CN103655315A - Black eye removal eye mask and preparation method thereof - Google Patents

Black eye removal eye mask and preparation method thereof Download PDF

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Publication number
CN103655315A
CN103655315A CN201310648526.6A CN201310648526A CN103655315A CN 103655315 A CN103655315 A CN 103655315A CN 201310648526 A CN201310648526 A CN 201310648526A CN 103655315 A CN103655315 A CN 103655315A
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parts
radix
black
minute
20rpm
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CN103655315B (en
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范太兵
丁利营
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Tianjin Jiashitang Science and Technology Co., Ltd.
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TIANJIN JIASHITANG SCIENCE AND TECHNOLOGY Co Ltd
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Abstract

The invention discloses a black eye removal eye mask and a preparation method thereof, the black eye removal eye mask is prepared from the following raw materials: by weight, 3-15 parts of a pharmaceutical composition, 1 - 5 parts of C18 alcohol, 5 - 15 parts of 1, 3 - butanediol, 1 - 5 parts of polyurethane powder, 1 - 5 parts of jojoba oil, 5-10 parts of isohexadecane, 1-5 parts of cetearyl based olive oil ester, 5-10 parts of propylene glycol, 45-60 parts of purified water, 0.1-0.5 part of phenoxyethanol and 0.1-0.5 part of ethylhexylglycerin, the black eye removal eye mask is prepared by years of clinical experience screen and use of dialectical therapy of Chinese medicine theories according to causes of the formation of black eye, and experiments prove that the black eye removal eye mask has black eye removal effects.

