CN104856900A - Pore cleanser mask and preparation method thereof - Google Patents
Pore cleanser mask and preparation method thereof Download PDFInfo
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- CN104856900A CN104856900A CN201510251495.XA CN201510251495A CN104856900A CN 104856900 A CN104856900 A CN 104856900A CN 201510251495 A CN201510251495 A CN 201510251495A CN 104856900 A CN104856900 A CN 104856900A
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Abstract
The invention provides a pore cleanser mask. The mask comprises components as follows: water, polyvinyl alcohol, ethanol, acrylic acid (acrylic ester) copolymers, rehmannia root extracts, blackberrglily rhizome extracts, tea leaf extracts, pawpaw extracts, extracts of fruiting bodies of tremella fuciformis berkeley, carbon black, triethanolamine, phenoxyethanol and essence. The pore cleanser mask has mild property, can effectively remove stubborn blackheads, dredge pores and balance oil and also can supplement skin with water and strengthen the skin defense ability.
Description
Technical field
The present invention relates to a kind of cosmetics, particularly relate to a kind of blackhead film and preparation method thereof.
Background technology
" blackhead " is the skin surface pore collar extension of a class distribution, the Huang showing as blackhead " burr " shape, to brown black color dot, not only has a strong impact on the attractive in appearance of skin of face, also because often along with the appearance of acne, make skin seem greasy and pain of itching, allow people feel to feel bad very much! The major histological composition of blackhead is sebum mixture, preliminary texturing horn cell mixture, microbial metabolic products fatty acid and dust and dirt dirt etc.
Show in crowd according to famous Derma Clinic investigation, adult's nose of 97% is more easily fuel-displaced, and wherein the blackhead that exists of 90% perplexs, and people's blackhead of 68% is more serious.If except clean factor, male and women occur that the ratio of blackhead is almost identical, and significantly, the appearance of blackhead affects the attractive in appearance of personal image.
The origin cause of formation of " blackhead " is divided into external and intrinsic factor, extrinsic factor: daily shortage is clean, air pollution, maror stimulate, stay up late for a long time; Intrinsic factor: sebum secretion is vigorous, pore road cell transition keratinization, melanin excessively generate.
The product removing blackhead at present on the market has blackhead to derive liquid, biological cleanser, and pore cleanser is pasted, pore cleanser facial film, ointment, blackhead sucking-off film etc.
Such as, commercially available one dew ocean water blackhead sucking-off film, it comprises turmeric extract, Flos Chrysanthemi Indici extract and licorice root extract, and it effectively can remove blackhead, but this blackhead sucking-off film need derive liquid with blackhead, repair elite is combined, and it is general to the cleaning force of obstinate blackhead.
Chinese patent CN 102085169B discloses a kind of blackhead that makes and dissolves the synchronous preparation receiving fine, soft fur hole, and it comprises propylene glycol, butanediol, glycolic acid, Eucalyptus globulus Labill.extract, tea tree extract and water.Blackhead can dissolve loose powdered by it, synchronous receives fine, soft fur hole, but its blackhead-removing effect or undesirable.
Chinese patent application CN103893104A discloses a kind of speckle dispelling and to dispel the nose film cream of blackhead, it comprises sea mud, active carbon, the Radix Angelicae Dahuricae, Rhizoma Typhonii, Rhizoma Chuanxiong, the Radix Paeoniae Alba, Semen Armeniacae Amarum, Semen Ginkgo, Radix Asparagi, Radix Scutellariae, Radix Glycyrrhizae, Fructus Amomi, Margarita powder, Sargassum, Radix Angelicae Sinensis, Radix Salviae Miltiorrhizae, Poria and Flos Rosae Rugosae, this invention is by the combination of natural sea mud and herbaceous plant elite, not only reach the cleaning action of blackhead speckle dispelling of dispelling, also there is whitening and softening skin simultaneously, control the effect of oily moisturizing, but its complicated components, production cost is high, is unfavorable for applying.
