CN104886754B - A kind of preparation method of the reconstituted tobacoo containing vetiver and application thereof - Google Patents
A kind of preparation method of the reconstituted tobacoo containing vetiver and application thereof Download PDFInfo
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- CN104886754B CN104886754B CN201510187831.9A CN201510187831A CN104886754B CN 104886754 B CN104886754 B CN 104886754B CN 201510187831 A CN201510187831 A CN 201510187831A CN 104886754 B CN104886754 B CN 104886754B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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Abstract
The invention discloses a kind of preparation method and application thereof of the reconstituted tobacoo containing vetiver, this preparation method adopts cus-cus grass blade stalk as primary raw material, concentrate, vetiver slurry, offal concentrate, offal concentrate and tobacco slurry is extracted, the final obtained reconstituted tobacoo containing vetiver by obtaining vetiver.This preparation method's simple process, is easy to produce and production cost is lower, and prepared reconstituted tobacoo takes into account the feasibility of physical strength performance, production, promotes the suction taste of tobacco simultaneously, and health environment-friendly more.The reconstituted tobacoo containing vetiver obtained, whole reconstituted tobacoo may be used for cigar exoperidium, can also be applied in cigarette after reconstituted tobacoo chopping.
Description
Technical field
The invention belongs to the reconstituted tobacoo preparation technology in cigarette field, specifically refer to a kind of preparation method and application thereof of the reconstituted tobacoo containing vetiver.
Background technology
In order to reduce the harmful components in cigarette smoke, reducing the consumption of raw materials of tobacco business, improving the mouthfeel of cigarette product, cigarette manufacturing mainly adopts tobacco sheets by paper making method to join method in pipe tobacco as filler, in order to promote the quality of cigarette.
At present, there is certain gap with external product in domestic tobacco sheets by paper making method in product quality.In physical property, the general became uneven of domestic reconstituted tobacoo, toughness and flexibility are all poor.In thin slice interior quality, there is the shortcomings such as excitant is large, flue gas is inharmonious, the soft degree difference of flue gas in domestic reconstituted tobacoo.
Because the physical property of tobacco material fiber own is poor, be ensure industrial production, must adding portion non-tobacco fiber to improve the physical strength of thin slice entirety, non-tobacco fiber is based on softwood pulp and jute pulp.Lignin in these fibers has the cancellated natural polymers of 3 D stereo, combustion quality and tobacco do not match, and there is negative effect to the local flavor of tobacco, make that reconstituted tobacoo xylon gas increases weight, papery gas is more obvious, wooden assorted gas is more obvious with the peppery gas of thorn, excitant is higher, reduces tobacco overall quality and local flavor.
Vetiver (VetiveriazizanioidesL.), common name cus-cus is perennial sturdy herbaceous plant, and original producton location is Mediterranean to India area.Within 1958, vetiver is introduced into China, mainly in the plantation of the ground such as Guangdong, Fujian, to extract the aromatic oil of Gen Yeli.After 1980, for controlling soil erosion, vetiver in south China, East China, the ground such as southwest is widely cultivated, and is a kind of natural plants being easy to obtain.
The stem stalk of vetiver can extract violet odor type essential oil, and be the natural flavor that country allows to add, perfume additive is encoded to N102.Vetiver oil is persimmon, has the advantages that consistence is large, volatility is low, can be used as fixastive.But vetiver oil has extraction process loaded down with trivial details and the low shortcoming of yield.High 1 ~ the 2m of stem stalk of vetiver, be the main part of plant, its fiber can make paper making raw material.
But be applied in reconstituted tobacoo using the stem stalk fiber of vetiver as natural solid plant perfume at present, the technology taking into account physical strength performance with the sucking quality improving the latter not yet occurs simultaneously.
Summary of the invention
An object of the present invention is to provide a kind of preparation method of the reconstituted tobacoo containing vetiver, this preparation method's simple process, is easy to produce and production cost is lower, and prepared reconstituted tobacoo takes into account the feasibility of physical strength performance, production, promote the suction taste of tobacco simultaneously, and health environment-friendly more.
