there is anti-inflammation, invigorate blood circulation, the effect such as antipyretic, blood pressure lowering and slow down aging.
Accompanying drawing explanation
Fig. 1 is a kind of structural representation of hydrogel eye paste of medical marine natural product;
In figure: 1-backing layer, 2-hydrogel layer, 3-adherent layer.
Detailed description of the invention
Below in conjunction with the embodiment of the present invention and accompanying drawing, be clearly and completely described the technical scheme in the embodiment of the present invention, obviously, described embodiment is only the present invention's part embodiment, instead of whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art, not making the every other embodiment obtained under creative work prerequisite, belong to the scope of protection of the invention.
Refer to Fig. 1, in the embodiment of the present invention, a kind of hydrogel eye paste of medical marine natural product, is made up of backing layer 1, hydrogel layer 2 and adherent layer 3.
Backing layer 1 is a kind of non-woven fabrics of pharmaceutical grade, permeable watertight, increases breathability and the slip-off preventing of product.Non-woven fabrics is the environment-friendly materials of a new generation, has protection against the tide, ventilative, pliable and tough, light weight, not combustion-supporting, easy decomposition, nontoxic non-stimulated, the capable of circulation feature such as to use again.
Hydrogel layer 2 is the main part of eye paste, and hydrogel layer 2 comprises carbomer 0.1-0.5 part, carboxymethyl chitosan 0.03-0.06 part, plants essential oil 0.01-0.1 part, Oleum menthae 0.01-0.03 part, Borneolum Syntheticum 0.01-0.03 part, propylene glycol 8-10 part, ethanol 3-5 part, polyvinylpyrrolidone 0.4-0.6 part, sodium carboxymethyl cellulose 0.4-0.6 part, disodiumedetate 0.1-0.2 part and sodium benzoate 0.08-0.12 part according to the raw material of quality hundred number.Hydrogel layer 2 can form moist environment in circumference of eyes, reduces eye temperature, alleviates eye strain, but also there is anti-inflammation, invigorate blood circulation, the effect such as antipyretic, blood pressure lowering and slow down aging.
The preparation method of described hydrogel layer 2, comprises the following steps:
(1) carbomer gel, oil phase, aqueous phase and ethanol phase is prepared first respectively:
1) carbomer gel: the carbomer appropriate amount of deionized water of getting 0.1-0.5 part is soaked swelling, is then neutralized to pH=7 and obtains carbomer gel;
2) oil phase: take propylene glycol 8-10 part, adds polyvinylpyrrolidone 0.4-0.6 part, sodium carboxymethyl cellulose 0.4-0.6 part, plants essential oil 0.01-0.1 part, disodiumedetate 0.1-0.2 part successively, stirs, obtain oil phase;
3) aqueous phase: take carboxymethyl chitosan 0.03-0.06 part, adds the 22-60 deionized water doubly of carboxymethyl chitosan quality, stirs, obtain aqueous phase;
4) ethanol phase: take ethanol 3-5 part, adds Oleum menthae 0.01-0.03 part, Borneolum Syntheticum 0.01-0.03 part successively, stirs, obtain ethanol phase;
(2) then successively oil phase, aqueous phase, ethanol are put in carbomer gel mutually and stir, add sodium benzoate 0.08-0.12 part, then add suitable quantity of water and dissolve;
(3) finally solution is stirred and obtain hydrogel.
The major gel skeleton of hydrogel layer 2 is carbomer hydrogel, also can be poloxamer hydrogel or chitin hydrogel.
Carboxymethyl chitosan is a kind of important derivatives of chitin, it is the macromolecular substances obtained through modification by the natural marine organism macromole chitin extracted from the shell such as shrimp, Eriocheir sinensis, it dissolves in the water of neutrality, and character is more stable, there is antibacterial anti-infection, blood fat reducing, prevent arteriosclerosis and antiviral effect.