In sum, be necessary that research and development one effectively removes blackhead, can nurse one's health oils and fats, supplement skin moisture, production cost is low simultaneously, the simple blackhead film of preparation method.
Summary of the invention
The technical problem to be solved in the present invention is to provide a kind of blackhead film, and its character is gentle, effectively removes obstinate blackhead, dredging pore, and conditioning oils and fats, supplements skin moisture simultaneously, promotes skin phylactic power defensive power.
For solving the problems of the technologies described above, technical scheme of the present invention is:
A kind of blackhead film, comprises following component: water, polyvinyl alcohol, ethanol, acrylic acid (ester) analog copolymer, Radix Rehmanniae extract, Rhizoma Belamcandae extract, Folium Camelliae sinensis extract, Fructus Chaenomelis extract, Tremella fructification extract, white carbon black, triethanolamine, phenoxyethanol and essence.
Preferably, blackhead film of the present invention comprises the component of following weight percent meter: water 50% ~ 60%, polyvinyl alcohol 15% ~ 22%, ethanol 15% ~ 22%, acrylic acid (ester) analog copolymer 1% ~ 3%, Radix Rehmanniae extract 0.3% ~ 0.6%, Rhizoma Belamcandae extract 0.3% ~ 0.7%, Folium Camelliae sinensis extract 0.3% ~ 0.7%, Fructus Chaenomelis extract 0.3% ~ 0.7%, Tremella fructification extract 0.3% ~ 0.7%, white carbon black 2% ~ 5%, triethanolamine 0.1% ~ 0.5%, phenoxyethanol 0.5% ~ 0.9% and essence 0.1% ~ 0.3%.
Preferred again, blackhead film of the present invention is made up of the component of following weight percent meter: water 57.05%, polyvinyl alcohol 19%, ethanol 15%, acrylic acid (ester) analog copolymer 2%, Radix Rehmanniae extract 0.5%, Rhizoma Belamcandae extract 0.5%, Folium Camelliae sinensis extract 0.6%, Fructus Chaenomelis extract 0.6%, Tremella fructification extract 0.5%, white carbon black 3%, triethanolamine 0.3%, phenoxyethanol 0.7% and essence 0.25%.
Radix Rehmanniae extract is described as vegetalitas " androsterone ", is 5α-reductase blocker, and the material of suppression 5α-reductase activity is considered to have vigorous effect chaeta being increased with keratinization of fat secretion suppressed because androsin causes.
Rhizoma Belamcandae extract is containing multiple isoflavone, and be that very safe aging resistance repairs class additive, experiment display Rhizoma Belamcandae extract also has the effect promoting collagen propagation, suppress pore blackhead to produce.
Folium Camelliae sinensis extract can significantly reduce sebum secretion speed, balance oiliness skin, has delaying skin sebum secretion, calmness, releives, the effect such as irritation.
Fructus Chaenomelis extract have softening, loosen acne again withhold excessive oils and fats, help acne to discharge, allow old useless cutin metabolism, effects such as pore of compacting.
Tremella fructification extract can be releived skin, supplements skin moisture instantaneously, promotes skin enrich the water, and strengthening moisture-retaining capacity makes skin reproduce gloss with beautiful, and the year light water of maintenance skin is tender.
The each component of the present invention is worked in coordination with, and reach and effectively remove obstinate blackhead, dredging pore, gentleness does not hinder skin, and conditioning oils and fats, supplements skin moisture simultaneously, promotes the object of skin phylactic power defensive power.
Another technical problem that the present invention will solve is to provide the preparation method of above-mentioned blackhead film.
