CN104799432B - A kind of Moistureproof treatment method of filter stick capsule - Google Patents
A kind of Moistureproof treatment method of filter stick capsule Download PDFInfo
- Publication number
- CN104799432B CN104799432B CN201510173747.1A CN201510173747A CN104799432B CN 104799432 B CN104799432 B CN 104799432B CN 201510173747 A CN201510173747 A CN 201510173747A CN 104799432 B CN104799432 B CN 104799432B
- Authority
- CN
- China
- Prior art keywords
- filter stick
- capsule
- stick capsule
- coating
- treatment method
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/062—Use of materials for tobacco smoke filters characterised by structural features
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/04—Tobacco smoke filters characterised by their shape or structure
Abstract
A kind of Moistureproof treatment method of filter stick capsule provided by the invention, comprising the following steps: 1) first take pulullan polysaccharide according to the proportional arrangement of 1:10-200 at aqueous solution, it is stand-by as coating solution；2) filter stick capsule semi-finished product are coated；3) the filter stick capsule for completing coating is put into rotating cage and is carried out shaping and predrying；4) it will be put into the drying room that humidity is 20-40%RH by sizing, pre-dried filter stick capsule, tiling standing and drying 24 hours, blanking substandard products after collection, obtain filter stick capsule finished product, the Moistureproof treatment method of the filter stick capsule is by forming pulullan polysaccharide coating membrane in filter stick capsule wall material outer surface, its water proof humidity resistance is improved, the characteristic of the clear and melodious sound of " clatter " is issued when filter stick capsule being kept to keep frangible and broken under the influence of air humidity or moisture of cigarette main stream smoke.
Description
Technical field
The invention belongs to capsules to process preparation technical field, it relates in particular to a kind of damp-proof treatment side of filter stick capsule
Method.
Background technique
The pre-buried filter stick capsule for changing cigarette odor-absorbing and fragrance belongs to breakable capsule in filter stick, it is desirable that has certain
Intensity and brittleness, the capsule material of capsule is broken under finger extruding, the release of core material liquid, changes the suction taste of cigarette and fragrant
Gas, therefore capsule wall material not only has breakable feature, should also have preferable humidity resistance.
Under normal circumstances, filter stick capsule is usually the primary raw material of wall material with gelatin, alginate, dextrin, glycerol etc., this
A little materials all have certain hygroscopicity mostly, are contacted with air or with its filter stick capsule wall shell prepared by cigarette main flue
Air water point can absorb moisture dampness and phenomena such as softening, bonding occurs after influencing, affect cracking pressure, the appearance of filter stick capsule
And using effect.
In response to this, existing filter stick capsule dampproof method mainly by filter stick capsule wall material add calcium from
The capsule prepared is put into chitosan solution by son, and chitosan is made to react film forming with polyvalent metal ion, is formed not soluble in water
Chitin metal salt chelate, be wrapped in the appearance of filter stick capsule, considerably increase the waterproof performance of filter stick capsule, it is ensured that filter
Sticklac capsule will not absorb moisture because of contacting with air from air, make moist and phenomena such as softening, bonding occur, and then occur
The problems such as influencing the quality, appearance and use of filter stick capsule, the characteristic that filter stick capsule keeps frangible is met, the type is extended
The holding time of filter stick reduces external environment to the quality of filter stick capsule, appearance and the influence of utilization.
But in the actual use of cigarette product, part user habit is after aspirating a period of time just by the glue in filter stick
Capsule is pinched brokenly, and it is jealous to the suction of cigarette bring difference sufficiently to experience the broken rear Release of core material of filter stick capsule.Cigarette is in burning, mainstream
Contain some moisture in flue gas, and under the conditions of main flume temperature is higher, softening of these moisture for filter stick capsule
Phenomenon is more serious, and filter stick capsule can generally be caused to soften and cause capsule when being difficult to pinch brokenly or pinch brokenly without the clear and melodious sound of " clatter "
Sound affects the using effect of filter stick capsule, even if being handled using above-mentioned dampproof method, effect is still bad.