Plants essential oil is the aromatic substance extracted by modes such as distillation, squeezings from the flower, leaf, root, fruit etc. of plant, its molecular weight is little, be easy to be absorbed by the body, the fragrance of plant itself, also directly Stimulation of The Brain pendant, ferment and hormonal secretion, function in balanced body, plays the effect of beauty and skin care.Plants essential oil comprises Flos Rosae Rugosae quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil and Fructus Citri Limoniae quintessence oil: Flos Rosae Rugosae quintessence oil has bactericidal antiphlogistic, promotes the effect of cell metabolism and cell regeneration, nourishes rough skin, slow down aging, Herba Lysimachiae foenum-graeci quintessence oil has the function solving congested and swelling, have calmness, sterilization, bactericidal action, Fructus Citri Limoniae quintessence oil has promoting the circulation of blood, antipyretic, blood pressure lowering, refrigerant effect.
Medical grade carbomer is cross-linked with acrylic acid the acrylic acid crosslinked resin obtained with tetramethylolmethane etc., and the carbomer after neutralization is good gel-type vehicle, has the important use such as thickening suspension, and technique is simple, and good stability.
Propylene glycol colorless and odorless, as wetting agent and penetrating agent in this gel.
Oleum menthae, Borneolum Syntheticum are all the extracts of refrigerant plant, have the effect of antibacterial, antiinflammatory, fast cooling, refreshment.
Adherent layer 3 is PC release paper protective clear layers, is attached to one deck polyester protecting film of patch surface, throws off, for antiseized, moisturizing before using.PC release paper all has barrier performance to water and air, can suppress chemical reaction, can extend the storage period of adhesive.Its tearability, wearability are better, harmless.
Embodiment 1
In the embodiment of the present invention, a kind of hydrogel eye paste of medical marine natural product, is made up of backing layer 1, hydrogel layer 2 and adherent layer 3.Backing layer 1 is a kind of non-woven fabrics of pharmaceutical grade; Adherent layer 3 is PC release paper; Hydrogel layer 2 is the main part of eye paste, comprises carbomer 0.1 part, carboxymethyl chitosan 0.05 part, plants essential oil 0.1 part, Oleum menthae 0.01 part, Borneolum Syntheticum 0.02 part, propylene glycol 10 parts, ethanol 3 parts, polyvinylpyrrolidone 0.5 part, sodium carboxymethyl cellulose 0.6 part, disodiumedetate 0.1 part and sodium benzoate 0.1 part according to the raw material of quality hundred number.
The preparation method of described hydrogel layer 2, comprises the following steps:
(1) carbomer gel, oil phase, aqueous phase and ethanol phase is prepared first respectively:
1) carbomer gel: the deionized water getting 20 times of the carbomer carbomer quality of 0.1 part soaks swelling, is then neutralized to pH=7 and obtains carbomer gel;
2) oil phase: take propylene glycol 10 parts, adds polyvinylpyrrolidone 0.5 part, sodium carboxymethyl cellulose 0.6 part, plants essential oil 0.1 part, disodiumedetate 0.1 part successively, stirs, obtain oil phase;
3) aqueous phase: take carboxymethyl chitosan 0.05 part, adds the deionized water of 22 times of carboxymethyl chitosan quality, stirs, obtain aqueous phase;
4) ethanol phase: take ethanol 3 parts, adds Oleum menthae 0.01 part, Borneolum Syntheticum 0.02 part successively, stirs, obtain ethanol phase;
(2) then successively oil phase, aqueous phase, ethanol are put in carbomer gel mutually and stir, add sodium benzoate 0.1 part, then add suitable quantity of water and dissolve;
(3) finally solution is stirred and obtain hydrogel.
Embodiment 2
In the embodiment of the present invention, a kind of hydrogel eye paste of medical marine natural product, is made up of backing layer 1, hydrogel layer 2 and adherent layer 3.Backing layer 1 is a kind of non-woven fabrics of pharmaceutical grade; Adherent layer 3 is PC release paper; Hydrogel layer 2 is the main part of eye paste, comprises poloxamer 0.3 part, carboxymethyl chitosan 0.06 part, plants essential oil 0.01 part, Oleum menthae 0.02 part, Borneolum Syntheticum 0.03 part, propylene glycol 8 parts, ethanol 4 parts, polyvinylpyrrolidone 0.6 part, sodium carboxymethyl cellulose 0.4 part, disodiumedetate 0.15 part and sodium benzoate 0.12 part according to the raw material of quality hundred number.