This purpose of the present invention realizes by following technical solution: a kind of preparation method of the reconstituted tobacoo containing vetiver, it is characterized in that, the method comprises the steps:
(1) cus-cus grass blade stalk is cut into the segment that 10 ~ 15mm is long, get the vetiver segment of certain mass and certain density organic solvent, in the ratio mixing that feed liquid mass ratio is 1:15 ~ 20, add extraction heat 2 ~ 4 times after mixing at a certain temperature, carry out Separation of Solid and Liquid, be extracted liquid, all previous extract is filtered respectively, carry out decompression distillation after mixing, being concentrated into solid content is 22 ± 2%, obtains vetiver concentrate;
(2) by the vetiver segment dehydration after extraction, conventional defibrination is adopted to make vetiver slurry;
(3) offal of certain mass is taken, the ratio being 1:3.5 ~ 7 in feed liquid mass ratio adds water mixing, extraction heat is added at a certain temperature after mixing, Separation of Solid and Liquid subsequently, offal after being extracted and extract, then extract is carried out decompression distillation, being concentrated into solid content is 40 ± 2%, obtains offal concentrate;
(4) offal of certain mass is taken, the ratio being 1:3.5 ~ 7 in feed liquid mass ratio adds water mixing, extraction heat is added at a certain temperature after mixing, Separation of Solid and Liquid subsequently, offal after being extracted and extract, then extract is carried out decompression distillation, being concentrated into solid content is 40 ± 2%, obtains offal concentrate;
(5) offal after the extraction obtained step (3) carries out fiber, and to discongest rear mill slurrying to beating degree be 11 ± 2 ° of SR, offal after the extraction obtained with step (4) is again that 1:1 ~ 1.5 mix defibrination by offal and offal oven dry stock mass ratio, be 20 ± 2 ° of SR to beating degree, obtain tobacco slurry;
(6) tobacco slurry that vetiver slurry step (2) obtained and step (5) obtain mixes in the ratio that oven dry stock mass ratio is 1:4 ~ 8, and then paper process obtains elementary thin slice routinely;
(7) the vetiver concentrate that the offal concentrate that offal concentrate step (3) obtained, step (4) obtain and step (1) obtain mixes in the ratio that three's mass ratio is 1:3 ~ 5:1, obtains mixing coating fluid;
(8) mixing coating solution step (7) obtained, on the elementary thin slice two sides that step (6) obtains, is then dried, and being dried to water content is 10% ~ 14%, can obtain the reconstituted tobacoo containing vetiver.
In the present invention, solid content in step (1), step (3), step (4) all refers to mass percentage, water content in step (8) is also mass percentage, and the solid content occurred in embodiment and water content are also this implications.
In the present invention, the finite concentration in described step (1) refers to that concentration is 50%, and described organic solvent is ethanol or propane diols, and described uniform temperature refers to that temperature is 60 DEG C.
In the present invention, the beating degree adopting conventional defibrination to make vetiver slurry in described step (2) is 60 ± 2 ° of SR.
In the present invention, the uniform temperature in described step (3) refers to that temperature is 65 ± 5 DEG C, and the time of extraction is 40min.
In the present invention, the uniform temperature in described step (4) refers to that temperature is 65 ± 5 DEG C, and the time of extraction is 40min.
Reconstituted tobacoo of the present invention adopts vetiver fiber as solid plant spices, substitute traditional additional non-tobacco fiber, become the important component part of reconstituted tobacoo, vetiver abundant raw material, and the physical strength of the reconstituted tobacoo adopting vetiver to obtain reaches the standard of the thin slice of traditional non-tobacco class plus fiber, make to adopt vetiver to be that primary raw material possesses feasibility to prepare reconstituted tobacoo in actual production.The reconstituted tobacoo simultaneously adding vetiver can promote suction taste, prepared reconstituted tobacoo is added in cigarette and replaces part pipe tobacco, fragrance can be provided to cigarette, the quality of cigarette can be improved, compared with the thin slice of traditional non-tobacco class plus fiber, the wooden assorted gas of reconstituted tobacoo containing vetiver and the peppery gas of thorn reduce, and excitant reduces, and inhale taste and are promoted.
In reconstituted tobacoo of the present invention, offal, offal are the leftover bits and pieces that cigarette shreds is produced, and are used for making reconstituted tobacoo and are backfilling in cigarette shreds, not only can give thin slice cigarette fragrant, but also can reduce the consumption of raw materials of tobacco business, improve the mouthfeel of cigarette product.Vetiver can provide unique fragrance to thin slice, makes it coordinate mutually with pipe tobacco in cigarette.Meanwhile, tobacco stalk fibre is shorter and thick, and offal does not have fiber, and vetiver fiber is long and thin, obviously can promote the physical strength of reconstituted tobacoo, is convenient to industrial production.