For solving the problems of the technologies described above, technical scheme is:
A preparation method for blackhead film, its step is as follows:
(1) water of polyvinyl alcohol with 3/4 weight is mixed, be heated to 85 ~ 90 DEG C while stirring, dissolve completely to polyvinyl alcohol, obtain mixture one, be incubated after 8 ~ 12 minutes and lower the temperature;
(2) when being cooled to 45 DEG C, ethanol is joined in mixture one, stir and evacuation, stir 13 ~ 17 minutes and continue cooling, obtaining mixture two;
(3) by the mixing of the water of acrylic acid (ester) analog copolymer and 1/4 weight, filter after join in mixture two, stir 13 ~ 17 minutes, after system is even, adds Radix Rehmanniae extract, Rhizoma Belamcandae extract, Folium Camelliae sinensis extract, Fructus Chaenomelis extract, Tremella fructification extract, white carbon black, triethanolamine, phenoxyethanol and essence, is stirred to evenly.
Preferably, the mixing speed of described stirring is 55 ~ 65 revs/min.
Preferably, vacuum is evacuated in described step (2) for-0.05Pa.s.
The using method of blackhead film of the present invention: after cleaning clean nose and surrounding with clean product, covering T district of face with hot towel makes pore expand, get appropriate blackhead film and be applied in blackhead skin place, treat to parch for 10 ~ 15 minutes, remove nose film from top to bottom, clean clean nose and around with clear water, blackhead film of the present invention also can with blackhead derive liquid and repair liquid with the use of.
Compared with prior art, the present invention has following technical advantage:
1) the gentle safety of blackhead film character of the present invention, while effectively removing obstinate blackhead, do not hinder skin, dredging pore, reduction T district is smooth soft and fine, is applicable to life-time service.
2) blackhead film of the present invention is made up of the formula cleaning synchronous cooking skin condition, effectively nurses one's health oils and fats, reaches the effect of comprehensive decontamination, control oil and anti-pox, skin care Be very effective.
3) blackhead film of the present invention can promote skin phylactic power defensive power, supplements skin moisture in time time clean, promotes skin phylactic power defensive power, prevention blackhead, acne regeneration.
4) blackhead membrane preparation method of the present invention is simple, and production cost is low, can be applicable.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following examples.Within the scope of the invention or not departing from content of the present invention, spirit and scope, blackhead film of the present invention is suitably improved, replaces the identical component of effect, will become apparent to those skilled in the art that they are all deemed to be included within scope of the present invention.
Radix Rehmanniae extract of the present invention is Radix Rehmanniae (REHMANINNIA CHINENSIS) root extract that Huzhou Zhenlu Biological Products Co., Ltd. produces, and lot number is H587625.
Described Rhizoma Belamcandae extract is Rhizoma Belamcandae (BELAMCANDA CHINENSIS) extract that Huzhou Zhenlu Biological Products Co., Ltd. produces, and lot number is H587627.
Described Folium Camelliae sinensis extract is tea (CAMELLIA SINENSIS) leaf extract that fragrant (Shanghai) Co., Ltd. of moral produces, and lot number is 660425.
Described Fructus Chaenomelis extract is Fructus Chaenomelis (CHAENOMELES SPECIOSA) extract that fragrant (Shanghai) Co., Ltd. of moral produces, and lot number is 660428.
Described Tremella fructification extract is Tremella (TREMELLA FUCIFORMIS) fruiting body extract that friendly bio tech ltd, Beijing three produces, and lot number is 30515C14A.
Described white carbon black is the white carbon black [CI 77266] that Xilong Chemical Co., Ltd produces, and lot number is 150320.
The producer of acrylic acid (ester) analog copolymer is Rhom and Hass of the U.S., and lot number is P13072101.
embodiment 1, blackhead film of the present invention and preparation thereof
Formula: water 570.5g, polyvinyl alcohol 190g, ethanol 150g, acrylic acid (ester) analog copolymer 20g, Radix Rehmanniae extract 5g, Rhizoma Belamcandae extract 5g, Folium Camelliae sinensis extract 6g, Fructus Chaenomelis extract 6g, Tremella fructification extract 5g, white carbon black 30g, triethanolamine 3g, phenoxyethanol 7g and essence 2.5g.
