CN102389380B - Konjac glucomannan eye mask and preparation method thereof - Google Patents

Konjac glucomannan eye mask and preparation method thereof Download PDF

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CN102389380B
CN102389380B CN 201110263877 CN201110263877A CN102389380B CN 102389380 B CN102389380 B CN 102389380B CN 201110263877 CN201110263877 CN 201110263877 CN 201110263877 A CN201110263877 A CN 201110263877A CN 102389380 B CN102389380 B CN 102389380B
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film
preparation
rhizoma amorphophalli
amorphophalli glucomannan
konjac glucomannan
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CN102389380A (en
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庞杰
潘廷跳
李沙
陈丽萍
张俊明
潘振华
王博华
姚闽娜
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Fujian Agriculture and Forestry University
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Abstract

本发明涉及一种魔芋葡甘聚糖眼贴膜的制备方法,包括制备魔芋葡甘聚糖混合液、制备膜液和制膜。本发明的主要原料中,魔芋葡甘聚糖具有优良的生物活性和流变性能,能防止皮肤失水和缓解衰老;大豆分离蛋白含有多种人体必需氨基酸、微量元素和很高的营养价值及保健功效。橄榄油富含与皮肤亲和力极佳的角鲨烯和人体必需脂肪酸,吸收迅速,有效保持皮肤弹性和润泽;蜂蜡是一种纯天然的滋润剂,能够在肌肤表面形成保护膜;胶原蛋白由19种氨基酸组成,具有保湿、滋养、紧肤、防皱等功效;甘油起到提高保湿的效果;单甘脂起到乳化的作用。本发明的魔芋葡甘聚糖眼贴膜具有保水、防皱及天然无副作用等优点。The invention relates to a preparation method of konjac glucomannan eye patch, which comprises preparation of konjac glucomannan mixed liquid, preparation of film liquid and film formation. Among the main raw materials of the present invention, konjac glucomannan has excellent biological activity and rheological properties, can prevent skin dehydration and alleviate aging; soybean protein isolate contains various essential amino acids, trace elements and high nutritional value and health benefits. Olive oil is rich in skin-friendly squalene and essential fatty acids, which can be absorbed quickly and effectively maintain skin elasticity and moisture; beeswax is a natural moisturizer that can form a protective film on the skin surface; collagen is composed of 19 Composed of amino acids, it has the functions of moisturizing, nourishing, firming and anti-wrinkle; glycerin can improve the moisturizing effect; monoglyceride can emulsify. The konjac glucomannan eye patch of the invention has the advantages of water retention, anti-wrinkle, natural and no side effects, and the like.

Description

一种魔芋葡甘聚糖眼贴膜及其制备方法A kind of konjac glucomannan eye patch and preparation method thereof

技术领域 technical field

本发明涉及一种化妆品及其制备方法,具体涉及一种魔芋葡甘聚糖眼贴膜及其制备方法。 The invention relates to a cosmetic and a preparation method thereof, in particular to a konjac glucomannan eye patch and a preparation method thereof.

背景技术 Background technique

随着网络时代的到来,一些上班族必须长时间面对电脑,使得眼睛承受了前所未有的重负,会产生双眼干涩,酸胀等眼疲劳现象;另外由于很多上班族经常加班熬夜,还出现了黑眼圈、眼袋等眼部问题。这些眼部问题不仅在一定程度上影响到眼部的美观,而且长期下去还会导致干眼症、暴露性结膜炎等眼部疾病。眼贴膜由于能有效起到抗氧化及抗衰老作用,从而有效地缓解眼部问题,逐渐成为人们关注的焦点。目前市场上已存在多种眼贴膜产品,但是这些产品中多数是通过添加一些化学物质来增强某种特殊的功效,而这些化学物质很可能引发接触性皮炎、过敏反应等更为严重的眼部问题,另外某些产品的保湿持久性也很差,不能有效解决皮肤失水的问题。因此,在绿色环保理念和人们对化妆品有着更高要求的前提下,寻求一种安全、稳定、性能优良,且无毒副作用的纯天然原料来取代这些化学物质有着重要的意义,而魔芋葡甘聚糖正是我们所寻求的这种原料。 With the advent of the Internet age, some office workers have to face the computer for a long time, which makes the eyes bear an unprecedented burden, which will cause dry eyes, soreness and other eye fatigue phenomena; Eye problems such as eye circles and bags under the eyes. These eye problems not only affect the beauty of the eyes to a certain extent, but also lead to eye diseases such as dry eye syndrome and exposure conjunctivitis in the long run. Eye patch has gradually become the focus of people's attention because it can effectively play an anti-oxidation and anti-aging effect, thereby effectively alleviating eye problems. There are a variety of eye patch products on the market, but most of these products enhance a special effect by adding some chemical substances, and these chemical substances are likely to cause more serious eye diseases such as contact dermatitis and allergic reactions. In addition, some products have poor moisturizing durability and cannot effectively solve the problem of skin dehydration. Therefore, under the premise of the concept of green environmental protection and people's higher requirements for cosmetics, it is of great significance to seek a pure natural raw material that is safe, stable, excellent in performance, and non-toxic and side effects to replace these chemical substances, and konjac glucan Glycans were exactly the raw material we were looking for.

