CN103655315B - Black eye removal eye mask and preparation method thereof - Google Patents
Black eye removal eye mask and preparation method thereof Download PDFInfo
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- CN103655315B CN103655315B CN201310648526.6A CN201310648526A CN103655315B CN 103655315 B CN103655315 B CN 103655315B CN 201310648526 A CN201310648526 A CN 201310648526A CN 103655315 B CN103655315 B CN 103655315B
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Abstract
The invention discloses a black eye removal eye mask and a preparation method thereof, the black eye removal eye mask is prepared from the following raw materials: by weight, 3-15 parts of a pharmaceutical composition, 1 - 5 parts of C18 alcohol, 5 - 15 parts of 1, 3 - butanediol, 1 - 5 parts of polyurethane powder, 1 - 5 parts of jojoba oil, 5-10 parts of isohexadecane, 1-5 parts of cetearyl based olive oil ester, 5-10 parts of propylene glycol, 45-60 parts of purified water, 0.1-0.5 part of phenoxyethanol and 0.1-0.5 part of ethylhexylglycerin, the black eye removal eye mask is prepared by years of clinical experience screen and use of dialectical therapy of Chinese medicine theories according to causes of the formation of black eye, and experiments prove that the black eye removal eye mask has black eye removal effects.
Description
Technical field
The present invention relates to a kind of removal black eye eye mask and preparation method thereof.
Background technology
The skin of around eyes is soft and fine especially slim, and has many gauffers, therefore skin around the eyes moisture evaporation rate is very fast; Meanwhile, the sweat gland of periocualr skin and sebaceous gland distribute less, easy especially dry hydropenia.It is the most aging and the place had problems that these factors determine eyes.Black eye are owing to often staying up late, emotional instability, eye strain, aging, vein blood vessel blood flow rate is too slow, eye part skin red blood cell is for hypoxgia, and in vein blood vessel, carbon dioxide and metabolic waste accumulation too much, form chronic hypoxia, comparatively dark also formation of blood remains in a standstill and causes eye pigmentation, thus can to human psychological bringing burden and shade.
Summary of the invention
The object of this invention is to provide the black-eyed eye mask of a kind of removal.
Second object of the present invention is to provide a kind of preparation method removing black eye eye mask.
Technical scheme of the present invention is summarized as follows:
The black-eyed eye mask of a kind of removal, it is characterized in that being made up of following raw material by weight: pharmaceutical composition 3-15 part, C18 alcohol 1-5 part, 1,3 butylene glycol 5-15 part, polyurethane powder 1-5 part, Jojoba oil 1-5 part, 2-Methylpentadecane 5-10 part, cetearyl Fructus Canarii albi grease 1-5 part, propylene glycol 5-10 part, purified water 45-60 part, phenoxyethanol 0.1-0.5 part, Sensiva SC50 0.1-0.5 part;
Described pharmaceutical composition is made as follows:
A. Radix Salviae Miltiorrhizae 10-20 part, Radix Astragali 10-20 part, Folium Ginkgo 10-20 part, Radix Glycyrrhizae 5-15 part, Radix Scutellariae 5-15 part, Rhizoma Curcumae Longae 5-15 part, Radix Rhodiolae 5-15 part is taken by weight;
B. be ethanol water heating and refluxing extraction 1-3 time of 60-75% by the volume fraction doubly of material gross weight 8-10 described in steps A, each 1-2 hour, filtration, filtrate reduced in volume becomes density to be the thick paste of 1-2g/mL;
C. deionized water 5-10 part is heated to 30-50 DEG C, adds Catergen-5 parts, vitamin E 3-5 part, hamamelis extract 5-10 part, be stirred to 15-20rpm and dissolve completely, for subsequent use;