The application of Ma Naifeiersa company " is incorporated to the smoking apparatus, breakable capsule and the production glue of breakable capsule
The method of capsule " in, it mentions and immerses breakable capsule in Coating Solution, or by the way that Coating Solution is sprayed onto capsule with spray pattern
On implement to be coated, used coating material is mainly wax, lac, ethyl cellulose, hydroxypropyl methyl cellulose, hydroxypropyl
Cellulose, latex composition, polyvinyl alcohol, the disadvantage is that coating material is that hot melt or alcohol are molten, with water-soluble capsule wall shell knot
Defective tightness is closed, and coating operations difficulty is big, be easy to cause the decrease in yield of filter stick capsule manufacture.
Pulullan polysaccharide is a kind of extracellular water solubility by the generated similar glucan of Aureobasidium pullulans fermentation, xanthan gum
Clayey polysaccharide.Pulullan polysaccharide has excellent filming performance, forms a film transparent, fine and close.The maximum feature of pulullan polysaccharide film
Be it is lower than the permeability of other polymer material films, film forms fine and close reticular structure, and oxygen, nitrogen, carbon dioxide etc. are almost
It cannot pass through completely, vapor is also difficult to pass through, even if pulullan polysaccharide water suction is reachable under 60%-80% relative humidity
10%-15%, but not softening occurs, coheres situation, therefore pulullan polysaccharide can be used for the fresh-keeping of fruit, main operational mode
For certain density pulullan polysaccharide aqueous solution even application is formed pulullan polysaccharide film on fruit, thus obstruct fruit with
Moisture and oxygen exchange between air postpone the freshness date of fruit significantly.It, can be with general using the film forming characteristics of pulullan polysaccharide
Shandong orchid polysaccharide solution is coated processing to filter stick capsule, in filter stick capsule wall shell outer surface shape after making pulullan polysaccharide dry
At dense film, the moisture of air or main flume can be effectively prevent directly to contact with filter stick capsule wall shell, to prevent filter stick glue
Capsule makes moist during storage or cigarette smoking and phenomena such as softening, bonding occurs, influences cracking pressure, the appearance of filter stick capsule
And use effect.
Summary of the invention
The purpose of the present invention is to provide one kind by forming pulullan polysaccharide coating membrane in filter stick capsule wall material outer surface,
Its water proof humidity resistance is improved, filter stick capsule is kept to keep frangible under the influence of air humidity or moisture of cigarette main stream smoke and break
The Moistureproof treatment method of the filter stick capsule of the characteristic of the clear and melodious sound of " clatter " is issued when broken.
To achieve this purpose, the present invention adopts the following technical scheme:
1. a kind of Moistureproof treatment method of filter stick capsule, comprising the following steps:
1) take pulullan polysaccharide according to the proportional arrangement of 1:10-200 at aqueous solution first, it is stand-by as coating solution；
2) filter stick capsule semi-finished product are coated；
3) the filter stick capsule for completing coating is put into rotating cage and is carried out shaping and predrying；
4) it will be put into the drying room that humidity is 20-40%RH by sizing, pre-dried filter stick capsule, tiling stands dry
Dry 24 hours, blanking substandard products after collection obtained filter stick capsule finished product.
Further, in step 1), what the pulullan polysaccharide was configured to aqueous solution is preferably in a proportion of 1:100-150.
Further, in step 2), filter stick capsule is put into rotation coating device and carries out spray coating.
Further, it in step 2), is placed in dehydrating agent after filter stick capsule is impregnated and sloughs capsule surface coating solution water
Divide and completes coating.
Further, the dehydrating agent includes ethyl alcohol.