In the present invention, described organic solvent concentration, the solid-liquid ratio of offal and offal extraction, offal concentrate, offal concentrate and vetiver concentrate mixed proportion, offal and offal defibrination forward slip value ratio, the mixed proportion of vetiver slurry and tobacco slurry, according to the specific requirement of reconstituted tobacoo, can carry out different combination allotments.
Two of object of the present invention is to provide the application of the above-mentioned reconstituted tobacoo containing vetiver.
This purpose of the present invention realizes by following technical solution: the above-mentioned application of reconstituted tobacoo on cigar exoperidium containing vetiver.
The above-mentioned application of reconstituted tobacoo in cigarette containing vetiver, the reconstituted tobacoo of acquisition is carried out chopping, wherein, the mass percent that tobacco thin filament accounts for whole cigarette shreds is 5 ~ 15%, here whole cigarette shreds comprises tobacco thin filament and tobacco leaf silk, the requirement of reconstituted tobacoo chopping is identical with tobacco leaf chopping, all adopts conventional tobacco leaf chopping technique and chopping requirement.After adding tobacco thin filament in cigarette shreds, during smoking cigarette, can mouthfeel be improved, increase fragrance, reduce the peppery gas of thorn, and be easier to health.
Compared with prior art, the present invention has following remarkable result:
(1) the present invention is containing the preparation method of reconstituted tobacoo of vetiver and the application in cigarette thereof, with cus-cus grass blade stalk for primary raw material, substitute the non-tobacco class plus fiber in traditional thin slice, mix with offal offal, the reconstituted tobacoo containing vetiver is made in shaping rear coating, and then the reconstituted tobacoo of gained adds in cigarette, the aesthetic quality of tobacco can be promoted, meanwhile, the present invention matches containing the reconstituted tobacoo combustion quality of vetiver and tobacco, has positive effect to the local flavor of tobacco.
(2) the present invention prepare containing the reconstituted tobacoo of vetiver, chopping can substitute part pipe tobacco in cigarette, the quality accounting of reconstituted tobacoo can reach 5-15%, also can for cigar exoperidium.
(3) reconstituted tobacoo that prepared by the present invention contains vetiver, the aroma chemical composition of vetiver mainly contains benzoic acid, vetiverol or vetiverol, furfural, vetivone, vetivene, the metabolism of health can be promoted, to invigorate blood circulation channels and collaterals, also positive curative effect is had, therefore prepared reconstituted tobacoo also more healthy and environmental protection to adjustment hormonal balance and Cure for insomnia.
(4) cus-cus grass blade stalk itself has good fiber properties, and substitute the reconstituted tobacoo containing vetiver solid spice made by additional non-tobacco fiber (as needlebush or flaxen fiber), processing characteristics is better than traditional thin slice.Containing natural aroma substance in vetiver, the reconstituted tobacoo and the pipe tobacco mixing manufacture cigarette that contain vetiver solid spice, the fragrance that cigarette can be provided to coordinate, improves mouthfeel, and can not bring negative effect to cigarette quality.The combustion quality of the reconstituted tobacoo of prepared vetiver comparatively mates with tobacco, and the aesthetic quality of cigarette is got a promotion, and wooden assorted gas and the peppery gas of thorn reduce, and excitant reduces, and thus can promote tobacco overall quality and local flavor.