D. the mixed liquor mix homogeneously that the thick paste obtained by step B and step C obtain.
Remove a preparation method for black-eyed eye mask, comprise the steps:
(1) C18 alcohol 1-5 part, 1,3 butylene glycol 3-10 part, polyurethane powder 1-5 part, Jojoba oil 1-5 part, 2-Methylpentadecane 5-10 part, cetearyl Fructus Canarii albi grease 1-5 part are put into oil phase heating tank, be heated to 80 ~ 85 DEG C, insulation 10-30 minute, for subsequent use;
(2) propylene glycol 5-10 part, purified water 45-60 part are joined in heated aqueous tank, be heated to 85 ~ 90 DEG C, insulation 10-30 minute, for subsequent use;
(3) by 1,3 butylene glycol 2-5 part, pharmaceutical composition 3-15 part at 70-90 DEG C, with 15-20rpm stir 5-15 minute, for subsequent use;
(4) in mixed liquor suction emulsion tank step (2) obtained, at 85 ~ 90 DEG C, low whipping speed is stir 15-30 minute under 15-20rpm condition; The product that step (1) and step (3) obtain is joined in emulsion tank, evacuation, vacuum-0.05-0Mpa, homogenizing rotating speed 3000-5000rpm, homogenizing 10-20 minute, homogenizing 1-3 time, with mixing speed 15-20rpm after homogenizing, stir 15-30 minute, then be cooled to 30-50 DEG C;
(5) phenoxyethanol 0.1-0.5 part, Sensiva SC50 0.1-0.5 part are added in emulsion tank, mixing speed 15-20rpm, stir 5-10 minute, namely make the black-eyed eye mask of a kind of removal;
Described pharmaceutical composition is made as follows:
A. Radix Salviae Miltiorrhizae 10-20 part, Radix Astragali 10-20 part, Folium Ginkgo 10-20 part, Radix Glycyrrhizae 5-15 part, Radix Scutellariae 5-15 part, Rhizoma Curcumae Longae 5-15 part, Radix Rhodiolae 5-15 part is taken by weight;
B. be ethanol water heating and refluxing extraction 1-3 time of 60-75% by the volume fraction doubly of material gross weight 8-10 described in steps A, each 1-2 hour, filtration, filtrate reduced in volume becomes density to be the thick paste of 1-2g/mL;
C. deionized water 5-10 part is heated to 30-50 DEG C, adds Catergen-5 parts, vitamin E 3-5 part, hamamelis extract 5-10 part, be stirred to 15-20rpm and dissolve completely, for subsequent use;
D. the mixed liquor mix homogeneously that the thick paste obtained by step B and step C obtain.
Of the present invention a kind of to remove black-eyed eye mask be the reason formed according to black eye, and adopt the dialectical principle treated in theory of Chinese medical science, the clinical experience screening combined for many years forms, and experiment proves, removes black-eyed eye mask and has the black-eyed effect of removal.
Detailed description of the invention
One of the present invention is removed black-eyed eye mask and is contained pharmaceutical composition, and in pharmaceutical composition, Radix Salviae Miltiorrhizae, the Radix Astragali, Folium Ginkgo Yiqi-Huoxue-Huayu medicine, have the effect applying flexibly regulating menstruation, stasis-dispelling and pain-killing, therefore can promote ocular angiogenesis microcirculation; Curcumin material in licoflavone in Radix Glycyrrhizae, the baicalin in Radix Scutellariae and noroxylin, Rhizoma Curcumae Longae all has the effect of restraint of tyrosinase activity, thus inhibits melanic generation; Radix Rhodiolae has magical effect of strengthening healthy qi, benefiting qi and nourishing blood, YIN nourishing lung benefiting, successive dynasties Tibetan medicine is regarded as one of " lucky three essentials-essence ", it can promote the nonspecific resistance of human body to destructive stimulus, strengthen the adaptability of human body, simultaneously, vitamin C and vitamin E are the antioxidants that body weight for humans is wanted, and the collocation of vitamin C and vitamin E can help cell to absorb the nutritional labeling of outside skin care item better in addition, can increase beauty functions; Hamamelis extract can regulate sebum secretion, the effect of have calmness, pacifying, and also has simultaneously and promotes the sanguimotor effect of lymph, have good inhibitory action to morning exercises eyes edema and black eye.
Hamamelis extract purchased from American Biocogent company.
Below in conjunction with specific embodiment, the present invention is further illustrated.