The beneficial effects of the present invention are: by being coated processing to filter stick capsule using pulullan polysaccharide, allow general Shandong
Dense film is formed in filter stick capsule wall shell outer surface after blue polysaccharide is dry, the moisture of air or main flume can be effectively prevent direct
Contacted with filter stick capsule wall shell, thus effectively prevent filter stick capsule to make moist during storage or cigarette smoking and occur softening,
Phenomena such as bonding, influences the cracking pressure of filter stick capsule, appearance and with effect.
Specific embodiment
Embodiment 1
A kind of Moistureproof treatment method of filter stick capsule, takes pulullan polysaccharide, distilled water, according to the mass ratio of 1:100 first
It is stand-by as coating solution that example is configured to aqueous solution；
Filter stick capsule is put into rotation coating device and carries out spray coating, coating solution dosage is filter stick capsules weight
15%.
The filter stick capsule that above-mentioned completion is coated is put into rotating cage and is carried out shaping and predrying 1 hour；
It is put into the drying room that humidity is 20-40%RH by sizing, pre-dried capsule, is tiled standing and drying 24 hours,
Blanking substandard products after collection, obtain capsule finished product；The filter stick capsule that above method preparation is handled is prepared into cigarette sample, is pressed
Conventional suction habit aspirates the cigarette sample to 1/2 fragment position, and the capsule dynamics of pinching brokenly is moderate when pinching brokenly filter stick capsule, and issues
The broken sound of " clatter "；By filter stick capsule that above method preparation is handled with the common filter stick capsule that is not handled by wet
Degree is detection effect such as table 1 in the space 70%RH:
| Capsule type | Rubber water content (%) | Pressure breaking deformation ratio (%) |
| It is untreated | 12.9 | 64% |
| After processing | 8.1 | 41% |
Table 1
Embodiment 2
A kind of Moistureproof treatment method of filter stick capsule, takes pulullan polysaccharide, distilled water first, matches according to the ratio of 1:150
It is stand-by as coating solution to be set to aqueous solution；
Filter stick capsule is immersed in configured coating solution after stirring 2 minutes and filter off coating solution, gained filter stick capsule is put into
Part of the surface moisture is sloughed after being dehydrated 1-30 minutes in ethyl alcohol completes coating；
The filter stick capsule that above-mentioned completion is coated is put into rotating cage and is carried out shaping and predrying 2 hours；
It is put into the drying room that humidity is 20-40%RH by sizing, pre-dried capsule, is tiled standing and drying 24 hours,
Blanking substandard products after collection, obtain capsule finished product, and the filter stick capsule that above method preparation is handled is prepared into cigarette sample, is pressed
Conventional suction habit aspirates the cigarette sample to 1/2 fragment position, and the capsule dynamics of pinching brokenly is moderate when pinching brokenly filter stick capsule, and issues
The broken sound of " clatter ", by filter stick capsule that above method preparation is handled with the common filter stick capsule that is not handled by wet
Degree is detection effect such as table 2 in the space 70%RH:
| Capsule type | Rubber water content (%) | Pressure breaking deformation ratio (%) |
| It is untreated | 12.2 | 59% |
| After processing | 9.1 | 44% |
Table 2
Embodiment 3
A kind of Moistureproof treatment method of filter stick capsule, takes pulullan polysaccharide, distilled water, according to the mass ratio of 1:10 first
It is stand-by as coating solution to be configured to aqueous solution；
Filter stick capsule is put into rotation coating device and carries out spray coating, coating solution dosage is filter stick capsules weight
15%.
The filter stick capsule that above-mentioned completion is coated is put into rotating cage and is carried out shaping and predrying 1 hour；
It is put into the drying room that humidity is 20-40%RH by sizing, pre-dried capsule, is tiled standing and drying 24 hours,
Blanking substandard products after collection, obtain capsule finished product；The filter stick capsule that above method preparation is handled is prepared into cigarette sample, is pressed
Conventional suction habit aspirates the cigarette sample to 1/2 fragment position, and the capsule dynamics of pinching brokenly is moderate when pinching brokenly filter stick capsule, and issues
The broken sound of " clatter ".