Preparation: polyvinyl alcohol mixes with 427.9g water by (1), is heated to 85 DEG C while stirring, dissolves completely to polyvinyl alcohol, and mixing speed is 60 revs/min, obtains mixture one, is incubated after 10 minutes and lowers the temperature;
(2) when being cooled to 45 DEG C, joined by ethanol in mixture one, stir and evacuation, mixing speed is 60 revs/min, and vacuum is-0.05Pa.s, stirs 15 minutes and continues cooling, obtaining mixture two;
(3) by acrylic acid (ester) analog copolymer and 142.6g water mixing, filter after join in mixture two, stir 15 minutes, mixing speed is 60 revs/min, after system is even, adds Radix Rehmanniae extract, Rhizoma Belamcandae extract, Folium Camelliae sinensis extract, Fructus Chaenomelis extract, Tremella fructification extract, white carbon black, triethanolamine, phenoxyethanol and essence, is stirred to evenly.
embodiment 2, blackhead film of the present invention and preparation thereof
Formula: water 571.5g, polyvinyl alcohol 200g, ethanol 150g, acrylic acid (ester) analog copolymer 10g, Radix Rehmanniae extract 6g, Rhizoma Belamcandae extract 7g, Folium Camelliae sinensis extract 3g, Fructus Chaenomelis extract 3g, Tremella fructification extract 7g, white carbon black 30g, triethanolamine 5g, phenoxyethanol 5g, essence 2.5g.
Preparation: (1), by polyvinyl alcohol and the mixing of 428.6g water, be heated to 90 DEG C while stirring, dissolve completely to polyvinyl alcohol, mixing speed is 65 revs/min, obtains mixture one, is incubated after 10 minutes and lowers the temperature;
(2) when being cooled to 45 DEG C, joined by ethanol in mixture one, stir and evacuation, mixing speed is 65 revs/min, and vacuum is-0.05Pa.s, stirs 13 minutes and continues cooling, obtaining mixture two;
(3) by acrylic acid (ester) analog copolymer and 142.9g water mixing, filter after join in mixture two, stir 13 minutes, mixing speed is 65 revs/min, after system is even, adds Radix Rehmanniae extract, Rhizoma Belamcandae extract, Folium Camelliae sinensis extract, Fructus Chaenomelis extract, Tremella fructification extract, white carbon black, triethanolamine, phenoxyethanol and essence, is stirred to evenly.
embodiment 3, blackhead film of the present invention and preparation thereof
Formula: water 534.5g, polyvinyl alcohol 150g, ethanol 200g, acrylic acid (ester) analog copolymer 30g, Radix Rehmanniae extract 3g, Rhizoma Belamcandae extract 3g, Folium Camelliae sinensis extract 7g, Fructus Chaenomelis extract 7g, Tremella fructification extract 3g, white carbon black 50g, triethanolamine 1g, phenoxyethanol 9g, essence 2.5g.
Preparation: (1), by polyvinyl alcohol and the mixing of 400.9g water, be heated to 85 DEG C while stirring, dissolve completely to polyvinyl alcohol, mixing speed is 55 revs/min, obtains mixture one, is incubated after 10 minutes and lowers the temperature;
(2) when being cooled to 45 DEG C, joined by ethanol in mixture one, stir and evacuation, mixing speed is 55 revs/min, and vacuum is-0.05Pa.s, stirs 17 minutes and continues cooling, obtaining mixture two;
(3) by acrylic acid (ester) analog copolymer and 133.6g water mixing, filter after join in mixture two, stir 17 minutes, mixing speed is 55 revs/min, after system is even, adds Radix Rehmanniae extract, Rhizoma Belamcandae extract, Folium Camelliae sinensis extract, Fructus Chaenomelis extract, Tremella fructification extract, white carbon black, triethanolamine, phenoxyethanol and essence, is stirred to evenly.
comparative example 1,
Formula: water 570.5g, polyvinyl alcohol 190g, ethanol 150g, acrylic acid (ester) analog copolymer 20g, Folium Camelliae sinensis extract 10g, Fructus Chaenomelis extract 10g, Tremella fructification extract 7g, white carbon black 30g, triethanolamine 3g, phenoxyethanol 7g and essence 2.5g.