由于魔芋葡甘聚糖具有抗菌性、吸水性、抗氧化性和成膜性等优良的生物活性和流变性能,能够防止皮肤失水,缓解衰老问题,已成为化妆品的主要的天然原料之一。目前已成功开发出魔芋系列润肤霜和防晒霜等多种产品,而本发明就是将魔芋葡甘聚糖用于眼贴膜的制备中,将魔芋葡甘聚糖的优良特性用于对眼部的护理。 Because konjac glucomannan has excellent biological activity and rheological properties such as antibacterial, water absorption, anti-oxidation and film-forming properties, it can prevent skin dehydration and alleviate aging problems, and has become one of the main natural raw materials for cosmetics . Konjac glucomannan and other products have been successfully developed at present, and the present invention is to use konjac glucomannan in the preparation of eye patches, and use the excellent properties of konjac glucomannan to protect the eyes. care.

申请号为200780013857.5的发明专利“眼贴膜”(申请日:2007/06/01),介绍了一种眼贴膜。该产品能减少由于新陈代谢减慢而引起的眼部周围皮肤松弛和细纹,从而保持皮肤健康;且能同时按摩双目周围并缩短所需时间,以满足用户的需要。但该产品是通过添加某些化学物质来实现这些功能的,没有添加某些保湿性较好的物质来解决皮肤容易失水的问题。因此,没有真正解决皮肤过敏、皮炎等问题,也不能解决皮肤失水的问题。 The invention patent "eye film" with application number 200780013857.5 (application date: 2007/06/01) introduces an eye film. The product can reduce the sagging and fine lines around the eyes caused by the slowing down of metabolism, so as to keep the skin healthy; and it can massage around the eyes at the same time and shorten the required time to meet the needs of users. However, this product realizes these functions by adding certain chemical substances, and does not add some substances with better moisturizing properties to solve the problem that the skin is prone to dehydration. Therefore, problems such as skin allergies and dermatitis are not really solved, and the problem of skin dehydration cannot be solved.

申请号为200910039541.4的发明专利“抗皱弹力眼贴膜”(申请日:2009/05/18),介绍了一种抗皱弹力眼贴膜。其美容物质包括卡波树脂、江醇胺、羚2基纤维素、透明质酸钠、尿囊素、金缕梅蒸馏液、尼泊金酯、Vb3、甘油、植物提取液及纯净水,其植物提取液包括EYELISS多肽成分、PHYTOLIGHT复合萃取物及CULCKLIFT黄原胶聚合物,并加入纳米金铂片,能起到抗氧化及衰老作用,且无毒副作用。它能有效地降低化学物质引起的皮肤疾病,但是这种眼贴膜对滋润和持久性的要求不高,因此还是不能解决皮肤失水的问题。 The invention patent "anti-wrinkle elastic eye patch" (application date: 2009/05/18) with application number 200910039541.4 introduces an anti-wrinkle elastic eye patch. Its cosmetic substances include carboresin, glycosolamine, anteline 2-based cellulose, sodium hyaluronate, allantoin, witch hazel distillate, paraben, Vb3, glycerin, plant extracts and purified water. The plant extracts include EYELISS polypeptide components, PHYTOLIGHT complex extracts and CULCKLIFT xanthan gum polymers, and add nano-gold and platinum flakes, which can have anti-oxidation and aging effects without toxic side effects. It can effectively reduce skin diseases caused by chemicals, but this kind of eye patch does not have high requirements for moisturizing and persistence, so it still cannot solve the problem of skin dehydration.