Embodiment 4
A kind of Moistureproof treatment method of filter stick capsule, takes pulullan polysaccharide, distilled water, according to the mass ratio of 1:200 first
It is stand-by as coating solution that example is configured to aqueous solution；
Filter stick capsule is put into rotation coating device and carries out spray coating, coating solution dosage is filter stick capsules weight
15%.
The filter stick capsule that above-mentioned completion is coated is put into rotating cage and is carried out shaping and predrying 1 hour；
It is put into the drying room that humidity is 20-40%RH by sizing, pre-dried capsule, is tiled standing and drying 24 hours,
Blanking substandard products after collection, obtain capsule finished product；The filter stick capsule that above method preparation is handled is prepared into cigarette sample, is pressed
Conventional suction habit aspirates the cigarette sample to 1/2 fragment position, and the capsule dynamics of pinching brokenly is moderate when pinching brokenly filter stick capsule, and issues
The broken sound of " clatter ".
Beneficial effects of the present invention: by being coated processing to filter stick capsule using pulullan polysaccharide, make Propiram more
Form dense film in filter stick capsule wall shell outer surface after sugar is dry, can effectively prevent the moisture of air or main flume directly with filter
Sticklac cyst wall shell contact, to effectively prevent filter stick capsule to make moist during storage or cigarette smoking and softening, bonding occur
Phenomena such as, influence the cracking pressure of filter stick capsule, appearance and with effect.
The above has been described in detail, described above, is only a preferred embodiment of the present invention, when cannot
It limit the scope of implementation of the present invention, i.e., it is all according to the made equivalent changes and modifications of the application range, it should still belong to covering scope of the present invention
It is interior.
Claims (2)
1. a kind of Moistureproof treatment method of filter stick capsule, which comprises the following steps:
1) pulullan polysaccharide and distilled water are taken first and according to the proportional arrangement of 1:100-200 at aqueous solution, wait for as coating solution
With；
2) filter stick capsule semi-finished product are coated, filter stick capsule is put into rotation coating device and carries out spray coating；Or it will
Coating solution is filtered off after stirring 2 minutes in the configured coating solution of filter stick capsule immersion, gained filter stick capsule, which is put into ethyl alcohol, to be dehydrated
Part of the surface moisture is sloughed after 1-30 minutes completes coating；
3) the filter stick capsule for completing coating is put into rotating cage and is carried out shaping and predrying；
4) it will be put into the drying room that humidity is 20-40%RH by sizing, pre-dried filter stick capsule, tile standing and drying 24
Hour, blanking substandard products after collection obtain filter stick capsule finished product.
2. the Moistureproof treatment method of filter stick capsule as described in claim 1, which is characterized in that in step 1), the general Shandong
The ratio that blue polysaccharide and distilled water are configured to aqueous solution is 1:100-150.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510173747.1A CN104799432B (en) | 2015-04-14 | 2015-04-14 | A kind of Moistureproof treatment method of filter stick capsule |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510173747.1A CN104799432B (en) | 2015-04-14 | 2015-04-14 | A kind of Moistureproof treatment method of filter stick capsule |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN104799432A CN104799432A (en) | 2015-07-29 |
| CN104799432B true CN104799432B (en) | 2019-01-15 |
Family
ID=53684982
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510173747.1A Active CN104799432B (en) | 2015-04-14 | 2015-04-14 | A kind of Moistureproof treatment method of filter stick capsule |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104799432B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107616546A (en) * | 2017-08-30 | 2018-01-23 | 武汉黄鹤楼香精香料有限公司 | The preparation method of the quick-fried pearl lapping of cigarette |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101203148A (en) * | 2005-06-21 | 2008-06-18 | 玛奈·菲尔萨公司 | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