Preparation method is with embodiment 1.
comparative example 2,
Formula: water 570.5g, polyvinyl alcohol 190g, ethanol 150g, acrylic acid (ester) analog copolymer 20g, Radix Rehmanniae extract 13g, Rhizoma Belamcandae extract 14g, white carbon black 30g, triethanolamine 3g, phenoxyethanol 7g and essence 2.5g.
Preparation method is with embodiment 1.
test example one, Product Safety evaluation (experiment of human body skin patch)
One, the blackhead film prepared by trial target: embodiment 1-3, comparative example 1-2
Tested crowd's number: 30 people
Age: between 20 ~ 50 years old
Sex: female 20 people, male 10 people
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Two, patch method: select qualified speckle examination device, with closed patch experiment method, tested material being about 0.020ml ~ 0.025ml drips in speckle examination device, external special adhesive tape is covered on experimenter back, tested material is removed after 24 hours, within after removing respectively 0.5,6,12,24,48 hour, observe dermoreaction, according to its result of dermoreaction grade scale record in " cosmetics health specification ".
Three, experimental result: human skin patch result shows: 30 experimenters are by blackhead film (embodiment 1-3) of the present invention, reference substance (comparative example 1-2) patch test, dermoreaction is observed at 0.5,6,12,24,48 hour, wherein there is skin adverse reaction in 0 example, and blackhead film use safety of the present invention is described.
test example two, product effect assessment
One, the blackhead film prepared by trial target: embodiment 1-3, comparative example 1-2
Two, tested crowd
Sex number: female, 50 people
Age: between 20 ~ 40 years old
Health status: subjects skin is healthy, without dermatosis allergies, meets experimenter and volunteers inclusion criteria.
Three, method of testing: after experimenter cleans face, is applied in T district of face by the blackhead film prepared by example 1-3, comparative example 1-2 respectively, observes and experience result of use.
Testing evaluation result is as follows:
(8 days) on probation feedback conclusive table of table 1 embodiment 1 blackhead film
(8 days) on probation feedback conclusive table of table 2 embodiment 2 blackhead film
(8 days) on probation feedback conclusive table of table 3 embodiment 3 blackhead film
(8 days) on probation feedback conclusive table of table 4 comparative example 1 blackhead film
(8 days) on probation feedback conclusive table of table 5 comparative example 2 blackhead film
From upper table 1 ~ 5, the blackhead film of tester to embodiment 1 is particularly approved.Tester all represents, the blackhead film of embodiment 1 is better than the blackhead film of embodiment 2 and embodiment 3 in every respect, and be all better than comparative example 1 ~ 2, illustrate that the penetrating power of blackhead film of the present invention is extremely strong, the blackhead in pore and tough stains can be drawn, and Fast Convergent pore, supplement skin moisture in time, conditioning fat secretion, reduces the regeneration of blackhead, acne, promotes skin phylactic power defensive power.People is not had to occur allergic phenomena in the questionnaire of simultaneously user.
Some component in blackhead film formulation of the present invention is all lacked in the formula of comparative example 1 and comparative example 2, its effect is all not so good as the embodiment of the present invention 1 ~ 3, illustrate that blackhead film formulation of the present invention is not obtained by the simple combination of each component, then further illustrate between each component of formula of the present invention and there is synergism.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.
Claims (6)
1. a blackhead film, it is characterized in that, comprise following component: water, polyvinyl alcohol, ethanol, acrylic acid (ester) analog copolymer, Radix Rehmanniae extract, Rhizoma Belamcandae extract, Folium Camelliae sinensis extract, Fructus Chaenomelis extract, Tremella fructification extract, white carbon black, triethanolamine, phenoxyethanol and essence.