Description

The black-eyed eye mask of a kind of removal and preparation method
Technical field
The present invention relates to a kind of removal black eye eye mask and preparation method thereof.
Background technology
The skin of around eyes is soft and fine especially slim, and has many gauffers, therefore skin around the eyes moisture evaporation rate is very fast; Meanwhile, the sweat gland of skin and sebaceous gland distribution are less near the eyes, especially easily dry hydropenia.These factors have determined that eyes are places easy the most aging and that have problems.Black eye are owing to often staying up late, emotional instability, eye is tired, old and feeble, vein blood vessel blood flow rate is too slow, eye part skin red blood cell is for hypoxgia, and in vein blood vessel, carbon dioxide and metabolic waste accumulation too much, form chronic hypoxia, dark also formation of blood remains in a standstill and causes eye pigmentation, thereby can be to bringing burden and shade on human psychological.
Summary of the invention
The object of this invention is to provide the black-eyed eye mask of a kind of removal.
Second object of the present invention is to provide a kind of preparation method of removing black eye eye mask.
Technical scheme of the present invention is summarized as follows:
The black-eyed eye mask of a kind of removal, it is characterized in that by following raw material, being made by weight: pharmaceutical composition 3-15 part, C18 alcohol 1-5 part, 1,3 butylene glycol 5-15 part, polyurethane powder 1-5 part, Jojoba oil 1-5 part, 2-Methylpentadecane 5-10 part, cetearyl Fructus Canarii albi grease 1-5 part, propylene glycol 5-10 part, purified water 45-60 part, phenoxyethanol 0.1-0.5 part, Sensiva SC50 0.1-0.5 part;
Described pharmaceutical composition is made as follows:
A. take by weight Radix Salviae Miltiorrhizae 10-20 part, Radix Astragali 10-20 part, Folium Ginkgo 10-20 part, Radix Glycyrrhizae 5-15 part, Radix Scutellariae 5-15 part, Rhizoma Curcumae Longae 5-15 part, Radix Rhodiolae 5-15 part;
B. the ethanol water heating and refluxing extraction that is 60-75% by the volume fraction doubly of material gross weight 8-10 described in steps A 1-3 time, each 1-2 hour, filters, and filtrate decompression is condensed into the thick paste that density is 1-2g/mL;
C. deionized water 5-10 part is heated to 30-50 ℃, adds Catergen-5 part, vitamin E 3-5 part, Radix Hamamelidis Mollis extract 5-10 part, with 15-20rpm, be stirred to completely and dissolve, standby;
D. the mixed liquor mix homogeneously that thick paste step B being obtained and step C obtain.
A preparation method of removing black-eyed eye mask, comprises the steps:
(1) C18 alcohol 1-5 part, 1,3 butylene glycol 3-10 part, polyurethane powder 1-5 part, Jojoba oil 1-5 part, 2-Methylpentadecane 5-10 part, cetearyl Fructus Canarii albi grease 1-5 part are put into oil phase heating tank, be heated to 80~85 ℃, insulation 10-30 minute, standby;
(2) propylene glycol 5-10 part, purified water 45-60 part are joined in water heating tank, be heated to 85~90 ℃, insulation 10-30 minute, standby;
(3) by 1,3 butylene glycol 2-5 part, pharmaceutical composition 3-15 part at 70-90 ℃, with 15-20rpm, stir 5-15 minute, standby;
(4), in mixed liquor suction emulsion tank step (2) being obtained, at 85~90 ℃, low whipping speed is to stir 15-30 minute under 15-20rpm condition; The product of step (1) and step (3) acquisition is joined in emulsion tank to evacuation, vacuum-0.05-0Mpa, homogenizing rotating speed 3000-5000rpm, homogenizing 10-20 minute, homogenizing 1-3 time, after homogenizing, with mixing speed 15-20rpm, stir 15-30 minute, then be cooled to 30-50 ℃;
(5) phenoxyethanol 0.1-0.5 part, Sensiva SC50 0.1-0.5 part are added in emulsion tank, mixing speed 15-20rpm, stirs 5-10 minute, makes the black-eyed eye mask of a kind of removal;
Described pharmaceutical composition is made as follows:
A. take by weight Radix Salviae Miltiorrhizae 10-20 part, Radix Astragali 10-20 part, Folium Ginkgo 10-20 part, Radix Glycyrrhizae 5-15 part, Radix Scutellariae 5-15 part, Rhizoma Curcumae Longae 5-15 part, Radix Rhodiolae 5-15 part;
B. the ethanol water heating and refluxing extraction that is 60-75% by the volume fraction doubly of material gross weight 8-10 described in steps A 1-3 time, each 1-2 hour, filters, and filtrate decompression is condensed into the thick paste that density is 1-2g/mL;
C. deionized water 5-10 part is heated to 30-50 ℃, adds Catergen-5 part, vitamin E 3-5 part, Radix Hamamelidis Mollis extract 5-10 part, with 15-20rpm, be stirred to completely and dissolve, standby;
D. the mixed liquor mix homogeneously that thick paste step B being obtained and step C obtain.
Of the present invention a kind of to remove black-eyed eye mask be the reason forming according to black eye, adopts the dialectical principle treating in theory of Chinese medical science, in conjunction with clinical experience screening for many years, forms, and experiment showed, that removing black-eyed eye mask has the black-eyed effect of removal.
The specific embodiment
The black-eyed eye mask of a kind of removal of the present invention contains pharmaceutical composition, and Radix Salviae Miltiorrhizae, the Radix Astragali, Folium Ginkgo Yiqi-Huoxue-Huayu medicine in pharmaceutical composition have the effect of the regulating menstruation of applying flexibly, stasis-dispelling and pain-killing, so can promote ocular angiogenesis microcirculation; Curcumin material in licoflavone in Radix Glycyrrhizae, the baicalin in Radix Scutellariae and noroxylin, Rhizoma Curcumae Longae all has the effect of restraint of tyrosinase activity, thereby has suppressed melanic generation; Radix Rhodiolae has the magical effect of strengthening healthy qi, benefiting qi and nourishing blood, YIN nourishing lung benefiting, successive dynasties Tibetan medicine is regarded as one of " lucky three essentials-essence ", it can promote the nonspecific resistance of human body to destructive stimulus, strengthen the adaptability of human body, simultaneously, vitamin C and vitamin E are the antioxidants that body weight for humans is wanted, and the collocation of vitamin C and vitamin E can help cell to absorb better the nutritional labeling of outside skin care item in addition, can increase beauty functions; Radix Hamamelidis Mollis extract can regulate sebum secretion, and the effect of have calmness, pacifying also has the sanguimotor effect of the lymph of promotion simultaneously, and morning exercises eyes edema and black eye are had to good inhibitory action.
Radix Hamamelidis Mollis extract is purchased from U.S. Biocogent company.
Below in conjunction with specific embodiment, the present invention is further illustrated.
Embodiment 1
The preparation of pharmaceutical composition:
(1) take by weight Radix Salviae Miltiorrhizae 10,20 parts of the Radixs Astragali, 10 parts of Folium Ginkgos, 5 parts, Radix Glycyrrhizae, 15 parts of Radix Scutellariaes, 15 parts, Rhizoma Curcumae Longae, 15 parts of Radix Rhodiolaes;
(2) the ethanol water heating and refluxing extraction that is 60% by the volume fraction of 10 times of the described material gross weights of step (1) 1 time, each 2 hours, filter, filtrate decompression is condensed into the thick paste that density is 2g/mL;
(3) 5 parts of deionized waters are heated to 30 ℃, add 5 parts of vitamin Cs, 5 parts of vitamin Es, 10 parts of Radix Hamamelidis Mollis extracts, with 20rpm, be stirred to completely and dissolve, standby;
(4) the mixed liquor mix homogeneously that thick paste step (2) being obtained and step (3) obtain.
Embodiment 2
The preparation of pharmaceutical composition:
(1) take by weight Radix Salviae Miltiorrhizae 15,15 parts of the Radixs Astragali, 15 parts of Folium Ginkgos, 10 parts, Radix Glycyrrhizae, 10 parts of Radix Scutellariaes, 10 parts, Rhizoma Curcumae Longae, 10 parts of Radix Rhodiolaes;
(2) the ethanol water heating and refluxing extraction that is 70% by the volume fraction of 9 times of the described material gross weights of step (1) 2 times, each 1.5 hours, filter, filtrate decompression is condensed into the thick paste that density is 1g/mL;
(3) 8 parts of deionized waters are heated to 40 ℃, add 4 parts of vitamin Cs, 4 parts of vitamin Es, 7 parts of Radix Hamamelidis Mollis extracts, with 15rpm, be stirred to CL, standby;
(4) the mixed liquor mix homogeneously that thick paste step (2) being obtained and step (3) obtain.
Embodiment 3
The preparation of pharmaceutical composition:
(1) take by weight Radix Salviae Miltiorrhizae 20,10 parts of the Radixs Astragali, 20 parts of Folium Ginkgos, 15 parts, Radix Glycyrrhizae, 5 parts of Radix Scutellariaes, 5 parts, Rhizoma Curcumae Longae, 5 parts of Radix Rhodiolaes;
(2) the ethanol water heating and refluxing extraction that is 75% by the volume fraction of 8 times of the described material gross weights of step (1) 3 times, each 1 hour, filter, filtrate decompression is condensed into the thick paste that density is 1g/mL;
(3) 10 parts of deionized waters are heated to 50 ℃, add Catergen part, 3 parts of vitamin Es, 5 parts of Radix Hamamelidis Mollis extracts, with 15rpm, be stirred to completely and dissolve, standby;
(4) the mixed liquor mix homogeneously that thick paste step (2) being obtained and step (3) obtain.
Embodiment 4
A preparation method of removing black-eyed eye mask, comprises the steps
(1) 5 parts of 1 part of C18 alcohol, 10 parts of 1,3 butylene glycols, 1 part, polyurethane powder, 5 parts of Jojoba oils, 5 parts of 2-Methylpentadecanes, cetearyl Fructus Canarii albi grease are put into oil phase heating tank, be heated to 80 ℃ (thermometer measures), be incubated 30 minutes, standby;
(2) 60 parts of 5 parts of propylene glycol, purified water are joined in water heating tank, be heated to 90 ℃, be incubated 10 minutes, standby;
(3) by 3 parts of the pharmaceutical compositions of 5 parts of 1,3 butylene glycols, embodiment 1 preparation at 70 ℃, with 15rpm, stir 15 minutes, standby;
(4), in mixed liquor suction emulsion tank step (2) being obtained, at 85 ℃, low whipping speed is under 20rpm condition, to stir 15 minutes; The product of step (1) and step (3) acquisition is joined in emulsion tank, evacuation, vacuum-0.05Mpa, homogenizing rotating speed 3000rpm, homogenizing 20 minutes, homogenizing 1 time, with mixing speed 15rpm, stirs 30 minutes, then is cooled to 30 ℃ after homogenizing;
(5) 0.5 part of 0.1 part of phenoxyethanol, Sensiva SC50 is added in emulsion tank, mixing speed 15rpm, stirs 10 minutes, makes the black-eyed eye mask of a kind of removal.
Embodiment 5
A kind of preparation method of removing black-eyed eye mask:
(1) 3 parts of 3 parts of C18 alcohol, 7 parts of 1,3 butylene glycols, 3 parts, polyurethane powder, 3 parts of Jojoba oils, 7 parts of 2-Methylpentadecanes, cetearyl Fructus Canarii albi grease are put into oil phase heating tank, be heated to 83 ℃ (thermometer measures), be incubated 20 minutes, standby;
(2) 53 parts of 7 parts of propylene glycol, purified water are joined in water heating tank, be heated to 88 ℃, be incubated 20 minutes, standby;
(3) by 10 parts of the pharmaceutical compositions of 4 parts of 1,3 butylene glycols, embodiment 2 preparations at 80 ℃, with 18rpm, stir 10 minutes, standby;
(4), in mixed liquor suction emulsion tank step (2) being obtained, at 87 ℃, low whipping speed is under 18rpm condition, to stir 25 minutes; The product of step (1) and step (3) acquisition is joined in emulsion tank, evacuation, vacuum-0.03Mpa, homogenizing rotating speed 4000rpm, homogenizing 15 minutes, homogenizing 2 times, with mixing speed 18rpm, stirs 25 minutes, then is cooled to 40 ℃ after homogenizing;
(5) 0.3 part of 0.2 part of phenoxyethanol, Sensiva SC50 is added in emulsion tank, mixing speed 18rpm, stirs 7 minutes, makes the black-eyed eye mask of a kind of removal.
Embodiment 6
A kind of preparation method of removing black-eyed eye mask:
(1) 1 part of 5 parts of C18 alcohol, 3 parts of 1,3 butylene glycols, 5 parts, polyurethane powder, 1 part of Jojoba oil, 10 parts of 2-Methylpentadecanes, cetearyl Fructus Canarii albi grease is put into oil phase heating tank, be heated to 85 ℃ (thermometer measures), be incubated 10 minutes, standby;
(2) 45 parts of 10 parts of propylene glycol, purified water are joined in water heating tank, be heated to 85 ℃, be incubated 30 minutes, standby;
(3) by 15 parts of the pharmaceutical compositions of 2 parts of 1,3 butylene glycols, embodiment 3 preparations at 90 ℃, with 20rpm, stir 5 minutes, standby;
(4), in mixed liquor suction emulsion tank step (2) being obtained, at 90 ℃, low whipping speed is under 15rpm condition, to stir 30 minutes; The product of step (1) and step (3) acquisition is joined in emulsion tank, evacuation, vacuum 0Mpa, homogenizing rotating speed 5000rpm, homogenizing 10 minutes, homogenizing 3 times, with mixing speed 20rpm, stirs 15 minutes, then is cooled to 50 ℃ after homogenizing;
(5) 0.1 part of 0.5 part of phenoxyethanol, Sensiva SC50 is added in emulsion tank, mixing speed 20rpm, stirs 5 minutes, makes the black-eyed eye mask of a kind of removal.
Embodiment 7
Therapeutic effect
1, number of cases on probation: choosing has black-eyed people, 25-55 year crowd, women's 60 examples, are divided into three groups at random, and male's 60 examples are divided into three groups at random.Black eye are a kind of common eye problems, and common people are after 25 years old, and the collagen protein in body starts to run off, the easy aging attenuation of eye skin, and the easy shade that presents lividity or black in eye socket bottom, forms black eye.
2. using method: thorough clean face skin, with the third finger, this product is applied in to brow ridge and eye below gently, after 10-15 minute, with moistening fur towel, wipe away gently, every three days 1 time, use and within 42 days, check result of use.
3. to show to use the effective percentage of embodiment 4 after 42 days be that the effective percentage of 92.5%, embodiment 5 is that the effective percentage of 100%, embodiment 6 is 95% to result on trial, and total effective rate is 95.8%, in Table 1.
Table 1

Claims (2)

1. remove black-eyed eye mask for one kind, it is characterized in that by following raw material, being made by weight: pharmaceutical composition 3-15 part, C18 alcohol 1-5 part, 1,3 butylene glycol 5-15 part, polyurethane powder 1-5 part, Jojoba oil 1-5 part, 2-Methylpentadecane 5-10 part, cetearyl Fructus Canarii albi grease 1-5 part, propylene glycol 5-10 part, purified water 45-60 part, phenoxyethanol 0.1-0.5 part, Sensiva SC50 0.1-0.5 part;
Described pharmaceutical composition is made as follows:
A. take by weight Radix Salviae Miltiorrhizae 10-20 part, Radix Astragali 10-20 part, Folium Ginkgo 10-20 part, Radix Glycyrrhizae 5-15 part, Radix Scutellariae 5-15 part, Rhizoma Curcumae Longae 5-15 part, Radix Rhodiolae 5-15 part;
B. the ethanol water heating and refluxing extraction that is 60-75% by the volume fraction doubly of material gross weight 8-10 described in steps A 1-3 time, each 1-2 hour, filters, and filtrate decompression is condensed into the thick paste that density is 1-2g/mL;
C. deionized water 5-10 part is heated to 30-50 ℃, adds Catergen-5 part, vitamin E 3-5 part, Radix Hamamelidis Mollis extract 5-10 part, with 15-20rpm, be stirred to completely and dissolve, standby;
D. the mixed liquor mix homogeneously that thick paste step B being obtained and step C obtain.
2. remove a preparation method for black-eyed eye mask, it is characterized in that comprising the steps:
(1) C18 alcohol 1-5 part, 1,3 butylene glycol 3-10 part, polyurethane powder 1-5 part, Jojoba oil 1-5 part, 2-Methylpentadecane 5-10 part, cetearyl Fructus Canarii albi grease 1-5 part are put into oil phase heating tank, be heated to 80~85 ℃, insulation 10-30 minute, standby;
(2) propylene glycol 5-10 part, purified water 45-60 part are joined in water heating tank, be heated to 85~90 ℃, insulation 10-30 minute, standby;
(3) by 1,3 butylene glycol 2-5 part, pharmaceutical composition 3-15 part at 70-90 ℃, with 15-20rpm, stir 5-15 minute, standby;
(4), in mixed liquor suction emulsion tank step (2) being obtained, at 85~90 ℃, low whipping speed is to stir 15-30 minute under 15-20rpm condition; The product of step (1) and step (3) acquisition is joined in emulsion tank to evacuation, vacuum-0.05-0Mpa, homogenizing rotating speed 3000-5000rpm, homogenizing 10-20 minute, homogenizing 1-3 time, after homogenizing, with mixing speed 15-20rpm, stir 15-30 minute, then be cooled to 30-50 ℃;
(5) phenoxyethanol 0.1-0.5 part, Sensiva SC50 0.1-0.5 part are added in emulsion tank, mixing speed 15-20rpm, stirs 5-10 minute, makes the black-eyed eye mask of a kind of removal;
Described pharmaceutical composition is made as follows:
A. take by weight Radix Salviae Miltiorrhizae 10-20 part, Radix Astragali 10-20 part, Folium Ginkgo 10-20 part, Radix Glycyrrhizae 5-15 part, Radix Scutellariae 5-15 part, Rhizoma Curcumae Longae 5-15 part, Radix Rhodiolae 5-15 part;
B. the ethanol water heating and refluxing extraction that is 60-75% by the volume fraction doubly of material gross weight 8-10 described in steps A 1-3 time, each 1-2 hour, filters, and filtrate decompression is condensed into the thick paste that density is 1-2g/mL;
C. deionized water 5-10 part is heated to 30-50 ℃, adds Catergen-5 part, vitamin E 3-5 part, Radix Hamamelidis Mollis extract 5-10 part, with 15-20rpm, be stirred to completely and dissolve, standby;
D. the mixed liquor mix homogeneously that thick paste step B being obtained and step C obtain.
CN201310648526.6A 2013-12-03 2013-12-03 Black eye removal eye mask and preparation method thereof Active CN103655315B (en)