| CN102824887A (en) * | 2012-09-14 | 2012-12-19 | 云南烟草科学研究院 | Preparation method of controlled-release soft capsules for cigarettes |
| WO2014170947A1 (en) * | 2013-04-15 | 2014-10-23 | 三生医薬株式会社 | Collapsible capsule, manufacturing method therefor and smoking implement |
| CN104172471A (en) * | 2014-07-16 | 2014-12-03 | 江西中烟工业有限责任公司 | Brittle capsule with ginseng characteristic aroma as well as preparation method and application thereof |
-
2015
- 2015-04-14 CN CN201510173747.1A patent/CN104799432B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101203148A (en) * | 2005-06-21 | 2008-06-18 | 玛奈·菲尔萨公司 | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule |
| CN102824887A (en) * | 2012-09-14 | 2012-12-19 | 云南烟草科学研究院 | Preparation method of controlled-release soft capsules for cigarettes |
| WO2014170947A1 (en) * | 2013-04-15 | 2014-10-23 | 三生医薬株式会社 | Collapsible capsule, manufacturing method therefor and smoking implement |
| CN104172471A (en) * | 2014-07-16 | 2014-12-03 | 江西中烟工业有限责任公司 | Brittle capsule with ginseng characteristic aroma as well as preparation method and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN104799432A (en) | 2015-07-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN102895926B (en) | Moistureproof treatment method for soft capsules | |
| WO2016123869A1 (en) | Aqueous capsule and preparation method therefor | |
| CN103815541B (en) | Three layers of cigarette capsule with diuresis promoting function and preparation method thereof | |
| RU2690278C2 (en) | Hydrophobic tipping paper | |
| CN101203148A (en) | Smoking device incorporating a breakable capsule, breakable capsule and process for manufacturing said capsule | |
| RU2015122406A (en) | CAPSULE PRODUCTS, THEIR APPLICATION AND MANUFACTURE | |
| CN105495686A (en) | Moisture-proof and embrittling treatment method of cigarette capsules and product obtained by treatment method | |
| CN105105334A (en) | Spice slow-release filter tip additive with polymer covering film as well as preparation method and application thereof | |
| CN106519310B (en) | A kind of quick-fried pearl noctilucence of cigarette is coated membrane material and noctilucence the cigarette preparation method of quick-fried pearl | |
| CN110506977B (en) | Low-temperature non-combustion tobacco particles for cigarettes and preparation method thereof, and smoke body and preparation method thereof | |
| CN110506984B (en) | Tobacco particles and preparation method thereof, low-temperature smoke body and preparation method thereof | |
| CN106333385A (en) | Filter stick for short cigarettes | |
| CN105985449B (en) | A kind of modified hydroxypropul starch and preparation method thereof, a kind of plant hollow capsule and preparation method thereof | |
| CN104799432B (en) | A kind of Moistureproof treatment method of filter stick capsule | |
| RU2019104876A (en) | ACID RESISTANT CAPSULES | |
| CN102242527A (en) | Functional cigarette paper and preparation method | |
| CN104479870A (en) | Water capsule for cigarettes using compound salts as wall material and preparation method thereof | |
| JP2020516743A5 (en) | ||
| CN105212273A (en) | A kind of electronic cigarette fat capsule | |
| CN109535489A (en) | A kind of cigarette hydrophobic membrane material of quick-fried pearl and preparation method thereof | |
| CN112438423B (en) | Tobacco particles, low-temperature smoke body, preparation method and heating non-combustion appliance | |
| CN110506976A (en) | A kind of full particle low temperature fuming liquids | |
| CN207912030U (en) | A kind of coffee perfume (or spice) cigarette paper | |
| WO2018184323A1 (en) | Aluminum-free cigarette lining paper capable of keeping humidity constant and preserving quality and aroma, and manufacturing process therefor | |
| CN105536656B (en) | Friable capsules for use in tobacco products, method for the production thereof and use thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| EXSB | Decision made by sipo to initiate substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |