CN104877802A - Cleaning agent for silk-wool and/or down feather clothes and preparation method of cleaning agent - Google Patents
Cleaning agent for silk-wool and/or down feather clothes and preparation method of cleaning agent Download PDFInfo
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- CN104877802A CN104877802A CN201510204371.6A CN201510204371A CN104877802A CN 104877802 A CN104877802 A CN 104877802A CN 201510204371 A CN201510204371 A CN 201510204371A CN 104877802 A CN104877802 A CN 104877802A
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Abstract
The invention discloses a cleaning agent for silk-wool and/or down feather clothes and a preparation method of the cleaning agent. The cleaning agent is prepared from the following raw materials in percentage by weight: 1-5% of ethoxylated alkyl sodium sulfate, 1-5% of fatty alcohol-polyoxyethylene ether, 1-4% of 1-methyl-1 oleoylamido-2 oleylimidazoline methyl ammonium sulfate, 0.5-2% of trisodium citrate, 0.1-2% of citric acid, 0.1-0.5% of ethylenediamine tetraacetic acid disodium salt, 3-6% of lauramidopropyl betaine, 3-6% of alkyl glycoside, 1-3% of sodium chloride, 0.1-1% of essence, 0.1-1% of preservative and 65-89% of water. The cleaning agent is applicable to cleaning silk, wool, silk-wool or down feather clothes, and is mild in properties and capable of reducing damage to protein fibers, and also has excellent cleaning, bacteriostasis and nursing effects.
Description
Technical field
The invention belongs to clothes detergent technical field, be specifically related to a kind of clean-out system for Si Mao and/or feather-down clothing and preparation method thereof.
Background technology
Silk is matured silkworm secreted silk liquid concretionary continuous fiber when cocooing, and also claiming natural silk, is a kind of natural protein fibre.The advantages such as silk is elongated because of its light weight, and fabric sheen is good, comfortable and easy to wear, and feel is smooth plentiful, poor heat conductivity, and moisture absorption is ventilative are used to knit in the various silks and satins of system and tricot.
Wool is a kind of natural protein fibre, and wool has the advantages such as good springiness, water absorbability is strong, heat retention is good, can be used for making the textiless such as woollen goods, knitting wool, woollen blanket, felting.The existing product also having silk and wool to combine, as silk wool blended yarn, silk woolen knitting shirt etc.
Eider down is the long belly duck, goose, become the fine hair of a reed catkins shape, it is a kind of animal protein fiber, it is higher than cotton (vegetative fiber element) heat retaining property, and ten million leg-of-mutton tiny pore that eider down nodular fibrous gathers, can the convergent-divergent with temperature Change, produce temperature adjustment function, Absorbable rod human body distributes the hot gas of flowing, the invasion of isolated cool ambient air.Cotton, silk, wool and eider down four large natural heat insulating material formed in, the thermal property of eider down is best, and therefore eiderdown quilt is widely used in and makes the heat-preserving clothes such as down jackets, eiderdown quilt.
Because silk, wool and eider down all belong to natural protein fibre; because of its equal not acid and alkali-resistance; if use soap and regular powder cleaning; because it all has stronger alkalescence, the protective membrane of destructible fiber surface, and meeting infiltrated fiber is inner; silk, wool and eider down is made to lose original soft and moist, elasticity and gloss; become dry, harden, withered crisp, aging, shorten the work-ing life of silk hair/feather-down clothing, therefore cleaning silk hair/feather-down clothing needs to select special clean-out system.
In currently available technology, special clean-out system is had for silk sweater thing, as Chinese patent application CN 101985584 B discloses a kind of silk sweater detergent composition, it is made up of aliphatic alcohol polyethenoxy (9) ether, aliphatic alcohol polyethenoxy (7) ether, Dodecyl Polyoxyethylene Ether sodium sulfate, amphoteric imidazoline, Nonyl pheno (10) ether, coconut acid diethanolamide, essence, ethylenediamine tetraacetic acid (EDTA) and sodium-chlor, wherein Nonyl pheno (10) ether because of its degradation property poor, successively by a lot of countries forbidding.