发明内容 Contents of the invention

鉴于现有技术的不足,本发明的目的在于提供一种配方合理,使用方便且能被皮肤快速吸收并能长时间保水,对眼部皮肤无毒副作用的魔芋葡甘聚糖眼贴膜及其制备方法。     In view of the deficiencies in the prior art, the purpose of the present invention is to provide a konjac glucomannan eye patch with reasonable formula, easy to use, fast absorption by the skin and long-term water retention, no toxic and side effects on the eye skin and its preparation method. 

为了实现上述目的,本发明的技术方案是:一种魔芋葡甘聚糖眼贴膜的制备方法,其特征在于操作步骤如下: In order to achieve the above object, the technical scheme of the present invention is: a kind of preparation method of konjac glucomannan eye patch, it is characterized in that operating steps are as follows:

(1)制备魔芋葡甘聚糖混合液:将0.01~1g的魔芋葡甘聚糖和0.01~1g的大豆分离蛋白分别加入到2只装有5~50ml橄榄油的100ml烧杯中,将其置于85~95℃的水浴锅中隔水加热20~40min,采用边倒边搅拌的方法合并2只烧杯中的溶液至成为稠状;并将3~30g熔化的蜂蜡倒入稠状液中,搅拌均匀,制成魔芋葡甘聚糖混合液,备用; (1) Preparation of konjac glucomannan mixture: Add 0.01-1g of konjac glucomannan and 0.01-1g of soybean protein isolate into two 100ml beakers filled with 5-50ml of olive oil respectively, and place them in Heat in a water bath at 85-95°C for 20-40 minutes, combine the solutions in 2 beakers with stirring while pouring until it becomes thick; pour 3-30g of melted beeswax into the thick liquid, Stir well to make konjac glucomannan mixture, set aside;

(2)制备膜液:将步骤(1)的魔芋葡甘聚糖混合液冷却至45℃后,分别加入0.1~0.5g的胶原蛋白、1~5ml的甘油以及0.01~1g的单甘脂,混匀,并用1mol/L的碳酸氢钠溶液将混合液的pH调至7~8,搅拌均匀后静置6~18h,制成膜液,备用; (2) Preparation of membrane solution: After cooling the konjac glucomannan mixture in step (1) to 45°C, add 0.1-0.5g of collagen, 1-5ml of glycerin and 0.01-1g of monoglyceride, Mix well, and use 1mol/L sodium bicarbonate solution to adjust the pH of the mixed solution to 7-8, stir evenly and let it stand for 6-18 hours to make a membrane solution for later use;

(3)制膜:取步骤(2)的膜液3~5ml倒入制膜的模具中,将模具中的膜液连同模具置于干燥箱内,58~60℃的条件下干燥2~4h,取出,冷却至室温,揭膜。 (3) Membrane production: Take 3-5ml of the membrane liquid from step (2) and pour it into the mold for film-making, put the membrane liquid in the mold together with the mold in a drying oven, and dry at 58-60°C for 2-4 hours , take it out, cool to room temperature, and remove the film.

所述的橄榄油和甘油为液体;魔芋葡甘聚糖、大豆分离蛋白、胶原蛋白为粉末;蜂蜡和单甘脂为固体。 The olive oil and glycerin are liquid; the konjac glucomannan, soybean protein isolate and collagen are powder; the beeswax and monoglyceride are solid.

本发明具有以下优点:本发明的一种魔芋葡甘聚糖眼贴膜的制备方法简单,其中魔芋葡甘聚糖具有优良的生物活性和流变性能,如抗菌性、吸水性、粘结性、抗氧化性和成膜性等,对皮肤有很好的保护作用,能防止皮肤失水,且能缓解衰老问题;大豆分离蛋白含有人体多种必需氨基酸和微量元素,具有很高的营养价值及保健功效,沿着它的肽链骨架,含有很多极性基团。因此,具有较好的吸水性、凝胶性、保水性和膨胀性,起到乳化、润湿和渗透的作用;橄榄油富含与皮肤亲和力极佳的角鲨烯和人体必需脂肪酸,吸收迅速,有效保持皮肤弹性和润泽;蜂蜡具有天然的抗菌特性,且是一种纯天然的滋润剂,能够在肌肤表面形成保护膜;胶原蛋白作为一类十分有效的化妆品原料,它由19种氨基酸组成的天然蛋白质,与人皮肤胶原的结构相似,具有低抗原性、良好的生物相容性,具有保湿、滋养、紧肤、防皱等功效;甘油起到提高保湿的效果;单甘脂起到乳化的作用,使大分子物质充分混合,相互之间结合更加紧密有利于成膜。用本发明的制备方法制备出的魔芋葡甘聚糖眼贴膜具有保水、防皱及天然无副作用等优点。    The present invention has the following advantages: the preparation method of a kind of konjac glucomannan eye patch of the present invention is simple, wherein konjac glucomannan has excellent biological activity and rheological properties, such as antibacterial properties, water absorption, cohesiveness, Anti-oxidation and film-forming properties, etc., have a good protective effect on the skin, prevent skin dehydration, and relieve aging problems; soybean protein isolate contains a variety of essential amino acids and trace elements for the human body, and has high nutritional value and Health benefits, along its peptide chain backbone, contains many polar groups. Therefore, it has good water absorption, gelation, water retention and swelling properties, and plays the role of emulsification, moisturizing and penetration; olive oil is rich in squalene and essential fatty acids with excellent skin affinity, and absorbs quickly , effectively maintain skin elasticity and moisture; beeswax has natural antibacterial properties, and is a natural moisturizer that can form a protective film on the skin surface; collagen, as a very effective cosmetic raw material, is composed of 19 amino acids The natural protein is similar to the structure of human skin collagen, has low antigenicity, good biocompatibility, and has moisturizing, nourishing, firming, anti-wrinkle and other effects; glycerin can improve moisturizing effect; monoglyceride can The effect of emulsification is to fully mix the macromolecular substances, and to combine them more tightly, which is conducive to film formation. The konjac glucomannan eye patch prepared by the preparation method of the invention has the advantages of water retention, anti-wrinkle, natural and no side effects, and the like. the

具体实施方式 Detailed ways

下面结合实施例对本发明做进一步的阐述。 Below in conjunction with embodiment the present invention is further elaborated.

实施例一:一种魔芋葡甘聚糖眼贴膜的制备方法 Embodiment 1: A kind of preparation method of konjac glucomannan eye patch

一种魔芋葡甘聚糖眼贴膜的制备方法,包括以下步骤: A preparation method of konjac glucomannan eye patch, comprising the following steps:

(1)制备魔芋葡甘聚糖混合液:将0.1g的魔芋葡甘聚糖和0.1g的大豆分离蛋白分别加入到2只装有20ml橄榄油的100ml烧杯中,置于90℃的水浴锅中隔水加热30min,采用边倒边搅拌的方法合并2只烧杯中的溶液至成为稠状;并将10g熔化的蜂蜡倒入稠状液中,搅拌均匀,制成魔芋葡甘聚糖混合液,备用; (1) Preparation of konjac glucomannan mixture: Add 0.1g of konjac glucomannan and 0.1g of soybean protein isolate to two 100ml beakers filled with 20ml of olive oil respectively, and place in a water bath at 90°C Heating with water for 30 minutes, using the method of pouring and stirring to combine the solutions in 2 beakers until it becomes thick; pour 10g of melted beeswax into the thick liquid, stir evenly, and make konjac glucomannan mixture ,spare;

(2)制备膜液:将步骤(1)的魔芋葡甘聚糖混合液冷却至45℃后,分别加入0.3g的胶原蛋白、2.5ml的甘油以及0.1g的单甘脂,充分混匀,并用1mol/L的碳酸氢钠溶液将混合液pH调至8,充分搅拌后静置12h,制成膜液,备用; (2) Preparation of membrane solution: After cooling the konjac glucomannan mixture in step (1) to 45°C, add 0.3g of collagen, 2.5ml of glycerin and 0.1g of monoglyceride, and mix well. And use 1mol/L sodium bicarbonate solution to adjust the pH of the mixed solution to 8, stir it well and let it stand for 12 hours to make a membrane solution for later use;

(3)制膜:取步骤(2)膜液4ml倒入制膜的模具中,将模具中的膜液连同模具置于干燥箱内,在60℃的条件下干燥3h,取出,冷却至室温,揭膜。 (3) Film making: Take 4ml of the film liquid from step (2) and pour it into the film-making mold, put the film liquid in the mold together with the mold in a drying oven, dry at 60°C for 3 hours, take it out, and cool to room temperature , peel off the film.

本发明的魔芋葡甘聚糖眼贴膜使用前,先用水将面部洗净,然后直接将眼贴膜敷于眼睛下睑部位即可。 Before using the konjac glucomannan eye patch of the present invention, the face is washed with water, and then the eye patch is directly applied to the lower eyelid of the eyes.

以上所述仅为本发明的较佳实施例,凡依本发明申请专利范围所做的均等变化与修饰,皆应属本发明的涵盖范围。  The above descriptions are only preferred embodiments of the present invention, and all equivalent changes and modifications made according to the scope of the patent application of the present invention shall fall within the scope of the present invention. the

Claims (3)

1. the method for preparing of a Rhizoma amorphophalli glucomannan eye patch is characterized in that operating procedure is following:
(1) preparation Rhizoma amorphophalli glucomannan mixed liquor: the soybean protein isolate of the Rhizoma amorphophalli glucomannan of 0.01~1g and 0.01~1g is joined respectively in 2 100ml beakers that 5~50ml olive oil is housed; Be placed on water proof heating 20~40min in 85~95 ℃ the water-bath, adopt limit bevelling stirring method to merge solution in 2 beakers to becoming thick shape; And the Cera Flava of 3~30g fusing poured in the thick shape liquid, stir, process the Rhizoma amorphophalli glucomannan mixed liquor, subsequent use;
(2) preparation film liquid: after the Rhizoma amorphophalli glucomannan mixed liquor of step (1) is cooled to 45 ℃; Add the collagen protein of 0.1~0.5g, the glycerol of 1~5ml and the monoglyceride of 0.01~1g respectively; Mixing, and the pH of mixed liquor is transferred to 7~8 with the sodium bicarbonate solution of 1mol/L, leave standstill 6~18h after stirring; Process film liquid, subsequent use;
(3) system film: the film liquid 3~5ml that gets step (2) pours in the mould of system film, and the film liquid in the mould is placed in the drying baker together with mould, and dry 2~4h takes out under 58~60 ℃ the condition, is cooled to room temperature, takes off film.
2. the method for preparing of a kind of Rhizoma amorphophalli glucomannan eye patch according to claim 1 is characterized in that operating procedure is following:
(1) preparation Rhizoma amorphophalli glucomannan mixed liquor: the soybean protein isolate of the Rhizoma amorphophalli glucomannan of 0.1g and 0.1g is joined respectively in 2 100ml beakers that the 20ml olive oil is housed; Place 90 ℃ water-bath water proof heating 30min, the solution in 2 beakers of employing limit bevelling stirring method merging is to becoming thick shape; And the Cera Flava of 10g fusing poured in the thick shape liquid, stir, process the Rhizoma amorphophalli glucomannan mixed liquor, subsequent use;
(2) preparation film liquid: after the Rhizoma amorphophalli glucomannan mixed liquor of step (1) is cooled to 45 ℃; Add the collagen protein of 0.3g, the glycerol of 2.5ml and the monoglyceride of 0.1g respectively; Abundant mixing, and pH of mixed is transferred to 8 with the sodium bicarbonate solution of 1mol/L, fully leave standstill 12h after the stirring; Process film liquid, subsequent use;
(3) system film: get step (2) film liquid 4ml and pour in the mould of making film, the film liquid in the mould is placed in the drying baker together with mould, dry 3h under 60 ℃ condition takes out, and is cooled to room temperature, takes off film.
3. by the Rhizoma amorphophalli glucomannan eye patch of the method for claim 1 or 2 preparation.
CN 201110263877 2011-09-07 2011-09-07 Konjac glucomannan eye mask and preparation method thereof Expired - Fee Related CN102389380B (en)

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