Detailed description of the invention
Embodiment 1
Containing a preparation method for the reconstituted tobacoo of vetiver, the method comprises the steps:
(1) cus-cus grass blade stalk is cut into the segment that 10 ~ 15mm is long, vetiver segment and the concentration of getting 200g are the ethanol of 50%, in the ratio mixing that feed liquid mass ratio is 1:20, at 60 DEG C, add extraction heat 3 times after mixing, carry out Separation of Solid and Liquid, be extracted liquid, all previous extract is filtered respectively, carry out decompression distillation after mixing, being concentrated into solid content is 20%, obtains vetiver concentrate;
(2) by the vetiver segment dehydration after extraction, adopt conventional defibrination to beating degree to be 60 ± 2 ° of SR, make vetiver slurry;
(3) offal of 800g is taken, the ratio being 1:3.75 in feed liquid mass ratio adds the mixing of 3000mL water, at 65 DEG C, extraction heat is added after mixing, the time of extraction is 40min, Separation of Solid and Liquid subsequently, the offal after being extracted and extract, then carry out decompression distillation by extract, being concentrated into solid content is 40%, obtains offal concentrate;
(4) offal of 1200g is taken, the ratio being 1:3.75 in feed liquid mass ratio adds the mixing of 4500mL water, at 65 DEG C, extraction heat is added after mixing, the time of extraction is 40min, Separation of Solid and Liquid subsequently, the offal after being extracted and extract, then carry out decompression distillation by extract, being concentrated into solid content is 40%, obtains offal concentrate;
(5) offal after the extraction obtained step (3) carries out fiber, and to discongest rear mill slurrying to beating degree be 11 ± 2 ° of SR, offal after the extraction obtained with step (4) is again 1:1 mixing defibrination by offal and offal oven dry stock mass ratio, be 20 ± 2 ° of SR to beating degree, obtain tobacco slurry;
(6) tobacco slurry that vetiver slurry step (2) obtained and step (5) obtain mixes in the ratio that oven dry stock mass ratio is 1:4, and then paper process obtains elementary thin slice routinely;
(7) the vetiver concentrate that the offal concentrate that offal concentrate step (3) obtained, step (4) obtain and step (1) obtain mixes in the ratio that three's mass ratio is 1:3:1, obtains mixing coating fluid;
(8) mixing coating solution step (7) obtained, on the elementary thin slice two sides that step (6) obtains, is then dried, and being dried to water content is 12%, can obtain the reconstituted tobacoo containing vetiver.
The reconstituted tobacoo containing vetiver that said method obtains, whole reconstituted tobacoo may be used for cigar exoperidium, if will the reconstituted tobacoo containing vetiver obtained be applied in cigarette, need to adopt filament cutter that the reconstituted tobacoo conventional means of acquisition is carried out chopping, obtain tobacco thin filament, the mass percent that tobacco thin filament accounts for whole cigarette shreds is respectively 5%, 10% and 15%.
Comparing embodiment
Adopt reconstituted tobacoo prepared by traditional handicraft, concrete steps are as follows:
(1) take offal 800g, the ratio being 1:3.75 according to solid-liquid ratio adds 3000mL water soaking, under the condition of temperature 65 DEG C, and extraction 40min, subsequently Separation of Solid and Liquid, the offal after being extracted and extract;
(2) take offal 1200g, the ratio being 1:3.75 according to solid-liquid ratio adds 4500mL water soaking, under the condition of temperature 65 DEG C, and extraction 40min, subsequently Separation of Solid and Liquid, the offal after being extracted and extract;
(3) the offal solution fibre after being extracted is 11 ± 2 ° of SR with mill slurrying to beating degree afterwards, then is 20 ± 2 ° SRs by over dry 1:1 mixing defibrination to beating degree with the offal after extraction, obtains tobacco slurry;
(4) add the softwood pulp that beating degree is 42 ± 2 ° of SR in the tobacco slurry obtained in step (3), softwood pulp mixes in the ratio that oven dry stock mass ratio is 1:4 with tobacco slurry, manufactures paper with pulp make reconstituted tobacoo sheet base through routine,
(5) after the extract after the extract after being extracted by offal and offal extract is concentrated into 50mL respectively, extracting concentrate ratio in 1 offal extraction concentrate and offal is 1:1 mixing, dip-coating is on reconstituted tobacoo sheet base two sides again, and drying cuts the tobacco sheets by paper making method that can obtain traditional handicraft.
The reconstituted tobacoo of gained traditional handicraft and embodiment 1 method gained are contained the reconstituted tobacoo chopping respectively of vetiver, the reconstituted tobacoo of traditional handicraft be numbered I, embodiment 1 method gained containing the tobacco of vetiver thin be numbered II, the mass percent accounting for whole cigarette shreds with reconstituted tobacoo be respectively 5%, 10% and 15% 3 kind of different proportion add in cigarette, carry out sensory quality assessment, with blank cigarette for contrast, tasting results contrast is as shown in table 1.
Table 1: the tobacco thin filament that the traditional handicraft of different proportion and the present invention obtain affects the aesthetic quality of cigarette
As can be seen from Table 1, the reconstituted tobacoo of traditional handicraft affects the aesthetic quality of cigarette and inhales taste, all has adverse effect to tobacco interior quality and local flavor, is mainly reflected in xylon gas and weighs and have on excitement.And with the addition of the cigarette of the reconstituted tobacoo containing vetiver, fragrance harmony rises, and igniting and sucking quality and tobacco match, and comparatively the former mouthfeel be better.Smoking result shows, containing the addition of the tobacco thin filament of vetiver about 10%, improves effect best to the overall sucking quality of cigarette.
