CN104817935A - Waterproof coating for surface of packaging wood case and preparation method of waterproof coating - Google Patents
Waterproof coating for surface of packaging wood case and preparation method of waterproof coating Download PDFInfo
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- CN104817935A CN104817935A CN201510203264.1A CN201510203264A CN104817935A CN 104817935 A CN104817935 A CN 104817935A CN 201510203264 A CN201510203264 A CN 201510203264A CN 104817935 A CN104817935 A CN 104817935A
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Abstract
The invention relates to a waterproof coating for the surface of a packaging wood case and a preparation method of the waterproof coating. The waterproof coating comprises the following ingredients in part by mass: 3-10 parts of polyester resin, 4-12 parts of polyacrylic emulsion, 1-5 parts of polyving akohol, 20-36 parts of organophosphorus ester, 5-12 parts of ammonium dihydrogen phosphate, 5-12 parts of pentaerythritol, 2-6 parts of expanded perlite, 3-9 parts of chlorinated paraffin, 0.5-2 parts of antimony oxide, 1-4 parts of barium sulfate, 1-4 parts of alums, 1-5 parts of cellulosic fibers, 0.7-2 parts of mica, 0.5-1.5 parts of fireproof cotton, 7-14 parts of asphalt, 10-20 parts of water and 5-15 parts of sodium hexametaphosphate. The waterproof coating has the excellent fireproof performance, is high in adhesive strength, high in strength, high in waterproofness, high in acid resistance, high in weather resistance, high in impact resistance and high in wear resistance, cannot peel when coated on the surface of wood, is high in decoration, and protects packaging wood well.
Description
Technical field
The present invention relates to technical field of coatings, particularly relate to a kind of packaging wooden case surface frie retardant coating and preparation method thereof.
Background technology
Packaging wooden case is the tr assembled after stifling and mothproof process by timber, is widely used for the packaging of hazardous substance.Be used for greatly the buffering of hazardous substance, heat insulation outer packaging.Because timber has good shock-absorbing capacity, and intensity is high, corrosion-resistant, hygroscopic property is good, is therefore widely used in packaging industry, and packaging wooden case is exactly modal a kind of Wooden package container.In order to improve practicality and the aesthetic property of packaging wooden case, just needing at wooden case surface coating paint, playing protection and effect attractive in appearance.
But the bonding force of current existing wooden case surface coating is poor, easily peels off; Acid resistance is poor, is easily corroded; Water resistance is poor, and timber is easily moist; And fire resistance is poor, can not heat-insulating, fire-preventing effectively.Such as Chinese invention patent (the patent No. 201410735567.3, the applying date 2014/12/08) disclose a kind of wood coating and preparation method thereof, comprise the following raw material according to weight parts: polyacrylate emulsion 40-50 part, Sodium hexametaphosphate 99 0.3-0.5 part, 2, 2, 4-trimethylammonium-1, 3-pentanediol mono isobutyrate 2-12 part, hydroxyl fluorocarbon resin 1-5 part, pentachlorodiphenyl 0.5-2.5 part, trolamine 0.3-5 part, defoamer 0.05-0.20 part, deionized water 15-20 part, thickening material 1-1.5 part, titanium dioxide 15-25 part, light calcium carbonate 10-15 part.The application that coating disclosed in this patent of invention is suitable for wood surface can form good coating result at wood surface.
Summary of the invention
the technical problem solved:for the shortcoming of existing wood coating bonding force, acid resistance, water tolerance, fire line difference, the invention provides a kind of packaging wooden case surface frie retardant coating and preparation method thereof, this coating has excellent fire resistance.
technical scheme:a kind of packaging wooden case surface frie retardant coating, in mass parts containing following composition: 3 ~ 10 parts, vibrin, ACRYLIC EMULSION 4 ~ 12 parts, polyvinyl alcohol 1 ~ 5 part, organophosphate 20 ~ 36 parts, primary ammonium phosphate 5 ~ 12 parts, tetramethylolmethane 5 ~ 12 parts, pearlstone 2 ~ 6 parts, clorafin 3 ~ 9 parts, stibium trioxide 0.5 ~ 2 part, 1 ~ 4 part, barium sulfate, 1 ~ 4 part, alum, cellulosic fibre 1 ~ 5 part, 0.7 ~ 2 part, mica, resistance to guncotton 0.5 ~ 1.5 part, pitch 7 ~ 14 parts, 10 ~ 20 parts, water, Sodium hexametaphosphate 99 5 ~ 15 parts.
One packaging wooden case surface frie retardant coating described above, in mass parts containing following composition: 4 ~ 8 parts, vibrin, ACRYLIC EMULSION 5 ~ 11 parts, polyvinyl alcohol 1.5 ~ 4 parts, organophosphate 23 ~ 33 parts, primary ammonium phosphate 6 ~ 10 parts, tetramethylolmethane 7 ~ 11 parts, pearlstone 3 ~ 5 parts, clorafin 4 ~ 8 parts, stibium trioxide 0.8 ~ 1.6 part, 1.8 ~ 3.5 parts, barium sulfate, 2 ~ 3.7 parts, alum, cellulosic fibre 2 ~ 4 parts, 0.9 ~ 1.8 part, mica, resistance to guncotton 0.7 ~ 1.3 part, pitch 9 ~ 13 parts, 12 ~ 17 parts, water, Sodium hexametaphosphate 99 6 ~ 13 parts.
One packaging wooden case surface frie retardant coating described above, in mass parts containing following composition: 5 ~ 7 parts, vibrin, ACRYLIC EMULSION 6 ~ 10 parts, polyvinyl alcohol 2 ~ 3.5 parts, organophosphate 26 ~ 30 parts, primary ammonium phosphate 7 ~ 9 parts, tetramethylolmethane 8 ~ 10 parts, pearlstone 3.5 ~ 4.5 parts, clorafin 5 ~ 7 parts, stibium trioxide 1 ~ 1.4 part, 2.2 ~ 3 parts, barium sulfate, 2.5 ~ 3.3 parts, alum, cellulosic fibre 2.5 ~ 3.5 parts, 1.1 ~ 1.6 parts, mica, resistance to guncotton 0.9 ~ 1.2 part, pitch 10 ~ 11 parts, 13 ~ 15 parts, water, Sodium hexametaphosphate 99 8 ~ 11 parts.
One packaging wooden case surface frie retardant coating described above, in mass parts containing following composition: 6 parts, vibrin, ACRYLIC EMULSION 8 parts, polyvinyl alcohol 2.8 parts, organophosphate 28 parts, primary ammonium phosphate 8 parts, tetramethylolmethane 9 parts, pearlstone 4 parts, clorafin 6 parts, stibium trioxide 1.2 parts, 2.6 parts, barium sulfate, 2.9 parts, alum, cellulosic fibre 3 parts, 1.4 parts, mica, resistance to guncotton 1 part, pitch 11 parts, 14 parts, water, Sodium hexametaphosphate 99 10 parts.
A kind of preparation method packing wooden case surface frie retardant coating described above, the preparation process of the method is as follows:
The first step: first vibrin, ACRYLIC EMULSION, polyvinyl alcohol, water, Sodium hexametaphosphate 99 are added in reactor, control stirring velocity is 600 ~ 700r/min, is stirred to dissolving, obtains mixed solution;
Second step: take out the mixed solution in the first step, mixed solution is added in material-compound tank, add organophosphate, primary ammonium phosphate, tetramethylolmethane, pearlstone, clorafin, stibium trioxide, barium sulfate, alum, cellulosic fibre, mica, resistance to guncotton, pitch again, being ground to fineness with three-roll grinder after stirring is 90 ~ 110 μm;
3rd step: finally disperse in stirrer, control stirring velocity is 1300 ~ 1500r/min, gets product after being uniformly dispersed.
Control stirring velocity in the first step described above is 650r/min.
Being ground to fineness with three-roll grinder in second step described above is 100 μm.
Controlling stirring velocity in the 3rd step described above is 1400r/min.
beneficial effect:one packaging wooden case surface provided by the invention frie retardant coating and preparation method thereof; this coating has excellent fire resistance; simultaneously its bonding force, intensity, water-fast, acidproof, weather-proof shock-resistant, wear resisting property is all very high; be coated in wood surface incrust; by force ornamental, to packaged timber, there is good provide protection.
Embodiment
embodiment
1
A kind of packaging wooden case surface frie retardant coating, in mass parts containing following composition: 3 parts, vibrin, ACRYLIC EMULSION 4 parts, polyvinyl alcohol 1 part, organophosphate 20 parts, primary ammonium phosphate 5 parts, tetramethylolmethane 5 parts, pearlstone 2 parts, clorafin 3 parts, stibium trioxide 0.5 part, 1 part, barium sulfate, 1 part, alum, cellulosic fibre 1 part, 0.7 part, mica, resistance to guncotton 0.5 part, pitch 7 parts, 10 parts, water, Sodium hexametaphosphate 99 5 parts.
Pack a preparation method for wooden case surface frie retardant coating, the preparation process of the method is as follows:
The first step: first vibrin, ACRYLIC EMULSION, polyvinyl alcohol, water, Sodium hexametaphosphate 99 are added in reactor, control stirring velocity is 600r/min, is stirred to dissolving, obtains mixed solution;
Second step: take out the mixed solution in the first step, mixed solution is added in material-compound tank, add organophosphate, primary ammonium phosphate, tetramethylolmethane, pearlstone, clorafin, stibium trioxide, barium sulfate, alum, cellulosic fibre, mica, resistance to guncotton, pitch again, being ground to fineness with three-roll grinder after stirring is 90 μm;
3rd step: finally disperse in stirrer, control stirring velocity is 1300r/min, gets product after being uniformly dispersed.
embodiment
2
A kind of packaging wooden case surface frie retardant coating, in mass parts containing following composition: 10 parts, vibrin, ACRYLIC EMULSION 12 parts, polyvinyl alcohol 5 parts, organophosphate 36 parts, primary ammonium phosphate 12 parts, tetramethylolmethane 12 parts, pearlstone 6 parts, clorafin 9 parts, stibium trioxide 2 parts, 4 parts, barium sulfate, 4 parts, alum, cellulosic fibre 5 parts, 2 parts, mica, resistance to guncotton 1.5 parts, pitch 14 parts, 20 parts, water, Sodium hexametaphosphate 99 15 parts.
Pack a preparation method for wooden case surface frie retardant coating, the preparation process of the method is as follows:
The first step: first vibrin, ACRYLIC EMULSION, polyvinyl alcohol, water, Sodium hexametaphosphate 99 are added in reactor, control stirring velocity is 700r/min, is stirred to dissolving, obtains mixed solution;
Second step: take out the mixed solution in the first step, mixed solution is added in material-compound tank, add organophosphate, primary ammonium phosphate, tetramethylolmethane, pearlstone, clorafin, stibium trioxide, barium sulfate, alum, cellulosic fibre, mica, resistance to guncotton, pitch again, being ground to fineness with three-roll grinder after stirring is 110 μm;
3rd step: finally disperse in stirrer, control stirring velocity is 1500r/min, gets product after being uniformly dispersed.
embodiment
3
A kind of packaging wooden case surface frie retardant coating, in mass parts containing following composition: 4 parts, vibrin, ACRYLIC EMULSION 5 parts, polyvinyl alcohol 1.5 parts, organophosphate 23 parts, primary ammonium phosphate 6 parts, tetramethylolmethane 7 parts, pearlstone 3 parts, clorafin 4 parts, stibium trioxide 0.8 part, 1.8 parts, barium sulfate, 2 parts, alum, cellulosic fibre 2 parts, 0.9 part, mica, resistance to guncotton 0.7 part, pitch 9 parts, 12 parts, water, Sodium hexametaphosphate 99 6 parts.
Pack a preparation method for wooden case surface frie retardant coating, the preparation process of the method is as follows:
The first step: first vibrin, ACRYLIC EMULSION, polyvinyl alcohol, water, Sodium hexametaphosphate 99 are added in reactor, control stirring velocity is 650r/min, is stirred to dissolving, obtains mixed solution;
Second step: take out the mixed solution in the first step, mixed solution is added in material-compound tank, add organophosphate, primary ammonium phosphate, tetramethylolmethane, pearlstone, clorafin, stibium trioxide, barium sulfate, alum, cellulosic fibre, mica, resistance to guncotton, pitch again, being ground to fineness with three-roll grinder after stirring is 100 μm;
3rd step: finally disperse in stirrer, control stirring velocity is 1400r/min, gets product after being uniformly dispersed.
embodiment
4
A kind of packaging wooden case surface frie retardant coating, in mass parts containing following composition: 5 parts, vibrin, ACRYLIC EMULSION 6 parts, polyvinyl alcohol 2 parts, organophosphate 26 parts, primary ammonium phosphate 7 parts, tetramethylolmethane 8 parts, pearlstone 3.5 parts, clorafin 5 parts, stibium trioxide 1 part, 2.2 parts, barium sulfate, 2.5 parts, alum, cellulosic fibre 2.5 parts, 1.1 parts, mica, resistance to guncotton 0.9 part, pitch 10 parts, 13 parts, water, Sodium hexametaphosphate 99 8 parts.
Pack a preparation method for wooden case surface frie retardant coating, the preparation process of the method is as follows:
The first step: first vibrin, ACRYLIC EMULSION, polyvinyl alcohol, water, Sodium hexametaphosphate 99 are added in reactor, control stirring velocity is 650r/min, is stirred to dissolving, obtains mixed solution;
Second step: take out the mixed solution in the first step, mixed solution is added in material-compound tank, add organophosphate, primary ammonium phosphate, tetramethylolmethane, pearlstone, clorafin, stibium trioxide, barium sulfate, alum, cellulosic fibre, mica, resistance to guncotton, pitch again, being ground to fineness with three-roll grinder after stirring is 100 μm;
3rd step: finally disperse in stirrer, control stirring velocity is 1400r/min, gets product after being uniformly dispersed.
embodiment
5
A kind of packaging wooden case surface frie retardant coating, in mass parts containing following composition: 6 parts, vibrin, ACRYLIC EMULSION 8 parts, polyvinyl alcohol 2.8 parts, organophosphate 28 parts, primary ammonium phosphate 8 parts, tetramethylolmethane 9 parts, pearlstone 4 parts, clorafin 6 parts, stibium trioxide 1.2 parts, 2.6 parts, barium sulfate, 2.9 parts, alum, cellulosic fibre 3 parts, 1.4 parts, mica, resistance to guncotton 1 part, pitch 11 parts, 14 parts, water, Sodium hexametaphosphate 99 10 parts.
Pack a preparation method for wooden case surface frie retardant coating, the preparation process of the method is as follows:
The first step: first vibrin, ACRYLIC EMULSION, polyvinyl alcohol, water, Sodium hexametaphosphate 99 are added in reactor, control stirring velocity is 650r/min, is stirred to dissolving, obtains mixed solution;
Second step: take out the mixed solution in the first step, mixed solution is added in material-compound tank, add organophosphate, primary ammonium phosphate, tetramethylolmethane, pearlstone, clorafin, stibium trioxide, barium sulfate, alum, cellulosic fibre, mica, resistance to guncotton, pitch again, being ground to fineness with three-roll grinder after stirring is 100 μm;
3rd step: finally disperse in stirrer, control stirring velocity is 1400r/min, gets product after being uniformly dispersed.
comparative example
1
Invention patent mandate notification number is that the patent of CN 104449155A comprises following processing step:
A, in a dispersion cup, add polyacrylate emulsion, Sodium hexametaphosphate 99,2,2,4-trimethylammonium-1,3-pentanediol mono isobutyrates, hydroxyl fluorocarbon resin, pentachlorodiphenyl and trolamine, be uniformly mixed;
B, add deionized water, titanium dioxide and light calcium carbonate again, be uniformly mixed;
C, add defoamer and be uniformly mixed;
D, said mixture to be poured out, and carry out blending dispersion in high speed dispersor, the material through dispersion is transferred to two roller
Machine is milled, and filters, adds thickening material, fully stir thickening, obtain wood coating in dispersion cup.
The above-mentioned technical performance index stating the coating of the coating of embodiment 1 ~ embodiment 5 and comparative example 1, its detected result is as follows:
| Test item | Technical indicator | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Comparative example 1 |
| Fire performance (min) | Coat-thickness 25mm | 135 | 138 | 142 | 145 | 152 | 115 |
| Shock-resistance (kgcm) | GB/T1732-1993 | 138 | 132 | 141 | 138 | 143 | 120 |
| Ultraviolet resistance irradiation time (h) | 850 | 854 | 857 | 861 | 865 | 720 |
Above the embodiment of the present invention is described in detail, for one of ordinary skill in the art, according to the thought of the embodiment of the present invention, all will change in specific embodiments and applications, in sum, this description should not be construed as limitation of the present invention.
Claims (8)
1. a packaging wooden case surface frie retardant coating, to it is characterized in that in mass parts containing following composition: 3 ~ 10 parts, vibrin, ACRYLIC EMULSION 4 ~ 12 parts, polyvinyl alcohol 1 ~ 5 part, organophosphate 20 ~ 36 parts, primary ammonium phosphate 5 ~ 12 parts, tetramethylolmethane 5 ~ 12 parts, pearlstone 2 ~ 6 parts, clorafin 3 ~ 9 parts, stibium trioxide 0.5 ~ 2 part, 1 ~ 4 part, barium sulfate, 1 ~ 4 part, alum, cellulosic fibre 1 ~ 5 part, 0.7 ~ 2 part, mica, resistance to guncotton 0.5 ~ 1.5 part, pitch 7 ~ 14 parts, 10 ~ 20 parts, water, Sodium hexametaphosphate 99 5 ~ 15 parts.
2. one packaging wooden case surface according to claim 1 frie retardant coating, to it is characterized in that in mass parts containing following composition: 4 ~ 8 parts, vibrin, ACRYLIC EMULSION 5 ~ 11 parts, polyvinyl alcohol 1.5 ~ 4 parts, organophosphate 23 ~ 33 parts, primary ammonium phosphate 6 ~ 10 parts, tetramethylolmethane 7 ~ 11 parts, pearlstone 3 ~ 5 parts, clorafin 4 ~ 8 parts, stibium trioxide 0.8 ~ 1.6 part, 1.8 ~ 3.5 parts, barium sulfate, 2 ~ 3.7 parts, alum, cellulosic fibre 2 ~ 4 parts, 0.9 ~ 1.8 part, mica, resistance to guncotton 0.7 ~ 1.3 part, pitch 9 ~ 13 parts, 12 ~ 17 parts, water, Sodium hexametaphosphate 99 6 ~ 13 parts.
3. one packaging wooden case surface according to claim 1 frie retardant coating, to it is characterized in that in mass parts containing following composition: 5 ~ 7 parts, vibrin, ACRYLIC EMULSION 6 ~ 10 parts, polyvinyl alcohol 2 ~ 3.5 parts, organophosphate 26 ~ 30 parts, primary ammonium phosphate 7 ~ 9 parts, tetramethylolmethane 8 ~ 10 parts, pearlstone 3.5 ~ 4.5 parts, clorafin 5 ~ 7 parts, stibium trioxide 1 ~ 1.4 part, 2.2 ~ 3 parts, barium sulfate, 2.5 ~ 3.3 parts, alum, cellulosic fibre 2.5 ~ 3.5 parts, 1.1 ~ 1.6 parts, mica, resistance to guncotton 0.9 ~ 1.2 part, pitch 10 ~ 11 parts, 13 ~ 15 parts, water, Sodium hexametaphosphate 99 8 ~ 11 parts.
4. one packaging wooden case surface frie retardant coating according to claim 1, to is characterized in that in mass parts containing following composition: 6 parts, vibrin, ACRYLIC EMULSION 8 parts, polyvinyl alcohol 2.8 parts, organophosphate 28 parts, primary ammonium phosphate 8 parts, tetramethylolmethane 9 parts, pearlstone 4 parts, clorafin 6 parts, stibium trioxide 1.2 parts, 2.6 parts, barium sulfate, 2.9 parts, alum, cellulosic fibre 3 parts, 1.4 parts, mica, resistance to guncotton 1 part, pitch 11 parts, 14 parts, water, Sodium hexametaphosphate 99 10 parts.
5. a kind of preparation method packing wooden case surface frie retardant coating as claimed in claim 1, is characterized in that the preparation process of the method is as follows:
The first step: first vibrin, ACRYLIC EMULSION, polyvinyl alcohol, water, Sodium hexametaphosphate 99 are added in reactor, control stirring velocity is 600 ~ 700r/min, is stirred to dissolving, obtains mixed solution;
Second step: take out the mixed solution in the first step, mixed solution is added in material-compound tank, add organophosphate, primary ammonium phosphate, tetramethylolmethane, pearlstone, clorafin, stibium trioxide, barium sulfate, alum, cellulosic fibre, mica, resistance to guncotton, pitch again, being ground to fineness with three-roll grinder after stirring is 90 ~ 110 μm;
3rd step: finally disperse in stirrer, control stirring velocity is 1300 ~ 1500r/min, gets product after being uniformly dispersed.
6. a kind of preparation method packing wooden case surface frie retardant coating according to claim 5, is characterized in that: the control stirring velocity in the described the first step is 650r/min.
7. a kind of preparation method packing wooden case surface frie retardant coating according to claim 5, is characterized in that: being ground to fineness with three-roll grinder in described second step is 100 μm.
8. a kind of preparation method packing wooden case surface frie retardant coating according to claim 5, is characterized in that: controlling stirring velocity in described 3rd step is 1400r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510203264.1A CN104817935A (en) | 2015-04-27 | 2015-04-27 | Waterproof coating for surface of packaging wood case and preparation method of waterproof coating |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510203264.1A CN104817935A (en) | 2015-04-27 | 2015-04-27 | Waterproof coating for surface of packaging wood case and preparation method of waterproof coating |
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| CN104817935A true CN104817935A (en) | 2015-08-05 |
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| CN201510203264.1A Pending CN104817935A (en) | 2015-04-27 | 2015-04-27 | Waterproof coating for surface of packaging wood case and preparation method of waterproof coating |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106318072A (en) * | 2016-08-24 | 2017-01-11 | 何国美 | Coating for solid wood |
| CN112574672A (en) * | 2020-11-25 | 2021-03-30 | 浙江欣苗化工有限公司 | Water-based asphalt bottom paint for outdoor floor and processing technology thereof |
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| CN1380368A (en) * | 2002-04-11 | 2002-11-20 | 海洋化工研究院 | Expanding fire-proof paint |
| CN1876740A (en) * | 2006-07-12 | 2006-12-13 | 海洋化工研究院 | Solvent-free expansion type fire-proof epoxy coating and its preparation method |
| CN101440249A (en) * | 2008-05-23 | 2009-05-27 | 海洋化工研究院 | Ultrathin section steel structure fire-resisting paint and preparation thereof |
| CN103013204A (en) * | 2012-08-09 | 2013-04-03 | 江苏科技大学 | Flame-retardant ultraviolet curable coating for wood |
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2015
- 2015-04-27 CN CN201510203264.1A patent/CN104817935A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1380368A (en) * | 2002-04-11 | 2002-11-20 | 海洋化工研究院 | Expanding fire-proof paint |
| CN1876740A (en) * | 2006-07-12 | 2006-12-13 | 海洋化工研究院 | Solvent-free expansion type fire-proof epoxy coating and its preparation method |
| CN101440249A (en) * | 2008-05-23 | 2009-05-27 | 海洋化工研究院 | Ultrathin section steel structure fire-resisting paint and preparation thereof |
| CN103013204A (en) * | 2012-08-09 | 2013-04-03 | 江苏科技大学 | Flame-retardant ultraviolet curable coating for wood |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106318072A (en) * | 2016-08-24 | 2017-01-11 | 何国美 | Coating for solid wood |
| CN112574672A (en) * | 2020-11-25 | 2021-03-30 | 浙江欣苗化工有限公司 | Water-based asphalt bottom paint for outdoor floor and processing technology thereof |
| CN112574672B (en) * | 2020-11-25 | 2021-12-03 | 浙江欣苗化工有限公司 | Water-based asphalt bottom paint for outdoor floor and processing technology thereof |
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Application publication date: 20150805 |