Also special clean-out system is had for feather-down clothing, as Chinese patent application CN 104312762 A discloses a kind of down detergent, it comprises water, trolamine, octadecane alcohol radical Soxylat A 25-7, polyoxylethylene abietate, Polyglycerine monostearate, Vltra tears, sodium laurate, trimethyl ammonium sulfate, Sodium Persulfate, N-octylisothiazolinone, phenyl silicone oil, aminomethyl propanol, morpholine, sodium bicarbonate, tea-polyphenol, vinyltrimethoxy silane, polyisobutene, polyvinylpyrrolidone, dimeracid, maleic anhydride modified polyethylene.
But the current one that still lacks can be closed for silk, wool or silk hair knot simultaneously; or the clean-out system of feather-down clothing cleaning; therefore be necessary to research and develop a kind of destruction of reducing thiozell, there is the clean-out system for Si Mao and/or feather-down clothing of excellent clean effect and protection opsonization simultaneously.
Summary of the invention
The object of the present invention is to provide a kind of clean-out system for Si Mao and/or feather-down clothing, its gentleness is non-stimulated, has excellent clean effect and nursing role, simultaneously can effective bactericidal.
The present invention is by the following technical programs to realize above-mentioned purpose, for a clean-out system for Si Mao and/or feather-down clothing, comprise the raw material of following weight percent meter: ethoxylated alkyl sulfate 1 ~ 5%, fatty alcohol-polyoxyethylene ether 1 ~ 5%, the oily acid based imidazolines sulfate methyl ammonium 1 ~ 4% of 1-methyl isophthalic acid oleoyl amido-2, trisodium citrate 0.5 ~ 2%, citric acid 0.1 ~ 2%, disodium ethylene diamine tetraacetate 0.1 ~ 0.5%, lauroyl amido CAB 3 ~ 6%, alkyl glycoside 3 ~ 6%, sodium-chlor 1 ~ 3%, essence 0.1 ~ 1%, sanitas 0.1 ~ 1%, water 65 ~ 89%.
As the preferred embodiment of the present invention, the clean-out system that the present invention is used for Si Mao and/or feather-down clothing is made up of the raw material of following weight percent meter: ethoxylated alkyl sulfate 3%, fatty alcohol-polyoxyethylene ether 3%, the oily acid based imidazolines sulfate methyl ammonium 2% of 1-methyl isophthalic acid oleoyl amido-2, trisodium citrate 1%, citric acid 0.5%, disodium ethylene diamine tetraacetate 0.3%, lauroyl amido CAB 5%, alkyl glycoside 5%, sodium-chlor 1.5%, essence 0.2%, sanitas 0.1%, water 78.4%.
Further, described fatty alcohol-polyoxyethylene ether is aliphatic alcohol polyethenoxy (9) ether.
Further, described alkyl glycoside to be carbon chain lengths be 12 alkyl glycoside.
Further, described sanitas is the mixture of Bronopol and Kathon CG, and the mass ratio of described Bronopol and Kathon CG is 7.5:1.
Present invention also offers the preparation method of the described clean-out system for Si Mao and/or feather-down clothing, comprise the following steps: in water, add fatty alcohol-polyoxyethylene ether, the oily acid based imidazolines sulfate methyl ammonium of 1-methyl isophthalic acid oleoyl amido-2 while stirring, stir; Then add disodium ethylene diamine tetraacetate, trisodium citrate, citric acid, ethoxylated alkyl sulfate, lauroyl amido CAB, alkyl glycoside, sodium-chlor, essence and sanitas while stirring, stir into homogeneous liquid.
In technique scheme, described ethoxylated alkyl sulfate is a kind of anion surfactant, described fatty alcohol-polyoxyethylene ether is a kind of nonionogenic tenside, the oily acid based imidazolines sulfate methyl ammonium of described 1-methyl isophthalic acid oleoyl amido-2 is a kind of cats product, described lauroyl amido CAB is a kind of amphoterics, and described alkyl glycoside is a kind of nonionogenic tenside.
The clean-out system that the present invention is used for Si Mao and/or feather-down clothing comprises " four ions " system that anion surfactant, cats product, nonionogenic tenside and zwitterionics form uniqueness, first in system, fatty alcohol-polyoxyethylene ether and alkyl glycoside well independently can wrap up the oily acid based imidazolines sulfate methyl ammonium of cats product 1-methyl isophthalic acid oleoyl amido-2 as nonionogenic tenside, intercept the charge neutralization of cationic and anionic surfactant, guarantee system is stablized.When washing, fatty alcohol-polyoxyethylene ether and the emulsification of alkyl glycoside energy rapid osmotic, coordinate anion surfactant ethoxylated alkyl sulfate rapidly and efficiently to remove multiple dirt, the oily acid based imidazolines sulfate methyl ammonium energy quick adsorption of 1-methyl isophthalic acid oleoyl amido-2 discharged from package status is on fabric fibre top layer; Zwitterionics lauroyl amido CAB in addition in formula, corresponding change can be there is with the change of wash environment pH, in the environment of slant acidity, show as cats product, can and formula in the oily acid based imidazolines sulfate methyl ammonium of 1-methyl isophthalic acid oleoyl amido-2 together with, electrostatic, the effect such as submissive are gone in increase; And in the environment of neutral or meta-alkalescence, then can well coordinate ethoxylated alkyl sulfate, fatty alcohol-polyoxyethylene ether and alkyl glycoside, give play to excellent cleaning performance, well can remove electrostatic simultaneously and reduce the generation of electrostatic, can also bring well submissive, keep color and luster, the effect such as fluffy and antibacterial.
The present invention is elite trisodium citrate and the composite buffer system forming gentleness of citric acid also, make the pH value of clean-out system system and human body skin close, coordinate the present invention each raw material, gentle non-stimulated, pro-skin is natural, can provide suitable wash environment for natural protein fiber clothing.
Therefore, compared with prior art, advantage of the present invention is:
1) to be used for the cleaning effect of the clean-out system of Si Mao and/or feather-down clothing good in the present invention, good washing effect is had to the dirt be attached on eider down, silk, grease etc., do not injure the structure of the natural protein fibers such as silk, wool and eider down simultaneously, the original elasticity of the gloss of silk, feather dress fabric and eider down and wool and bulk shape can be kept after washing, keep original thermal property.
2) the present invention effectively can eliminate the microorganisms such as the bacterium be attached on silk hair, feather-down clothing for the clean-out system of Si Mao and/or feather-down clothing, and simultaneously effectively the microbial growth such as anti-bacteria, keeps the sanitary cleaning of silk hair, feather-down clothing.
3) the present invention also can be effectively antistatic for the clean-out system of Si Mao and/or feather-down clothing, and its antistatic effect is obviously better than commercially available fabric softener product, has washing and nursing, conditioning functions concurrently.
4) the present invention be used for each raw material of clean-out system of Si Mao and/or feather-down clothing collaborative to silk hair, feather-down clothing is clean, nursing role is strong, antibacterial bacteriostatic is effective, and gentle non-stimulated, pro-skin is natural, nontoxic residue-free, and its preparation method is simple simultaneously, can be applicable.
Embodiment
Further describe the present invention below by way of embodiment, but the present invention is not limited only to following examples.Within the scope of the invention or not departing from content of the present invention, spirit and scope, clean-out system for Si Mao and/or feather-down clothing of the present invention and preparation method thereof is suitably improved, replaces the identical component of effect, will become apparent to those skilled in the art that they are all deemed to be included within scope of the present invention.
Embodiment 1 ~ 3 the present invention is used for the clean-out system of Si Mao and/or feather-down clothing
Embodiment 1 ~ 3 for Si Mao and/or the clean-out system of feather-down clothing and the preparation method of comparative example 1 ~ 4 as follows:
In water, add aliphatic alcohol polyethenoxy (9) ether, the oily acid based imidazolines sulfate methyl ammonium of 1-methyl isophthalic acid oleoyl amido-2 while stirring, stir; Then disodium ethylene diamine tetraacetate, trisodium citrate, citric acid, ethoxylated alkyl sulfate, lauroyl amido CAB, C is added while stirring
12alkyl glycoside, sodium-chlor, essence and sanitas, stir into homogeneous liquid.
Embodiment 1 ~ 3, each raw material of comparative example 1 ~ 4 and consumption as shown in table 1 below
Table 1
test example one, the present invention are used for the cleaning effect test of the clean-out system of Si Mao and/or feather-down clothing
Prepare the cleaning effect of clean-out system according to the mensuration embodiment of the present invention 1 ~ 3 and comparative example 1 ~ 4 in GB/T13174-2008 " mensuration of dress material washing composition detersive power and circulation cleaning performance ", its result is as following table 2.
Table 2 the present invention is used for the cleaning effect of the clean-out system of Si Mao and/or feather-down clothing
Can be obtained by upper table 2, the cleaning effect of the embodiment of the present invention 1 ~ 3 is good, good washing effect is had to the dirt be attached on eider down, silk, grease etc., do not injure the natural protein fibers such as silk, wool and eider down simultaneously, wherein the cleaning effect of embodiment 1 is best, each ratio is the highest, illustrates that the synergy of each raw material of embodiment 1 and proportioning is best; The cleaning effect of comparative example 1 ~ 4 is than the difference of embodiment 1 ~ 3, ethoxylated alkyl sulfate, fatty alcohol-polyoxyethylene ether, alkyl glycoside, the oily acid based imidazolines sulfate methyl ammonium of 1-methyl isophthalic acid oleoyl amido-2 and lauroyl amido CAB four kinds of tensio-active agents are described, to lack wherein a kind of all can affect the cleaning effect of the present invention for the clean-out system of Si Mao and/or feather-down clothing.
test example two, the present invention are used for antibacterial, the bacteriostatic test of the clean-out system of Si Mao and/or feather-down clothing
1, the present invention is used for the antibacterial tests of the clean-out system of Si Mao and/or feather-down clothing
Measure the antibacterial effect of the embodiment of the present invention 1 ~ 3 and comparative example 1 ~ 4 preparation according to the analogue method in QB/T 2738-2012 " evaluation method of daily chemical products antibacterial bacteriostatic effect ", its result is as following table 3 and table 4:
Table 3 the present invention is used for the antibacterial effect (colon bacillus) of the clean-out system of Si Mao and/or feather-down clothing
Table 4 the present invention is used for the antibacterial effect (streptococcus aureus) of the clean-out system of Si Mao and/or feather-down clothing
Can be obtained by upper table 3 and table 4, the good anti-bacterial effect of the embodiment of the present invention 1 ~ 3, can effectively sterilization, eliminates the microorganisms such as the bacterium be attached on silk hair, feather-down clothing, wherein the antibacterial effect of embodiment 1 is best, illustrates that the synergy of each raw material of embodiment 1 and proportioning is best; The antibacterial effect of comparative example 1 ~ 4 is than the difference of embodiment 1 ~ 3, ethoxylated alkyl sulfate, fatty alcohol-polyoxyethylene ether, alkyl glycoside, the oily acid based imidazolines sulfate methyl ammonium of 1-methyl isophthalic acid oleoyl amido-2 and lauroyl amido CAB four kinds of tensio-active agents are described, to lack wherein a kind of all can affect the antibacterial effect of the present invention for the clean-out system of Si Mao and/or feather-down clothing.
2, the present invention is used for the bacteriostatic test of the clean-out system of Si Mao and/or feather-down clothing
Measure the fungistatic effect of the clean-out system of the embodiment of the present invention 1 ~ 3 and comparative example 1 ~ 4 preparation according to the analogue method in QB/T 2738-2012 " evaluation method of daily chemical products antibacterial bacteriostatic effect ", its result is as following table 5 and table 6:
Table 5 the present invention is used for the fungistatic effect (colon bacillus) of the clean-out system of Si Mao and/or feather-down clothing
Table 6 the present invention is used for the fungistatic effect (streptococcus aureus) of the clean-out system of Si Mao and/or feather-down clothing
Can be obtained by upper table 5 and table 6, the good antimicrobial effect of the embodiment of the present invention 1 ~ 3, effectively can to suppress on silk hair, feather-down clothing the microbial growths such as bacterium, and wherein the fungistatic effect of embodiment 1 is best, bacteriostasis rate reaches 99.8%, illustrates that the synergy of each raw material of embodiment 1 and proportioning is best; The fungistatic effect of comparative example 1 ~ 4 is than the difference of embodiment 1 ~ 3, ethoxylated alkyl sulfate, fatty alcohol-polyoxyethylene ether, alkyl glycoside, the oily acid based imidazolines sulfate methyl ammonium of 1-methyl isophthalic acid oleoyl amido-2 and lauroyl amido CAB four kinds of tensio-active agents are described, to lack wherein a kind of all can affect the fungistatic effect of the present invention for the clean-out system of Si Mao and/or feather-down clothing.
test example three, the present invention are used for the antistatic property test of the clean-out system of Si Mao and/or feather-down clothing
Measure the antistatic effect of the clean-out system of the embodiment of the present invention 1 ~ 3 and comparative example 1 ~ 4 preparation according to GB/T16801-1997 " mensuration of fabric conditioner antistatic property ", its result is as following table 7:
Table 7 the present invention is used for the antistatic effect of the clean-out system of Si Mao and/or feather-down clothing
Can be obtained by upper table 7, the embodiment of the present invention 1 ~ 3 antistatic effect is good, before and after the process of pure woolen fabric model, electrostatic potential decreases by more than 40%, before and after the process of real silk fabric model, electrostatic potential decreases by more than 30%, obviously be better than commercially available fabric softener product, illustrate that the present invention has good nursing, opsonization for the clean-out system of Si Mao and/or feather-down clothing to silk, wool and eider down, wherein especially the highest with the electrostatic potential range of decrease after the process of embodiment 1 clean-out system, antistatic effect is best.The fungistatic effect of comparative example 1 ~ 4 is than the difference of embodiment 1 ~ 3, ethoxylated alkyl sulfate, fatty alcohol-polyoxyethylene ether, alkyl glycoside, the oily acid based imidazolines sulfate methyl ammonium of 1-methyl isophthalic acid oleoyl amido-2 and lauroyl amido CAB four kinds of tensio-active agents are described, to lack wherein a kind of all can affect the antistatic effect of the present invention for the clean-out system of Si Mao and/or feather-down clothing.
Below be only the preferred embodiment of the present invention, it should be pointed out that above-mentioned preferred implementation should not be considered as limitation of the present invention, protection scope of the present invention should be as the criterion with claim limited range.For those skilled in the art, without departing from the spirit and scope of the present invention, can also make some improvements and modifications, these improvements and modifications also should be considered as protection scope of the present invention.
Claims (6)
1. the clean-out system for Si Mao and/or feather-down clothing, it is characterized in that, comprise the raw material of following weight percent meter: ethoxylated alkyl sulfate 1 ~ 5%, fatty alcohol-polyoxyethylene ether 1 ~ 5%, the oily acid based imidazolines sulfate methyl ammonium 1 ~ 4% of 1-methyl isophthalic acid oleoyl amido-2, trisodium citrate 0.5 ~ 2%, citric acid 0.1 ~ 2%, disodium ethylene diamine tetraacetate 0.1 ~ 0.5%, lauroyl amido CAB 3 ~ 6%, alkyl glycoside 3 ~ 6%, sodium-chlor 1 ~ 3%, essence 0.1 ~ 1%, sanitas 0.1 ~ 1%, water 65 ~ 89%.
2. as claimed in claim 1 for the clean-out system of Si Mao and/or feather-down clothing, it is characterized in that, be made up of the raw material of following weight percent meter: ethoxylated alkyl sulfate 3%, fatty alcohol-polyoxyethylene ether 3%, the oily acid based imidazolines sulfate methyl ammonium 2% of 1-methyl isophthalic acid oleoyl amido-2, trisodium citrate 1%, citric acid 0.5%, disodium ethylene diamine tetraacetate 0.3%, lauroyl amido CAB 5%, alkyl glycoside 5%, sodium-chlor 1.5%, essence 0.2%, sanitas 0.1%, water 78.4%.
3., as claimed in claim 1 or 2 for the clean-out system of Si Mao and/or feather-down clothing, it is characterized in that, described fatty alcohol-polyoxyethylene ether is aliphatic alcohol polyethenoxy (9) ether.
4., as claimed in claim 1 or 2 for the clean-out system of Si Mao and/or feather-down clothing, it is characterized in that, described alkyl glycoside to be carbon chain lengths be 12 alkyl glycoside.
5., as claimed in claim 1 or 2 for the clean-out system of Si Mao and/or feather-down clothing, it is characterized in that, described sanitas is the mixture of Bronopol and Kathon CG, and the mass ratio of described Bronopol and Kathon CG is 7.5:1.
6. one kind prepare as arbitrary in claim 1 ~ 5 as described in the method for the clean-out system for Si Mao and/or feather-down clothing, it is characterized in that, comprise the following steps: in water, add fatty alcohol-polyoxyethylene ether, the oily acid based imidazolines sulfate methyl ammonium of 1-methyl isophthalic acid oleoyl amido-2 while stirring, stir; Then add disodium ethylene diamine tetraacetate, trisodium citrate, citric acid, ethoxylated alkyl sulfate, lauroyl amido CAB, alkyl glycoside, sodium-chlor, essence and sanitas while stirring, stir into homogeneous liquid.
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CN105255598A (en) * | 2015-11-17 | 2016-01-20 | 孙铭岐 | Detergent |
CN105985870A (en) * | 2016-07-13 | 2016-10-05 | 西南大学 | Quick-drying antimicrobial mildewproof multifunctional laundry detergent and preparation method thereof |
CN106190627A (en) * | 2016-08-03 | 2016-12-07 | 安徽三祥羽毛有限公司 | A kind of washed feather & down washing deodorizer and preparation method thereof |
CN106635499A (en) * | 2016-12-22 | 2017-05-10 | 江西宜信堂医疗科技有限公司 | Down clothing cleaning agent and preparation method thereof |
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CN109321383A (en) * | 2018-10-18 | 2019-02-12 | 张永伍 | Environment-friendly cleaning agent is used in a kind of processing of down products |
CN110396827A (en) * | 2019-09-04 | 2019-11-01 | 石家庄贝洁日化有限公司 | A kind of solvent-free water-soluble natural feather leavening agent and preparation method thereof |
CN110819467A (en) * | 2019-11-11 | 2020-02-21 | 荆州市活力二八家化有限公司 | Detergent without harmful substances or skin irritative substances |
CN111234945A (en) * | 2020-03-30 | 2020-06-05 | 于澜海 | Biological enzyme laundry detergent and preparation method thereof |
CN112358917A (en) * | 2020-11-10 | 2021-02-12 | 江苏千雅日用品有限公司 | Detergent for silk and/or down clothes |
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