Embodiment 2
Containing a preparation method for the reconstituted tobacoo of vetiver, the method comprises the steps:
(1) cus-cus grass blade stalk is cut into the segment that 10 ~ 15mm is long, vetiver segment and the concentration of getting 200g are the propane diols of 50%, in the ratio mixing that feed liquid mass ratio is 1:18, at 60 DEG C, add extraction heat 3 times after mixing, carry out Separation of Solid and Liquid, be extracted liquid, all previous extract is filtered respectively, carry out decompression distillation after mixing, being concentrated into solid content is 22%, obtains vetiver concentrate;
(2) by the vetiver segment dehydration after extraction, adopt conventional defibrination to beating degree to be 60 ± 2 ° of SR, make vetiver slurry;
(3) offal of 800g is taken, the ratio being 1:5 in feed liquid mass ratio adds the mixing of 4000mL water, at 65 DEG C, extraction heat is added after mixing, the time of extraction is 40min, Separation of Solid and Liquid subsequently, the offal after being extracted and extract, then carry out decompression distillation by extract, being concentrated into solid content is 42%, obtains offal concentrate;
(4) offal of 1200g is taken, the ratio being 1:5 in feed liquid mass ratio adds the mixing of 6000mL water, at 65 DEG C, extraction heat is added after mixing, the time of extraction is 40min, Separation of Solid and Liquid subsequently, the offal after being extracted and extract, then carry out decompression distillation by extract, being concentrated into solid content is 42%, obtains offal concentrate;
(5) offal after the extraction obtained step (3) carries out fiber, and to discongest rear mill slurrying to beating degree be 11 ± 2 ° of SR, offal after the extraction obtained with step (4) is again 1:1.2 mixing defibrination by offal and offal oven dry stock mass ratio, be 20 ± 2 ° of SR to beating degree, obtain tobacco slurry;
(6) tobacco slurry that vetiver slurry step (2) obtained and step (5) obtain mixes in the ratio that oven dry stock mass ratio is 1:6, and then paper process obtains elementary thin slice routinely;
(7) the vetiver concentrate that the offal concentrate that offal concentrate step (3) obtained, step (4) obtain and step (1) obtain mixes in the ratio that three's mass ratio is 1:4:1, obtains mixing coating fluid;
(8) mixing coating solution step (7) obtained, on the elementary thin slice two sides that step (6) obtains, is then dried, and being dried to water content is 12%, can obtain the reconstituted tobacoo containing vetiver.
The reconstituted tobacoo containing vetiver that said method obtains, whole reconstituted tobacoo may be used for cigar exoperidium, if will the reconstituted tobacoo containing vetiver obtained be applied in cigarette, need to adopt filament cutter that the reconstituted tobacoo conventional means of acquisition is carried out chopping, obtain tobacco thin filament, the mass percent that tobacco thin filament accounts for whole cigarette shreds is respectively 6%, 9% and 12%.
Embodiment 3
Containing a preparation method for the reconstituted tobacoo of vetiver, the method comprises the steps:
(1) cus-cus grass blade stalk is cut into the segment that 10 ~ 15mm is long, vetiver segment and the concentration of getting 200g are the ethanol of 50%, in the ratio mixing that feed liquid mass ratio is 1:15, at 60 DEG C, add extraction heat 2 times after mixing, carry out Separation of Solid and Liquid, be extracted liquid, all previous extract is filtered respectively, carry out decompression distillation after mixing, being concentrated into solid content is 24%, obtains vetiver concentrate;
(2) by the vetiver segment dehydration after extraction, adopt conventional defibrination to beating degree to be 60 ± 2 ° of SR, make vetiver slurry;
(3) offal of 800g is taken, the ratio being 1:3.5 in feed liquid mass ratio adds the mixing of 2800mL water, at 60 DEG C, extraction heat is added after mixing, the time of extraction is 40min, Separation of Solid and Liquid subsequently, the offal after being extracted and extract, then carry out decompression distillation by extract, being concentrated into solid content is 40%, obtains offal concentrate;
(4) offal of 1200g is taken, the ratio being 1:3.5 in feed liquid mass ratio adds the mixing of 4200mL water, at 60 DEG C, extraction heat is added after mixing, the time of extraction is 40min, Separation of Solid and Liquid subsequently, the offal after being extracted and extract, then carry out decompression distillation by extract, being concentrated into solid content is 40%, obtains offal concentrate;
(5) offal after the extraction obtained step (3) carries out fiber, and to discongest rear mill slurrying to beating degree be 11 ± 2 ° of SR, offal after the extraction obtained with step (4) is again 1:1 mixing defibrination by offal and offal oven dry stock mass ratio, be 20 ± 2 ° of SR to beating degree, obtain tobacco slurry;
(6) tobacco slurry that vetiver slurry step (2) obtained and step (5) obtain mixes in the ratio that oven dry stock mass ratio is 1:4, and then paper process obtains elementary thin slice routinely;
(7) the vetiver concentrate that the offal concentrate that offal concentrate step (3) obtained, step (4) obtain and step (1) obtain mixes in the ratio that three's mass ratio is 1:3:1, obtains mixing coating fluid;
(8) mixing coating solution step (7) obtained, on the elementary thin slice two sides that step (6) obtains, is then dried, and being dried to water content is 10%%, can obtain the reconstituted tobacoo containing vetiver.