2. blackhead film as claimed in claim 1, it is characterized in that, comprise the component of following weight percent meter: water 50% ~ 60%, polyvinyl alcohol 15% ~ 22%, ethanol 15% ~ 22%, acrylic acid (ester) analog copolymer 1% ~ 3%, Radix Rehmanniae extract 0.3% ~ 0.6%, Rhizoma Belamcandae extract 0.3% ~ 0.7%, Folium Camelliae sinensis extract 0.3% ~ 0.7%, Fructus Chaenomelis extract 0.3% ~ 0.7%, Tremella fructification extract 0.3% ~ 0.7%, white carbon black 2% ~ 5%, triethanolamine 0.1% ~ 0.5%, phenoxyethanol 0.5% ~ 0.9% and essence 0.1% ~ 0.3%.
3. blackhead film as claimed in claim 2, it is characterized in that, be made up of the component of following weight percent meter: water 57.05%, polyvinyl alcohol 19%, ethanol 15%, acrylic acid (ester) analog copolymer 2%, Radix Rehmanniae extract 0.5%, Rhizoma Belamcandae extract 0.5%, Folium Camelliae sinensis extract 0.6%, Fructus Chaenomelis extract 0.6%, Tremella fructification extract 0.5%, white carbon black 3%, triethanolamine 0.3%, phenoxyethanol 0.7% and essence 0.25%.
4. the preparation method of the blackhead film according to claim 1 ~ 3 any one, is characterized in that, comprise the following steps:
(1) water of polyvinyl alcohol with 3/4 weight is mixed, be heated to 85 ~ 90 DEG C while stirring, dissolve completely to polyvinyl alcohol, obtain mixture one, be incubated after 8 ~ 12 minutes and lower the temperature;
(2) when being cooled to 45 DEG C, ethanol is joined in mixture one, stir and evacuation, stir 13 ~ 17 minutes and continue cooling, obtaining mixture two;
(3) by the mixing of the water of acrylic acid (ester) analog copolymer and 1/4 weight, filter after join in mixture two, stir 13 ~ 17 minutes, after system is even, adds Radix Rehmanniae extract, Rhizoma Belamcandae extract, Folium Camelliae sinensis extract, Fructus Chaenomelis extract, Tremella fructification extract, white carbon black, triethanolamine, phenoxyethanol and essence, is stirred to evenly.
5. the preparation method of blackhead film as claimed in claim 4, it is characterized in that, the mixing speed of described stirring is 55 ~ 65 revs/min.
6. the preparation method of blackhead film as claimed in claim 4, is characterized in that, is evacuated to vacuum for-0.05Pa.s in described step (2).
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106109395A (en) * | 2016-07-11 | 2016-11-16 | 佛山杰致信息科技有限公司 | A kind of mineral mud facial film of replenishing water and preserving moisture pore cleanser and preparation method thereof |
| CN106176511A (en) * | 2016-07-12 | 2016-12-07 | 广州市哲科生物科技有限公司 | A kind of propolis pore cleanser nose film and its preparation method and application |
| CN107281078A (en) * | 2017-05-27 | 2017-10-24 | 王义娟 | A kind of tearing type pore cleanser patch |
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| KR20130060571A (en) * | 2011-11-30 | 2013-06-10 | (주)아모레퍼시픽 | Oil-in-water type make-up cosmetic composition |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106109395A (en) * | 2016-07-11 | 2016-11-16 | 佛山杰致信息科技有限公司 | A kind of mineral mud facial film of replenishing water and preserving moisture pore cleanser and preparation method thereof |
| CN106176511A (en) * | 2016-07-12 | 2016-12-07 | 广州市哲科生物科技有限公司 | A kind of propolis pore cleanser nose film and its preparation method and application |
| CN106176511B (en) * | 2016-07-12 | 2019-11-08 | 广州市哲科生物科技有限公司 | A kind of propolis pore cleanser nose film and its preparation method and application |
| CN107281078A (en) * | 2017-05-27 | 2017-10-24 | 王义娟 | A kind of tearing type pore cleanser patch |
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| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Li Hongjun Inventor after: Chen Jiansheng Inventor after: He Zhiqing Inventor before: Li Hongjun Inventor before: Chen Jiansheng |
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| GR01 | Patent grant | ||
| GR01 | Patent grant |