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CN106109331A (en) * 2016-08-01 2016-11-16 广州赛莱拉干细胞科技股份有限公司 A kind of eye mask and preparation method thereof
CN110169941A (en) * 2019-07-01 2019-08-27 广州市如馨化妆品有限公司 A kind of biologic fiber eye mask Essence, preparation method and the eye mask using eye mask Essence preparation
CN111759786A (en) * 2020-08-19 2020-10-13 何礼明 Eye cream for removing dark eye circles and under-eye puffiness and preparation method thereof
CN111939229A (en) * 2019-05-15 2020-11-17 北京利普松生物科技有限公司 Composition for resisting asthenopia and xerophthalmia and treating pseudomyopia and preparation method thereof

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Publication number Priority date Publication date Assignee Title
CN106109331A (en) * 2016-08-01 2016-11-16 广州赛莱拉干细胞科技股份有限公司 A kind of eye mask and preparation method thereof
CN111939229A (en) * 2019-05-15 2020-11-17 北京利普松生物科技有限公司 Composition for resisting asthenopia and xerophthalmia and treating pseudomyopia and preparation method thereof
CN110169941A (en) * 2019-07-01 2019-08-27 广州市如馨化妆品有限公司 A kind of biologic fiber eye mask Essence, preparation method and the eye mask using eye mask Essence preparation
CN111759786A (en) * 2020-08-19 2020-10-13 何礼明 Eye cream for removing dark eye circles and under-eye puffiness and preparation method thereof
CN111759786B (en) * 2020-08-19 2021-04-27 何礼明 Eye cream for removing dark eye circles and under-eye puffiness and preparation method thereof

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Address after: 300457 Tianda Science Park, Fourth Avenue, Jinshi Economic and Technological Development Zone

Patentee after: Tianjin Jiashitang Science and Technology Co., Ltd.

Address before: 450000 Zhengzhou Economic and Technological Development Zone, Zhengzhou City, Henan Province, No. 2 Building, No. 4, No. 409, South Xinghua Science and Technology Industrial Park, West and Jingnan Road

Patentee before: Henan Xin Yi Medical Technology Co., Ltd.

CP02 Change in the address of a patent holder
CP02 Change in the address of a patent holder

Address after: 300480 No. 453 Hengshan Road, modern industrial zone, economic and Technological Development Zone, Binhai New Area, Tianjin

Patentee after: TIANJIN CACHET TECHNOLOGY CO.,LTD.

Address before: 300457 Tianda Science Park, Fourth Avenue, Jinshi Economic and Technological Development Zone

Patentee before: TIANJIN CACHET TECHNOLOGY CO.,LTD.