The reconstituted tobacoo containing vetiver that said method obtains, whole reconstituted tobacoo may be used for cigar exoperidium, if will the reconstituted tobacoo containing vetiver obtained be applied in cigarette, need to adopt filament cutter that the reconstituted tobacoo conventional means of acquisition is carried out chopping, obtain tobacco thin filament, the mass percent that tobacco thin filament accounts for whole cigarette shreds is respectively 5%, 8% and 10%.
Embodiment 4
Containing a preparation method for the reconstituted tobacoo of vetiver, the method comprises the steps:
(1) cus-cus grass blade stalk is cut into the segment that 10 ~ 15mm is long, vetiver segment and the concentration of getting 200g are the propane diols of 50%, in the ratio mixing that feed liquid mass ratio is 1:20, at 60 DEG C, add extraction heat 4 times after mixing, carry out Separation of Solid and Liquid, be extracted liquid, all previous extract is filtered respectively, carry out decompression distillation after mixing, being concentrated into solid content is 20%, obtains vetiver concentrate;
(2) by the vetiver segment dehydration after extraction, adopt conventional defibrination to beating degree to be 60 ± 2 ° of SR, make vetiver slurry;
(3) offal of 800g is taken, the ratio being 1:7 in feed liquid mass ratio adds the mixing of 5600mL water, at 70 DEG C, extraction heat is added after mixing, the time of extraction is 40min, Separation of Solid and Liquid subsequently, the offal after being extracted and extract, then carry out decompression distillation by extract, being concentrated into solid content is 38%, obtains offal concentrate;
(4) offal of 1200g is taken, the ratio being 1:7 in feed liquid mass ratio adds the mixing of 8400mL water, at 70 DEG C, extraction heat is added after mixing, the time of extraction is 40min, Separation of Solid and Liquid subsequently, the offal after being extracted and extract, then carry out decompression distillation by extract, being concentrated into solid content is 38%, obtains offal concentrate;
(5) offal after the extraction obtained step (3) carries out fiber, and to discongest rear mill slurrying to beating degree be 11 ± 2 ° of SR, offal after the extraction obtained with step (4) is again 1:1.5 mixing defibrination by offal and offal oven dry stock mass ratio, be 20 ± 2 ° of SR to beating degree, obtain tobacco slurry;
(6) tobacco slurry that vetiver slurry step (2) obtained and step (5) obtain mixes in the ratio that oven dry stock mass ratio is 1:8, and then paper process obtains elementary thin slice routinely;
(7) the vetiver concentrate that the offal concentrate that offal concentrate step (3) obtained, step (4) obtain and step (1) obtain mixes in the ratio that three's mass ratio is 1:5:1, obtains mixing coating fluid;
(8) mixing coating solution step (7) obtained, on the elementary thin slice two sides that step (6) obtains, is then dried, and being dried to water content is 14%, can obtain the reconstituted tobacoo containing vetiver.
The reconstituted tobacoo containing vetiver that said method obtains, whole reconstituted tobacoo may be used for cigar exoperidium, if will the reconstituted tobacoo containing vetiver obtained be applied in cigarette, need to adopt filament cutter that the reconstituted tobacoo conventional means of acquisition is carried out chopping, obtain tobacco thin filament, the mass percent that tobacco thin filament accounts for whole cigarette shreds is respectively 10%, 12% and 15%.