Embodiment 1
The preparation of pharmaceutical composition:
(1) Radix Salviae Miltiorrhizae 10, the Radix Astragali 20 parts, Folium Ginkgo 10 parts, 5 parts, Radix Glycyrrhizae, Radix Scutellariae 15 parts, 15 parts, Rhizoma Curcumae Longae, Radix Rhodiolae 15 parts is taken by weight;
(2) by the volume fraction of the described material gross weight of step (1) 10 times be 60% ethanol water heating and refluxing extraction 1 time, each 2 hours, filter, filtrate reduced in volume becomes density to be the thick paste of 2g/mL;
(3) deionized water 5 parts is heated to 30 DEG C, adds vitamin C 5 parts, vitamin E 5 parts, hamamelis extract 10 parts, be stirred to 20rpm and dissolve completely, for subsequent use;
(4) the mixed liquor mix homogeneously that thick paste step (2) obtained and step (3) obtain.
Embodiment 2
The preparation of pharmaceutical composition:
(1) Radix Salviae Miltiorrhizae 15, the Radix Astragali 15 parts, Folium Ginkgo 15 parts, 10 parts, Radix Glycyrrhizae, Radix Scutellariae 10 parts, 10 parts, Rhizoma Curcumae Longae, Radix Rhodiolae 10 parts is taken by weight;
(2) by the volume fraction of the described material gross weight of step (1) 9 times be 70% ethanol water heating and refluxing extraction 2 times, each 1.5 hours, filter, filtrate reduced in volume becomes density to be the thick paste of 1g/mL;
(3) deionized water 8 parts is heated to 40 DEG C, adds vitamin C 4 parts, vitamin E 4 parts, hamamelis extract 7 parts, be stirred to CL with 15rpm, for subsequent use;
(4) the mixed liquor mix homogeneously that thick paste step (2) obtained and step (3) obtain.
Embodiment 3
The preparation of pharmaceutical composition:
(1) Radix Salviae Miltiorrhizae 20, the Radix Astragali 10 parts, Folium Ginkgo 20 parts, 15 parts, Radix Glycyrrhizae, Radix Scutellariae 5 parts, 5 parts, Rhizoma Curcumae Longae, Radix Rhodiolae 5 parts is taken by weight;
(2) by the volume fraction of the described material gross weight of step (1) 8 times be 75% ethanol water heating and refluxing extraction 3 times, each 1 hour, filter, filtrate reduced in volume becomes density to be the thick paste of 1g/mL;
(3) deionized water 10 parts is heated to 50 DEG C, adds Catergen part, vitamin E 3 parts, hamamelis extract 5 parts, be stirred to 15rpm and dissolve completely, for subsequent use;
(4) the mixed liquor mix homogeneously that thick paste step (2) obtained and step (3) obtain.
Embodiment 4
Remove a preparation method for black-eyed eye mask, comprise the steps
(1) C18 alcohol 1 part, 1,3 butylene glycol 10 parts, polyurethane powder 1 part, Jojoba oil 5 parts, 2-Methylpentadecane 5 parts, cetearyl Fructus Canarii albi grease 5 parts are put into oil phase heating tank, be heated to 80 DEG C (thermometer measures), be incubated 30 minutes, for subsequent use;
(2) propylene glycol 5 parts, purified water 60 parts are joined in heated aqueous tank, be heated to 90 DEG C, be incubated 10 minutes, for subsequent use;
(3) pharmaceutical composition 3 parts 1,3 butylene glycol 5 parts, embodiment 1 prepared, at 70 DEG C, stirs 15 minutes with 15rpm, for subsequent use;
(4) in mixed liquor suction emulsion tank step (2) obtained, at 85 DEG C, low whipping speed is stir 15 minutes under 20rpm condition; The product that step (1) and step (3) obtain is joined in emulsion tank, evacuation, vacuum-0.05Mpa, homogenizing rotating speed 3000rpm, homogenizing 20 minutes, homogenizing 1 time, with mixing speed 15rpm after homogenizing, stir 30 minutes, then be cooled to 30 DEG C;
(5) phenoxyethanol 0.1 part, Sensiva SC50 0.5 part are added in emulsion tank, mixing speed 15rpm, stir 10 minutes, namely make the black-eyed eye mask of a kind of removal.