The preparation method of described hydrogel layer 2, comprises the following steps:
(1) poloxamer gel, oil phase, aqueous phase and ethanol phase is prepared first respectively:
1) poloxamer gel: the deionized water getting 50 times of the poloxamer poloxamer quality of 0.3 part soaks swelling, is then neutralized to pH=7 and obtains poloxamer gel;
2) oil phase: take propylene glycol 8 parts, adds polyvinylpyrrolidone-0.6 part, sodium carboxymethyl cellulose 0.4 part, plants essential oil 0.01 part, disodiumedetate 0.15 part successively, stirs, obtain oil phase;
3) aqueous phase: take carboxymethyl chitosan 0.06 part, adds the deionized water of 60 times of carboxymethyl chitosan quality, stirs, obtain aqueous phase;
4) ethanol phase: take ethanol 4 parts, adds Oleum menthae 0.02 part, Borneolum Syntheticum 0.03 part successively, stirs, obtain ethanol phase;
(2) then successively oil phase, aqueous phase, ethanol are put in poloxamer gel mutually and stir, add sodium benzoate 0.12 part, then add suitable quantity of water and dissolve;
(3) finally solution is stirred and obtain hydrogel.
Embodiment 3
In the embodiment of the present invention, a kind of hydrogel eye paste of medical marine natural product, is made up of backing layer 1, hydrogel layer 2 and adherent layer 3.Backing layer 1 is a kind of non-woven fabrics of pharmaceutical grade; Adherent layer 3 is PC release paper; Hydrogel layer 2 is the main part of eye paste, comprises chitin 0.5 part, carboxymethyl chitosan 0.03 part, plants essential oil 0.05 part, Oleum menthae 0.03 part, Borneolum Syntheticum 0.01 part, propylene glycol 9 parts, ethanol 5 parts, polyvinylpyrrolidone 0.4 part, sodium carboxymethyl cellulose 0.5 part, disodiumedetate 0.2 part and sodium benzoate 0.08 part according to the raw material of quality hundred number.
The preparation method of described hydrogel layer 2, comprises the following steps:
(1) chitin hydrogel, oil phase, aqueous phase and ethanol phase is prepared first respectively:
1) chitin hydrogel: the deionized water getting 100 times of the chitin chitin quality of 0.5 part soaks swelling, is then neutralized to pH=7 and obtains chitin hydrogel;
2) oil phase: take propylene glycol 9 parts, adds polyvinylpyrrolidone 0.4 part, sodium carboxymethyl cellulose 0.5 part, plants essential oil 0.05 part, disodiumedetate 0.2 part successively, stirs, obtain oil phase;
3) aqueous phase: take carboxymethyl chitosan 0.03 part, adds the deionized water of 40 times of carboxymethyl chitosan quality, stirs, obtain aqueous phase;
4) ethanol phase: take ethanol 5 parts, adds Oleum menthae 0.03 part, Borneolum Syntheticum 0.01 part successively, stirs, obtain ethanol phase;
(2) then successively oil phase, aqueous phase, ethanol are put in chitin hydrogel mutually and stir, add sodium benzoate 0.08 part, then add suitable quantity of water and dissolve;
(3) finally solution is stirred and obtain hydrogel.
To those skilled in the art, obviously the invention is not restricted to the details of above-mentioned one exemplary embodiment, and when not deviating from spirit of the present invention or basic feature, the present invention can be realized in other specific forms.Therefore, no matter from which point, all should embodiment be regarded as exemplary, and be nonrestrictive, scope of the present invention is limited by claims instead of above-mentioned explanation, and all changes be therefore intended in the implication of the equivalency by dropping on claim and scope are included in the present invention.
In addition, be to be understood that, although this description is described according to embodiment, but not each embodiment only comprises an independently technical scheme, this narrating mode of description is only for clarity sake, those skilled in the art should by description integrally, and the technical scheme in each embodiment also through appropriately combined, can form other embodiments that it will be appreciated by those skilled in the art that.