Embodiment 5
Containing a preparation method for the reconstituted tobacoo of vetiver, the method comprises the steps:
(1) cus-cus grass blade stalk is cut into the segment that 10 ~ 15mm is long, vetiver segment and the concentration of getting 200g are the ethanol of 50%, in the ratio mixing that feed liquid mass ratio is 1:16, at 60 DEG C, add extraction heat 3 times after mixing, carry out Separation of Solid and Liquid, be extracted liquid, all previous extract is filtered respectively, carry out decompression distillation after mixing, being concentrated into solid content is 20%, obtains vetiver concentrate;
(2) by the vetiver segment dehydration after extraction, adopt conventional defibrination to beating degree to be 60 ± 2 ° of SR, make vetiver slurry;
(3) offal of 800g is taken, the ratio being 1:4 in feed liquid mass ratio adds the mixing of 3200mL water, at 65 DEG C, extraction heat is added after mixing, the time of extraction is 40min, Separation of Solid and Liquid subsequently, the offal after being extracted and extract, then carry out decompression distillation by extract, being concentrated into solid content is 40%, obtains offal concentrate;
(4) offal of 1200g is taken, the ratio being 1:4 in feed liquid mass ratio adds the mixing of 4800mL water, at 65 DEG C, extraction heat is added after mixing, the time of extraction is 40min, Separation of Solid and Liquid subsequently, the offal after being extracted and extract, then carry out decompression distillation by extract, being concentrated into solid content is 40%, obtains offal concentrate;
(5) offal after the extraction obtained step (3) carries out fiber, and to discongest rear mill slurrying to beating degree be 11 ± 2 ° of SR, offal after the extraction obtained with step (4) is again 1:1.4 mixing defibrination by offal and offal oven dry stock mass ratio, be 20 ± 2 ° of SR to beating degree, obtain tobacco slurry;
(6) tobacco slurry that vetiver slurry step (2) obtained and step (5) obtain mixes in the ratio that oven dry stock mass ratio is 1:5, and then paper process obtains elementary thin slice routinely;
(7) the vetiver concentrate that the offal concentrate that offal concentrate step (3) obtained, step (4) obtain and step (1) obtain mixes in the ratio that three's mass ratio is 1:4:1, obtains mixing coating fluid;
(8) mixing coating solution step (7) obtained, on the elementary thin slice two sides that step (6) obtains, is then dried, and being dried to water content is 12%, can obtain the reconstituted tobacoo containing vetiver.
The reconstituted tobacoo containing vetiver that said method obtains, whole reconstituted tobacoo may be used for cigar exoperidium, if will the reconstituted tobacoo containing vetiver obtained be applied in cigarette, need to adopt filament cutter that the reconstituted tobacoo conventional means of acquisition is carried out chopping, obtain tobacco thin filament, the mass percent that tobacco thin filament accounts for whole cigarette shreds is respectively 5%, 10% and 15%.
The above embodiment of the present invention is not limiting the scope of the present invention; embodiments of the present invention are not limited thereto; all this kind is according to foregoing of the present invention; according to ordinary technical knowledge and the customary means of this area; do not departing under the present invention's above-mentioned basic fundamental thought prerequisite; to the amendment of other various ways that said structure of the present invention is made, replacement or change, all should drop within protection scope of the present invention.
Claims (7)
1., containing a preparation method for the reconstituted tobacoo of vetiver, it is characterized in that, the method comprises the steps:
(1) cus-cus grass blade stalk is cut into the segment that 10 ~ 15mm is long, get the vetiver segment of certain mass and certain density organic solvent, in the ratio mixing that feed liquid mass ratio is 1:15 ~ 20, add extraction heat 2 ~ 4 times after mixing at a certain temperature, carry out Separation of Solid and Liquid, be extracted liquid, all previous extract is filtered respectively, carry out decompression distillation after mixing, being concentrated into solid content is 22 ± 2%, obtains vetiver concentrate;
(2) by the vetiver segment dehydration after extraction, conventional defibrination is adopted to make vetiver slurry;
(3) offal of certain mass is taken, the ratio being 1:3.5 ~ 7 in feed liquid mass ratio adds water mixing, extraction heat is added at a certain temperature after mixing, Separation of Solid and Liquid subsequently, offal after being extracted and extract, then extract is carried out decompression distillation, being concentrated into solid content is 40 ± 2%, obtains offal concentrate;
(4) offal of certain mass is taken, the ratio being 1:3.5 ~ 7 in feed liquid mass ratio adds water mixing, extraction heat is added at a certain temperature after mixing, Separation of Solid and Liquid subsequently, offal after being extracted and extract, then extract is carried out decompression distillation, being concentrated into solid content is 40 ± 2%, obtains offal concentrate;
(5) offal after the extraction obtained step (3) carries out fiber, and to discongest rear mill slurrying to beating degree be 11 ± 2 ° of SR, offal after the extraction obtained with step (4) is again that 1:1 ~ 1.5 mix defibrination by offal and offal oven dry stock mass ratio, be 20 ± 2 ° of SR to beating degree, obtain tobacco slurry;
(6) tobacco slurry that vetiver slurry step (2) obtained and step (5) obtain mixes in the ratio that oven dry stock mass ratio is 1:4 ~ 8, and then paper process obtains elementary thin slice routinely;
(7) the vetiver concentrate that the offal concentrate that offal concentrate step (3) obtained, step (4) obtain and step (1) obtain mixes in the ratio that three's mass ratio is 1:3 ~ 5:1, obtains mixing coating fluid;
(8) mixing coating solution step (7) obtained, on the elementary thin slice two sides that step (6) obtains, is then dried, and being dried to water content is 12 ± 2%, can obtain the reconstituted tobacoo containing vetiver.