Embodiment 5
A kind of preparation method removing black-eyed eye mask:
(1) C18 alcohol 3 parts, 1,3 butylene glycol 7 parts, polyurethane powder 3 parts, Jojoba oil 3 parts, 2-Methylpentadecane 7 parts, cetearyl Fructus Canarii albi grease 3 parts are put into oil phase heating tank, be heated to 83 DEG C (thermometer measures), be incubated 20 minutes, for subsequent use;
(2) propylene glycol 7 parts, purified water 53 parts are joined in heated aqueous tank, be heated to 88 DEG C, be incubated 20 minutes, for subsequent use;
(3) pharmaceutical composition 10 parts 1,3 butylene glycol 4 parts, embodiment 2 prepared, at 80 DEG C, stirs 10 minutes with 18rpm, for subsequent use;
(4) in mixed liquor suction emulsion tank step (2) obtained, at 87 DEG C, low whipping speed is stir 25 minutes under 18rpm condition; The product that step (1) and step (3) obtain is joined in emulsion tank, evacuation, vacuum-0.03Mpa, homogenizing rotating speed 4000rpm, homogenizing 15 minutes, homogenizing 2 times, with mixing speed 18rpm after homogenizing, stir 25 minutes, then be cooled to 40 DEG C;
(5) phenoxyethanol 0.2 part, Sensiva SC50 0.3 part are added in emulsion tank, mixing speed 18rpm, stir 7 minutes, namely make the black-eyed eye mask of a kind of removal.
Embodiment 6
A kind of preparation method removing black-eyed eye mask:
(1) C18 alcohol 5 parts, 1,3 butylene glycol 3 parts, polyurethane powder 5 parts, Jojoba oil 1 part, 2-Methylpentadecane 10 parts, cetearyl Fructus Canarii albi grease 1 part are put into oil phase heating tank, be heated to 85 DEG C (thermometer measures), be incubated 10 minutes, for subsequent use;
(2) propylene glycol 10 parts, purified water 45 parts are joined in heated aqueous tank, be heated to 85 DEG C, be incubated 30 minutes, for subsequent use;
(3) pharmaceutical composition 15 parts 1,3 butylene glycol 2 parts, embodiment 3 prepared, at 90 DEG C, stirs 5 minutes with 20rpm, for subsequent use;
(4) in mixed liquor suction emulsion tank step (2) obtained, at 90 DEG C, low whipping speed is stir 30 minutes under 15rpm condition; The product that step (1) and step (3) obtain is joined in emulsion tank, evacuation, vacuum 0Mpa, homogenizing rotating speed 5000rpm, homogenizing 10 minutes, homogenizing 3 times, with mixing speed 20rpm after homogenizing, stir 15 minutes, then be cooled to 50 DEG C;
(5) phenoxyethanol 0.5 part, Sensiva SC50 0.1 part are added in emulsion tank, mixing speed 20rpm, stir 5 minutes, namely make the black-eyed eye mask of a kind of removal.
Embodiment 7
Therapeutic effect
1, number of cases on probation: choosing has black-eyed people, 25-55 year crowd, women 60 example, is divided into three groups at random, male 60 example, is divided into three groups at random.Black eye are a kind of common eye problems, and common people are after 25 years old, and the collagen protein in body starts to run off, and eye skin is easy to be aging thinning, bottom eye socket, easily present the shade of lividity or black, forms black eye.
2. using method: thoroughly clean face skin, is applied in below brow ridge and eye with the third finger gently by this product, after 10-15 minute, wipes away gently with moistening fur towel, every three days 1 time, use and check result of use in 42 days.
3. result on trial shows that the effective percentage of use embodiment 4 after 42 days is 92.5%, and the effective percentage of embodiment 5 is 100%, and the effective percentage of embodiment 6 is 95%, and total effective rate is 95.8%, in table 1.