Claims (5)
1. a hydrogel eye paste for medical marine natural product, is characterized in that, is made up of backing layer (1), hydrogel layer (2) and adherent layer (3); The non-woven fabrics of pharmaceutical grade that what described backing layer (1) adopted is; Described hydrogel layer (2) comprises carbomer 0.1-0.5 part, carboxymethyl chitosan 0.03-0.06 part, plants essential oil 0.01-0.1 part, Oleum menthae 0.01-0.03 part, Borneolum Syntheticum 0.01-0.03 part, propylene glycol 8-10 part, ethanol 3-5 part, polyvinylpyrrolidone 0.4-0.6 part, sodium carboxymethyl cellulose 0.4-0.6 part, disodiumedetate 0.1-0.2 part and sodium benzoate 0.08-0.12 part according to the raw material of quality hundred number; What described adherent layer (3) adopted is PC release paper.
2. the hydrogel eye paste of medical marine natural product according to claim 1, is characterized in that, described plants essential oil comprises Flos Rosae Rugosae quintessence oil, Herba Lysimachiae foenum-graeci quintessence oil and Fructus Citri Limoniae quintessence oil.
3. the hydrogel eye paste of medical marine natural product according to claim 1, is characterized in that, the preparation method of described hydrogel layer (2), comprises the following steps:
(1) carbomer gel, oil phase, aqueous phase and ethanol phase is prepared first respectively:
1) carbomer gel: the carbomer appropriate amount of deionized water of getting 0.1-0.5 part is soaked swelling, is then neutralized to pH=7 and obtains carbomer gel;
2) oil phase: take propylene glycol 8-10 part, adds polyvinylpyrrolidone 0.4-0.6 part, sodium carboxymethyl cellulose 0.4-0.6 part, plants essential oil 0.01-0.1 part, disodiumedetate 0.1-0.2 part successively, stirs, obtain oil phase;
3) aqueous phase: take carboxymethyl chitosan 0.03-0.06 part, add appropriate amount of deionized water, stir, obtain aqueous phase;
4) ethanol phase: take ethanol 3-5 part, adds Oleum menthae 0.01-0.03 part, Borneolum Syntheticum 0.01-0.03 part successively, stirs, obtain ethanol phase;
(2) then successively oil phase, aqueous phase, ethanol are put in carbomer gel mutually and stir, add sodium benzoate 0.08-0.12 part, then add appropriate amount of deionized water and dissolve;
(3) finally solution is stirred and obtain hydrogel.
4. the hydrogel eye paste of medical marine natural product according to claim 3, is characterized in that, in described step 1), the quality of the deionized water added is 20-100 times of carbomer; In described step 3), the quality of the deionized water added is 22-60 times of carboxymethyl chitosan.
5. according to the hydrogel eye paste of the arbitrary described medical marine natural product of claim 1-4, it is characterized in that, adopt poloxamer or chitin to replace carbomer.
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| CN108125829A (en) * | 2017-12-27 | 2018-06-08 | 广州市澳键丰泽生物科技股份有限公司 | A kind of preparation containing plants essential oil and its preparation method and application |
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| CN112168717A (en) * | 2020-10-06 | 2021-01-05 | 青岛姿之妍化妆品科技有限责任公司 | Hydrogel-based sustained-release mask and preparation method and use method thereof |
| CN112168717B (en) * | 2020-10-06 | 2023-12-01 | 广东碧素堂生物科技有限公司 | Hydrogel-based slow-release mask and preparation method and application method thereof |
| CN112089763A (en) * | 2020-10-12 | 2020-12-18 | 滕智勇 | Medical mint gel eye protection patch and preparation method thereof |
| CN114504425A (en) * | 2020-11-16 | 2022-05-17 | 湖北舒邦药业有限公司 | Cold compress patch preparation method, cold compress patch and application method thereof |
| CN113499323A (en) * | 2021-06-17 | 2021-10-15 | 西安申兰生物医学工程有限公司 | Chitin sugar film eye mask manufacturing process |
| CN113402991A (en) * | 2021-06-24 | 2021-09-17 | 山东优杰生物科技有限公司 | Medical hydrogel coiled material and preparation method thereof |
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Application publication date: 20150909 |