2. the preparation method of the reconstituted tobacoo containing vetiver according to claim 1, it is characterized in that: the finite concentration in described step (1) refers to that mass concentration is 50%, described organic solvent is ethanol or propane diols, and described uniform temperature refers to that temperature is 60 DEG C.
3. the preparation method of the reconstituted tobacoo containing vetiver according to claim 1, is characterized in that: the beating degree adopting conventional defibrination to make vetiver slurry in described step (2) is 60 ± 2 ° of SR.
4. the preparation method of the reconstituted tobacoo containing vetiver according to claim 1, it is characterized in that: the uniform temperature in described step (3) refers to that temperature is 65 ± 5 DEG C, the time of extraction is 40min.
5. the preparation method of the reconstituted tobacoo containing vetiver according to claim 1, it is characterized in that: the uniform temperature in described step (4) refers to that temperature is 65 ± 5 DEG C, the time of extraction is 40min.
6. the application of reconstituted tobacoo on cigar exoperidium containing vetiver as described in any one of claim 1 to 5.
7. the application of reconstituted tobacoo in cigarette containing vetiver as described in any one of claim 1 to 5, the reconstituted tobacoo of acquisition is carried out chopping, and the mass percent that tobacco thin filament accounts for whole cigarette shreds is 5 ~ 15%.
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| CN105595401A (en) * | 2016-01-06 | 2016-05-25 | 云南中烟再造烟叶有限责任公司 | Preparation method of non-burning low-temperature smoking tobacco shreds |
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| US4517990A (en) * | 1980-12-04 | 1985-05-21 | International Flavors & Fragrances Inc. | 3,4,5,6,6-Pentamethyl hexanol-2 and alkyl homologues thereof; process for preparing same and organoleptic uses thereof |
| CN1911120A (en) * | 2005-08-09 | 2007-02-14 | 陈文霞 | Cigarette with function of improving air quality |
| CN101416776B (en) * | 2008-10-21 | 2011-02-09 | 深圳烟草工业有限责任公司 | Flavoring formulation capable of increasing tobacco leaf quality |
| CN101619271B (en) * | 2009-07-02 | 2011-09-21 | 华顺香料(上海)有限公司 | Traditional Chinese medicine combination spice for cigarette as well as preparation method and application thereof |
| CN102031197B (en) * | 2009-09-30 | 2013-03-27 | 湖北中烟工业有限责任公司 | Cigarette flavoring essence for supplementing bean aroma note |
| CN103396889A (en) * | 2013-07-10 | 2013-11-20 | 红云红河烟草(集团)有限责任公司 | Preparation method of vetiver oil and application of vetiver oil in cigarettes |
| CN104366687B (en) * | 2014-09-15 | 2016-03-16 | 云南中烟新材料科技有限公司 | A kind of low temperature does not burn cigarette sucked material and preparation method thereof |
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| CN105595401A (en) * | 2016-01-06 | 2016-05-25 | 云南中烟再造烟叶有限责任公司 | Preparation method of non-burning low-temperature smoking tobacco shreds |
| CN105595401B (en) * | 2016-01-06 | 2017-01-25 | 云南中烟再造烟叶有限责任公司 | Preparation method of non-burning low-temperature smoking tobacco shreds |
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