Table 1
Claims (1)
1. remove a preparation method for black-eyed eye mask, it is characterized in that comprising the steps:
(1) by C18 alcohol 1-5 part, 1,3-butanediol 3-10 part, polyurethane powder 1-5 part, Jojoba oil 1-5 part, 2-Methylpentadecane 5-10 part, cetearyl Fructus Canarii albi grease 1-5 part put into oil phase heating tank, be heated to 80 ~ 85 DEG C, insulation 10-30 minute, for subsequent use;
(2) propylene glycol 5-10 part, purified water 45-60 part are joined in heated aqueous tank, be heated to 85 ~ 90 DEG C, insulation 10-30 minute, for subsequent use;
(3) by 1,3 butylene glycol 2-5 part, pharmaceutical composition 3-15 part at 70-90 DEG C, with 15-20rpm stir 5-15 minute, for subsequent use;
(4) in mixed liquor suction emulsion tank step (2) obtained, at 85 ~ 90 DEG C, low whipping speed is stir 15-30 minute under 15-20rpm condition; The product that step (1) and step (3) obtain is joined in emulsion tank, evacuation, vacuum-0.05-0Mpa, homogenizing rotating speed 3000-5000rpm, homogenizing 10-20 minute, homogenizing 1-3 time, with mixing speed 15-20rpm after homogenizing, stir 15-30 minute, then be cooled to 30-50 DEG C;
(5) phenoxyethanol 0.1-0.5 part, Sensiva SC50 0.1-0.5 part are added in emulsion tank, mixing speed 15-20rpm, stir 5-10 minute, namely make the black-eyed eye mask of a kind of removal;
Described pharmaceutical composition is made as follows:
A. Radix Salviae Miltiorrhizae 10-20 part, Radix Astragali 10-20 part, Folium Ginkgo 10-20 part, Radix Glycyrrhizae 5-15 part, Radix Scutellariae 5-15 part, Rhizoma Curcumae Longae 5-15 part, Radix Rhodiolae 5-15 part is taken by weight;
B. be ethanol water heating and refluxing extraction 1-3 time of 60-75% by the volume fraction doubly of material gross weight 8-10 described in steps A, each 1-2 hour, filtration, filtrate reduced in volume becomes density to be the thick paste of 1-2g/mL;
C. deionized water 5-10 part is heated to 30-50 DEG C, adds Catergen-5 parts, vitamin E 3-5 part, hamamelis extract 5-10 part, be stirred to 15-20rpm and dissolve completely, for subsequent use;
D. the mixed liquor mix homogeneously that the thick paste obtained by step B and step C obtain.
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| CN103655315B true CN103655315B (en) | 2015-04-22 |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106109331A (en) * | 2016-08-01 | 2016-11-16 | 广州赛莱拉干细胞科技股份有限公司 | A kind of eye mask and preparation method thereof |
| CN111939229A (en) * | 2019-05-15 | 2020-11-17 | 北京利普松生物科技有限公司 | Composition for resisting asthenopia and xerophthalmia and treating pseudomyopia and preparation method thereof |
| CN110169941A (en) * | 2019-07-01 | 2019-08-27 | 广州市如馨化妆品有限公司 | A kind of biologic fiber eye mask Essence, preparation method and the eye mask using eye mask Essence preparation |
| CN111759786B (en) * | 2020-08-19 | 2021-04-27 | 何礼明 | Eye cream for removing dark eye circles and under-eye puffiness and preparation method thereof |
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| CN102274151A (en) * | 2011-09-01 | 2011-12-14 | 烟台新时代健康产业日化有限公司 | Skin caring composition with freckle removing effect |
| CN102579972A (en) * | 2011-12-05 | 2012-07-18 | 北京工商大学 | Traditional Chinese medicine composition and preparation with effect of relieving dark eye circles and preparation method of traditional Chinese medicine composition and preparation |
| CN102935061A (en) * | 2012-12-03 | 2013-02-20 | 晓健科技（大连）有限公司 | Witch hazel moisturizing eye mask |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004026740A (en) * | 2002-06-27 | 2004-01-29 | Naris Cosmetics Co Ltd | Cosmetic |
| JP2004026741A (en) * | 2002-06-27 | 2004-01-29 | Naris Cosmetics Co Ltd | Cosmetic |
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Patent Citations (3)
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| CN102274151A (en) * | 2011-09-01 | 2011-12-14 | 烟台新时代健康产业日化有限公司 | Skin caring composition with freckle removing effect |
| CN102579972A (en) * | 2011-12-05 | 2012-07-18 | 北京工商大学 | Traditional Chinese medicine composition and preparation with effect of relieving dark eye circles and preparation method of traditional Chinese medicine composition and preparation |
| CN102935061A (en) * | 2012-12-03 | 2013-02-20 | 晓健科技（大连）有限公司 | Witch hazel moisturizing eye mask |
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